TY - CONF A1 - Baeßler, Matthias T1 - A perspective on research on OWEA substructures considering the authorities approval process N2 - Die BAM unterstützt das Bundesamt für Seeschifffahrt und Hydrografie bei der bautechnischen Bewertung von Tragstrukturen für Offshore-Windparks. Im Hinblick auf die vielfältigen nationalen Aktivitäten in Forschung und Entwicklung wird in der eingeladenen Präsentation auf Schwerpunkte behördlicher Erfahrungen und Bedenken Bezug genommen um eine Perspektive auf zukünftigen Forschungsbedarf zu eröffnen. T2 - 7. Gigawind Symposium CY - Leibniz Universität Hannover, Germany DA - 02.03.2017 KW - OWEA KW - Substructures KW - Authorities approval process PY - 2017 AN - OPUS4-39377 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lazik, D. A1 - Neumann, Patrick P. A1 - Bartholmai, Matthias T1 - Characteristic length measurement of a subsurface gas anomaly - an integrating monitoring approach over heterogeneous distributed gas flow paths N2 - Geogenic gases such as CH4 or CO2 from natural sources, gases (CCS-CO2, H2, Natural gas, City gas …) from a geological repository, or a leaking gas pipeline can present serious risks in industrial and urban areas where the density of infrastructural elements increases as well as above and below ground. To extend the lead time for risk treatment in such critical regions, reliable detection of gases within the shallow subsurface is required to observe critical gas accumulations before degassing into the atmosphere. A near real-time monitoring approach is introduced to determine the volumetric expansion of such a gas escaping from a leak in the subsurface. Considering the pressure relaxation with the ambient air pressure, the approach enables the forecasting of the final size of a pressurized gas body in terms of characteristic lengths. According to theoretical basics, such a characteristic length, which allows to perform a gas (safety) measurement based on a purely geometrical measure, behaves independently of subsurface properties, i.e., it enables a reliable quantification of the escaping gas, irrespective of its heterogeneous flow path distribution. A field test for a 10 l/min pinhole leakage of CO2 injected in an unsaturated Chernozemic soil (agricultural test field Bad Lauchstädt)that was equipped with linear gas sensors demonstrates the lateral-vertical volumetric gas expansion along the environment of these gas sensors, and confirms the applicability of the new characteristic length approach. T2 - UFZ EnergyDays 2017 CY - Leipzig, Germany DA - 15.03.2017 KW - CO2 KW - Carbon capture and storage KW - Leakage KW - Monitoring PY - 2017 AN - OPUS4-39400 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schröder, Volkmar T1 - Sicherheitstechnische Kenngrößen für Biogase N2 - Im Poster wird die Ermittlung sicherheitstechnischer Kenngrößen für Biogase mit Hilfe von Dreistoff-Diagrammen dargestellt. Insbesondere wird die Berechnung der unteren und oberen Explosionsgrenzen (UEG, OEG) und die Ermittlung der Sauerstoffgrenzkonzentration (LOC)beschrieben. T2 - Biogas Infotage 2017 CY - Ulm, Germany DA - 18.01.2017 KW - Biogas KW - Explosionsschutz KW - Explosionsgrenzen KW - Sauerstoffgrenzkonzentration KW - Explosionsdiagramme PY - 2017 AN - OPUS4-39063 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schröder, Volkmar T1 - Explosionsschutz für Biogas-Wasserstoff-Gemische N2 - Bei neueren Verfahren zur Biogasgewinnung wird zusätzlich Wasserstoff in den Fermenter eingespeist, um den Methananteil im Biogas zu erhöhen. Dieses Verfahren bewirkt neben der CO2-Vermeidung eine Erhöhung des Brennwerts und der Qualität des Biogases. Zudem kann dafür, ähnlich wie bei der Einspeisung von Wasserstoff in das Erdgasnetz, Elektrolysewasserstoff aus Überschüssen von Wind- und Solarstrom verwendet werden (Power-to-Gas). Im Poster werden die sicherheitstechnischen Kenngrößen für den Explosionsschutz bei Prozessgasen dargestellt und diskutiert. T2 - Biogas Infotage 2017 CY - Ulm, Germany DA - 18.01.2017 KW - Biogas-Wasserstoff-Gemische KW - Explosionsschutz KW - Sicherheitstechnische Kenngrößen KW - Explosionsgrenzen KW - Explosionsdrücke KW - Normspaltweite PY - 2017 AN - OPUS4-39064 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schröder, Volkmar T1 - Kenngrößen für Gase im Explosionsschutz N2 - Im Poster werden die wichtigsten sicherheitstechnischen Kenngrößen von Gasen für den Explosionsschutz dargestellt. Es wird gezeigt, wie mit Hilfe von Dreistoff-Diagrammen (Explosionsdiagrammen) die Explosionsgrenzen, die Entzündbarkeit und die Sauerstoffgrenzkonzentration von Gemischen aus Brenn- und Inertgasen bestimmt werden. Weiterhin wird eine Zuordnung der Kenngrößen zu den gebräuchlichen Schutzmaßnahmen vorgenommen. T2 - Biogas Infotage 2017 CY - Ulm, Germany DA - 18.01.2017 KW - Explosionsschutz KW - Sicherheitstechnische Kenngrößen KW - Biogas KW - Explosionsgrenzen KW - Explosionsdruck KW - Normspaltweite KW - Explosionsgruppen PY - 2017 AN - OPUS4-39065 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Stengel, Dominik A1 - Mehdianpour, Milad T1 - Windbeanspruchung von Hochspannungs-Freileitungsseilen in Naturmessungen, Zeitbereichssimulation und Norm T1 - Wind load of high voltage overhead transmission line con ductors in field measurements, time domain simulations and standard N2 - Die Beanspruchung von Freileitungen erfolgt hauptsächlich durch Naturlasten. Dabei spielt für die bemessungsbestimmenden Lastfälle häufig der Wind eine entscheidende Rolle. Die Leiter, die mehrere hundert Meter weit spannen, tragen einen wesentlichen Anteil zur Gesamtbeanspruchung von Tragmasten bei, die wiederum Eigengewicht und Windlasten der Leiter zwischen zwei Abspannmasten abtragen. Wenn die Reaktion der Seile auf Starkwindereignisse abgeschätzt werden soll, müssen sowohl geometrische Nichtlinearitäten durch die großen Verformungen wie auch aerodynamische Nichtlinearitäten berücksichtigt werden. Insbesondere für die Anwendung und Berücksichtigung in Bemessungsvorschriften werden hierfür Vereinfachungen vorgenommen. In diesem Beitrag wird eine umfassende Untersuchung vorgestellt, über Naturmessungen, FEM-Simulationen kombiniert mit Windkanalversuchen und generierten Windzeitreihen. Ziel ist es, existierende Bemessungsvorschriften im Hinblick auf die Abschätzung der Beanspruchung aus Wind auf Leiter zu validieren. Hierbei sind insbesondere die Turbulenzannahmen und das dynamische Verhalten von weitgespannten Leitern wichtig, um die Extremschnittgrößen zu beschreiben. Mithilfe von so genannten Spannweitenfaktoren sollen die relevanten Parameter, wie Spannweite und Windturbulenz, bei der Beanspruchungsabschätzung berücksichtigt werden. N2 - The loading of overhead lines comprises of natural actions mainly. Wind loading signifies an important load case in the design of overhead transmission line structures. Conductors spanning often several hundreds of meters contribute significantly to the overall loading of suspension towers. Those towers are often designed as a mass product to support the dead and wind load of the conductors between two dead end towers. Estimating the reaction of the conductors to strong winds, both geometric nonlinearities because of the large deformations as well as aerodynamic nonlinearities need to be considered. Particularly for design procedures, those effects should be simplified. This paper presents a thorough investigation comprising field measurements along an existing overhead line, simulations with FEM combined with wind tunnel tests and generated wind fields. It is the aim of the study to validate the actual design procedure regarding loading of wind acting on conductors. Most important herein in order to describe the extreme response are assumptions on turbulence distribution and dynamic behavior of wide spanning overhead line conductors. According to usual design procedure, by means of so called span reduction factors, relevant parameters such as span length and wind turbulence can be considered. KW - Langzeitmessung KW - FEM-Simulation KW - Dynamik PY - 2017 DO - https://doi.org/10.1002/stab. 201710437 SN - 1437-1049 VL - 86 IS - 1 SP - 45 EP - 53 PB - Ernst & Sohn CY - Berlin AN - OPUS4-38899 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Trappe, Volker T1 - Betriebsfestigkeit von imperfekten und reparierten Rotorblättern N2 - Die Betriebsbeanspruchung für Rotorblätter ist aus Messungen bekannt. Schäden an Rotorblättern treten im Betrieb meistens an der Blattschale nach 4-5Jahren, weit vor der projektierten Lebensdauer von 20 Jahren auf und führen zum Anlagenstillstand, wenn sie nicht repariert werden. Mittels eines an der BAM entwickelten FKV-Sandwich-Schalenprüfkörpern kann effizient die Betriebs-festigkeit von Imperfektionen und Reparaturstellen studiert werden. Fertigungsbedingte Imperfektionen (Lagenstöße, Schaumstöße) verkürzen die Lebensdauer ggf. erheblich und führen zu Reparaturen. Experimentell konnte gezeigt werden, dass ein(e) aus-reparierte(r) Schaden/Imperfektion die Betriebsbeanspruchung deutlich besser erträgt, als die schadhafte Struktur.Die numerische Betriebsfestigkeitsvorhersage für FKV ist Gegenstand der Forschung. Gleiches gilt für die Abschätzung der Lebensdauerverkürzung infolge bekannter Fertigungsabweichungen. T2 - OFFSHORETAGE 15.03 - 16.03.2017, CY - Heiligendamm, Germany DA - 15.03.2017, KW - Rotorblätter KW - Windenergie KW - Faser-Kunststoff-Verbunde KW - Betriebsfestigkeit KW - Reparatur PY - 2017 AN - OPUS4-39440 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Browne, D. A1 - García-Moreno, F. A1 - Nguyen-Thi, H. A1 - Zimmermann, G. A1 - Kargl, F. A1 - Mathiesen, R. H. A1 - Griesche, Axel A1 - Minster, O. ED - Solanki, K. N. ED - Orlov, D. ED - Singh, A. ED - Neelameggham, N. R. T1 - Overview of In situ X-ray studies of light alloy solidification in microgravity N2 - Gravity has significant effects on alloy solidification, primarily due to thermosolutal convection and solid phase buoyancy. Since 2004, the European Space Agency has been supporting investigation of these effects by promoting in situ X-ray monitoring of the solidification of aluminium alloys on microgravity platforms, on earth, and in periodically varying g conditions. The first microgravity experiment-investigating foaming of liquid metals - was performed on board a sounding rocket, in 2008. In 2012 the first ever X-ray-monitored solidification of a fully dense metallic alloy in space was achieved: the focus was columnar solidification of an Al-Cu alloy. This was followed in 2015 by a similar experiment, investigating equiaxed solidification. Ground reference experiments were completed in all cases. In addition, experiments have been performed on board parabolic flights-where the effects of varying gravity have been studied. We review here the technical and scientific progress to date, and outline future perspectives. KW - Dendritic growth KW - Materials in space KW - Columnar and equiaxed structures PY - 2017 SN - 978-3-319-52392-7 SN - 978-3-319-52391-0 DO - https://doi.org/10.1007/978-3-319-52392-7_80 SN - 2367-1181 SP - 581 EP - 590 PB - Springer CY - Berlin, Heidelberg AN - OPUS4-39442 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR T1 - Amts- und Mitteilungsblatt, Band 47, Heft 1 T3 - Amts- und Mitteilungsblatt der BAM - 1/2017 PY - 2017 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-397023 SN - 0340-7551 VL - 47 IS - 1 SP - 1 EP - 358 PB - Bundesanstalt für Materialforschung und -prüfung (BAM) CY - Berlin AN - OPUS4-39702 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Martin, S. A1 - Walnsch, A. A1 - Nolze, Gert A1 - Leineweber, A. A1 - Léaux, F. A1 - Scheuerlein, C. T1 - The crystal structure of (Nb0.75Cu0.25)Sn-2 in the Cu-Nb-Sn system N2 - During the processing of superconducting Nb3Sn wire, several intermediate intermetallic phases including a previously encountered Cu-Nb-Sn phase show up. The yet unknown crystal structure of this phase is now identified by a combination of different experimental techniques and database search to be of the hexagonal NiMg2 type with a proposed composition of about (Nb0.75Cu0.25)Sn2. The structure determination started from an evaluation of the lattice parameters from EBSD Kikuchi patterns from quenched material suggesting hexagonal or orthorhombic symmetry. A database search then led to the hexagonal NiMg2 type structure, the presence of which was confirmed by a Rietveld analysis on the basis of high energy synchrotron X-ray powder diffraction data. Assuming a partial substitution of Nb in orthorhombic NbSn2 by Cu, the change of the valence electron concentration provokes a structural transformation from the CuMg2 type for NbSn2 to the NiMg2 type for (Nb0.75Cu0.25)Sn2. In the previous literature the (Nb0.75Cu0.25)Sn2 phase described here has occasionally been referred to as Nausite. KW - Electron backscatter diffraction KW - X-ray diffraction KW - Intermetallic compound KW - Structure solution KW - Superconductor PY - 2017 DO - https://doi.org/10.1016/j.intermet.2016.09.008 SN - 0966-9795 SN - 1879-0216 VL - 80 SP - 16 EP - 21 PB - Elsevier Ltd. AN - OPUS4-37874 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Keller, Christian A1 - Herbrich, Uwe T1 - Plastic Instability of Rate-Dependent Materials - A Theoretical Approach in Comparison to FE-Analyses - N2 - The condition for plastic instability is a material characteristic and defines the onset of necking in tensile tests. In large deformation problems of ductile materials it is fundamental to determine the strain at which necking starts as well as the post-necking behaviour in the instability region properly. For verification purposes of material models, usually results of numerical analyses are compared to experimental outcomes. For tensile tests with ductile materials under dynamic loading, it is challenging to obtain comparable experimental and numerical results in terms of the onset of necking and the post-critical deformation behaviour. This paper focuses on the derivation of a theoretical criterion describing the plastic instability in rate-dependent materials based on the time variation of the strain gradient in a tensile specimen under isothermal conditions. We examine the influence of various constitutive equations on the theoretical stability condition predicted by different multiplicative as well as additive approaches. For multiplicative relations, the results indicate that the onset of necking is, in principle, independent of the strain rate, whereas for the considered additive relation, the dynamic necking strain must decrease with increasing strain rate. In conclusion, the theoretical stability condition is related to results from finite element simulations of dynamic tensile tests with various loading rates. It is shown that the simulated and the theoretical predicted onset of plastic instability agree reasonably. T2 - 11th European LS-DYNA Conference CY - Salzburg, Austria DA - 09.05.2017 KW - FEM KW - Plastic Instability KW - Dynamic Tensile Test PY - 2017 UR - http://www.dynalook.com/11th-european-ls-dyna-conference/crash-metal-failure/plastic-instability-of-rate-dependent-materials-a-theoretical-approach-in-comparison-to-fe-analyses SP - 1 EP - 10 AN - OPUS4-40660 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Keller, Christian T1 - Plastic Instability of Rate-Dependent Materials - A Theoretical Approach in Comparison to FE-Analyses - N2 - The condition for plastic instability is a material characteristic and defines the onset of necking in tensile tests. In large deformation problems of ductile materials it is fundamental to determine the strain at which necking starts as well as the post-necking behaviour in the instability region properly. For verification purposes of material models, usually results of numerical analyses are compared to experimental outcomes. For tensile tests with ductile materials under dynamic loading, it is challenging to obtain comparable experimental and numerical results in terms of the onset of necking and the post-critical deformation behaviour. This paper focuses on the derivation of a theoretical criterion describing the plastic instability in rate-dependent materials based on the time variation of the strain gradient in a tensile specimen under isothermal conditions. We examine the influence of various constitutive equations on the theoretical stability condition predicted by different multiplicative as well as additive approaches. For multiplicative relations, the results indicate that the onset of necking is, in principle, independent of the strain rate, whereas for the considered additive relation, the dynamic necking strain must decrease with increasing strain rate. In conclusion, the theoretical stability condition is related to results from finite element simulations of dynamic tensile tests with various loading rates. It is shown that the simulated and the theoretical predicted onset of plastic instability agree reasonably. T2 - 11th European LS-DYNA Conference CY - Salzburg, Austria DA - 09.05.2017 KW - FEM KW - Plastic Instability KW - Dynamic Tensile Test PY - 2017 AN - OPUS4-40662 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eisermann, René T1 - Akustische Überwachung von Transformatoren mit Glasfasern?! N2 - Vorstellung aktueller Ergebnisse der Quasi-verteilten faseroptische Sensorik für die Echtzeit-Diagnostik von Hochspannungstransformatoren. T2 - Seminar Hochspannungstechnik und Energieversorgung CY - Technische Universität Berlin, Germany DA - 30.05.2017 KW - C-OTDR KW - Distributed acoustic sensing KW - Quasi-distributed vibration sensing KW - Structural health monitoring PY - 2017 AN - OPUS4-40637 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eisermann, René T1 - Advanced distributed acoustic monitoring N2 - New progress of developments of distributed acoustic monitoring. Review of previous results and lastest improvements. T2 - Seminar Angewandte Photonik CY - Goslar, Germany DA - 15.06.2017 KW - Distributed acoustic sensing KW - Structural health monitoring KW - Quasi-distributed sensing KW - Fibre optic sensors PY - 2017 AN - OPUS4-40640 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kühnel, C. A1 - Bardl, Richard A1 - Stengel, Dominik A1 - Kiewitt, W. A1 - Grossmann, S. T1 - Investigations on the mechanical and electrical behaviour of HTLS conductors by accelerated ageing tests N2 - To cope with future requirements, the transfer capacities of distribution systems as well as of transmission systems in Europe need to be increased. Therefore repowering of existing overhead lines with high temperature low sag con-ductors (HTLS) can be one interesting possibility. Because of limited experiences with that technology, current re-search of TU Dresden, the Federal Institute for Materials Research and Testing (BAM) and 50Hertz Transmission GmbH investigates the ageing behaviour of several differ-ent HTLS technologies in a consortium with other Euro-pean partners. In this context, accelerated ageing tests of conductors and its corresponding fittings with combined mechanical and electrical loads are done. To evaluate the changes due to ageing, several mechanical tests of the con-ductors are carried out and the contact behaviour of the fittings is analysed. T2 - CIRED Conference CY - Glasgow, Scotland, UK DA - 12.06.2017 KW - HTLS KW - High temperature low sag KW - Resistance KW - Self-damping PY - 2017 SP - Paper 0200, 1 EP - 5 AN - OPUS4-40869 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Palkowski, Carsten T1 - Technical and economical evaluation of energy efficiency testing for heat pumps N2 - In order to increase the total amount of energy savings to be reached in 2020 and 2050 the German government launched a number of initiatives. One of the associated projects aims to support market surveillance authorities in the field of Ecodesign and Energy Labelling, thereby increasing confidence in these instruments. The surveillance of heating appliances is of great importance as the energy consumed by space heaters accounts for a significant share of the total energy demand in the European Union. In this study heat pumps are analyzed as a high efficiency technology and prospective candidate for large energy savings. It is focused on both validating the current measurement standards for heat pumps and further developing these methods for the benefit of market surveillance authorities. The test method standards, EN 14511 and EN 14825, for testing heat pumps regarding their performance and energy efficiency are validated by conducting round robin tests in independent and accredited test laboratories. Based on these tests the reproducibility and repeatability of the standardized test methods and the laboratories in Europe are assessed. Identifying deficiencies in the methods is a fundamental step towards a sustained improvement process. Optimization proposals will be developed based on these fundamental investigations and brought to the attention of standardization bodies. It was figured out that the currently used test methods exhibit high complexity, high financial effort and reveal significant deviations of testing results depending on whether they were determined under laboratory or field test conditions. New testing and calculation methodologies are developed to simplify the process with the aim to increase the accuracy and affordability of the energy efficiency testing of heat pumps. T2 - 9th Asia-Pacific Power and Energy Engineering Conference (APPEEC 2017) CY - Chengdu, China DA - 15.04.17 KW - Heat pump KW - Energy efficiency KW - Test method standard optimization KW - Energy labelling KW - Climate change PY - 2017 AN - OPUS4-40800 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Palkowski, Carsten T1 - EU Energy Label for heating appliances - Optimization of test standards for heat pumps N2 - The European Standards EN14511 and EN14825 are representing standardized procedures for testing the energy efficiency of heat pumps and air conditioners with electrically driven compressors for both space heating and cooling. In this study, these standards are analyzed and validated. It was figured out that the currently used methods implicate high complexity and high financial effort. In order to clarify the circumstances and to identify the deficits more in detail, a round robin test with independent and accredited laboratories was initiated. The aim is to develop an optimized test procedure that improves the feasibility of the testing procedure and finally its application. This study should lead to a repeatable and reproducible testing procedure, which is also compatible with the state of the art in heat pump technology and real operation conditions. T2 - ECEEE Summer Study 2017 CY - Hyerès, France DA - 29.05.2017 KW - Heat pump KW - Energy efficiency KW - Test method standard optimization KW - Energy labelling KW - Climate change PY - 2017 AN - OPUS4-40801 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR T1 - Amts- und Mitteilungsblatt, Band 47, Heft 2 T3 - Amts- und Mitteilungsblatt der BAM - 2/2017 PY - 2017 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-408040 SN - 0340-7551 VL - 47 IS - 2 SP - 359 EP - 453 PB - Bundesanstalt für Materialforschung und -prüfung (BAM) CY - Berlin AN - OPUS4-40804 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Bauer, Ute A1 - Behrens, H. A1 - Reinsch, Stefan A1 - Morin, E. I. A1 - Stebbins, J. F. T1 - Structural investigation of hydrous sodium borosilicate glasses N2 - The structural properties of a borosilicate glass with nominal 16 mol% Na2O, 10 mol% B2O3 and 74mol% SiO2 and water contents between 0 and 8wt% H2O (0–22 mol% H2O)were investigated with IR, Raman and 11BMAS NMR spectroscopy. In addition to the pronounced OH stretching vibration band of weakly H-bonded species at 3580 cm−1 the MIR spectra show a triplet at 2900, 2350 and 1750 cm−1, similar as observed in water-bearing silicate glasses. These bands are assigned to OH groups and water molecules which are strongly H-bonded, to non-bridging oxygen. Water species contents determined from absorption bands in the NIR at 5200 cm−1 (molecular H2O), 4700 cm−1 (B\\OH), and 4500 cm−1 (Si\\OH) indicate that hydroxyl groups dominate up to ~6 wt% total H2O. Based on the absorption coefficients known from literature for silicate and borate glasses the B\\OH/Si\\OH ratio is estimated to be ≈0.8. As indicated by density, Raman and NMR data the incorporation ofwater has strong structural impacts in particular at low water contents up to 3 wt% H2O. While the nominally dry glasses still contain a significant fraction (12%) of three-fold coordinated boron, almost all boron is four-fold coordinated in hydrous glasses. The increase of band components in the Raman spectra near 900 cm−1 relative to the region N 1050 cm−1 gives evidence for depolymerization of the network upon hydration. Fitting of the spectra with Gaussians implies that silica tetrahedra with two non-bridging oxygen (Q2) are preferentially formed by reactionwithwater on expense of tetrahedra linked to four tetrahedra (Q4). KW - Glass structure KW - Borosilicate glasses KW - Water-bearing glasses KW - Spectroscopy PY - 2017 DO - https://doi.org/10.1016/j.jnoncrysol.2017.03.023 SN - 0022-3093 SN - 1873-4812 VL - 465 SP - 39 EP - 48 PB - Elsevier B. V. AN - OPUS4-40805 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Barnefske, Lena T1 - Entwicklung eines mechanisch verstärken und selbstheilenden Silikonelastomers auf Basis eines Kapsel-basierten Ansatzes N2 - Im Arbeitskreis von Herrn Prof. Dr. Menzel (TU Braunschweig) wurde in Sievershausen ein Vortrag zum Thema „Self-healing and mechanically reinforced silicone rubber by the use of multifuctional capsules“ gehalten. Der Vortrag beginnt mit einer kurzen Motivation und einem Überblick über selbstheilende Materialien. Daraufhin werden die Ergebnisse zur Entwicklung eines selbstheilenden Silikonelastomers auf Basis von Kapseln, bestehend aus einem PDMS Kern und einer POS Hülle, dargestellt. Es folgt die Analytik, die auf DLS, TGA, UV/Vis und Fluoreszenzspektroskopie sowie SEM beruht. Der Vortrag endet mit einem Ausblick über zukünftige Arbeiten auf dem Gebiet. T2 - Seminar in Sievershausen CY - Sievershausen, Lehrte, Germany DA - 07.06.2017 KW - Selbstheilung KW - PDMS PY - 2017 AN - OPUS4-40857 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hüllmann, Dino T1 - Aerial Robot Olfaction - Mobile Gas Sensors N2 - An introduction to BAM, gas source localisation and gas distribution mapping is given. Both an example for in-situ and open-path gas sensors is shown. The flight platforms used at BAM are introduced. T2 - Workshop "Drohnen in der Wissenschaft" CY - Potsdam, Germany DA - 30.06.2017 KW - Gassensor KW - Olfaction KW - Multicopter PY - 2017 AN - OPUS4-40858 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Krankenhagen, Rainer T1 - Detektion von Fertigungsschäden mithilfe thermografischer Tiefenprüfung N2 - Thermografie als zerstörungsfreies Prüfverfahren ist prinzipiell gut geeignet, um innen liegende Fehler in Rotorblättern zu detektieren. Im Vortrag wird die Anwendbarkeit des Messprinzips zuerst theoretisch und dann an Hand von Praxisfällen gezeigt. Weiterhin werden erste Ergebnisse aus einem laufenden FuE-Projekt zur Tiefenreichweite der Messmethode demonstriert und erläutert. T2 - 6. VDI-Fachkonferenz "Rotorblätter von Windenergieanlagen" CY - Bremen, Germany DA - 27.06.2017 KW - Thermografie KW - Fertigungsfehler KW - Rotorblatt PY - 2017 AN - OPUS4-40861 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kuschke, Christian A1 - Wille, Frank A1 - Ballheimer, Viktor A1 - Sterhaus, Jens A1 - Apel, Andreas T1 - Standards and guidelines for design of trunnions of RAM transport packages N2 - Trunnion systems of packages for the transport of radioactive materials have to guarantee the safe handling of package during crane operations (lifting, tilting) and to secure package tie down to the transport vehicle, if the trunnions are used as attachment points during transport. The design of trunnions is based on IAEA Regulations SSR-6, the supporting Advisory Material SSG-26 and further appropriate technical standards and/or guidelines. For package approval procedures in Germany the guideline BAM-GGR 012 has to be applied. If a package is handled inside a german nuclear power plant, the standard KTA 3905 has to be fulfilled additionally. In this paper the requirements of KTA 3905 concerning the trunnion systems as load attaching points (LAP) are discussed in connection with the recommendations in the guideline BAM-GGR 012. This guideline is prepared at BAM Federal Institute for Materials Research and Testing for analysis and assessment of bolted lid and trunnion systems of Type B(U) transport packages. The Quality assurance questions concerning trunnion systems are discussed as well. T2 - WM 2017 conference CY - Phoenix, USA DA - 05.03.2017 KW - RAM transport package KW - Trunnions PY - 2017 SP - Paper 17365, 1 EP - 12 AN - OPUS4-40815 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eisermann, René T1 - Applications of distributed acoustic sensing N2 - Review of early AIP related early developments. Overview of distributed methods at BAM. Examples of applications of distributed acoustic sensing for infrastructure monitoring. T2 - innoFPSEC Photonik Seminar CY - Potsdam, Germany DA - 07.06.2017 KW - Fibre-optic sensing KW - Distributed acoustic sensing KW - Structural health monitoring PY - 2017 AN - OPUS4-40641 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eisermann, René T1 - Reducing sensitivity fading in C-OTDR by use of enhanced scattering fiber segments N2 - We have shown that for C-ODTR based DAS two UV-inscribed scattering segments within an optical fiber have a significant influence on the local sensitivity Fading characteristics. This method was experimental proven to be suitable for distributed dynamic strain measurement in a thermally unstable environment. Signal-to-noise ratio analyses for detecting a signal peak within the time-dependent spectra were performed. Results show an increase in SNR and additionally that the occurrence of total loss of sensitivity (SNR <1) could be decreased by a factor of six when compared to an untreated standard fiber. T2 - 25th International Conference on Optical Fiber Sensors CY - Jeju-City, Jeju, Republic of Korea DA - 24.04.2017 KW - Coherent Rayleigh OTDR KW - Distributed acoustic sensing KW - Distributed vibration sensing KW - Fiber sensors KW - Quasi-distributed sensing KW - Rayleigh scattering PY - 2017 AN - OPUS4-40643 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kapa, Thomas T1 - Distributed Brillouin Sensors N2 - This presentation starts with an overview of various optical sensing applications of Department 8.6 Fiber Optic Sensors. Main topic of presentation is distributed Brillouin sensing of strain and temperature by Brillouin Optical Frequency Domain Analysis (BOFDA). For power grids of offshore wind farms temperature and strain sensing should prevent or rapidly reveal costly break downs. T2 - Seminarvortrag TU Clausthal CY - Goslar, Germany DA - 15.06.2017 KW - Fibre Optic Sensors KW - Stimulated Brillouin Scattering KW - Distributed Sensing PY - 2017 AN - OPUS4-40966 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Geißler, Peter T1 - Verdichtungsinjektionen - numerische und experimentelle Betrachtungen N2 - Die Verdichtungsinjektion stellt ein Verfahren in der Geotechnik dar, bei dem der Baugrund durch Einpressen eines Mörtels mit hoher innerer Reibung verdichtet wird, ohne ihn aufzubrechen. Dieses Verfahren wird weithin verwendet zur Setzungskontrolle oder Erhöhung der Tragfähigkeit des Baugrunds unter neuen bzw. bestehenden Bauwerken. Da die Injektion innerhalb des Bodens stattfindet, ist eine visuelle Beurteilung des Verdichtungserfolgs nicht möglich. Bisher beruht die Beurteilung bzw. Bewertung daher zumeist auf Erfahrungen. Ziel ist es somit mittels numerischer und experimenteller Untersuchungen eine Methode zu erschaffen, die es ermöglicht den Verdichtungserfolg nicht nur vorherzusagen sondern auch bezüglich der Materialparameter des Injektionsguts zu optimieren. Bezüglich der Numerik werden sowohl die grundsätzliche Eignung als auch die ersten notwendigen Anpassungen der impliziten "Material Point Method" zur Simulation einer Verdichtungsinjektion präsentiert. Für die experimentellen Untersuchungen wurde eigens ein Versuchsstand konstruiert, in dem es möglich ist, den Injektionsprozess an einer Glasscheibe zu beobachten und mittels digitaler Bildverarbeitung zu bewerten. T2 - Workshop "Große Verformungen" CY - Berlin, Germany DA - 13.06.2017 KW - Verdichtungsinjektionen KW - Material point method KW - Nichtlinearitäten KW - Updated Lagrange Formulierung KW - u-p-Formulierung KW - Digitale Bildverarbeitung KW - Particle image velocimetry KW - Close range photogrammetry PY - 2017 AN - OPUS4-40894 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - INPR A1 - Schlichting, S. A1 - Hönig, Gerald A1 - Müßener, J. A1 - Hille, P. A1 - Grieb, T. A1 - Teubert, J. A1 - Schörmann, J. A1 - Wagner, M. R. A1 - Rosenauer, A. A1 - Eickhoff, M. A1 - Hoffmann, A. A1 - Callsen, G. T1 - Tuning of the Quantum-Confined Stark Effect in wurtzite [000-1] group-III-nitride nanostructures by the Internal-Field-Guarded-Active-Region Design N2 - Recently, we suggested an unconventional approach [the so-called Internal-Field-Guarded-Active-Region Design (IFGARD)] for the elimination of the crystal polarization field induced quantum confined Stark effect (QCSE) in polar semiconductor heterostructures. And in this work, we demonstrate by means of micro-photoluminescence techniques the successful tuning as well as the elimination of the QCSE in strongly polar [000-1] wurtzite GaN/AlN nanodiscs while reducing the exciton life times by more than two orders of magnitude. The IFGARD based elimination of the QCSE is independent of any specific crystal growth procedures. Furthermore, the cone-shaped geometry of the utilized nanowires (which embeds the investigated IFGARD nanodiscs) facilitates the experimental differentiation between quantum confinement- and QCSE-induced emission energy shifts. Due to the IFGARD, both effects become independently adaptable. KW - Piezoelectricity KW - Quantum Confined Stark Effect (QCSE) KW - Nanophotonics KW - Semiconductor nanostructures KW - Spontaneous polarization KW - Internal-Field-Guarded-Active-Region Design (IFGARD) PY - 2017 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-411013 DO - https://doi.org/10.48550/arXiv.1707.06882 SN - 2331-8422 SP - 1 EP - 9 PB - Cornell University CY - Ithaca, NY AN - OPUS4-41101 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Stengel, Dominik A1 - Thiele, K. A1 - Clobes, M. A1 - Mehdianpour, Milad T1 - Aerodynamic damping of nonlinear movement of conductor cables in wind tunnel tests, numerical simulations and full scale measurements N2 - Aerodynamic damping is a decisive parameter influencing the dynamic response of overhead transmission line conductors. Methods of how to account for the effects of aerodynamic damping differ significantly and so might do the results. In this work, the source of aerodynamic damping being the result of the relative velocity between the structure and wind flow will be revised. Based on wind tunnel tests and validated by simulations, the differences of linear movement compared to a pendulum movement of a sagging cable are shown. The reasons for that Deviation are the large deflections, resulting in a movement non-parallel to the acting wind flow. For analysis in frequency domain, it is not possible to incorporate aerodynamic damping implicitly by fluid structure interaction. If the dynamic movement can be linearized at a working point of the mean deflection, a modification to the linear approach is suggested. This approach is validated by simulation with a finite element model of an existing overhead transmission line, calibrated with full scale measurements. Aerodynamic damping is incorporated in time step analysis by Rayleigh damping and modal damping. The differences between both approaches are emphasized and modal damping is shown to be the most adequate. KW - Aerodynamic damping KW - Overhead transmission lines KW - Conductors KW - Nonlinearities PY - 2017 DO - https://doi.org/10.1016/j.jweia.2017.07.002 SN - 0167-6105 SN - 1872-8197 VL - 169 SP - 47 EP - 53 PB - Elsevier AN - OPUS4-41028 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schönhals, Andreas T1 - Molecular dynamics of discotic liquid crystals in the bulk and embedded in nanochanels N2 - Discotic liquid crystals (DLCs) are self-assembled materials where self-assembly is driven by non-covalent intermolecular interactions. The corresponding molecules consist of a flat and rigid aromatic core substituted by flexible aliphatic side chains. While the former is responsible for the π-stacking, the latter gives rise to an increased solubility, processability, and rich thermotropic behavior. The disc-shaped molecules form columns that further assemble into two-dimensional arrays with a hexagonal mesophase. The alkyl chains fill the intracolumnar space giving rise to a nanophase separated state. These soft matter materials with highly ordered columnar structures have a great potential in molecular electronic devices such as active semiconductors in organic field-effect transistors and photovoltaic devices with a charge carrier mobility of up to 1.1 cm2/Vs. Two different homologous systems based on triphenylene derivatives were investigated as model systems for DLCs where the length of the aliphatic side chains is widely varied. Structural information is retrieved by X-ray diffraction carried out on a synchrotron. Experiments were carried out in the bulk state and confined to the nanometer wide channels of anodic aluminum membranes (Pore diameter 20 nm, 40nm, 80 nm and 180 nm). The latter case can be considered as a promising way to prepare nanowires. As method broadband dielectric spectroscopy (frequency range 10-2 Hz to 109 Hz) is employed. These experiments were accompanied by thermal investigations (Differential Scanning Calorimetry as well as Thermogravimetric Analysis) as well as inelastic neutron scattering (neutron Time-of-Flight and neutron Backscattering). The dynamics of these unique soft matter materials are discussed in detail considering their structure (length of the aliphatic side chain), the effect of self-confinement (of the aliphatic chains in the intracolumnar space) and of the outer confinement (influence of the pore size). Comparison is further made to a pyrene based system. T2 - THE 9th INTERNATIONAL CONFERENCE ON ADVANCED MATERIALS, ROCAM 2017 CY - Bucharest, Romania DA - 11.07.2017 KW - Dicotic liquid crystals PY - 2017 AN - OPUS4-41023 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Dutto, Paola T1 - Suction buckets behaviour under tensile loads: A numerical study with FEM N2 - Suction Bucket Jackets (SBJ) are found as a suitable alternative to driven piles for the support of foundations for offshore wind energy converters. In the case of jackets or multipods, a predominant vertical load is to be expected. The effect of such a tensile loading is the generation of suction in the soil inside the bucket which leads to an increment of tensile capacity. This paper aims to study the bearing behaviour of a suction foundation by taking into account how the soil permeability and the loading rate influence the foundation behaviour. Moreover, after submitting the structure to a storm load, the bearing capacity is studied again, in order to see the effect of such a load on the bucket's bearing behaviour. This study is carried out by means of Finite Element numerical simulations based on the formulation of Biot's equations combined with a constitutive model that reproduces the key aspects of cyclic soil behaviour in the frame of Generalized Plasticity. T2 - International Ocean and Polar Engineering Conference CY - San Francisco, USA DA - 25/06/2017 KW - Finite element method KW - Offshore wind energy converter KW - Suction bucket KW - Generalized plasticity KW - Sand KW - Numerical simulation KW - Tensile capacity PY - 2017 AN - OPUS4-41054 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Hüllmann, Dino A1 - Kohlhoff, Harald A1 - Erdmann, Jessica A1 - Neumann, Patrick P. ED - Emri, Igor T1 - Current-independent torque control of permanent-magnet synchronous motors N2 - A current-independent torque equation for the permanent-magnet synchronous motor (PMSM) aiming at direct-drive servo applications is derived from a first principles model. Instead of measuring currents, all required control parameters are derived from optical incremental encoder measurements. The results are verified on a real system in test series showing the effect of static friction and proving the obtained torque model. T2 - 33rd Danubia Adria Symposium on Advances in Experimental Mechanics CY - Portorož, Slovenia DA - 20.09.2016 KW - BLDC KW - Motor control KW - PMSM KW - Servo drive PY - 2017 UR - http://www.sciencedirect.com/science/article/pii/S2214785317308271 DO - https://doi.org/10.1016/j.matpr.2017.06.052 SN - 2214-7853 VL - 4 IS - 5 SP - 5821 EP - 5826 PB - Elsevier CY - Amsterdam, Netherlands AN - OPUS4-41580 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Neumann, Patrick P. A1 - Lazik, D. A1 - Bartholmai, Matthias ED - Emri, Igor T1 - Validation of membrane-based linear soil gas sensors under field conditions N2 - A 400 m2 soil test field with gas injection system was built up, which enables an experimental validation of linear membrane-based gas sensors – a sensor technology which was developed based on the selective permeation of gases through membranes. Several soil watering and injection experiments with carbon dioxide at different days with varying boundary conditions were performed showing that the sensor behaves mostly insensitive to the environmental conditions investigated, i.e., barometric pressure fluctuations, soil temperature, air temperature and humidity, sun duration, and wind speed. Furthermore, depending on water infiltration, a gas phase displacement could be observed in-situ based on the changed measurement signal. The results of the validation experiments highlight the potential of the method for rapid leak detection and localization qualifying the sensor particularly for safety applications, e.g., in underground gas storage areas. T2 - 33nd Danubia Adria Symposium on Advances in Experimental Mechanics CY - Portorož, Slovenia DA - 20.09.2016 KW - Distributed linear sensor KW - Membrane-based gas sensing KW - Subsurface monitoring KW - Gas storage areas KW - Validation PY - 2017 UR - http://www.sciencedirect.com/science/article/pii/S2214785317308404 DO - https://doi.org/10.1016/j.matpr.2017.06.065 SN - 2214-7853 VL - 4 IS - 5, Part 1 SP - 5893 EP - 5897 PB - Elsevier Ltd. AN - OPUS4-41584 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Neumann, Martin A1 - Eisenacher, Germar A1 - Schönfelder, Thorsten A1 - Wille, Frank T1 - Development of a material model for the crush of spruce wood N2 - Typical transport packages used in Germany are equipped with wooden impact limiting devices. In this paper we give an overview of the latest status regarding the development of a finite element material model for the crush of spruce wood. Although the crush of wood – mainly in longitudinal direction – is a phenomenon governed by macroscopic fracture and failure of wood fibres we smear fracture and failure mechanisms over the continuous voume. In first step we altered an existing LS-DYNA material model for foams, which considers an ellipse shaped yield surface written in terms of the first two stress invariants. The evolution of the yield surface in the existing model depends on the volumetric strain only. For the use with spruce wood, we modified the existing material model to consider the deviatoric strain for the evolution of the yield surface as well. This is in accordance with the results of crush tests with spruce wood specimens, where the crushing deformation was rather deviatoric for uniaxial stress states and rather volumetric for multiaxial stress states We rate the basic idea of this approach to be reasonable, though other problems exist regarding the shape of the yield surface and the assumption of isotropic material properties. Therefore we developed a new transversal isotropic material model with two main directions, which considers different yield curves according to the multiaxiality of the stress state via a multi-surface yield criterion and a non-associated flow rule. The results show the ability to reproduce the basic strength characteristics of spruce wood. Nevertheless, problems with regularization etc. show that additional investigations are necessary. T2 - ASME PVP 2017 CY - Waikaloa, HY, USA DA - 16.07.2017 KW - Chrush KW - Spruce KW - Wood KW - FEM PY - 2017 SN - 978-0-7918-5802-8 VL - 7 SP - Article UNSP V007T07A037, 1 EP - 9 AN - OPUS4-41613 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Neumann, Martin T1 - Development of a material model for the crush of spruce wood N2 - Typical transport packages used in Germany are equipped with wooden impact limiting devices. In this paper we give an overview of the latest status regarding the development of a finite element material model for the crush of spruce wood. Although the crush of wood – mainly in longitudinal direction – is a phenomenon governed by macroscopic fracture and failure of wood fibres we smear fracture and failure mechanisms over the continuous voume. In first step we altered an existing LS-DYNA material model for foams, which considers an ellipse shaped yield surface written in terms of the first two stress invariants. The evolution of the yield surface in the existing model depends on the volumetric strain only. For the use with spruce wood, we modified the existing material model to consider the deviatoric strain for the evolution of the yield surface as well. This is in accordance with the results of crush tests with spruce wood specimens, where the crushing deformation was rather deviatoric for uniaxial stress states and rather volumetric for multiaxial stress states We rate the basic idea of this approach to be reasonable, though other problems exist regarding the shape of the yield surface and the assumption of isotropic material properties. Therefore we developed a new transversal isotropic material model with two main directions, which considers different yield curves according to the multiaxiality of the stress state via a multi-surface yield criterion and a non-associated flow rule. The results show the ability to reproduce the basic strength characteristics of spruce wood. Nevertheless, problems with regularization etc. show that additional investigations are necessary. T2 - ASME PVP 2017 CY - Waikaloa, HY, USA DA - 16.07.2017 KW - Crush KW - Wood KW - Spruce KW - FEM PY - 2017 AN - OPUS4-41617 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Le, Quynh Hoa A1 - Bäßler, Ralph A1 - Yevtushenko, Oleksandra A1 - Kratzig, Andreas A1 - Bettge, Dirk T1 - Synergistic effects of impurities in the condensate on the corrosion of CO2 transport pipeline N2 - For the reliability of transport pipelines the corrosion resistance of the materials used needs to be determined in conditions, which are possible during the transport process. In some situations condensation of components out of the CO2 stream can occur. To study the effect of condensate on transport pipeline steel, a “worst-case scenario” gas mixture, containing 2.5 % H2O, 1.8 % O2, 1000 ppmv NO2, and 220 ppmv SO2, was proposed, fed (1.5 L/min) into a glass reactor containing coupon-shaped specimens for 120 600 h at 278 K (to simulate the underground pipeline transport), and resulted in the condensate containing 0.114 M H2SO4 and 0.0184 M HNO3 (pH 2.13). Basing on this “original” condensate, exposure tests and electrochemical characterization together with pH and conductivity in CO2 saturated condition at the same temperature were carried out. The role of each gas impurity and the combination of them, when the condensate is formed, was studied by investigating the role of individual and varying combination of acidic components in the condensate on the corrosion behaviors of the commercial pipeline-steel (L360NB). It can be concluded that although the condensation of NOx in form of HNO3 causes faster corrosion rate, it is the condensation of SOx or the combination of SOx and NOx that may cause much more severe problems in form of localized and pitting corrosions. Different to the corrosion products formed in CO2 atmosphere without impurities (mainly iron carbonate) the corrosion products resulted from these acidic condensation have no protectability, indicating the need of controlling gas quality during the transportation within the pipeline network. T2 - EUROCORR 2017 - PRAG CY - Prague, Czech Republic DA - 03.09.2017 KW - CCUS KW - CO2 corrosion KW - Carbon steels KW - Condensate PY - 2017 SP - Paper 75636,.1 EP - 4 AN - OPUS4-41874 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schneider, Ronald T1 - Konzept zur Einbindung der Strukturüberwachung in die risikobasierte Inspektionsplanung von Offshore-Strukturen N2 - Das Ermüdungsverhalten einzelner Schweißverbindungen in Offshore-Strukturen ist stark korreliert. Diese Korrelation entsteht zum einen durch die Verwendung gleicher Prozesse und Materialien bei der Herstellung der Verbindungen, zum anderen sind die ermüdungswirksamen Lasten an verschiedene Hospots im Tragwerk ebenfalls von einander abhängig. Hieraus ergeben sich Systemeffekte, die es ermöglichen, durch stichprobenartige Inspektion des Zustandes einzelner Hotspots auf den Zustand der verbleibenden Hotspots im Tragwerk zu schließen. Auf dieser Grundlage können Inspektions- und Reparaturstrategien für ermüdungsbeanspruchte Offshore-Strukturen mit Hilfe von riskobasierten Methoden optimiert werden. In diesem Vortrag wird weiterführend ein Konzept zur Einbindung von globalen Monitoringergebnissen in die risikobasierte Inspektionsplanung vorgestellt. T2 - 29. Sitzung des VDI/VDE-GMA Fachausschuss 2.12 Strukturanalyse und -überwachung in der Bautechnik im Fachbereich Prozessmesstechnik und Strukturanalyse CY - Bremen, Germany DA - 06.09.2017 KW - Ermüdung KW - Offshore-Strukturen KW - Risikobasierte Inspektionsplanung KW - Monitoring PY - 2017 AN - OPUS4-41865 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schlegel, Moritz-Caspar T1 - Nano-porous Materials - Introduction into Metal-organic Frameworks N2 - Metallic organic frameworks are the materials stirring great interest by their large variety of structure types and chemical composition as well as low density and very high surface area, which are desirable properties for gas storage such as for hydrogen, methane or carbon dioxide. Using different so called secondary building units offer an opportunity to form tunable structures with channels of various geometry and allow in this way to study the absorption of the molecular hydrogen, methane or carbon dioxid in the systematic way. T2 - Neutron Scattering Application to Hydrogen Storage Materials CY - Berlin, Germany DA - 07.08.2017 KW - MOFs KW - Hydrogen KW - Crystallography PY - 2017 AN - OPUS4-41285 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Palkowski, Carsten A1 - Schlegel, Moritz-Caspar A1 - Akkerman, Floris A1 - Simo, Anne T1 - EU Energy Label for heating appliances - Optimization of test standards for heat pumps N2 - The European Standards EN14511 and EN14825 are representing standardized procedures for testing the energy efficiency of heat pumps and air conditioners with electrically driven compressors for both space heating and cooling. In this study, these standards are analyzed and validated. It was figured out that the currently used methods implicate high complexity and high financial effort. In order to clarify the circumstances and to identify the deficits more in detail, a round robin test with independent and accredited laboratories was initiated. The aim is to develop an optimized test procedure that improves the feasibility of the testing procedure and finally its application. This study should lead to a repeatable and reproducible testing procedure, which is also compatible with the state of the art in heat pump technology and real operation conditions. T2 - ECEEE Summer Study 2017 CY - Hyères, France DA - 29.05.2017 KW - Climate change KW - Energy efficiency KW - Energy labelling KW - Heat pumps KW - Test method standard optimization PY - 2017 SN - 978-91-983878-1-0 SN - 2001-7960 SP - 1551 EP - 1555 AN - OPUS4-41287 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Akkerman, Floris T1 - Die Ökodeisgn-Richtlinie N2 - Allgemeiner Vortrag zur Ökodesign-Richtlinie und ihrer Bedeutung für die Industrie. T2 - Großes Netzwerktreffen Süd CY - IHK Ulm, Germany DA - 30.05.2017 KW - Ökodeisgn KW - Energieeffizienz KW - EU-Recht PY - 2017 AN - OPUS4-41255 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Knieschewski, Arno T1 - How standards can better reflect consumer relevance on the example of range Hoods N2 - The performance test of range hoods can be improved by using an atomizer nozzle. T2 - ECEEE 2017 summer study on energy efficiency CY - Hyères, France DA - 29.05.2017 KW - Range hood KW - Energy efficiency PY - 2017 AN - OPUS4-41139 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Knieschewski, Arno T1 - How standards can better reflect consumer relevance on the example of range hoods N2 - The EU’s Ecodesign and Energy Labelling Regulations for domestic cooking appliances became legally binding in 2015. To determine the classes on the energy label, the regulations refer to the European Standard for performance measurements of range hoods EN 61591. The standard EN 61591 has been analysed and evaluated within the National Action Plan on Energy Efficiency (NAPE), a government programme that aims to increase the energy efficiency in Germany. The analysis revealed several drawbacks of the test standard. The standard used for the evaluation of range hoods is composed of methods for determining: (i) volumetric airflow, (ii) odour extraction, (iii) effectiveness of the lighting system and (iv) grease absorption. Currently, the grease absorption class is obtained by heating up oil and water in a pot, which creates vapour and splashes of grease. In this paper different alternative methods for the evaluation of the grease absorption efficiency will be discussed. In the proposed test method an atomizer nozzle is used. Consequently, the exact amount of atomized oil is known and the ratio of filtered to atomized oil can be measured. Thereby the proposed new method is able to take into account aerodynamic designs and leaks. Furthermore, it enables to alter the classification guideline of the energy label to give more significant and consumer relevant declarations. It allows manufacturers to develop innovative grease absorption methods with little airflow. This study revealed that it can be beneficial to review more of the existing standards in the light of improving their consumer relevance. T2 - ECEEE 2017 - Summer Study on energy efficiency CY - Hyères, France DA - 29.05.2017 KW - Range hood KW - Energy efficiency KW - Energy label PY - 2017 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-411425 SN - 978-91-983878-0-3 SN - 978-91-983878-1-0 SN - 2001-7960 SN - 1653-7025 SP - 1557 EP - 1561 AN - OPUS4-41142 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Sie, M. A1 - Susca, Tiziana A1 - Portal, Natalie Williams A1 - During, O. A1 - Fontana, Patrick A1 - Sjöström, C. ED - de Schutter, G. ED - de Belie, N. ED - Janssens, A. ED - van den Bossche, N. T1 - Influence of life span prediction on building component's LCA performance N2 - The life span of a building product is a key Parameter when it comes to Life Cycle Assessment (LCA) performance. Nevertheless, many uncertainties affect this parameter due to a lack of long-term performance data. The sensitivity of the LCA outcomes to this parameter has been studied within the framework of the FP7 project H-House (Healthier Life with Eco-innovative Components for Housing Constructions) funded by the European Commission. The paper Features two comparative studies conducted within the scope of this project: one for new construction and another for renovation. An innovative precast sandwich panel made of Textile Reinforced Concrete (TRC) and Foamed Concrete (FC), used for external walls in new construction, is compared with a steel reinforced concrete (SRC) wall of the same thermal resistance. For renovation, a novel halfsandwich panel made of Ultra-High-Performance-Concrete (UHPC) and Autoclaved Aerated Concrete (AAC) is compared with cladding having the same thermal performance. The Evaluation was conducted using a multi-criteria basis according to the LCA methodology (ISO 14040- 44). In each case, an identical life span for both scenarios leads to the fact that H-House components have a better environmental performance. The ISO 15686 and ist relevant parts have been considered for the estimation of the service life span. The sensitivity analysis shows the link between the impact savings of the innovative walls and the life span of the walls and their components. In particular, it was found that since both scenarios need to fulfil the same service during an identical reference period, and since some maintenance and replacement of materials are necessary over time for standard Solutions compared to the innovative ones, the chosen life span of the components plays a role of utmost importance. The sensitivity analysis discloses the effect of the assumptions on these aspects. T2 - XIV DBMC - 14th International Conference on Durability of Building Materials and Components CY - Ghent, Belgium DA - 29.05.2017 KW - LCA KW - Life span KW - TRC KW - UHPC KW - ISO 15686 PY - 2017 SN - 978-2-35158-159-9 VL - PRO 107 SP - 371 EP - 372 PB - RILEM Publications S.A.R.L. AN - OPUS4-40999 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wagner, M. R. A1 - Schlichting, S. A1 - Müßener, J. A1 - Hille, P. A1 - Teubert, J. A1 - Schörmann, J. A1 - Rosenauer, A. A1 - Eickhoff, M. A1 - Hoffmann, A. A1 - Callsen, G. A1 - Hönig, Gerald T1 - Suppression of the quantum confined Stark effect in polar III-nitride heterostructures N2 - One of the most significant limitations for the quantum efficiency of group III-nitride based light emitters is the spatial electron-hole separation due to the quantum-confined Stark effect (QCSE). To overcome this problem, Hönig et al. [1] proposed a novel concept, the Internal-Field-Guarded-Active-Region Design (IFGARD), which suppresses the QCSE for wurtzite crystals in the [0001] direction. Here, we show how encapsulating the active region by additional guard layers results in a strong reduction of the built-in electric field in c-plane wurtzite nanostructures. Even more importantly, we demonstrate the first experimental evidence for the successful realization of an IFGARD structure based on GaN/AlN heterostructures embedded in GaN nanowires. By means of power-dependent and time-resolved µ-photoluminescence (µ-PL) we experimentally proof the validity of the unconventional IFGARD structure. We managed to tune the emission of 4-nm-thick GaN nano-discs up to 3.32 eV at low excitation powers, which is just 150 meV below the bulk GaN bandgap. Our results demonstrate an almost complete elimination of the QCSE in comparison to conventional structures which show approximately 1 eV red-shifted emission. The suppression of the QCSE results in a significant increase of the radiative exciton decay rates by orders of magnitude and demonstrates the potential of IFGARD structures for future light sources based on polar heterostructures. [1] Hönig et al., Phys. Rev. Applied 7, 024004 (2017) T2 - International Conference on Nitride Semiconductors 12 of the European Materials Research Society CY - Strasbourg, France DA - 24.07.2017 KW - Nanophotonics KW - Piezoelectricity KW - Quantum confined stark effect KW - Semiconductor nanostructures KW - Spontaneous polarization PY - 2017 AN - OPUS4-41194 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Yin, Huajie A1 - Chapala, P. A1 - Bermeshev, M. A1 - Schönhals, Andreas A1 - Böhning, Martin T1 - Molecular Mobility and Physical Aging of a Highly Permeable Glassy Polynorbornene as Revealed by Dielectric Spectroscopy N2 - Polymeric membranes represent a cost- and energy efficient solution for gas separation. Recently superglassy polymers with high free volume outperform many conventional dense polymers in terms of gas permeability and selectivity. However, such polymers are prone to pronounced physical aging, resulting in a dramatic reduction in the gas permeability. Molecular mobility of polymer segments plays an important role in the physical aging and the gas transport performance of polymeric membranes. Molecular mobility and physical aging of a representative superglassy polynorbornene with very high gas permeability, PTCNSi2g, was monitored by using dielectric spectroscopy with state-of-the-art high-resolution analyzers. This work helps to shed some light on the structure−property relationship of superglassy polymers on a molecular level and to provide practical “design rules” for the development of high performance polymers for gas separation. KW - Molecular mobility KW - Gas separation membrane KW - Broadband dielectric spectroscopy KW - Polymer KW - Physical ageing PY - 2017 DO - https://doi.org/10.1021/acsmacrolett.7b00456 SN - 2161-1653 VL - 6 IS - 8 SP - 813 EP - 818 PB - ACS CY - Washington DC, USA AN - OPUS4-41354 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Shamsuddoha, Md T1 - Critical Factors Affecting the Capacity of Cylindrical Grouted Connections in Offshore Energy Structures N2 - Current trend suggests that global energy consumption will increase in the future. This growing energy demand and advancement of technology lead to explore all potential offshore fossil and non-fossil energy sources, necessitating erection of exploration and production structures, rigs, platforms and towers, which are susceptible to adverse environmental conditions along with their maintenances. Cylindrical grouted joints provide suitable connections between steel substructure and foundation in these offshore platforms and wind structures especially monopiles for ease of installation. However, these are composite connections with exterior sleeve, interior pile and infill grout. The capacity of these connections is affected by number of factors. The literature over last four decades by numerous researchers has shown the development of these connections with increasingly higher capacities and influences on these capacities due to various factors. This paper provides a comprehensive review on the factors affecting the connection capacity along with technical challenges for the future. Critical aspects and shortcomings of the current connection systems and potential solutions may be sought after for these issues are also discussed. T2 - 36th International Conference on. Ocean, Offshore and Arctic Engineering CY - Trondheim, Norway DA - 25.06.2017 KW - Offshore wind energy KW - Grouted connection KW - Joint capacity KW - Shear keys PY - 2017 AN - OPUS4-42389 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Shamsuddoha, Md A1 - Hüsken, Götz A1 - Baeßler, Matthias A1 - Kühne, Hans-Carsten A1 - Thiele, Marc T1 - Critical factors affecting the capacity of cylindrical grouted connections in offshore energy structures N2 - Current trend suggests that global energy consumption will increase in the future. This growing energy demand and advancement of technology lead to explore all potential offshore fossil and non-fossil energy sources, necessitating erection of exploration and production structures, rigs, platforms and towers, which are susceptible to adverse environmental conditions along with their maintenances. Cylindrical grouted joints provide suitable connections between steel substructure and foundation in these offshore platforms and wind structures especially monopiles for ease of installation. However, these are composite connections with exterior sleeve, interior pile and infill grout. The capacity of these connections is affected by number of factors. The literature over last four decades by numerous researchers has shown the development of these connections with increasingly higher capacities and influences on these capacities due to various factors. This paper provides a comprehensive review on the factors affecting the connection capacity along with technical challenges for the future. Critical aspects and shortcomings of the current connection systems and potential solutions may be sought after for these issues are also discussed. T2 - 36th International Conference on Ocean, Offshore and Arctic Engineering CY - Trondheim, Norway DA - 25.06.2017 KW - Offshore wind energy KW - Grouted connection KW - Joint capacity KW - Shear keys PY - 2017 SN - 978-0-7918-5766-3 DO - https://doi.org/10.1115/OMAE2017-62510 VL - 3B SP - UNSP V03BT02A037, 1 EP - 10 AN - OPUS4-42387 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Baeßler, Matthias T1 - Aktuelle Entwicklungen und Herausforderungen bei Offshore-Gründungen mit Blick auf Forschung und Zulassung N2 - Der Seminarvortrag gibt einen Überblick über den Stand des Ausbaus Offshore Wind, der technischen Fragestellungen für die Tragstrukturen und Gründungen und die zu erwartenden Entwicklungen T2 - Geotechnische Seminarreihe des IBF/KIT CY - Karlsruhe, Germany DA - 23.11.2017 KW - Offshore-Gründungen KW - Windenergie PY - 2017 AN - OPUS4-43130 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Reinsch, Stefan T1 - Sub-Tg relaxation in hydrous soda-lime-silicate and sodium-borosilicate glasses N2 - Water plays an important role for the depolymerization of silicate glasses which becomes noticeable by a distinct decrease of glass transformation temperature, Tg. Thus, it has a considerable influence on aging and fatigue as well as on sub-critical crack growth in glasses. In this connection also sub-Tg relaxation processes play a major role, but they are poorly investigated in glasses with high contents of structural bonded water. Therefore, soda-lime-silicate and sodium-borosilicate glasses with water contents up to 5 wt.% H2O were investigated by differential thermal analysis and sphere penetration viscometry, as well as internal friction measurements. The latter was applied to study network related relaxation mechanisms (α-relaxation) in the range of glass transition, as well as faster relaxation modes occurring at lower temperatures (β-, γ- relaxation). Total water content and concentrations of H2O molecules (CH2O) and OH groups (COH) in the glasses were determined by infrared spectroscopy. For low water contents two sub-Tg internal friction peaks were observed and assigned to the low-temperature motion of alkali ions (γ-relaxation) and cooperative movements of dissimilar mobile species under participation of OH at higher temperature (βOH relaxation). For large water contents, where significant amounts of molecular water are evident, a low temperature shoulder appears on the β-relaxation peak. This emerging relaxation mode (βH2O relaxation) was assigned to the motions of H2O molecules. T2 - 91. Glastechnische Tagung CY - Weimar, Germany DA - 28.05.2017 KW - Water-bearing glasses KW - Mechanical loss spectroscopy KW - Relaxation PY - 2017 AN - OPUS4-40810 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kiefer, P. T1 - Viscosity of water bearing glasses in the glass transition range – Phosphates vs. silicates and borates N2 - Water has a strong impact on the viscosity and the transition temperature of oxide glasses. It acts as a fluxing agent, reducing viscosity particularly in the glass transition range, and by that flattening the viscosity-temperature curve and decreasing the fragility of hydrous glass melts. This general behavior is found for silicate and borate as well as in borosilicate compositions. However, there is still a lack of data with respect to hydrous phosphate glasses. Here, we study the influence of structural water on the viscosity of Li2O-MgO-(Al2O3-)P2O5 glasses. The glasses were synthesized in an internally heated pressure vessel (IHPV) at a pressure of 0.5 GPa. The selected pressure allows for the synthesis of glass specimens with water contents of several wt.%. The viscosity measurements were carried out in the glass transition range, i.e. log η ≈ 10-13 (η in Pa s), using a sphere penetration viscometer. The measured data agree with glass transition temperatures measured by differential thermo analysis. First results further suggest that the fragility of the analyzed phosphates decreases with increasing water content. T2 - 91. Glastechnische Tagung CY - Weimar, Germany DA - 28.05.2017 KW - Water-bearing glasses KW - Viscosity PY - 2017 AN - OPUS4-40812 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Waurischk, Tina T1 - New device for inert crack growth measurements in ultra-strong glasses N2 - The practical strength of glasses under ambient conditions is substantially lower compared to its intrinsic strength because of sub-critical crack growth (SCCG) from microscopic flaws. While SCCG is related to the humidity of the ambient atmosphere, leading to stress corrosion phenomena, the detailed kinetics are still not fully understood. To get better insight to the contribution of water on the crack-tip, highly water bearing glasses will be investigated by a new device for inert SCCG-measurements using double cantilever beam (DCB) geometry specimens. This device was designed to investigate the stress intensity factor in modus I and crack velocity in vacuum, but different atmospheres can also be introduced. For validation of the new device, first experiments were performed on microscope slides as well as on a soda-lime silicate and a borosilicate crown glass. The results achieved will be presented in comparison to the published results of Wiederhorn. T2 - 91. Glastechnische Tagung CY - Weimar, Germany DA - 29.05.2017 KW - Double cantilever beam KW - DCB KW - Crack intensity factor KW - Crack growth velocity KW - Glass PY - 2017 AN - OPUS4-40680 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Welter, T. T1 - Glass structures with low helium and hydrogen permeability N2 - An efficient energy provision using fuel cells is linked to effecitve hydrogen storage capabilities. Because of its low intrinsic hydrogen permeability, glass has a huge potential in modern concepts of hydrogen storage. Previous studies on oxidic glasses showed an empirical connection between glass composition and gas permeation, which was mainly derived from the behavior of silica glass. In this study we focus on the relationship between topologic (free volume; network polymerization) and thermodynamic (configurational entropy) parameters. The comparison of three glasses within the meta (earth-) alkaline alumino silicate system to silica glass shows that an increase of the atomic packing factor (APF) does not necessarily decrease the permeability. Furthermore, the results suggest a connection between ΔCp at Tg and hydrogen permeability of the glass. All experiments were performed assuming that chemical hydrogen solubiltity in glass is negligible at temperatures well below the glass transition temperature. T2 - 91. Glastechnische Tagung CY - Weimar, Germany DA - 29.05.2017 KW - Hydrogen permeability KW - Glass composition KW - Atomic packing factor KW - Configurational entropy KW - Diffusion coefficient PY - 2017 AN - OPUS4-40488 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Marzok, Ulrich T1 - Measurement of H2 permeability of glasses with VHE powder method N2 - The development of glassy hydrogen barriers requires the determination of low H2 permeabilities. Previous studies and numerical simulations have shown that the VHE powder method (vacuum hot extraction with mass spectrometric gas detection) is suitable for this purpose. The measured isothermal gas emission is fitted to a classical diffusion model for spherical particles from which the diffusion coefficient of the glass is calculated. The H2 permeability is determined by means of the solubility determined from the same measurement data. This presentation is referring to the optimization of the method regarding sample preparation and measurement data evaluation using suitable experimentally determined particle size distributions is reported. For quartz glass, it is shown that the accuracy of classical measuring methods is achieved with the VHE powder method. Furthermore, other examples of substantially gas-tighter glasses are given. T2 - 91. Glastechnische Tagung CY - Weimar, Germany DA - 29.05.2017 KW - Hydrogen permeation KW - Glass KW - Vacuum hot extraction KW - Powder method KW - Diffusion coefficient PY - 2017 AN - OPUS4-40441 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Waurischk, Tina T1 - New device for inert sub-critical crack growth: measurements in crystallized glasses N2 - Compared to its intrinsic strength, the practical strength of glasses is substantially lowered by microscopic flaws. Their sub critical growth from the surface is strongly affected by ambient humidity. A new device was designed to enable the observation of sub critical crack growth (SCCG) in vacuum and controlled atmosphere. It allows measurements in transparent and semi-transparent materials in double cantilever beam (DCB) geometry. The aim of the present work is to study the effect of crystals on crack growth. T2 - 12th International Symposium on Crystallization in Glasses and Liquids CY - Segovia, Spain DA - 10.09.2017 KW - Double cantilever beam KW - DCB KW - Crack intensity factor KW - Crack growth velocity KW - Glass KW - Glass ceramic PY - 2017 AN - OPUS4-41995 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Müller, Ralf A1 - Körner, S. T1 - Dissolution and reprecipitation of silver in sintering silver-glass dispersions N2 - Electric contacts based on silver-glass dispersions are key components in optoelectronic microsystems and control modules for medical, information & communication and energy technology in our networked society. Driven by the complexity of modern production processes and ever shorter time-to-market requirements, the fast and specific development of tailored silver-glass dispersions has become a bottleneck of technology development. Nevertheless, the underlying mechanisms of silver dissolution, transport, and reprecipitation, and the resulting micro structure evolution during firing are poorly understood. The broad literature on the precipitation of colloidal silver particles and the related processes of silver dissolution and diffusion mostly refer to very small volume fractions of silver. Transferring these results to the sintering of glass-containing silver dispersions, is therefore highly questionable. In this case, silver dissolution, electrical contact between silver particles, transport and reprecipitation take place under special conditions. This includes short diffusion lengths (particle size < 10 μm), the presence of three-phase contacts silver - glass - sintering atmosphere, as well as silver reprecipitation at the sintering contacts as the driving force of silver transport. Here, a dynamic balance of the silver concentration can be expected to result from the ratio between silver dissolution and reprecipitation. The aim of the project is to gain basic insight into the mechanisms of dissolution, transport and reprecipitation of silver in sintering silver glass dispersions. In this context, the main focus is on gaining basic knowledge about the dissolution of metallic silver in low melting oxide glasses as the limiting factor of the sintering of silver-glass composites. In particular, we will strive to gain insight into the effect of the oxygen content of the sintering atmosphere, of the oxygen dissolved in the silver particles, of silver oxide on the surface of the silver powder, of the electric contact between the silver particles, as well as the basicity of the glass. Furthermore, we strive for insights into the silver mobility and the silver concentration that can be attained (silver solubility) in oxide glasses with a low melting point. Summing up all these aspects, a closed explanatory model for silver dissolution, transport and reprecipitation during the sintering of glass silver dispersions will be introduced. T2 - DFG Begutachtungskolloquium (PAK 949/1 und PAK 950/1) CY - Bonn, Germany DA - 07.03.2017 KW - Sintering KW - Silver KW - Glass KW - Solubility KW - Reprecipitation PY - 2017 AN - OPUS4-44227 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Blaeß, Carsten T1 - Crack healing in glass matrix composites N2 - Partially crystalline glasses are predominantly used as solid oxide fuel cell (SOFC) sealants due to their superior long term durability. However, cracks caused by thermal cycling still remain a substantial bottleneck in developing durable SOFC sealants inasmuch as, in contrast to crystal free glasses, large crystal volume fractions can retard healing. Hence, the basic understanding of crack healing in glassy crystalline materials and the effects of micro structure are important for finding optimum micro structures for both, durability and crack healing. For studying these effects, several model glass matrix composites (GMC), for which simultaneous crystal growth and crack healing can be excluded, have been synthesized. Sodium calcium silicate glass – zirconia GMC turned out to provide sufficiently homogeneous, dense and durable model GMC for our studies. The microstructure of this GMC shows large crystal free glassy regions embedded in network of finely dispersed ZrO2 nanoscale crystals. Whereas the glassy regions allow easy local crack healing, the network of dispersed crystals increases the effective viscosity on a global scale. This effect substantially retards crack broadening during later healing stages, which often ends up in large pores. Therefore, this type of microstructure seems to be an interesting candidate for crack healing optimized sealants. T2 - Crystallization 2017 CY - Segovia, Spain DA - 10.09.2017 KW - Glass KW - Glass ceramic KW - Crack healing KW - Microstructure PY - 2017 AN - OPUS4-42291 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Blaeß, Carsten T1 - Crack healing in glasses and glass matrix composites N2 - Fundamental understanding of crack healing in glassy crystalline materials is very important for solid oxide fuel cell (SOFC) sealants, since cracks caused by sealing or thermal cycling still remain a substantial bottleneck in developing durable SOFC. Previous studies on soda lime silicate glass [Sin14] showed that crack healing is driven by viscous flow and that healing progress is proportional to time t and inverse viscosity η. This finding would allow to present healing data of a given glass for different temperatures in a master curve healing progress versus t/η. Such master curves would be a helpful tool in understanding crack healing kinetics. Against this background, crack healing in non-crystallizing sodium calcium silicate (NCS) and sodium borosilicate glasses (NBS) have been studied. Moreover, to evaluate the influence of micro structure in crystallized glass on crack healing process, glass matrix composites (GMC) were prepared from NCS and zirconia as inert ceramic filler material mimicking a partially crystalline micro structure. By this way, the micro structure can be kept constant during crack healing. Cracks were generated by Vickers indention and healed isothermally at different temperatures. Crack healing progress was monitored by optical and electron microscopy. Results show that the above mentioned proportionality actually applies for the studied glasses for which such a master curve could be obtained. In comparison to a non-crystallized glass, the effective viscosity of GMC is increased by the rigid filler content. This effect substantially retards crack broadening during later healing stages, which often ends up in large pores. On the other hand, local viscous crack healing is still possible in larger glassy regions. This behavior seems to be very interesting for crack healing optimized micro structures. T2 - Crystallization 2017 CY - Segovia, Spain DA - 10.09.2017 KW - Glass KW - Glass ceramic KW - Crack healing KW - Microstructure PY - 2017 AN - OPUS4-42285 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Blaeß, Carsten T1 - Master curve for crack healing in silicate glasses N2 - Fundamental understanding of crack healing in glassy crystalline materials is very important for many applications, especially for solid oxide fuel cells (SOFC) sealants since cracks caused by mechanical stress or thermal cycling still remain a substantial bottleneck in developing durable SOFC. Previous studies on soda lime silicate glass published by Singh showed that crack healing is driven by viscous flow. He postulated that the healing progress is proportional to time, t, and the inverse viscosity. For a given glass, this finding would allow to present data of crack healing measured at different temperatures in a master curve, if the healing progress is plotted versus t/. Such master curves would be a helpful tool in understanding crack healing kinetics. To verify the applicability of such master curves, crack healing in non-crystallizing soda-lime-silicate (NCS) and sodium-borosilicate glasses (NBS) was studied. Cracks were generated by Vickers indention and healed isothermally at different temperatures. Crack healing progress was monitored by optical and electron microscopy. The results show that the above mentioned proportionality applies to the two glasses and the afore developed master curve could be obtained in both cases. T2 - Crystallization 2017 CY - Segovia, Spain DA - 10.09.2017 KW - Glass KW - Crack healing KW - Vickers PY - 2017 AN - OPUS4-42293 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Stajanca, Pavol A1 - Woyessa, G. A1 - Schukar, Marcus A1 - Bang, O. A1 - Krebber, Katerina T1 - Response of microstructured plastic optical fiber Bragg grating to gamma radiation N2 - Response of PMMA-based plastic optical fiber Bragg grating (FBG) to gamma radiation is investigated for the first time. FBG wavelength shift as large as 150 pm is observed for irradiation to 18 kGy. T2 - 5th Workshop on specialty optical fibers and their applications CY - Limassol, Cyprus DA - 11.10.2017 KW - Fiber Bragg gratings KW - Optical sensing and sensors KW - Plastic optical fibers KW - Gamma radiation PY - 2017 SP - Poster 19, 1 EP - 2 AN - OPUS4-42586 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Stajanca, Pavol T1 - Response of microstructured plastic optical fiber Bragg grating to gamma radiation N2 - Response of PMMA-based plastic optical fiber Bragg grating (FBG) to gamma radiation is investigated for the first time. FBG wavelength shift as large as 250 pm is observed for irradiation to 20 kGy. T2 - 5th Workshop on specialty optical fibers and their applications (WSOF2017) CY - Limassol, Cyprus DA - 11.10.2017 KW - Fiber Bragg gratings KW - Optical sensing and sensors KW - Plastic optical fibers KW - Gamma radiation PY - 2017 AN - OPUS4-42585 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Becker, Ben A1 - Mair, Georg W. A1 - Schoppa, Andre A1 - Duffner, Eric A1 - Szczepaniak, Mariusz A1 - Klauke, Andre A1 - Lenz, Stefan A1 - Lehr, Christian A1 - Hoffmann, Martin A1 - Gregor, Christian ED - Mair, Georg W. T1 - CryoCode: Kryodruck Tanksystem und Betankung – Validierung bis zum Normierungsvorschlag N2 - Entwicklung und Validierung eines Kryodruck-Tanksystems für Wasserstoff-Fahrzeuge. Darstellung der Versuchsergebnisse und des Normierungsvorschlags. KW - Kryodruck KW - Wasserstoff KW - Druckbehälter KW - Composite KW - Normierungsvorschlag PY - 2017 SP - 1 EP - 56 AN - OPUS4-40714 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schoppa, Andre A1 - Szczepaniak, Mariusz A1 - Mair, Georg W. ED - Schoppa, Andre T1 - Die Anwendung der hydraulischen Prüfverfahren in der Praxis Teil 1: Die hydraulische Berstprüfung N2 - Um die Resultate aus den hydraulischen Prüfungen statistisch bewerten zu können, benötigt man Prüfergebnisse, die auf reproduzierbaren Prüfverfahren basieren. Dabei geht es nicht nur um ein funktionierendes Qualitätsmanagementsystem im Prüflabors, sondern vornehmlich um die Reduzierung des Einflusses der Prüftechnik und des Prüfverfahrens auf die Streuung der Ergebnisse. Dieser Einfluss kann erst durch ins Detail konkretisierte Prüfungsanforderungen minimiert werden. Dieser Anforderung entsprechend wurde ein Verfahren beschrieben, das den Spielraum bei der Durchführung der hydraulischen Berstprüfung verringert und somit eine Streuung der Ergebnisse garantiert, die annähernd ausschließlich aus den Prüfmustern kommt. Die Prüfmusterdokumentation spielt dabei eine zentrale Rolle. Zwischen den hydraulischen Prüfungen im Zuge der Zulassung eines Baumusters und den hydraulischen Prüfungen zur Prüffristenfestlegung liegt eine Zeitspanne von mehreren Jahren. Um die Prüfergebnisse auch nach einer längeren Preisfestlegung (z.B. 10 Jahre) miteinander vergleichen zu können, müssen die zerstörenden Prüfungen reproduzierbar durchgeführt und vollständig dokumentiert und archiviert werden. Die Prüfung an neuen Materialien oder neuen Produkten erfordert eine moderne Prüftechnik, die sich mit dem Stand der Technik stetig weiterentwickeln muss. Demzufolge ist die zunehmende Automatisierung in der Prüftechnik ein wichtiger Schritt um Prüfungen reproduzierbarer durchzuführen. Wie ein konkretisierte Verfahren zur hydraulischen Lastwechselprüfung in der Praxis aussieht, wird in einem nächsten Beitrag betrachtet. Dabei wird ebenfalls Bezug zur verwendeten Prüftechnik genommen unter dem Hauptgesichtspunkt, welche Anforderungen in der Bundesanstalt für Materialforschung und -prüfung BAM an eine moderne Lastwechselanlage zur Prüfung von Druckbehältern bis 1200 bar gestellt werden. KW - Druckbehälter KW - Berstprüfung KW - Hydraulische Prüfeinrichtung KW - Prüffristenfestlegung PY - 2017 SN - 2191-007 VL - 7 IS - 5 SP - 25 EP - 30 PB - Springer VDI Verlag CY - Düsseldorf AN - OPUS4-41518 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. A1 - Becker, Ben A1 - Duffner, Eric A1 - John, Sebastian T1 - Composite storage systems for CGH2- systematic improvement of RC&S N2 - Conventional approval requirements exclusively ask for minimum strength values, which have to be met. The probabilistic approach estimates how likely none of the comparatively manufactured units fails during operation. Both questions are juxtaposed and compared here with respect to the load cycle tests. The influence of the sample sizes is discussed additionally. T2 - 10th INTERNATIONAL CONFERENCE ON SUSTAINABLE ENERGY & ENVIRONMENTAL PROTECTION CY - Bled, Slovenia DA - 27.06.2017 KW - Probabilistic KW - Hydrogen KW - Composite KW - Cylinder KW - Regulations KW - Load cycles KW - GTR 13 PY - 2017 AN - OPUS4-41677 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. T1 - The UN-Service Life Test Procedure & Lebensdauerüberwachung Typ II N2 - Der Vortrag führt in die Vorgaben der UN-Modellvorschriften ein, ein „Gas cylinders - service life testing for cylinders and tubes of composite construction“ zu gewährleisten. Hierzu werden kurz die betroffenen Umschließungen vorgestellt und die Interaktion von relevanten Regelwerksänderungen und der Beauftragung von ISO, einen TR hierzu zu erstellen, erläutert. Dies wird ergänzt durch eine zusammenführende Darstellung der Veränderungen im Regelwerk zum Thema und den vorbereitenden und begleitenden Maßnahmen durch die BAM über die letzten fasst 20 Jahre. Die im Regelwerk vorgeschlagene Maßnahme, zwischen Auslegungslebensdauer und Betriebslebensdauer zu unterscheiden, wird erläutert und begründet. Die Interaktion mit der Genehmigung einer Frist von 10 Jahren durch die BAM für die wiederkehrende Prüfung wird dargestellt. Am Beispiel der umfangsgewickelten Stahlflaschen für den Wasserstofftransport in Batteriefahrzeugen wird dargestellt, wie das dt. Verfahren in der Praxis aussieht. Hierzu werden die Prüfergebnisse und die daraus bzgl. der Lebensdauerüberwachung gezogenen Schlüsse erläutert. Der Vortrag schließt mit einem Ausblick zur Verwendung des BAM-Verfahrens zur unmittelbaren Anwendung und zur Bewertung von für die Zukunft angestrebten ZfP-Verfahren. T2 - BAM-DIN-IGV-DVFG Gespräch 2017 CY - DIN Berlin, Germany DA - 15.02.2017 KW - Auslegungslebensdauer KW - Betriebslebensdauer KW - Prüffristenfestlegung KW - Probabilistischer Ansatz PY - 2017 AN - OPUS4-39181 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Saul, Herbert A1 - Mair, Georg W. T1 - Zuständigkeit im Gefahrguttransport - Formale Umsetzung nach nationalem Verwaltungsrecht N2 - Der Vortrag fasst zunächst die Arbeitsgrundlage des Verwaltungshandelns im Gefahrguttransport zusammen: die internationalen Transportvorschriften und die nationalen Verordungen auf Basis des GGBefG. Danach geht er auf die wichtigsten verwaltungsrechtlichen Begrifflichkeiten und Zusammenhänge verschiedener Gesetze ein. Darauf aufbauend wird der Ablauf zur Bearbeitung eines Verwaltungsvorgangs und die Schnittstelle zu Z.01 erläutert. T2 - Colloquium der Abteilung 3 CY - BAM, Berlin, Germany DA - 16.02.2017 KW - Völkerrechtliche Verträge KW - Gesetzesgrundlagen KW - Zuständigkeit KW - Verwaltungsvorgang KW - Frist KW - Verwaltungsakt KW - Bescheid PY - 2017 AN - OPUS4-39284 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. A1 - Becker, Ben T1 - Monte-Carlo-analysis of minimum load cycle requirements for composite cylinders for hydrogen N2 - Existing regulations and standards for the approval of composite cylinders in hydrogen service are currently based on deterministic criteria (ISO 11119-3, UN GTR No. 13). This paper provides a systematic analysis of the load cycle properties resulting from these regulations and standards. Their characteristics are compared with the probabilistic approach of the BAM. Based on Monte-Carlo simulations the available design range of all concepts is compared. In addition, the probability of acceptance for potentially unsafe design types is determined. T2 - ICHS 2017 CY - Hamburg, Germany DA - 11.09.2017 KW - Monte-Carlo KW - Hydrogen KW - Regulations KW - Probabilitic approach PY - 2017 SP - ID 202, 1 EP - 11 PB - HySafe CY - Hamburg AN - OPUS4-41944 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - BOOK A1 - Mair, Georg W. T1 - Safety Assessment of Composite Cylinders for Gas Storage by Statistical Methods N2 - Featuring a detailed analysis of current approval requirements and the relevant safety assessment methods for gas cylinders in general and with main focus on composite cylinders for storing ompressed natural gas and hydrogen, this book demonstrates how current regulations and standards limit the ability to reduce cost and weight. Based on this data, it then highlights the potential offered by the proposed approval procedure based on probabilistic safety assessment. After addressing the economic potential of probabilistic safety assessments, the book details working procedures and improving cycles and (slow) bursts as methods for assessing residual strength. It then discusses methods for statistically evaluating test data, as well as sample- size and distribution character considerations. A definition of sample strength is elaborated in terms of the performance sheets developed by the author. On this basis, it discusses safety as a property of service life and interpreted as an issue of degradation, and explores aspects of artificial aging for simulating the end-of-life reliability level. Lastly, the book considers control and inspection aspects: quality of production, degradation prediction using destructive sample tests parallel to operation, retesting periods and correcting for underand overestimates of safe lifetime. Presented in schematic diagrams, illustrations and tables, this information enables manufacturers and operators to use this new approach in practice and supports the improvement of current regulations and standards. KW - Probabilistic KW - Statistics KW - Slow burst testing KW - Fire engulfment KW - Crash loads KW - Degradation KW - Production scatter KW - Operational loads KW - Residual strength KW - Service life KW - Design life KW - Safety KW - Risk KW - Consequences KW - Failure rate KW - Survival rate KW - Confidence level KW - Acceptance rate PY - 2017 SN - 978-3-319-49708-2 SN - 978-3-319-49710-5 DO - https://doi.org/10.1007/978-3-319-49710-5 VL - 2017 SP - I ; 1 EP - XXI; 269 PB - Springer International Publishing CY - Cham, Switzerland ET - 1. AN - OPUS4-42324 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schoppa, Andre A1 - Szczepaniak, Mariusz A1 - Mair, Georg W. ED - Schoppa, Andre T1 - Die Anwendung der hydraulischen Prüfverfahren in der Praxis - Teil 2 Die hydraulische Lastwechselprüfung N2 - Die bisherigen Erfahrungen mit der bestehenden Impulsprüfanlage PN020 der BAM zeigen Potential für Verbesserungen auf. Dies betrifft insbesondere die Aspekte nutzbares Impulsvolumen, Wartungsaufwand und Stillstandszeiten, sowie Abmessungen und Gestaltung der Prüfkammer hinsichtlich Nutzraum und Handling der Prüfmuster. Im Zuge eines optimierten Anlagekonzeptes besteht großes Interesse an einer flexiblen Neuausrichtung der Druckerzeugung. Eine moderne Prüfanlage sollte in der Lage sein, die zu bewegenden Massen an die gewünschte Prüfaufgabe und den jeweils benötigten Volumenbedarf anzupassen. Die technische Lösung für die Druckerzeugung sollte deshalb modular gestaltet sein, sodass zusätzlich benötigtes Fördervolumen im Bedarfsfall nachgerüstet werden kann. Ein anderes Konzept als eines, das auf Druckübersetzern basiert, scheidet für Extremtemperaturprüfungen aus, da das vorzutemperierende Medium hierzu in einer Säule pendeln und nicht zirkulieren darf. Wesentlicher Aspekt der Modularität ist die Redundanz bei Teillast (reduzierter Volumenbedarf - Arbeitsfähigkeit bleibt mit Einschränkung erhalten). Es wird davon ausgegangen, dass einzelne Druckerzeugungs-/Antriebseinheiten so demontiert, repariert oder ausgetauscht werden können, dass die Nicht-Verfügbarkeit der gesamten Anlage auf den Ein- und Ausbau von Elementen der Anlage und Ausfälle in der Steuerung beschränkt bleibt. Auch im teil-demontierten Zustand sollte die Anlage mit eingeschränkter Leistungsfähigkeit grundsätzlich einsetzbar sein. Die Wartungskosten sollen durch die Verwendung von identischen und kleineren Druckerzeugereinheiten „von der Stange“ gesenkt werden. Eine moderne Anlage wäre zur Verbesserung der Diagnosemöglichkeiten mit erheblich mehr Sensorik auszurüsten. Die Druckerzeugung muss mit der Art der Medienkonditionierung kompatibel gestaltet sein. Das heißt, das Prüfmedium sollte unabhängig von der Umgebungsluft aktiv temperiert werden können, um die Konditionierzeiten bis zum Prüfungsstart zu verkürzen und um einen Temperaturanstieg infolge der Reibung zu verringern. Die „Prüfkammer“ sollte keine starre Kammer im herkömmlichen Sinne mehr sein. Stattdessen ist eine thermisch isolierte und mechanisch hoch belastbare Versuchsfläche aufzubauen, auf der sowohl mechanische Schutzelemente (vergl. aktueller Berstkäfig) wie auch mobile Isolierhauben verwendet werden können. Wesentlich ist eine Optimierung einer solchen Anlage auf die eingangs erwähnte Reproduzierbarkeit von Prüfprozeduren und die Vergleichbarkeit der Prüfergebnisse mit Blick auf die statistische Auswertung. Hierzu sollten eine möglichst exakte Regelung, eine statistische Auswertung der Duckextremwerte (zumindest in Klassen), eine Aufzeichnung der Temperatur- und Feuchtewerte sowie des geförderten Volumens jedes Zyklusses und verschiedene Methoden der Leckerkennung/automatischen Versuchsabbruches selbstverständlich implementiert sein. KW - Druckbehälter KW - Lastwechselprüfung KW - Hydraulische Prüfeinrichtung PY - 2017 SN - 2191-007 VL - 7 IS - 7/8 SP - 28 EP - 34 PB - Springer VDI Verlag CY - Düsseldorf AN - OPUS4-41519 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Yin, Huajie T1 - Molecular mobility of super glassy polymers for gas separation membranes investigated by dielectric spectroscopy N2 - Super glassy polymers such as poly(trimethylsilylpropyne) (PTMSP) or polymers with intrinsic microporosity (PIMs) play an important role in the current development of membrane materials for gas separation because of their high permeability and selectivity. Unfortunately, such materials which have a high fractional free volume (FFV) are prone to pronounced physical aging. The initial microporous structures approach a more dense state via local chain rearrangements which results in a dramatic reduction in the gas permeability. For the first time, broadband dielectric spectroscopy was employed to investigate the molecular dynamics of two representative groups of super glassy polymers: PIMs (PIM-1 & PIM-EA-TB) and Si-containing polynobornenes (PTCNSi1 & PTCNSi2). The dielectric behavior of the solution-cast polymeric films was measured by isothermal frequency scans during the different heating cycles in a broad temperature range. Structural relaxation of the films was observed during the measurements. Molecular relaxation processes following Arrhenius behavior with unusually high activation energies were observed for all the investigated polymers. The PIMs showed furthermore a significant conductivity in the glassy state which is explained with the formation of local intermolecular agglomerated structures due to interaction of π-electrons in aromatic moieties of the polymer backbone. T2 - 8th International Discussion Meeting on Relaxations in Complex Systems CY - Wisla, Poland DA - 23.07.2017 KW - Broadband dielectric spectroscopy KW - Molecular mobility KW - Physical aging KW - Membranes KW - Gas separation PY - 2017 AN - OPUS4-41162 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Konnertz, Nora A1 - Ding, Yi A1 - Harrison, W.J. A1 - Budd, P.M. A1 - Schönhals, Andreas A1 - Böhning, Martin T1 - Molecular mobility and gas transport properties of nanocomposites based on PIM-1 and polyhedral oligomeric phenethyl-silsesquioxanes (POSS) N2 - Polymers with intrinsic microporosity (PIMs) are of great interest in the field of gas separation membranes. Already the first synthesized PIM-1 shows extraordinary permeability and selectivity. Unfortunately, PIM-1 is susceptible to physical aging and thus gradually loses its outstanding properties. In this study a polyhedral oligomeric silsesquioxane with phenethyl substituents (PhenethylPOSS) was used as a nanofiller (0–40 wt%) in the PIM-1 matrix to potentially improve the gas transport properties and prevent physical aging. The molecular mobility of the solution-cast nanocomposite films was analyzed by Broadband Dielectric Spectroscopy (BDS). Furthermore, gas permeability was determined with the time lag method (0–20 bar upstream pressure) at 35 °C for N2, O2, CH4 and CO2. KW - Broadband Dielectric Spectroscopy KW - Gas separation KW - Gas permeation KW - Polymers of intrinsic microporosity KW - Nanocomposite KW - POSS KW - PIM-1 PY - 2017 DO - https://doi.org/10.1016/j.memsci.2017.02.007 SN - 0376-7388 SN - 1873-3123 VL - 529 SP - 274 EP - 285 PB - Elsevier B.V. CY - Amsterdam AN - OPUS4-39169 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Yin, Huajie T1 - Molecular Mobility and Physical aging of SuperGlassy Polymers for Gas Separation Membranes as revealed by Dielectric Spectroscopy N2 - Polymeric membranes represent a cost- and energy efficient solution for gas separation. Recently superglassy polymers with high free volume outperform many conventional dense polymers in terms of gas permeability and selectivity. However, such materials with a high fractional free volume (FFV) are prone to pronounced physical aging. The initial microporous structures approach a denser state via local chain rearrangements which results in a dramatic reduction in the gas permeability. For the first time, dielectric spectroscopy with state-of-the-art high-resolution analyzers was employed to investigate the molecular mobility and physical aging of two representative groups of superglassy polymers: PIMs (PIM-1 & PIM-EA-TB) and Si-containing polynobornenes (PTCNSi1 & PTCNSi2). The dielectric behavior of the solution-cast polymeric films was measured by isothermal frequency scans during the different heating cycles in a broad temperature range. Structural relaxation of the films was observed during the measurements. Multiple dielectric processes following Arrhenius behavior were observed for all the investigated polymers. Moreover, they all showed conductivity in the glassy state. The significant increase in the conductivity with increasing temperature especially for PIMs is explained in terms of the formation of local intermolecular agglomerated structures due to interaction of π-electrons in aromatic moieties of the polymer backbone. T2 - 8th International Conference on Advanced Fibers and Polymer Materials CY - Shanghai, China DA - 08.10.2017 KW - Physical aging KW - Membranes KW - Broadband dielectric spectroscopy KW - Gas separation KW - Molecular mobility PY - 2017 AN - OPUS4-42877 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Baeßler, Matthias T1 - Untersuchungen zu Tragstrukturen für die Energiewende N2 - Die BAM ist vielfältig mit der Untersuchung von für die Energiewende relevanten Strukturen beschäftigt. Aus dem speziellen Blickwinkel des FB 7.2 werden im Vortrag die Aktivitäten FE, PAZ und BI umfassend für Studenten der BU Weimar dargestellt. T2 - Einblick (#53) CY - Bauhaus Universität Weimar, Germany DA - 19.01.2017 KW - Tragstrukturen KW - Energiewende PY - 2017 AN - OPUS4-39376 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Thiele, Marc T1 - Experimental investigation of damage evolution in concrete under high-cycle fatigue N2 - The current knowledge about fatigue behavior of concrete is still incomplete. This concerns especially the progress of fatigue which precedes the fatigue failure. Therefore, the process of fatigue itself under cyclic compressive loading was investigated in a systematic and comprehensive way. The aim of this investigation was to obtain a deeper insight and to provide a better understanding of the damage process occurring within the material during fatigue loading. Concrete cylinders were tested with a number of cycles to failure between 106 and 107. To investigate macroscopic and microscopic changes in the material, various methods of non-destructive and destructive testing were used. One main result was, in contrast to other authors, that the investigated changes in macroscopic material behavior could not be explained only by a development of micro-cracks. The results indicated rather, that the related changes in the fatigue behavior are mainly a result of viscous processes in the hardened cement paste, similar to the processes of creep. Based on the experimental results a description of the possible processes was derived which take place in the material structure during fatigue loading and also leads to the observed macroscopic changes in the material behavior. In this context, the results have shown that in case of isotropic material behavior a stiffness reduction related to a scalar value could not capture the damage effect on the stress-strain-relationship caused by fatigue. T2 - INFRASTAR Workshop CY - BAM, Berlin, Gemany DA - 27.03.2017 KW - Fatigue KW - Concrete KW - High-Cycle KW - Damage Evolution PY - 2017 AN - OPUS4-39576 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Stengel, Dominik T1 - Lebensdauerverlängerung von Offshore-Windenergieanlagen im Betrieb N2 - Vorschlag zur möglichen Lebensdauerverlängerung einzelner Bauteile einer im Betrieb befindlichen Offshore-Windenergieanlage durch Beschreibung der Versagenswahrscheinlichkeiten Beschreibung der Versagenswahrscheinlichkeit durch geeignete Schädigungsmodelle Aktualisierung der Versagenswahrscheinlichkeiten aufgrund von Inspektionsergebnissen und möglichen Reparaturen auf Basis der Bayes‘schen Entscheidungstheorie Quantifizierte Bewertung von Inspektionsmethoden und Reparaturmaßnamen im Hinblick auf die Zuverlässigkeit der Bauteile Grundlage für Entscheidungen für Inspektionen und Reparaturen T2 - Offshoretage CY - Heiligendamm, Germany DA - 15.03.2017 KW - Risikobasierte Maßnahmenplanung KW - Kostenoptimierung KW - Offshore Windenergie PY - 2017 AN - OPUS4-39448 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Baeßler, Matthias T1 - Einführung zum Workshop Groutverbindungen in der Betriebsphase N2 - Mit der Fertigstellung von mehr und mehr Offshore-Windparks rückt die Betriebsphase in den Mittelpunkt des Interesses. Hierbei sind auch die Groutverbindungen, die häufig so konzeptioniert sind, dass wenige Möglichkeiten zur Prüfung und Instandhaltung bestehen, von Interesse. Naturgemäß können auch kaum Erfahrungen für diese Ziele vorliegen. Der geplante Workshop hat folgende Schwerpunkte im Fokus: – Wiederkehrende Prüfung – Instandhaltung und Reparaturkonzepte – Inspektionskonzepte – Zerstörungsfreie Prüfung und – Schadensszenarien – Condition Monitoring Systeme (CMS) Beiträge aus dem Bereich Betrieb, Begutachtung, Forschung, Produktherstellung, Zertifizierung, behördliche Aufsicht und Condition Monitoring sind vorgesehen. Diskutiert werden sollen die technischen Anforderungen an die Überwachung im Betrieb im Hinblick auf die tatsächlich vorhandenen Probleme und Möglichkeiten. Die Präsentation leitet in die Thematik ein. T2 - Workshop Groutverbindung in der Betriebsphase CY - BAM, Berlin, Germany DA - 22.03.2017 KW - Groutverbindung KW - Inspektion KW - WKP KW - Instandhaltung PY - 2017 AN - OPUS4-39495 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kühne, Hans-Carsten A1 - Shamsuddoha, Md T1 - Instandsetzung und Verbesserung von Groutverbindungen: Potentiale-Strategien-Grenzen N2 - In den vergangenen 10 Jahren hat die Errichtung von Windkraftanlagen zur Deckung des zukünftigen Energiebedarfs stark zugenommen. Dabei bilden vor allem Offshore-Windenergieanlagen (OWEA) den Hauptanteil im Bereich der erneuerbaren Energien. Aufgrund der einfachen Installation werden hierbei Grout-Verbindungen sowohl bei Monopile als auch bei Jacket-Konstruktionen zwischen den gerammten Gründungsrohren und einem Adapterstück (Transition Piece) ausgeführt. Die Bemessung der Grout-Verbindung stellt aktuell im Bereich von OWEA weitgehendes Neuland ohne Langzeiterfahrung dar. Lediglich im Bereich der Offshore Erdöl- und Erdgasindustrie kann man auf über 30 Jahre Erfahrung mit dieser Verbindungstechnologie zurückblicken. Hier wurden jedoch für vergleichbare Strukturen Schädigungen und Setzungen während des Betriebs festgestellt. Gleichzeitig sind die Bedingungen bei der Montage Offshore sehr schwierig und die eingesetzten Materialien sind aufgrund ihrer technischen Merkmale in Verbindung mit den Verarbeitungsbedingungen nicht unproblematisch. Dies betrifft insbesondere den Fall, wenn sich die Verbindung unterhalb des Meerwasserspiegels befindet oder das Grout-Material im jungen Alter dynamisch beansprucht wird. Vor diesem Hintergrund sollen Strategien zur Instandsetzung schadhaft installierter oder im Betrieb geschädigter Grout-Verbindungen mit Hilfe von zementgebundenen Injektionsstoffen entwickelt werden. Hierzu werden zunächst die grundlegenden Schädigungsmechanismen und deren Auswirkung auf die Rissbildungsprozesse untersucht, da diese entscheidend für die Entwicklung eines geeigneten Instandsetzungskonzeptes sind. In diesem Zusammenhang werden Schädigungsmechanismen im Rahmen eines Modellversuchs anhand einer skalierten Grout-Verbindung untersucht. Des Weiteren werden potenzielle Instandsetzungsmaßnahmen und deren Grenzen diskutiert. T2 - BAM Workshop Groutverbindung in der Betriebsphase CY - Berlin, Germany DA - 22.03.2017 KW - Grout-Verbindung KW - Instandsetzung KW - Offshore-Windenergieanlagen PY - 2017 AN - OPUS4-39635 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Shamsuddoha, Md A1 - Baeßler, Matthias A1 - Hüsken, Götz A1 - Pirskawetz, Stephan A1 - Kühne, Hans-Carsten A1 - Thiele, Marc ED - Banjad Pecur, Ivana ED - Baricevic, Ana ED - Stirmer, Nina ED - Bjegovic, Dubravka T1 - Identification of failure pattern in cylindrical grouted connection for wind structures - a pilot study N2 - At present, Wind Turbine Generators (WTGs) operating in onshore and offshore wind farms are primary sources of renewable energy around the world. Cylindrical grouted sleeve connections are usually adopted in these WTG structures to connect the upper structure and foundation for ease of installation. These structures including grouted connections experience considerable adverse loading during their lifetimes. Settlements were reported inside similar connections used in energy structures especially oil and gas platforms, which were installed in last three decades. Thus, repair and rehabilitation of such connections in existing wind structures should also be planned ahead to keep them operating in the future. The nature of failure and crack generation in grouted connections are crucial prior to adopt a strengthening strategy. This pilot study is carried out to actualize the failure mechanism in the grouted connection, when subjected to axial loading. A novel reusable scaled cylindrical grouted connection with shear keys was designed and tested for its load bearing behaviour. The mechanical test was accompanied by classical measuring techniques (e.g. displacement transducer) as well as non-destructive measuring techniques (e.g. digital image correlation (DIC), acoustic emission analysis (AE)). The failure mechanism incorporating slippage of the shear keys and cracking of the grout was investigated. The capacity and applicability of such test mould were also discussed. The knowledge is expected to pave way towards repair of deteriorated grouted connections with similar geometry and failure pattern. T2 - 1st International Conference on Construction Materials for Sustainable Future (CoMS_2017) CY - Zadar, Croatia DA - 19.04.2017 KW - Grouted connections KW - Cracks KW - Failure KW - Strengthening strategy KW - Digital image correlation KW - Acoustic emission analysis PY - 2017 SN - 978-953-8168-04-8 SP - 544 EP - 551 AN - OPUS4-39914 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hüsken, Götz T1 - Identification of failure pattern in cylindrical grouted connection for wind structures – a pilot study N2 - At present, Wind Turbine Generators (WTGs) operating in onshore and offshore wind farms are primary sources of renewable energy around the world. Cylindrical grouted sleeve connections are usually adopted in these WTG structures to connect the upper structure and foundation for ease of installation. These structures including grouted connections experience considerable adverse loading during their lifetimes. Settlements were reported inside similar connections used in energy structures especially oil and gas platforms, which were installed in last three decades. Thus, repair and rehabilitation of such connections in existing wind structures should also be planned ahead to keep them operating in the future. The nature of failure and crack generation in grouted connections are crucial prior to adopt a strengthening strategy. This pilot study is carried out to actualize the failure mechanism in the grouted connection, when subjected to axial loading. A novel reusable scaled cylindrical grouted connection with shear keys was designed and tested for its load bearing behaviour. The mechanical test was accompanied by classical measuring techniques (e.g. displacement transducer) as well as non-destructive measuring techniques (e.g. digital image correlation (DIC), acoustic emission analysis (AE)). The failure mechanism incorporating slippage of the shear keys and cracking of the grout was investigated. The capacity and applicability of such test mould were also discussed. The knowledge is expected to pave way towards repair of deteriorated grouted connections with similar geometry and failure pattern. T2 - 1st International Conference on Construction Materials for Sustainable Future (CoMS_2017) CY - Zadar, Croatia DA - 19.04.2017 KW - Grouted connections KW - Cracks KW - Failure KW - Strengthening strategy KW - Digital image correlation KW - Acoustic emission analysis PY - 2017 AN - OPUS4-39915 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Baeßler, Matthias T1 - Structural Health Monitoring – How and to what extent a condition monitoring of the foundation may replace periodical subsea inspections? N2 - Der Betrieb von Offshore-Windenergieanlagen wird zunehmend zum wichtigen Thema im Bereich Windenergie. Anforderungen an Wiederkehrende Prüfungen und den Einsatz von ergänzenden Monitoringsystemen werden in der Präsentation dargestellt und durch Hinweise auf Perspektiven ergänzt. N2 - Operation of Offshore Windfarms has an increasing significance for Wind Energy. Content of the presentation are requirements for inspection and for complementary monitoring. Special focus is on future prospects. T2 - Windforce 2017 CY - Bremerhaven, Germany DA - 09.05.2017 KW - Inspektion KW - Wiederkehrende Prüfung KW - Offshore-Wind KW - Monitoring KW - Inspection KW - Regular inspection KW - Offshore-Wind KW - Monitoring PY - 2017 AN - OPUS4-40256 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Dutto, Paola A1 - Baeßler, Matthias A1 - Geißler, Peter T1 - Suction buckets behaviour under tensile loads: A numerical study with FEM N2 - Suction Bucket Jackets (SBJ) are found as a suitable alternative to driven piles for the support of foundations for offshore wind energy converters. In the case of jackets or multipods, a predominant vertical load is to be expected. The effect of such a tensile loading is the generation of suction in the soil inside the bucket which leads to an increment of tensile capacity. This paper aims to study the bearing behaviour of a suction foundation by taking into account how the soil permeability and the loading rate influence the foundation behaviour. Moreover, after submitting the structure to a storm load, the bearing capacity is studied again, in order to see the effect of such a load on the bucket's bearing behaviour. This study is carried out by means of Finite Element numerical simulations based on the formulation of Biot's equations combined with a constitutive model that reproduces the key aspects of cyclic soil behaviour in the frame of Generalized Plasticity. T2 - International Ocean and Polar Engineering Conference CY - San Francisco, USA DA - 25/06/2017 KW - Finite element method KW - Offshore wind energy converter KW - Suction bucket KW - Generalized plasticity KW - Sand KW - Numerical simulation KW - Tensile capacity PY - 2017 SN - 978-1-880653-97-5 SP - 485 AN - OPUS4-41051 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Geißler, Peter T1 - Modelling of compaction grouting using the implicit MPM N2 - Compaction grouting involves the injection under high pressure of a highly viscous grout into the soil to displace and compact the surrounding soil without fracturing it. This ground improvement technique has been used widely for settlement control, increasing liquefaction resistance or bearing capacity of soil under new or existing structures. The work presented here aims to show some numerical and experimental investigations being carried out to understand the compaction mechanism and the soil-grout interaction, which is crucial for a successful usage of this technique. To investigate compaction grouting in the laboratory under various stress conditions, a large-scale testing chamber has been developed. The grout was injected directly at the transparent vertical window of the chamber in order to investigate the possibility to monitor the injection process with a camera to measure the in-plane soil displacements and strains by means of the PIV technique. The other aim of this study is to develop a numerical model, which should be able to deal with large displacements and deformations and to simulate the change in shape of the distinct soil-grout interface solely as a result of the interaction between the injected grout and the surrounding soil. Based on these considerations, as a numerical technique, we employ the implicit Material Point Method based on a mixed formulation, which is implemented in the open source Kratos Multiphysics framework. In contrast to standard FE formulations, the usage of the MPM avoids both the numerical instability caused by extensive mesh distortion and the high computational costs of remeshing. The main results focus on the different evolution of the grout bulb inside the soil under various stress states. T2 - 28th ALERT Workshop CY - Aussois, France DA - 02.10.2017 KW - Compaction grouting KW - Soil-grout interface KW - Material point method (MPM) KW - Mixed formulation KW - Particle image velocimetry (PIV) PY - 2017 AN - OPUS4-42432 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Kannengießer, Thomas A1 - Schröpfer, Dirk T1 - Einsatz modifizierter Sprühlichtbogenprozesse zur Optimierung schweißbedingter Beanspruchungen an Bauteilen aus hochfesten Feinkornbaustählen N2 - Aufgrund aktueller Leichtbaubestrebungen sowie Forderungen nach Energie- und Ressourceneffizienz werden zunehmend hochfeste Feinkornbaustähle mit Streckgrenzen ≥ 690 MPa in modernen Stahlkonstruktionen eingesetzt. Vorrangig werden diese mit Streckgrenzen bis 960 MPa verarbeitet und mittels MAG-Schweißprozessen gefügt. Moderne Invertertechnik ermöglichte jüngst zahlreiche Firmenentwicklungen (bspw. „DeepARC“, „forceArc“), die zu modifizierten Sprühlichtbögen (mod. SLB) mit ähnlichen Eigenschaften führten. Neben den bekannten wirtschaftlichen Vorteilen dieser mod. SLB, lassen gerade die reduzierten möglichen Nahtöffnungswinkel und die geringere Wärmeeinbringung eine positive Wirkung auf schweißbedingte Beanspruchungen erwarten. Erste Eigenspannungsanalysen bei vorangegangenen Schweißeignungsuntersuchen mit mod. SLB zeigten bereits bei freischrumpfenden Laborproben geringere Zugeigenspannungen in der Schweißnaht im Vergleich zu konventionell geschweißten Proben. Die betriebsfeste Auslegung von hochfesten Schweißkonstruktionen und die Ausnutzung hoher Streckgrenzen erfordern jedoch eine ausreichende Quantifizierung schweißbedingter Beanspruchungen der mod. SLB unter definierter, bauteilrelevanter Schrumpfbehinderung. Dies betrifft sowohl die Kräfte und Spannungen im lokalen Schweißnahtbereich als auch die Gesamtbeanspruchung sowie den Einfluss von Wärmeführung, Bauteilgeometrie, Einspanngrad und Nahtöffnungswinkel. Hierzu lagen in der Industrie, besonders bei den KMU, kaum Kenntnisse vor und sollten deshalb als Ziel dieses Forschungsprojektes erarbeitet werden. Die vergleichenden Untersuchungen mit konventionellen Lichtbogen und mod. SLB mit angepasster Nahtkonfiguration erfolgten mithilfe von speziellen Prüfanlagen, mit der reale Bauteilsteifigkeiten abgebildet werden können. Bei beiden Prozessvarianten waren mit den gewählten Parametern Schweißnähte unter Erfüllung der Anforderungen an die mechanisch-technologischen Eigenschaften realisierbar. Bei den Analysen konnte eine signifikante Reduzierung der Eigenbeanspruchungen durch eine verminderte Wärmeeinbringung bei dem Einsatz einer Nahtkonfiguration mit abgesenktem Nahtöffnungswinkel beobachtet werden. Insbesondere erwiesen sich zur Absenkung mehrachsiger Beanspruchungszustände aufgrund von Biegemomenten in den bauteilnahen Schweißungen die engeren Nahtspalte als zielführend. Eine Vorstellung der erarbeiteten Kenntnisse und Empfehlungen in entsprechenden Gremien zur Normung erfolgten, um mittelfristig vor allem den KMU eine einfachere Konstruktionsauslegung und sichere Verarbeitung hochfester Feinkornbaustähle zu ermöglichen. Mit einer normativen Absicherung kann Qualifizierungs- und Zulassungsaufwand eingespart werden, der aktuell beim Einsatz hochfester Stähle vielfach notwendig ist. Ferner werden die Betriebe durch die Ergebnisse in die Lage versetzt, die technischen und wirtschaftlichen Vorteile der mod. SLB-Prozesse auszunutzen und signifikante Einsparungen bei Schweißzusatz, Schweiß- und Rüstzeit sowie unter Berücksichtigung der Eigenbeanspruchung optimierte Ergebnisse hinsichtlich der Tragfähigkeit von Bauteilen zu erreichen und die Produktivität zu erhöhen. KW - MAG-Schweißen KW - Hochfester Stahl KW - Eigenspannungen KW - Kaltrisssicherheit PY - 2017 UR - https://matplus.shop/produkt/p-1011-einsatz-modifizierter-spruehlichtbogenprozesse-zur-optimierung-schweissbedingter-beanspruchungen-an-bauteilen-aus-hochfesten-feinkornbaustaehlen-2 SN - 978-3-946885-12-2 N1 - Das IGF-Vorhaben 17978 N wurde über die Arbeitsgemeinschaft industrieller Forschungsvereinigungen "Otto von Guericke" (AiF) im Rahmen des Programms zur Förderung der Industriellen Gemeinschaftsforschung (IGF) vom Bundesministerium für Wirtschaft und Energie (BMWi) aufgrund eines Beschlusses des Deutschen Bundestages gefördert VL - P 1011 SP - 1 EP - 136 PB - Verlag und Vertriebsgesellschaft CY - Düsseldorf AN - OPUS4-59257 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael T1 - Hydrogen trapping in T24 steel weld joints - microstructure influence vs. experimental design effect on activation energy for diffusion N2 - In general, hydrogen assisted cracking is a result of a critical combination of local microstructure, mechanical load and hydrogen concentration. In that connection, welded microstructures of low-alloyed creep-resistant steels can show different hydrogen trapping kinetics. That influences the adsorbed hydrogen concentration as well as the diffusion itself in terms of moderate or strong trapping. A common approach to describe trapping is by the activation energy that is necessary to release hydrogen from a specific trap site. In the present study, T24 base material and weld metal were investigated. For that purpose, electrochemically hydrogen charged specimens were analyzed by thermal desorption analysis(TDA) with linear heating using a mass spectrometer. The results showed a microstructure effect on hydrogen trapping kinetics at elevated temperatures. Additionally, it is necessary to monitor the specimen temperature. A comparison between idealized temperature profile and real specimen temperature showed that the calculated activation energy varied up to a factor of two. Thus, the assigned trap character(moderate or strong) changed. In case of high temperature peaks, this effect could be more important compared to the microstructure effect itself. T2 - 70th IIW Annual Assembly, Commission II-A CY - Shanghai, People's Republic of China DA - 25.06.2017 KW - Creep resisting materials KW - Welding KW - Hydrogen diffusion KW - Thermal desorption analysis KW - Microstructure KW - Experimental design PY - 2017 AN - OPUS4-40954 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Becker, Ben A1 - Mair, Georg W. T1 - Risks and safety level of composite cylinders N2 - The increasing amount of composite transport systems for hydrogen leads to new and therefore unknown potential hazards for general public. Due to lack of experience, risks of new technologies tend to be rated higher than existing familiar applications. An approach for probabilistic safety assessment of technologies or products requires the definition of minimal acceptable reliability levels. This ensures that the probability of a critical failure with a certain consequence is limited to an acceptable risk. But what is the acceptable risk and which risk results from specific probabilities of occurrence and consequences? This is always a very complex question. The following example is based on a probabilistic approach for safety assessment of composite cylinders developed at the BAM (Federal Institute for Materials Research and Testing). KW - Reliability KW - Cylinder KW - Safety KW - Consequence PY - 2017 UR - http://www.sciencedirect.com/science/article/pii/S0360319917303117 DO - https://doi.org/10.1016/j.ijhydene.2017.01.145 SN - 0360-3199 SN - 1879-3487 VL - 42 IS - 19 SP - 13810 EP - 13817 PB - Elsevier Ltd. AN - OPUS4-40691 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. A1 - Becker, Ben T1 - Practical applications of CPVs - ESR 11: Accumulation of fibre breaks under time-dependent loads in CFRP materials of composite cylinders N2 - Das Anwendungsspektrum von CPV (composite pressure vessels) ist vielschichtig. Aber auch die Versagensformen und das Spektrum der Messmethoden ist vielfältig. Anhand verschiedener, in der BAM festgestellter Effekte wird gezeigt, warum die micromechnanische Betrachtung des Composties von so großem Interesse für die Vorhersage der Alterung von CPVn ist. N2 - The application range of CPV (composite pressure vessels) is multifaceted. But also the failure forms and the spectrum of measurement methods is manifold. On various, at BAM observed effects, it is shown why the micromechanical analysis of the composites is of such great interest for the prediction of aging effects of CPVs. T2 - Kick-Off Meeting FiBreMoD CY - KU Leuven, Belgium DA - 27.03.2017 KW - Composite KW - Degradation KW - Pressure increase rate KW - Slow burst test PY - 2017 AN - OPUS4-41711 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. A1 - Becker, Ben T1 - Monte-Carlo-analysis of minimum load cycle requirements for composite cylinders for hydrogen N2 - Existing regulations and standards for the approval of composite cylinders in hydrogen service are currently based on deterministic criteria (ISO 11119-3, UN GTR No. 13). This paper provides a systematic analysis of the load cycle properties resulting from these regulations and standards. Their characteristics are compared with the probabilistic approach of the BAM. Based on Monte-Carlo simulations the available design range of all concepts is compared. In addition, the probability of acceptance for potentially unsafe design types is determined. T2 - ICHS 2017 CY - Hamburg, Germany DA - 11.09.2017 KW - Composite KW - Sample performance chart KW - Regulations KW - GTR No 13 PY - 2017 AN - OPUS4-41942 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. T1 - GAS ALS ENERGIETRÄGER - Die Kompetenz der BAM in Fragen der sicheren Druckspeicherung N2 - Der Vortrag stellte kurz die Abteilung vor und wo der Arbeitsbereich Druckgefäße einzuordnen ist. Er weist auf die Verwendung von Wasserstoff und auf unsere Kompetenz in der Beurteilung von Sicherheit, unsere Beratung und Forschung hin. Darüber hinaus werden die in der BAM auf Wasserstoffspeicher angewendeten Prüfverfahren dargestellt und als ein Schwerpunkt die hydraulische Prüfung erläutert. Über die Monte-Carlo-Simulation zur Beurteilung von Vorschriften führt er zum probabilistischen Sicherheitsansatz. T2 - Besuch der BAM durch die China Energy-saving Insulation Materials Association, China CY - BAM-FB, Berlin, Germany DA - 07.06.2017 KW - Monte-Carlo KW - Sample Performance Chart KW - Zuverlässigkeit KW - Langsame Berstprüfung PY - 2017 AN - OPUS4-41737 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Becker, Ben A1 - Mair, Georg W. T1 - Statistical analysis of burst requirements from regulations for composite cylinders in hydrogen transport N2 - Existing standards for the approval of composite cylinders for the transport of compressed hydrogen are currently based on deterministic (ISO 11119-3) and semi-probabilistic (UN GTR No. 13) criteria. This paper analysis the capabilities of these procedures with respect to the evaluation of burst strength. Their characteristics are compared with the probabilistic approach developed at BAM. Based on Monte-Carlo simulations the available design range (mean value and scatter of burst strength) of all concepts are assessed. In addition, the probability of acceptance for potentially unsafe design types is determined. The results show large areas of burst properties with a sufficient reliability which cannot be used for the design of composite cylinders, due to current approval criteria. On the other hand, existing standards allow the approval of potentially unsafe designs in case of a very high scatter regarding their burst strength. It is also shown that existing design types are already designed to the limits of the available design area. A further weight and cost reduction of composite cylinders is therefore closely related to the approval criteria. An example based on UN GTR No. 13 shows how an approval criterion can be optimized by using statistical methods. The example shows that a reduced minimum burst pressure can be combined with a lower probability of acceptance for potentially unsafe design types. KW - Composite cylinder KW - Monte Carlo simulation KW - Burst requirements PY - 2017 UR - http://www.hanser-elibrary.com/doi/pdf/10.3139/120.110988 DO - https://doi.org/10.3139/120.110988 SN - 0025-5300 VL - 59 IS - 3 SP - 226 EP - 232 PB - Carl Hanser Verlag CY - München AN - OPUS4-39526 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Duffner, Eric T1 - Schallemissionsprüfung an Druckbehältern N2 - Neben Anwendungsbeispielen für die Schallemissionsprüfung bei der wiederkehrenden Prüfung von Druckspeichern, wird insbesondere auf Forschungsaspekte der Schallemissionsmessung an Composite-Druckbehältern eingegangen. T2 - Erfahrungsaustausch für amtlich anerkannte Sachverständige der Anlagenüberwachung der Industrie CY - Würzburg, Germany DA - 04 April 2017 KW - Schallemissionsprüfung KW - Druckspeicher KW - Composite-Druckbehältern PY - 2017 AN - OPUS4-39684 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Saul, Herbert T1 - Gefahrguttransport - Ablaufdiagramm "Verwaltungsvorgang" N2 - Das Poster stellt die verschiedenen Schritte zur Bearbeitung eines Verwaltungsvorangs dar. Dieser beginnt mit der Anbahnung des Vorgangs, mit Prüfung der Rechtsvorschriften und der Erforschung des Kundenwillens. Im nächsten Schritt wird die Vollständigkeit der Unterlagen geprüft, bevor im Fall positiv geprüfter Unterlagen (Nachweis der Erfüllung der Rechtsanforderungen) der Bescheid erstellt und der Verwaltungsakt abgeschlossen werden kann. T2 - Abteilungskolloquium "Verwaltungsrecht für Zulasser" CY - BAM-Berlin, Germany DA - 16.02.2017 KW - Antragstellung KW - Verwaltungsakt KW - Bescheid KW - Nachforderung PY - 2017 AN - OPUS4-39213 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. T1 - Needs for safe hydrogen storage - Contributions of BAM N2 - This presentation provides general data about BAM, the structure of department 3 and a short impression of the application of pressure vessels for hydrogen in stationary use, supply chain and onboard storage. It guides to the actions of BAM as competent authority on this area and shows a lot different methods for testing operated at BAM. Based on this additional research has been detected as necessary for a competent tackling of the tasks as competent authority. After having mentioned several important research projects a figure is presented that compares the development of regulations with relevant re-actions of BAM. The outcome was a concept of a risk based definition of accepted failure rates in combination with probability-oriented safety assessment over entire service life. The second aspect raised at INERIS is the issue of advising the BMVI concerning pressure vessels for hydrogen. Since the pressure is high for saving material consumption and weight there is still high interest in changing regulatory requirements. Therefor we developed an approach for the display of minimum requirements of regulations in diagrams (sample performance charts; SPC) and the probabilistic analysis for these deterministic requirements. This is done by Monte-Carlo simulation and the analysis of acceptance rate and survival rate of basic populations all over the SPC. This finally provide same knowledge of non-approvable but safe ranges of parameters and even approvable but non-safe constellations. In addition, this analysis allows to optimise deterministic requirements in regulations to the intended level of safety for approved populations of pressure vessels, which is shown on the example of the GTR#13. T2 - WORKING MEETING Cooperation BAM - INERIS CY - INERIS, Verneuil-en-Halatte, France DA - 23.10.2017 KW - Competent authority KW - Monte-Carlo KW - Composite KW - Sample performance chart KW - Regulations PY - 2017 AN - OPUS4-42637 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. T1 - Monte-Carlo-analysis of requirements for CGH2-CPVs N2 - This presentation explains how the evaluation of technical requirements in regulations effects safety level. This shown by using the Monte-Carlo experiment consequently. The first step is to explain how deterministic requirements and how probabilistic requirements work. Then the statistical behaviour of the generally unknown basic population can be described and that his behaviour is independent from the regulatory approach. Subsequently, the concept of evaluating sample test results with respect to deterministic requirements is explained. The item “acceptance rate” of the basic population that is behind each sample and behind each individuum in a sample is defined. On this collective understanding, the differences in evaluation between the probabilistic approach PA and the most important RC&S are discussed. Some areas are validated in contradictorily. Then the parameters for acceptance of burst strength in the UN-GTR#13 are varied and opens the door for an accurate improvement of acceptance criteria. Finally, the special aspects of degradation in load cycle testing are shown. There, two aspects must be differentiated, the current reliability and its degradation by ongoing load cycles. This is a convincing argument against the very common opinion, which means that the number of hydraulically tested load cycles pro-vides a figure for the number of acceptable filling cycles. T2 - FiBreMoD Training Unit #5 CY - BAM-FB, Berlin, Germany DA - 05.10.2017 KW - Composite pressure vessels KW - Basic population KW - Acceptance criteria KW - Acceptance rate KW - Sample size KW - Lucky punch area KW - Load cycle test KW - Burst test KW - Scatter PY - 2017 AN - OPUS4-43112 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. T1 - Open Issues of Insuring Safety of CPVs by Strength Testing N2 - This presentation mentions the most important safety items that should be improved from the perspective of Germany. These are the improvement of the understanding and definition of term "safety", the agreement on procedures for the measurement of safety and the issue of degradation in combination with the safety level to be ensured until end of life. For using probabilistic experience for the whole production adequate measures for surveillance of the production should additionally become mandatory to be taken into account. The essential aspects of these issues are shortly explained and highlighted by especially aspects of the slow burst testing with respect to non-cycle fatigue sensitive designs and the hint on the general scatter of properties (Monte-Carlo simulation). T2 - 1st Meeting of the informal working group on Hydrogen and Fuel Cell Vehicles Global Technical Regulation No. 13 (Phase 2) CY - Brussels, Belgium - European Commission Directorate-General for Internal Market, Industry, Entrepreneurship and SMEs Automotive and Mobility Industries (DG GROW C.4) DA - 17.10.2017 KW - Safety KW - Scatter KW - Cycle-fatigue sensitivity KW - ECE R134 KW - GTR 13 KW - Degradation PY - 2017 AN - OPUS4-42638 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. T1 - The Sample Performance Chart & its use for the display of degradation N2 - This presentation explains how BAM operates the PA approach for the life-time surveillance based on the measurement of degradation. The starting point is the sample performance chart (SPC) as developed by BAM. There it is possible to show minimum requirements, sample properties and lines of constant survival rates, these lines are called isoasfalia. The BAM provides a tool for the safety evaluation of results from sample testing. Then the interaction to the micro-mechanical approach of the FiBreMoD-project is linked with the idea of a degradation of strength and reliability. This leads to the methods of burst and cycle testing. For both methods examples are shown and degradation is explained by showing data of two design types. This visualise the determination of safe service life. Finally, statistical aspects of misinterpretation of test results and the reasons for the decision in favour of the slow burst tests are explained. T2 - FiBreMoD Training Unit #5 CY - BAM-FB, Berlin, Germany DA - 05.10.2017 KW - Sample performance chart KW - End of Life KW - Loss of safety KW - Micro-mechanics KW - Creep effects PY - 2017 AN - OPUS4-43110 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. T1 - Concept of a Probabilistic Approval Approach (PAA) N2 - This presentation explains how an PA-based approval concept could work and would substitute the most of deterministic requirements based on a risk based quantification of accepted failure rates. The concept of a probabilistic approval approach is based on 5 separate types of requirements: 1. Testing and evaluation of properties at Beginning of Life (BoL) 2. Artificial aging with residual strength assessment 3. Testing against dedicated accidental loads 4. Surveillance of production quality 5. Surveillance of degradation/ check of estimated end of life (EoL) Each of these aspects is visualised by photos and diagrams. T2 - FiBreMoD Training Unit #5 CY - BAM-FB, Berlin, Germany DA - 04.10.2017 KW - Beginning of life KW - End of safe service life KW - Artificial ageing KW - Design type testing KW - Accidental loads KW - Survaillance of degradation PY - 2017 AN - OPUS4-43111 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. T1 - Tasks and needs of a competent authority for gas storage N2 - This presentation provides an impression of the boundary condition of the work on composite cylinders on a competent authority. It shows the various kinds of usage, the different tasks and duties around this kind of storage units and the wide spread of technical competence necessary for the substantial research when addressing the legislation. Based on this it shows how we react on changes in the regulations by research and how this influences the regulations, again. As an example, our probabilistic approach is mentioned and drafted for getting mentioned several times during the ongoing set of presentations. T2 - FiBreMoD Training Unit #5 CY - BAM-FB, Berlin, Germany DA - 05.10.2017 KW - Advisement KW - Frequency KW - Consequence KW - Safety assessment KW - NDT PY - 2017 AN - OPUS4-43085 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. A1 - Saul, Herbert A1 - Duffner, Eric T1 - Composite Pressure Vessels for Hydrogen - Research for Safety N2 - Referring to the inter-departmental project group "Pressure Equipment" and the section "Pressure Equipment-pressure receptacles; Fuel Gas Storage Systems" developed from, it is shown here how research on safety aspects, technical regulations and the activities of the Federal Institute BAM in its role as competent authority interact to the advantage of safety of composite pressure vessels. T2 - FiBreMoD Steering Committee Meeting and Training Unit #5 CY - BAM Berlin, Germany DA - 04.10.2017 KW - Pressure Equipment KW - ECE R110 KW - TPED KW - StorHy KW - HyComp KW - Service life tests KW - UN composite cylinders KW - PN020 KW - GTR KW - ECE R134 KW - Competent authority PY - 2017 AN - OPUS4-42461 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Neumann, Patrick P. T1 - Bringing Mobile Robot Olfaction to the Next Dimension – UAV-based Remote Sensing of Gas Clouds and Source Localization N2 - This presentation introduces a novel robotic platform for aerial remote gas sensing. Spectroscopic measurement methods for remote sensing of selected gases lend themselves for use on mini-copters, which offer a number of advantages for inspection and surveillance. No direct contact with the target gas is needed and thus the influence of the aerial platform on the measured gas plume can be kept to a minimum. This allows to overcome one of the major issues with gas-sensitive mini-copters. On the other hand, remote gas sensors, most prominently Tunable Diode Laser Absorption Spectroscopy (TDLAS) sensors have been too bulky given the payload and energy restrictions of mini-copters. Here, we introduce and present the Unmanned Aerial Vehicle for Remote Gas Sensing (UAV-REGAS), which combines a novel lightweight TDLAS sensor with a 3-axis aerial stabilization gimbal for aiming on a versatile hexacopter. The proposed system can be deployed in scenarios that cannot be addressed by currently available robots and thus constitutes a significant step forward for the field of Mobile Robot Olfaction (MRO). It enables tomographic reconstruction of gas plumes and a localization of gas sources. We also present first results showing the gas sensing and aiming capabilities under realistic conditions. T2 - IEEE International Conference on Robotics and Automation (ICRA) CY - Singapore DA - 29.05.2017 KW - Tunable Diode Laser Absorption Spectroscopy (TDLAS) KW - 3-axis gimbal KW - Mobile Robot Olfaction KW - Tomographic reconstruction of gas plumes KW - Localization of gas sources KW - Aerial platform PY - 2017 AN - OPUS4-40546 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Rücker, Werner A1 - Cuéllar, Pablo A1 - Georgi, Steven A1 - Karabeliov, Krassimire A1 - Baeßler, Matthias A1 - Johnsen, Björn ED - Durstewitz, M. ED - Lange, B. T1 - Please Avoid Tilting - Application-Oriented Design and Monitoring Model for Foundation Structures Subjected to Cyclic Loads N2 - A great deal is possible, even on the seabed. Together, wind and waves shake the foundations of the offshore wind turbines. "ere is also the “normal” current and ebb and #ow of the tides that are so distinctive in the North Sea. Pore water pressure can also occur on the seabed, loosening it. Where monopiles are involved, the worst case is that the stability of the whole turbine can be altered – even if such a monopile rammed into the seabed has a diameter of up to eight metres. Over half the planned offshore wind turbines in the North and Baltic Seas are to have monopile foundations, and over 40 % are to have multi-pile foundations, designed for example as a tripod. "is is why pile foundations and their loads deserve special attention. For one thing above all is to be avoided in plant operations, and that is the risk of turbine tilt. KW - Pile foundations KW - Offshore wind turbines KW - Cyclic loads PY - 2017 SN - 978-3-662-53178-5 DO - https://doi.org/10.1007/978-3-662-53179-2 SP - 53 EP - 59 PB - Springer AN - OPUS4-39340 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kullolli, Borana T1 - On contact problem application for the local behavior of soil-pile interaction N2 - In this paper a shear test, which helps to study local behavior of the soil-pile interaction, is modelled numerically with the Finite Element Method as a 2D plane strain problem. A normal pressure on top and shear displacement on side were applied. So far, the material behavior was considered elastic for the sake of simplicity. The effect of thickness on contact elements and the presence of in plane stress has been highlighted. The purpose of the paper is to find a suitable contact element which represents more close to reality a soil-pile interaction problem under cyclic axial loading. Moreover, an insight on the presence of in-plane stress shows that it needs to be considered cautiously. T2 - ICCE 2017 CY - Tirana, Albania DA - 12.10.2017 KW - Contact problem KW - Numerical problem PY - 2017 AN - OPUS4-42963 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -