TY - CONF A1 - Hicke, Konstantin T1 - Distributed fiber optic radiation sensors for nuclear applications N2 - Advantages and underlying principles of distributed fiber optic radiation sensing are discussed. Differences with regard to dose measurement range and resolution between glass optical fiber based sensing and polymer optical fiber based sensing are outlined. T2 - DGZfP SMIRT26 Laborbesuch (BAM) CY - Berlin, Germany DA - 10.07.2022 KW - Distributed fiber optic sensing KW - Fiber optic radiation monitoring KW - Distributed fiber optic radiation sensing PY - 2022 AN - OPUS4-55264 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Caruso, Stefano A1 - Vlassopoulos, Efstathios A1 - Dagan, Ron A1 - Fiorito, Luca A1 - Herm, Michel A1 - Jansson, Peter A1 - Kromar, Marjan A1 - Király, Márton A1 - Leppanen, Jaakko A1 - Feria Marquez, Francisco A1 - Metz, Volker A1 - Papaioannou, Dimitrios A1 - Herranz, Luis Enrique A1 - Rochman, Dimitri A1 - Schillebeeckx, Peter A1 - Seidl, Marcus A1 - Hernandez Solis, Augusto A1 - Stankovskiy, Alexey A1 - Alvarez Velarde, Francisco A1 - Verwerft, Marc A1 - Rodriguez Villagra, Nieves A1 - Zencker, Uwe A1 - Žerovnik, Gasper T1 - EURAD - Work Package 8 - Deliverable 8.1 - State-of-the-art report N2 - A state-of-the-art (SOTA) review on characterisation of spent nuclear fuel (SNF) properties in terms of source term and inventory assessment (neutron, gamma-ray emission, decay heat, radionuclide inventory, elemental content) and in terms of out-of-core fuel performance (cladding performance and fuel integrity in view of the safety criteria for SNF interim storage, transport and canister packaging) using several numerical and experimental approaches and methodologies is presented. This SOTA report is a result of the spent fuel characterisation (SFC) work package as part of the European Joint Programme on Radioactive Waste Management (EURAD), which offers an overview of the status of knowledge in the field of SNF characterisation and assessment during the pre-disposal phase. The document aims to focus on the current safety-significant gaps and related challenges, providing a direct link to the goals of the mandated actors of EURAD. The report is expected to be used by all EURAD colleagues in their national programmes as a key resource for knowledge management programmes and to contribute to demonstrating and documenting the state-of-the-art. KW - Radioactive waste management KW - Spent fuel characterisation KW - Extended interim storage KW - Predisposal PY - 2022 UR - https://www.ejp-eurad.eu/publications/eurad-d81-state-art-report SP - 1 EP - 112 PB - Agence Nationale pour la Gestion des Déchets Radioactifs (ANDRA) CY - Châtenay-Malabry AN - OPUS4-59154 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Pittner, Andreas A1 - Schürmann, Karsten ED - Böhmer, Heike ED - Brinkmann-Wicke, Tanja ED - Sell, Sabine ED - Simon, Janet ED - Tebben, Cornelia T1 - Automatisierte Rohrknotenfertigung in der Offshore-Windenergie – Potenzial zum Leichtbau im schweren Stahlbau N2 - Um den Klimawandel wirksam zu bekämpfen, ist es entscheidend, fossile Brennstoffe durch erneuerbare Energiequellen wie Wind-, Solar- und Wasserkraft sowie alternative Energieträger, beispielsweise grünen Wasserstoff, zu ersetzen. Offshore-Windenergie spielt hierbei eine zentrale Rolle, da sie dank der Kombination aus globaler Verfügbarkeit, relativ geringen Betriebskosten und fortgeschrittenem technischen Entwicklungsstand besonders geeignet ist, zur regenerativen Stromerzeugung beizutragen. Sie ist zudem ein Schlüsselelement für die Umsetzung des Europäischen Green Deals, der das Ziel verfolgt, bis 2050 Klimaneutralität in der EU zu erreichen. Expertenschätzungen zufolge ist eine Steigerung der aktuellen Kapazität von 25 GW im Jahr 2020 auf etwa 450 GW notwendig, um diese ambitionierten Ziele zu erfüllen. Bei der Entwicklung zukünftiger Offshore-Windparks, insbesondere in tieferen Gewässern, gewinnen Jacket-Gründungsstrukturen an Bedeutung. Diese Strukturen, die eine höhere Steifigkeit bei geringerem Materialeinsatz im Vergleich zu den bisher vorherrschenden Monopile-Gründungen bieten, basieren auf komplexen, räumlich aufgelösten Konstruktionen, die ähnlich den Öl- und Gasplattformen entwickelt werden. Die Herstellung der Jacketknoten, die bislang überwiegend manuell geschweißt wurden, birgt erhebliches Optimierungspotential. Durch Automatisierung und Digitalisierung der Fertigungsprozesse könnten nicht nur die Effizienz gesteigert, sondern auch die Qualität der Endprodukte durch präzise Überwachung und Kontrolle der Produktionsparameter verbessert werden. Diese technologischen Fortschritte sind für die Skalierung der Offshore-Windenergie und die Erreichung der Klimaziele von entscheidender Bedeutung. KW - Automatisierte Fertigung KW - Offshore Windenergie KW - Jacket-Gründungsstrukturen KW - Aufgelöste Tragstrukturen KW - Leichtbau PY - 2022 SN - 978-3-7388-0719-6 SP - 260 EP - 266 PB - Fraunhofer IRB Verlag CY - Stuttgart AN - OPUS4-59502 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Linnemann, Konrad A1 - Quercetti, Thomas A1 - Sterthaus, Jens A1 - Ballheimer, Viktor T1 - Experimental and numerical investigation of prestressed bolt connections under lateral displacements N2 - The containment system of transport packages for spent nuclear fuel and high-level waste usually includes bolted lids with metal gaskets. The packages are assessed to specific transport conditions which are specified in the IAEA safety standards SSR-6 (IAEA 2018). These transport conditions, especially the so-called accident conditions of transport, imply high dynamic loading on the lids and the bolt connections of the package. The response of the lid systems on the mechanical accident conditions is generally investigated by experimental drop tests or numerically, e.g., by finite element analyses. The interpretation of the drop test results for the verification of the numerical models is often not obvious due to the complex superposition of different effects in the real tests. BAM has started a research project to get a better understanding about the behavior of prestressed bolt connections under loadings typical for these drop tests. In this context an experimental test set-up was developed to investigate the response of a single bolt connection under a prescribed lateral displacement of clamped parts. The bolt is instrumented by strain gauges to get the pretensional, the torsional and the bending stress in the bolt shank. Furthermore, the lateral movement and the tilt of the bolt head is measured during the test. A finite element model of the test set-up has been created in Abaqus FEA (Simulia 2021). The very detailed instrumentation of the test set-up shall give the opportunity to investigate and validate the numerical model. The aim of this paper is to give an overview about the proposed research project and to present first results. T2 - SMIRT 26 (26th conference on Structural Mechanics in Reactor Technology) CY - Potsdam, Germany DA - 10.07.2022 KW - Bolt connections KW - Finite element anaylsis KW - Experimental testing KW - Transport package for radioactive materials PY - 2022 UR - https://www.lib.ncsu.edu/resolver/1840.20/40614 SP - 1 EP - 7 PB - IASMiRT AN - OPUS4-59378 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Feldkamp, Martin T1 - Fire Reference Tests for Qualification of IAEA Fire N2 - A small cylindrical fire reference package was designed. A fire test setup was created using the fire reference package in accordance with IAEA standards. Four propane gas fire tests were conducted to determine heat fluxes into the fire reference package. The initial test setup was modified to create the final design of the fire test facility. This allowed for the heat flux to be adjusted to meet the regulatory IAEA fire qualification criteria. Furthermore, a numerical model of the fire reference package was created using boundary conditions derived from the experimental data. The simulation results demonstrated good agreement with the experimental data and provided additional insights. T2 - Technical Exchange IRSN – BAM Transport & Storage of Packages for Radioactive Material CY - Cadarache, France DA - 13.10.2022 KW - Fire KW - IAEA KW - Propane PY - 2022 AN - OPUS4-57251 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Gerards-Wünsche, Paul T1 - Der Weg vom Labor zur industriellen Einsetzbarkeit der Risslumineszenz N2 - Der Vortrag beschreibt die Relevanz der Zuverlässigkeitsbewertung von klassischen ZfP- und SHM-Verfahren. Diese Zuverlässigkeitsbewertung soll auch für das an der BAM entwickelte Risslumineszenzverfahren durchgeführt werden. Die Risslumineszenz wird zunächst vorgestellt und es wird beschrieben welchen Weg man beschreiten muss, um eine Zuverlässigkeitsbewertung für eine Technik durchzuführen, die nicht nur als ZfP-Verfahren genutzt werden soll, sondern auch für die Dauerüberwachung unter der Einbindung einer KI-basierten automatisierten Risserkennung. Die mit dieser Erweiterung des Einsatzspektrums einhergehenden Faktoren für Messunsicherheit und -variabilität wird als Problematik erkannt und als zukünftige Aufgabe, die es zu lösen gilt, definiert. T2 - ZfP-Seminar Prof. Große TU München WS22 CY - Online meeting DA - 15.12.2022 KW - Rissprozes KW - Structural Health Monitoring KW - Risslumineszenz KW - Ermüdungsprüfung KW - Rissprozess PY - 2022 AN - OPUS4-56643 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Stamm, Michael A1 - Krankenhagen, Rainer T1 - EvalTherm - Weather-dependent passive thermography of unheated wind turbine blades N2 - Evaluation of passive Thermography for the inspection of wind turbine blades. Comparison of passive thermography from the ground with drone-supported images and active thermography. Better understand the influence of weather conditions through field measurements. Development of an inspection planning tool that incorporates weather forecasts. Use FEM simulations to predict thermal contrasts of different damages under different environmental conditions. T2 - Kolloquium CY - Saarbrücken, Germany DA - 28.09.2022 KW - Thermography KW - Wind turbine rotor blades KW - FEM PY - 2022 AN - OPUS4-56913 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Das, P. A1 - Chakraborty, Gouri A1 - Roeser, J. A1 - Vogl, S. A1 - Rabeah, J. A1 - Thomas, A. T1 - Integrating Bifunctionality and Chemical Stability in Covalent Organic Frameworks via One-Pot Multicomponent Reactions for Solar-Driven H2O2 Production N2 - Multicomponent reactions (MCRs) can be used to introduce different functionalities into highly stable covalent organic frameworks (COFs). In this work, the irreversible three-component Doebner reaction is utilized to synthesize four chemically stable quinoline-4-carboxylic acid DMCR-COFs (DMCR-1−3 and DMCR-1NH) equipped with an acid−base bifunctionality. These DMCR-COFs show superior photocatalytic H2O2 evolution (one of the most important industrial oxidants) compared to the imine COF analogue (Imine-1). This is achieved with sacrificial oxidants but also in pure water and under an oxygen or air atmosphere. Furthermore, the DMCR-COFs show high photostability, durability, and recyclability. MCR-COFs thus provide a viable materials’ platform for solar to chemical energy conversion. KW - Reactions KW - Bifunctionality KW - Postsynthetic modification KW - Multicomponent PY - 2022 DO - https://doi.org/10.1021/jacs.2c11454 SN - 0002-7863 VL - 145 IS - 5 SP - 2975 EP - 2984 PB - ACS Publications AN - OPUS4-56922 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera T1 - Innovations in cemented waste handling and pre-disposal storage (WP7 project PREDIS) N2 - During the webinar "Dismantling and waste management: a playground for innovation" the innovative aspects of the PREDIS work package "innovations in cemented waste handling and pre-disposal storage" are presented. The webinar is jointly organised by Women in Nuclear Decommissioning (WINDI) and Women in Nuclear Innovation (WINI). The shown innovations include quality assurance (mainly NDE) and monitoring technologies with associated sensor systems, digital twin technology, and appropriate data handling including a decision framework. An overview of the on-going research in the field of pre-disposal waste management in the project Predis (WP7) is summarised. T2 - Webinar "Dismantling and waste management: a great playground for innovation" CY - Online meeting DA - 13.10.2022 KW - Predis KW - Waste management KW - Concrete PY - 2022 AN - OPUS4-56926 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Völzke, Holger T1 - Container requirements for high-level radioactive waste disposal in rock salt, claystone, and crystalline rock – Outcomes of the research project KoBrA N2 - Suitable containers for receiving high-level radioactive waste are a key elements of every repository system concerning different host rocks like rock salt, claystone and crystalline rock as being considered in Germany. The disposal container design is decisive regarding boundary conditions for the transport, emplacement techniques, and the operational and long-term safety assessment. The systematic derivation of the requirements to be placed on disposal containers forms the basis for a targeted, comprehensible and transparent development of containers that meet the requirements. The presentation summarizes the outcomes of the research project KoBrA. T2 - IGD-TP Symposium CY - Zurich, Switzerland DA - 20.09.2022 KW - Disposal KW - Container KW - Radioactive waste KW - Safety PY - 2022 AN - OPUS4-57021 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Liepold, Philipp T1 - Anwendung von CNNs zur verbesserten Auswertung von MVT-Tests N2 - Durch die Anwendung von Convolutional Neural Networks (CNNs) kann die Auswertung von Modifizierten Varestraint-Transvarestraint-Tests (MVT) erheblich verbessert werden. Im MVT-Test werden Proben während des Schweißvorgangs über einen Zylinder gebogen. Die auf der Oberfläche der Probe sichtbare Rissstruktur gibt über Parameter wie die Gesamtrisslänge Auskunft über die Erstarrungsrissbeständigkeit der verwendeten Kombination aus Grundstoff, Schweißzusatz und Schweißparametern. Jedoch kann eine Auswertung unter dem Mikroskop sehr aufwendig sein und je nach Beobachter unterschiedliche Ergebnisse liefern. Mit Hilfe von CNNs wird die Auswertung der Risse automatisiert was Genauigkeit, Geschwindigkeit und Vergleichbarkeit verbessert. T2 - BMDK CY - Magdeburg, Germany DA - 05.12.2022 KW - CNN KW - MVT KW - KI PY - 2022 AN - OPUS4-56839 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rieck, Arielle A1 - Schwarz, Irina T1 - Electrochemical CO2 reduction (CO2RR) coupled to gas fermentation with acetogenic bacteria N2 - For the realization of a sustainable energy economy, it is of great importance to develop CO2 -neutral methods producing multi-carbon organic chemicals used as feedstock in the chemical industry as well as carbon-neutral fuels. A promising method to alleviate the greenhouse effect and thereby forming value-added chemicals or syngas as an energy carrier, is through the electrochemical CO2 reduction reaction (CO2RR). In this work, a bioelectrotechnological approach is developed, in which the CO2RR reaction products (CO and H2) are directly fed to bacteria (acetogens), who use them as “reduction equivalents” to further metabolize CO2 to valuable carbon compounds. Therefore, a bio-electrochemical system consisting of a bioreactor coupled to a CO2 electrolysis cell will be established. Currently, scarce catalysts such as Ag and Au are used as for the CO2RR which may hamper the use of decentral CO2 conversion technology for cost reasons. The technological viability of the bacteria-assisted electrolysis depends on the usage of efficient, biocompatible, and selective electrocatalysts prepared from inexpensive precursors. Porous transition metal and nitrogen co-doped carbons (M-N-Cs) have emerged as precious-metal free electrocatalysts for the direct electrochemical reduction of CO2 into CO and are excellent candidates for scale-up and deployment in technological applications. Furthermore, Co/Ni/Zn functioning as the catalytically active sites will be used, as they are expected to depict non-bactericidal properties in contrast to Cu and Ag catalysts. The non-bactericidal property could e.g., allow for application within the hybrid device (bio-electrochemical system), without the need to separate bacteria and cathode catalyst. The MNCs with the most promising electrocatalytic activity and selectivity will be evaluated in abiotic conditions in the hybrid bio-electrochemical reactor system. T2 - DFG Summer School Workshop CY - Hamburg, Germany DA - 01.09.2022 KW - Katalysator KW - CO2 Reduktion KW - Bioelectrochemical CO2 reduction PY - 2022 AN - OPUS4-56618 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rieck, Arielle A1 - Schwarz, Irina T1 - Valorization of CO2 by electrocatalytic reduction coupled to acetogens via multiple electron carriers (Ecat-acetogens) N2 - For the realization of a sustainable energy economy, it is of great importance to develop CO2 -neutral methods producing multi-carbon organic chemicals used as feedstock in the chemical industry as well as carbon-neutral fuels. A promising method to alleviate the greenhouse effect and thereby forming value-added chemicals or syngas as an energy carrier, is through the electrochemical CO2 reduction reaction (CO2RR). In this work, a bioelectrotechnological approach is developed, in which the CO2RR reaction products (CO and H2) are directly fed to bacteria (acetogens), who use them as “reduction equivalents” to further metabolize CO2 to valuable carbon compounds. Therefore, a bio-electrochemical system consisting of a bioreactor coupled to a CO2 electrolysis cell will be established. Currently, scarce catalysts such as Ag and Au are used as for the CO2RR which may hamper the use of decentral CO2 conversion technology for cost reasons. The technological viability of the bacteria-assisted electrolysis depends on the usage of efficient, biocompatible, and selective electrocatalysts prepared from inexpensive precursors. Porous transition metal and nitrogen co-doped carbons (M-N-Cs) have emerged as precious-metal free electrocatalysts for the direct electrochemical reduction of CO2 into CO and are excellent candidates for scale-up and deployment in technological applications. Furthermore, Co/Ni/Zn functioning as the catalytically active sites will be used, as they are expected to depict non-bactericidal properties in contrast to Cu and Ag catalysts. The non-bactericidal property could e.g., allow for application within the hybrid device (bio-electrochemical system), without the need to separate bacteria and cathode catalyst. The MNCs with the most promising electrocatalytic activity and selectivity will be evaluated in abiotic conditions in the hybrid bio-electrochemical reactor system. T2 - DFG Summer School Workshop CY - Hamburg, Germany DA - 01.09.2022 KW - CO2 Reduktion KW - MNC catalyst KW - Clostridium ragsdalei PY - 2022 AN - OPUS4-56619 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kolmangadi, Paulina T1 - Molecular dynamics of nanophase-separated Janus polynorbornenes by neutron scattering, dielectric spectroscopy, and fast scanning calorimetry N2 - The structure and molecular dynamics of a homologous series of Janus polytricyclononenes (PTCN) with rigid backbones and flexible n-alkyl (n = propyl, butyl, hexyl, octyl) side groups were studied. These polymers are novel, innovative materials that show potential in separating hydrocarbons. Janus PTCNs were designed to show an enhanced and controllable gas permeability via flexible alkyl side chains that promote mass transport, as opposed to conventional microporous polymers, where permeability is a function of the free-volume entities. The materials, studied by small angle X-ray scattering (SAXS), show nanophase separation between the n-alkyl side chains and the backbones. The size of the nanodomains increases with the length of the n-alkyl side groups. In addition, for the alkyl chain-rich nanodomains a distinct α-relaxation (dynamic glass transition) was found by means of broadband dielectric spectroscopy (BDS) and temperature modulated DSC (TMDSC). The glass transition of the backbone-rich domains, which is beyond or near to the degradation of the materials, was evidenced by fast scanning calorimetry (FSC) by decoupling it from decomposition by employing high heating rates up to 104 K/s. Janus PTCNs were studied by quasielastic neutron scattering employing the backscattering instrument IN16B. For an overview of dynamic processes setting in at different temperatures inelastic (IFWS) and elastic fixed window scans (EFWS) were conducted. IFWS showed that the segmental motions of alkyl-rich nanodomains shift to higher temperatures with increasing alkyl chain length, which agrees with SAXS and BDS findings. For the lowest side chain lengths an additional low temperature relaxation process was found, assigned to methyl group rotations. T2 - QENS / WINS 2022 CY - San Sebastian, Spain DA - 23.05.2022 KW - Gas separation KW - Membranes PY - 2022 AN - OPUS4-55898 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Szymoniak, Paulina T1 - Molecular Dynamics of nNanophase-Separated Janus Polynorbornenes for gas separation N2 - Janus polytricyclononenes (PTCN) with rigid backbones and flexible n-alkyl (n = propyl, butyl, hexyl, octyl, decyl) are novel, innovative materials that show potential in separating hydrocarbons. These superglassy polymers were designed to show an enhanced and controllable gas permeability via flexible alkyl side chains that promote mass transport, as opposed to conventional microporous polymers, where permeability is a function of the free-volume entities. PTCNs, investigated by small angle X-ray scattering (SAXS), show nanophase separation between the n-alkyl side chains and the backbones. The size of the nanodomains increases with the length of the n-alkyl side groups. In addition, for the alkyl chain-rich nanodomains a distinct α-relaxation was found by means of broadband dielectric spectroscopy (BDS) and temperature modulated DSC (TMDSC). The glass transition of the backbone-rich domains, which is beyond or near to the degradation of the materials, was evidenced by fast scanning calorimetry (FSC) by decoupling it from decomposition, employing high heating rates up to 104 K/s. Further, Janus PTCNs were studied by quasielastic neutron scattering (QENS) employing the backscattering IN16B (ILL, Grenoble) and time of flight FOCUS (PSI, Villigen) instruments. For an overview of dynamic processes setting in at different temperatures inelastic (IFWS) and elastic fixed window scans (EFWS) were conducted. IFWS showed that the segmental motions of alkyl-rich nanodomains shift to higher temperatures with increasing alkyl chain length, which agrees with SAXS and BDS findings. For the lowest side chain lengths an additional low temperature relaxation process was found, assigned to methyl group rotations. T2 - IDS 2022 CY - San Sebastian, Spain DA - 03.09.2022 KW - Gas separation KW - Membranes PY - 2022 AN - OPUS4-55899 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zencker, Uwe T1 - EURAD WP 8 Task 3 Overview: Behaviour of nuclear fuel and cladding after discharge N2 - Task 3 of Work package 8 (Spent Fuel Characterization) of the European Joint Programme on Radioactive Waste Management (EURAD) investigates the behaviour of nuclear fuel and cladding after discharge. The aim of the work is to understand and describe the behaviour of spent nuclear fuel (SNF), irradiated cladding, fuel/cladding chemical interaction (FCCI) and ageing under conditions of extended interim storage, transportation and emplacement in a final disposal system. BAM contributes to the project as partner and leads Task 3. The presentation gives an overview of the project status, main achievements in experimental work and modelling studies, deviations from the plan, delays and challenges ahead. T2 - EURAD Work Package 8 (SFC) Annual Meeting CY - Kalmar, Sweden DA - 19.09.2022 KW - Nuclear fuel KW - Cladding KW - Discharge PY - 2022 AN - OPUS4-56120 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zencker, Uwe T1 - EURAD WP 8 (SFC) Task 3 - Update: Behaviour of nuclear fuel and cladding after discharge N2 - The European Joint Programme on Radioactive Waste Management (EURAD) is working on Spent Fuel Characterization (SFC) in its work package (WP) 8. Inspired by the EURAD activities, the International Atomic Energy Agency (IAEA) established an international Coordinated Research Project (CRP) on SFC. The EURAD WP SFC participants are collaborating as a team on the IAEA CRP on SFC. The EURAD WP SFC project consists of four tasks. Task 3 investigates the behaviour of nuclear fuel and cladding after discharge. The aim of these activities is to understand and describe the evolution of the cladding-pellet system and its ageing under conditions of extended interim storage, transportation and emplacement in a final disposal system. At the Second Research Coordination Meeting on Spent Fuel Characterization, BAM as leader of Task 3 reported on the status of the research work. T2 - IAEA 2nd Research Coordination Meeting of the Coordinated Research Project on Spent Fuel Characterization CY - Kalmar, Sweden DA - 20.09.2022 KW - Nuclear fuel KW - Cladding KW - Discharge PY - 2022 AN - OPUS4-56121 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rolle, Annette A1 - Wille, Frank ED - Czarwinski, R. T1 - Radioaktive Stoffe in besonderer Form-wichtige Aspekte im Zulassungsverfahren N2 - Für die Beförderung von umschlossenen radioaktiven Stoffen (Strahler) können Transporterleichterungen gelten, wenn das Strahlerdesign nachweislich unfallsicher ausgelegt ist und eine Zulassung als radioaktiver Stoff in besonderer Form vorliegt. Die in Deutschland zuständige Behörde für die Prüfung und Zulassung radioaktiver Stoffe in besonderer Form ist die Bundesanstalt für Materialforschung und –prüfung (BAM). Eine oft langfristige Nutzung der Strahler kann eine alterungsbedingte Schwächung der Umschließung des radioaktiven Stoffes zur Folge haben. Jeder Strahler einer zugelassenen Bauart muss jedoch im Beförderungsfall zu jeder Zeit, auch nach längerer Nutzung, den vorgeschriebenen Prüfanforderungen genügen. Die Alterungsbewertung auf der Grundlage einer vom Antragsteller zu spezifizierenden Nutzungsdauer des radioaktiven Stoffes in besonderer Form ist seit langer Zeit Bestandteil des Zulassungsverfahrens in Deutschland. Ein von Deutschland eingebrachter Vorschlag im Rahmen der anstehenden Revision der IAEA Empfehlungen für die sichere Beförderung von radioaktiven Stoffen (SSR-6) soll die Lesbarkeit des Regelwerkes bezüglich der Alterungsbewertung verbessern, Klarheit über die damit verbundenen Anforderungen erzeugen und damit zu einer Harmonisierung der Zulassungsverfahren auf internationaler Ebene beitragen. In diesem Beitrag sollen wichtige Einflussfaktoren auf das Alterungsverhalten von radioaktiven Stoffen in besonderer Form aufgezeigt und die Notwendigkeit für die Spezifikation einer Nutzungsdauer als Grundlage für die Alterungsbewertung begründet werden. Der deutsche Vorschlag für die Revision des IAEA Regelwerks zum sicheren Transport radioaktiver Stoffe (SSR-6) wird vorgestellt und erläutert. T2 - Jahrestagung des FS 2022 CY - Konstanz, Germany DA - 26.09.2022 KW - Strahlenschutz KW - Radioaktive Stoffe KW - Beförderung KW - Zulassung PY - 2022 SN - 1013-4506 SP - 15 EP - 20 PB - Fachverband für Strahlenschutz e.V. CY - Berlin AN - OPUS4-56134 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rolle, Annette T1 - Radioaktive Stoffe in besonderer Form - wichtige Aspekte im Zulassungsverfahren N2 - Für die Beförderung von umschlossenen radioaktiven Stoffen (Strahler) können Transporterleichterungen gelten, wenn das Strahlerdesign nachweislich unfallsicher ausgelegt ist und eine Zulassung als radioaktiver Stoff in besonderer Form vorliegt. Die in Deutschland zuständige Behörde für die Prüfung und Zulassung radioaktiver Stoffe in besonderer Form ist die Bundesanstalt für Materialforschung und –prüfung (BAM). Eine oft langfristige Nutzung der Strahler kann eine alterungsbedingte Schwächung der Umschließung des radioaktiven Stoffes zur Folge haben. Jeder Strahler einer zugelassenen Bauart muss jedoch im Beförderungsfall zu jeder Zeit, auch nach längerer Nutzung, den vorgeschriebenen Prüfanforderungen genügen. Die Alterungsbewertung auf der Grundlage einer vom Antragsteller zu spezifizierenden Nutzungsdauer des radioaktiven Stoffes in besonderer Form ist seit langer Zeit Bestandteil des Zulassungsverfahrens in Deutschland. Ein von Deutschland eingebrachter Vorschlag im Rahmen der anstehenden Revision der IAEA Empfehlungen für die sichere Beförderung von radioaktiven Stoffen (SSR-6) soll die Lesbarkeit des Regelwerkes bezüglich der Alterungsbewertung verbessern, Klarheit über die damit verbundenen Anforderungen erzeugen und damit zu einer Harmonisierung der Zulassungsverfahren auf internationaler Ebene beitragen. In diesem Beitrag sollen wichtige Einflussfaktoren auf das Alterungsverhalten von radioaktiven Stoffen in besonderer Form aufgezeigt und die Notwendigkeit für die Spezifikation einer Nutzungsdauer als Grundlage für die Alterungsbewertung begründet werden. Der deutsche Vorschlag für die Revision des IAEA Regelwerks zum sicheren Transport radioaktiver Stoffe (SSR-6) wird vorgestellt und erläutert. T2 - Jahrestagung des FS 2022 CY - Konstanz, Germany DA - 26.09.2022 KW - Strahlenschutz KW - Radioaktive Stoffe KW - Beförderung KW - Alterung KW - Zulassung PY - 2022 AN - OPUS4-56137 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rolle, Annette T1 - Safety assessment of aged metal seals N2 - With our experiments we want to simulate a load situation which can result from a cask vertical drop test. The lid can lift a little for a very short moment and that can perhaps result in a little movement of the seal, a little rotation or a little lateral movement, so that the contact section can change. The aim of the project is to learn more about the sealing efficiency after the seal is compressed again. What we know from former component tests with non-aged seals is, that the leakage rate measured after one or more decompression /compression cycles with seal movement becomes significant higher. And this result is considered for specification of design leakage rates for release calculation in safety cases. In the recent years we all have learned more about the significant influence of temperature and time on seal behavior and so the plan was to do similar experiments with aged seals, just to get an idea about seal behavior and achievable leakage rates. What we did in detail is: We compressed Helicoflex-seals of both design types, with Aluminum and Silver outer jackets, in testflanges and aged them in an oven at a temperature of 125°C for 3 months to produce seal properties comparable with properties after several years use at more typical operating temperatures between 90 and 100°C. After this ageing procedure we opened the flanges completely, moved the seal a little to vary the contact area and compressed the flanges again. What we measured during all compression and decompression cycles was the load, the deformation and -as long as possible- the leakage rates. T2 - Workshop IRSN/BAM CY - Cadarache, France DA - 12.10.2022 KW - Transport KW - Radioactive KW - Seal behavior KW - Ageing PY - 2022 AN - OPUS4-56141 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Hahn, S.-K. A1 - Tschirschwitz, Rico A1 - Bernardy, Christopher T1 - Forschung zur Sicherheit stationärer Energiespeicher - Zwischenspeicher als wichtiger Beitrag für eine erfolgreiche Energiewende N2 - Der Artikel stellt das BMBF-Vorhaben SEE-2L dar. Der Schwerpunkt liegt dabei auf dem Beitrag des Vorhabens für die Sicherheit von stationären Energiespeichern. Darüber hinaus wird aufgezeigt, welche Versuche bisher durchgeführt wurden und mit welchen Ergebnissen bis Projektende zu rechnen ist. KW - Stationäre Energiespeicher KW - Elektrische Energiespeicher KW - Auswirkungsbetrachtungen KW - Batterie KW - Thermal runaways PY - 2022 UR - https://www.behoerden-spiegel.de/e-mobility-magazin-2022/ SN - 1437-8337 VL - 2022 IS - Sonderheft E-Mobility Magazin 2022 SP - 23 EP - 24 PB - ProPress CY - Bonn AN - OPUS4-56401 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Niederleithinger, Ernst T1 - PREDIS The pre-disposal management of radioactive waste N2 - This presentation summarizes the opbjectives and the progress of the EURATOM project PREDIS (pre-disposal management of radioactive waste) and its workpackage 7 in particular. Focus is on the development of wireless sensors for monitoring radioactive waste packages, measuring radiation, temperature, pressure and humidity. T2 - DigiDecom 2022 CY - Halden, Norway DA - 18.10.2022 KW - Radioactive waste KW - Monitoring KW - Wireless KW - RFID PY - 2022 AN - OPUS4-56321 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bonse, Jörn T1 - Surface nanotexturing by ultrashort laser pulses N2 - The presentation reviews the BAM activities in the field of surface processing by ultrashort laser pulses. A focus is laid on the generation of laser-induced periodic surface structures (LIPSS) which allow various surface functionalizations for applications in optics, tribology, liquid management, and medicine. T2 - Photonics Days Berlin Brandenburg 2022 CY - Berlin, Germany DA - 05.10.2022 KW - Laser-induced periodic surface structures (LIPSS) KW - Femtosecond laser KW - Surface functionalization PY - 2022 AN - OPUS4-55921 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tschirschwitz, Rico T1 - Projekttreffen BMBF-Vorhaben SEE-2L, Teilvorhaben BAM: Aufbau eines Großversuchsstandes N2 - Der Vortrag stellt den aktuellen Bearbeitungsstand des Teilvorhabens an der BAM dar. Der Schwerpunkt liegt dabei auf der ersten Versuchsserie mit Batteriezellen und -modulen bis zu 6.8 kWh. Aus diesen Versuche werden die wesentlichen Ergebnisse gezeigt, insbesondere die Teperatur-, Spannungs, Gas- und Gewichtsmessung beim thermischen Durchgehen. T2 - Projekttreffen zum BMBF-Vorhaben SEE-2L (Sicherheit elektrochemischer Energiespeicher in Second Life Anwendungen) CY - BAM TTS, Baruth/Mark - Horstwalde, Germany DA - 08.11.2022 KW - Stationäre Energiespeicher KW - Elektrische Energiespeicher KW - Auswirkungsbetrachtungen KW - EES PY - 2022 AN - OPUS4-56212 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Zencker, Uwe A1 - Simbruner, Kai A1 - Völzke, Holger T1 - Entwicklung eines bruchmechanischen Berechnungsansatzes zur Beschreibung des Festigkeitsverhaltens von Brennstabhüllrohren bei längerfristiger Zwischenlagerung (BRUZL) N2 - Es werden Methoden zur sicherheitstechnischen Bewertung des mechanischen Verhaltens von Brennstabhüllrohren entwickelt, um sprödes Versagen in Belastungsszenarien nach längerfristiger trockener Zwischenlagerung zu verhindern. Unbestrahlte Brennstabhüllrohrsegmente aus der Zirkoniumlegierung ZIRLO® wurden hydriert und thermomechanischen Behandlungen unterzogen, um Hüllrohrmaterial durch Ausscheidung radialer Hydride zu verspröden. Die Proben mit radialen Hydriden wurden im Ring Compression Test (RCT) bei Raumtemperatur untersucht. Bereits bei kleinen Probenverformungen wurden abrupte Kraftabfälle mit instabiler Rissausbreitung durch das Netzwerk radialer Hydride beobachtet. Die Risslängen erreichten in einigen Fällen bis zu 90 % der Wanddicke. Der mikromechanische Versagensmechanismus ist Quasi-Spaltbruch in den Hydriden und Porenbildung, -wachstum und -vereinigung in der Zirkoniummatrix an den duktilen Brücken zwischen benachbarten Hydriden. Es wurde ein Finite-Elemente-Modell des Ring Compression Tests erstellt, um das Versagensverhalten zirkoniumbasierter Legierungen mit radialen Hydriden im RCT zu analysieren. Die Fließkurve für das elastisch-plastische Materialmodell des Matrixmaterials wurde durch eine inverse Finite-Elemente-Analyse ermittelt. Kohäsivzonenmodelle wurden benutzt, um die plötzlichen Kraftabfälle zu reproduzieren. Es wurde ein mikromechanisches Modell mit statistisch generierten Matrix-Hydrid-Verteilungen entwickelt, das zwischen sprödem Versagen entlang der Hydride und duktilem Versagen der Zirkoniummatrix in der Kohäsivzone unterscheidet. Für das jeweilige Materialverhalten wird ein lokales zweiparametriges Versagenskriterium auf Grundlage der Kohäsionsfestigkeit und der Separationsenergie bei einer festgelegten Form des Kohäsivgesetzes vorgeschlagen. Geeignete Kohäsivparameter lassen sich mit einer inversen Finite-Elemente-Analyse des Versagensverhaltens von hydrierten Proben im Ring Compression Test bestimmen. In den Simulationen lag der Schwerpunkt auf dem ersten Kraftabfall. Die Berechnungsergebnisse stimmen gut mit den RCT-Ergebnissen überein. Es konnte gezeigt werden, dass die Rissinitiierung und -ausbreitung stark von der speziellen Anordnung der radialen Hydride und Matrixbrücken in der Bruchzone abhängt. Die numerische Modellbildung wurde an Versuchen mit bestrahlten Proben aus der Zirkoniumlegierung M5® validiert. KW - Zwischenlagerung KW - Brennstabhüllrohr KW - Versagensmechanismus KW - Kohäsivzonenmodell KW - Ring Compression Test PY - 2022 SP - 1 EP - 106 PB - Bundesanstalt für Materialforschung und -prüfung (BAM) CY - Berlin AN - OPUS4-56853 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Xie, Yongliang A1 - Lv, Na A1 - Huang, Yan A1 - Wu, Dejian A1 - Gong, Liang A1 - Yang, Xufeng A1 - Zeng, Yikai T1 - Comparative analysis on temperature characteristics of hydrogen-powered and traditional fossil-fueled vehicle fires in the tunnel under longitudinal ventilations N2 - Vehicle fires in the tunnel are a great threat to the safe operation of the tunnel. Due to the rapid development of the hydrogen economy, the fire due to the hydrogen leakage could not be avoided and may bring great damage to the passengers and infrastructure. Due to the large difference between pool fires of traditional fossil-fueled and jet fires of hydrogen-powered vehicles, it is in doubt whether the existing longitudinal ventilation design could still be effective for the safety issue of hydrogen powered vehicles. To solve this problem, it is necessary to compare temperature characteristics of hydrogen-powered and traditional vehicle fires with and without longitudinal ventilations. In present work, we conducted a numerical investigation to discuss the different temperature distributions of traditional and hydrogen-fueled vehicle fires. Results indicate that the high temperature zone of the pool fire only exists above the ceiling of the vehicle. For hydrogen-powered vehicle fire, the high-speed hydrogen jet with the strong inertial force could push the hot smoke flows back to the ground. The ceiling temperature of hydrogen-powered vehicle fire is larger since hydrogen-powered vehicle has a larger heat release rate and the fire hazard of jet fires bring more danger compared with the pool fire. Although the temperature stratification is also obvious for the hydrogen-powered vehicle fire, the air temperature in the lower region could be heated and still high enough to bring a great damage to the passengers’ lives. This is quite different with the traditional pool fire. In addition, the critical ventilation velocity is also discussed. The theoretical equation could well predict the critical ventilation velocity of traditional vehicle fires. For hydrogen-powered vehicle fires, the critical ventilation velocity could reach up to 6 m/s. The theoretical equation could not well predict the critical ventilation velocity of hydrogen-powered vehicle fires due to exist of hydrogen jet fires. KW - Hydrogen fire KW - Tunnel KW - Longitudinal ventilation KW - Comparative study PY - 2022 DO - https://doi.org/10.1016/j.ijhydene.2022.05.203 SN - 0360-3199 VL - 47 IS - 57 SP - 24107 EP - 24118 PB - Elsevier CY - Oxford AN - OPUS4-62839 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bonse, Jörn T1 - Laser-induced Periodic Surface Structures - Mechanisms, Applications, and unsolved Problems N2 - Laser-induced Periodic Surface Structures (LIPSS, ripples) are a universal phenomenon and can be generated in a contactless, single-step process on almost any type of solid upon irradiation with intense laser pulses. They represent a (quasi-)periodic modulation of the surface topography in the form of a linear grating and are typically formed in a “self-ordered” way in the focus of a laser beam. Thus, they are often accompanying laser material processing applications. The structural sizes of LIPSS typically range from several micrometers down to less than 100 nanometers – far beyond the optical diffraction limit – while their orientations exhibit a clear correlation with the local polarization direction of the laser radiation. From a theoretical point of view, a controversial debate has emerged during the last decades, whether LIPSS originate from electromagnetic effects (seeded already during the laser irradiation) – or whether they emerge from matter-reorganization processes (distinctly after the laser irradiation). From a practical point of view, however, LIPSS represent a simple and robust way for the nanostructuring of solids that allows creating a wide range of different surface functionalities featuring applications in optics, tribology, medicine, energy technologies, etc. While the currently available laser and scanner technology already allows surface processing rates at the m^2/min level, industrial applications of LIPSS are sometimes limited by the complex interplay between the nanoscale surface topography and the specific surface chemistry. This typically manifests in difficulties to control the processing of LIPSS and in limitations to ensure the long-term stability of the created surface functions. This presentation reviews the currently existent theories of LIPSS. A focus is laid on the historic development of the fundamental ideas behind the LIPSS, their corresponding mathematical descriptions and numerical implementations, along with a comparison and critical assessment of the different approaches. Moreover, some unsolved scientific problems related to LIPSS are identified and the pending technological limitations are discussed. Hereby, it is intended to stimulate further research and developments in the field of LIPSS for overcoming these limitations and for supporting the transfer of the LIPSS technology into industry. T2 - SPIG 2022 - 31st Summer School and International Symposium on the Physics of Ionized Gases CY - Belgrade, Serbia DA - 05.09.2022 KW - Laser-induced periodic surface structures (LIPSS) KW - Surface functionalization KW - Femtosecond laser processing PY - 2022 AN - OPUS4-55813 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Florian, Camilo T1 - Influence of oxidation in the formation and performance of laser-induced periodic surface structures N2 - The fabrication of laser-induced periodic surface structures (LIPSS) has been reported for metallic, semiconductor and dielectric materials when irradiated with linearly polarized ultrashort laser pulses. Different sets of processing parameters have been identified and extensively studied, allowing the use of LIPSS for applications in medicine, tribology and surface wetting to name a few. One important parameter that is often not considered is the laser-induced oxidation that is produced especially when oxidation prone materials are irradiated in air environment. This surface oxidation can potentially influence the final structures size, shape and orientation and modify their functionality in some specific applications. In this work, we first study the influence of the laser-induced oxidation layer on the formation of LIPSS by characterizing the response of the oxidation prone hard-coating material chromium nitride. Moreover, we employ complementary surface and depth-profiling analytic techniques to reveal morphological, chemical and structural features of different types of surface structures and LIPSS produced on titanium-based substrates. Finite-difference time-domain (FDTD) calculations finally explain how this superficial oxidation layer promotes the formation of a new type of low spatial frequency LIPSS. Also, we measure the depth-extent of the different oxides formed and demonstrate its beneficial influence for friction reduction and wear resistance applications. T2 - SPIE Photonics West Conference, Symposium "Laser-Based Micro- and Nano-Processing XVI" CY - San Francisco, CA, USA DA - 22.01.2022 KW - Laser-induced periodic surface structures (LIPSS) KW - Oxidation KW - Femtosecond laser KW - Laser processing KW - Finite-difference time-domain calculations (FDTD) PY - 2022 AN - OPUS4-54322 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR T1 - Amts- und Mitteilungsblatt, Band 52, Heft 2 T3 - Amts- und Mitteilungsblatt der BAM - 2/2022 KW - Festlegungen KW - Zulassungen KW - Richtlinien KW - Anerkennungen PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-550917 SN - 0340-7551 VL - 52 IS - 2 SP - 55 EP - 158 PB - Bundesanstalt für Materialforschung und -prüfung (BAM) CY - Berlin AN - OPUS4-55091 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Porta-Velilla, L. A1 - Turan, N. A1 - Cubero, Á. A1 - Shao, W. A1 - Li, H. A1 - de la Fuente, G.F. A1 - Martínez, E. A1 - Larrea, Á. A1 - Castro, M. A1 - Koralay, H. A1 - Çavdar, Ş. A1 - Bonse, Jörn A1 - Angurel, L.A. T1 - Highly Regular Hexagonally-Arranged Nanostructures on Ni-W Alloy Tapes upon Irradiation with Ultrashort UV Laser Pulses N2 - Nickel tungsten alloy tapes (Ni—5 at% W, 10 mm wide, 80 µm thick, biaxially textured) used in second-generation high temperature superconductor (2G-HTS) technology were laser-processed in air with ultraviolet ps-laser pulses (355 nm wavelength, 300 ps pulse duration, 250–800 kHz pulse repetition frequency). By employing optimized surface scan-processing strategies, various laser-generated periodic surface structures were generated on the tapes. Particularly, distinct surface microstructures and nanostructures were formed. These included sub-wavelength-sized highly-regular hexagonally-arranged nano-protrusions, wavelength-sized line-grating-like laser-induced periodic surface structures (LIPSS, ripples), and larger irregular pyramidal microstructures. The induced surface morphology was characterized in depth by electron-based techniques, including scanning electron microscopy (SEM), electron back scatter diffraction (EBSD), cross-sectional transmission electron microscopy (STEM/TEM) and energy dispersive X-ray spectrometry (EDS). The in-depth EBSD crystallographic analyses indicated a significant impact of the material initial grain orientation on the type of surface nanostructure and microstructure formed upon laser irradiation. Special emphasis was laid on high-resolution material analysis of the hexagonally-arranged nano-protrusions. Their formation mechanism is discussed on the basis of the interplay between electromagnetic scattering effects followed by hydrodynamic matter re-organization after the laser exposure. The temperature stability of the hexagonally-arranged nano-protrusion was explored in post-irradiation thermal annealing experiments, in order to qualify their suitability in 2G-HTS fabrication technology with initial steps deposition temperatures in the range of 773–873 K. KW - Laser-induced periodic surface structures (LIPSS) KW - Ultrashort laser processing KW - Hexagonally-arranged nano-protrusions KW - Second-generation high temperature superconductor technology KW - Electron microscopy PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-552551 DO - https://doi.org/10.3390/nano12142380 SN - 2079-4991 VL - 12 IS - 14 SP - 1 EP - 23 PB - MDPI CY - Basel, Switzerland AN - OPUS4-55255 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Qiao, Linan A1 - Nagelschmidt, Sven A1 - Herbrich, Uwe A1 - Keller, Christian T1 - Introduction of a Power Law Time-Temperature Equivalent Formulation for the Description of Thermorheologically Simple and Complex Behavior N2 - Abstract: In this work, a conceptual framework is suggested for analyzing thermorheologically simple and complex behavior by using just one approach. Therefore, the linear relation between master time and real time which is required in terms of the time-temperature superposition principle was enhanced to a nonlinear equivalent relation. Furthermore, we evaluate whether there is any relation among well-known existing time-temperature equivalent formulations which makes it possible to generalize different existing formulations. For this purpose, as an example, the power law formulation was used for the definition of the master time. The method introduced here also contributes a further framework for a unification of established time-temperature equivalent formulations, for example the time-temperature superposition principle and time-temperature parameter models. Results show, with additional normalization conditions, most of the developed time-temperature parameter models can be treated as special cases of the new formulation. In the aspect of the arrow of time, the new defined master time is a bended arrow of time, which can help to understand the corresponding physical meaning of the suggested method. KW - bended arrow of time KW - time-temperature superposition principle KW - time-temperature equivalent formulation PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-543800 DO - https://doi.org/10.3390/ma15030726 VL - 15 IS - 3 SP - 1 EP - 11 PB - MDPI AN - OPUS4-54380 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Lifka, S. A1 - Harsányi, K. A1 - Baumgartner, E. A1 - Pichler, L. A1 - Baiko, D. A1 - Wasmuth, Karsten A1 - Heitz, J. A1 - Meyer, M. A1 - Joel, A.-C. A1 - Bonse, Jörn A1 - Baumgartner, W. ED - Mail, M. T1 - Laser-processed antiadhesive bionic combs for handling nanofibers inspired by nanostructures on the legs of cribellate spiders N2 - Nanofibers are drawing the attention of engineers and scientists because their large surface-to-volume ratio is favorable for applications in medicine, filter technology, textile industry, lithium-air batteries, and optical sensors. However, when transferring nanofibers to a technical product in the form of a random network of fibers, referred to as nonwoven fabric, the stickiness of the freshly produced and thus fragile nanofiber nonwoven remains a problem. This is mainly because nanofibers strongly adhere to any surface because of van der Waals forces. In nature, there are animals that are actually able to efficiently produce, process, and handle nanofibers, namely cribellate spiders. For that, the spiders use the calamistrum, a comb-like structure of modified setae on the metatarsus of the hindmost (fourth) legs, to which the 10–30 nm thick silk nanofibers do not stick due to a special fingerprint-like surface nanostructure. In this work, we present a theoretical model of the interaction of linear nanofibers with a sinusoidally corrugated surface. This model allows for a prediction of the adhesive interaction and, thus, the design of a suitable surface structure to prevent sticking of an artificially nonwoven of nanofibers. According to the theoretical prediction, a technical analogon of the nanoripples was produced by ultrashort pulse laser processing on different technically relevant metal surfaces in the form of so-called laser-induced periodic surface structures (LIPSS). Subsequently, by means of a newly established peel-off test, the adhesion of an electrospun polyamide fiber-based nonwoven was quantified on such LIPSS-covered aluminium alloy, steel, and titanium alloy samples, as well as on polished (flat) control samples as reference and, additionally, on samples with randomly rough surfaces. The latter revealed that the adhesion of electrospun nanofiber nonwoven is significantly lowered on the nanostructured surfaces compared with the polished surfaces. KW - Laser-induced periodic surface structures (LIPSS) KW - Cribellate spiders KW - Calamistrum KW - Electrospinning KW - Nanofibers PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-561799 DO - https://doi.org/10.3762/bjnano.13.105 SN - 2190-4286 VL - 13 SP - 1268 EP - 1283 PB - Beilstein-Institut zur Förderung der Chemischen Wissenschaften CY - Frankfurt, M. AN - OPUS4-56179 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - THES A1 - Nielow, Dustin T1 - Einfluss fertigungsbedingter Imperfektionen auf die Schwingfestigkeit von FKV-Schalenstrukturen in Sandwichbauweise N2 - Rotorblätter von Windenergieanlagen (WEA) weisen häufig nach wenigen Jahren, lange vor dem Erreichen der prognostizierten Lebensdauer von 20 bis 30 Jahren Risse in der Blattschale auf. Die Folge sind aufwendige Reparaturen am installierten und schwer zugänglichen Rotorblatt und der kostenintensive Nutzungsausfall durch den Stillstand der WEA. Als mögliche Initiatoren für die Schäden in der Blattschale der Rotorblätter gelten fertigungsbedingte Imperfektionen. Für die Untersuchung des Einflusses dieser Imperfektionen auf das Ermüdungsverhalten der Rotorblätter wurde an der BAM (Bundesanstalt für Mate-rialforschung und -prüfung) ein Prüfstand für statische und zyklische Versuche von Schalensegmenten im intermediate scale entwickelt und betrieben. Die untersuchten Schalensegmente in Sandwichbauweise sind der Rotorblattschale von WEA im Hinblick auf die Strukturmechanik, die eingesetzten Halbzeuge, den Laminataufbau und dem eingesetzten Fertigungsverfahren ähnlich. Als Imperfektionen wurden verschiedenen Variationen von Lagenstößen in die Hautlagen und Schaumstöße mit Breitenvariation in den Stützkern reproduzierbar eingebracht. Die Überwachung des Schädigungszustandes während der Schwingversuche unter realistischen Lastszenarien erfolgt über eine kombinierte in situ Schädigungsüberwachung mittels passiver Thermografie und Felddehnungsmessung. Mit den durchgeführten Schwingversuchen und der begleitenden Überwachung des Schädigungszustandes ließen sich die Schadensinitiation und die signifikante Herabsetzung der Lebensdauer durch die eingebrachten Imperfektionen zweifelsfrei nachweisen und entsprechende Konstruktionshinweise für die betriebssichere Auslegung von Sandwichstrukturen ableiten. N2 - Wind turbines often exhibit cracks in the blade shells after only a few years in service, significantly before their expected 20 to 30 year design lifespan. This leads to complicated repairs on difficult to reach rotor blades, and can cause a cost-intensive standstill of the turbine. A possible source of these defects in the rotor blade shells are the imperfections which occur during production. In order to investigate the effect of these imperfections on the fatigue behavior of rotor blades, a test rig was developed at the BAM (Bundesanstalt für Materialforschung und -prüfung) upon which intermediate scale static and cyclic-fatigue testing could be performed. The complementary sandwich shell specimens developed and investigated with the test rig are representative of the outer shell of wind turbine rotor blades in terms of materials and manufacturing processes, as well as structural mechanics. The specimens were built with reproducible imperfections, including laminate overlaps in the face sheets and gaps of varying size in the foam core. The damage condition was monitored during cyclic-fatigue testing under realistic load cases using a combination of in-situ passive thermography and strain field measurement. The cyclic testing and parallel non-destructive structural health monitoring of the shell specimens showed the imperfections to significantly influence the damage initiation and decrease the component service life. The results can be used accordingly as recommendations for operationally more reliable design of sandwich structures. T3 - BAM Dissertationsreihe - 170 KW - Erneuerbare Energien KW - Windenergie KW - Verbundwerkstoffe KW - Betriebsfestigkeit KW - Komponentenprüfung KW - Renewable ernergy KW - Wind energy KW - Intermediate scale KW - Composites KW - Fatigue PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-546701 SN - 1613-4249 VL - 170 SP - 1 EP - 178 PB - Bundesanstalt für Materialforschung und -prüfung (BAM) CY - Berlin AN - OPUS4-54670 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Baeßler, Matthias A1 - Herrmann, Ralf A1 - Hille, Falk A1 - Wille, Frank T1 - Dynamisches Verhalten und Überwachung des Großen Fallturms der BAM in Horstwalde N2 - Falltürme sind Bauwerke, die als Versuchsanlagen sehr speziellen, impulsartigen Belastungen ausgesetzt sind. Am Fallturm auf dem Testgelände Technische Sicherheit (TTS) der BAM wurde bei Routineinspektionen eine Abnahme der strukturellen Integrität in Form von Vorspannungsverlusten in den Bolzen der Stahlverbindungen festgestellt. Um ein Verständnis für die zugrundeliegenden Trag- und Schädigungsmechanismen zu erlangen, wurde ein umfassendes Structural Health Monitoring (SHM) System geplant und am Bauwerk installiert unter Nutzung von digitalen Bauwerksmodellen. Für die Auslegung des Überwachungssystems, insbesondere aber zur Unterstützung der Untersuchung des Schädigungsprozesses, wurden Finite-Elemente-Modelle erstellt. Um sicherzustellen, dass die FE-Modelle das reale Tragwerksverhalten mit ausreichender Genauigkeit abbilden, mussten sie jedoch in Bezug auf die gemessenen Antworten des Tragwerks kalibriert werden. Der vorliegende Beitrag beschreibt experimentelle und numerische Untersuchungen zur Identifizierung des strukturellen Systems des Stahlrohrgitterturms in Vorbereitung einer Überwachungskampagne. Die Auswertung von gemessenen Schwingungen unter ambienter Anregung ermöglichte die Identifizierung der Eigenfrequenzen mehrerer globaler Schwingungsmoden des Fallturms. Zur Modellvalidierung wurde zunächst eine Sensitivitätsanalyse durchgeführt, um die Parameter mit dem größten Einfluss zu ermitteln. Anschließend wurde ein evolutionärer Algorithmus (EA) zur Optimierung nach dem Prinzip der Minimierung der Differenzen zwischen gemessenen und simulierten charakteristischen Antworten eingesetzt. Das aktualisierte Modell wurde schließlich an der dynamischen Reaktion der Turmstruktur infolge einer realen Falltest-induzierten Stoßbelastung validiert. Die Ergebnisse zeigten eine gute Übereinstimmung zwischen numerischen und experimentellen Ergebnissen. N2 - Drop test towers are structures subjected to very specific dynamic loadings. At the drop test tower at the Test Site Technical Safety (TTS) of BAM routine inspections revealed a decline of structural integrity in form of loss of pretension in bolts of structural steel connections. To get an understanding about the underlying damage mechanisms as well as to assure the structural safety in operation, a multifaceted Structural Health Monitoring (SHM) system was planned and installed at the structure with the help of digital models. For planning the monitoring system but especially for supporting the investigation of the damaging process finite element models are deployed. Though, to ensure the capability of the FE model to reproduce the real structural behavior in sufficient accuracy, it needs to be calibrated in respect to measured responses of the structure. The present contribution describes experimental and numerical investigations to identify the structural system of the steel tube lattice tower in preparation of the monitoring campaign. An ambient vibration test allowed the identification of the natural frequencies of several global vibrational modes of the drop test tower. For model updating first a sensitivity analysis is applied to identify the most influencing parameter. In succession a genetic algorithm was applied for optimization in the sense of minimization of the difference between measured and simulated characteristic responses. The updated model is finally validated on the dynamic response of the tower structure to a real drop test induced impact loading. The results showed a good agreement between numerical and experimental results though the robustness of the simulation should be improved by more sophisticated numerical modelling. T2 - 7. VDI-Fachtagung Baudynamik CY - Würzburg, Germany DA - 27.04.2022 KW - Großer Fallturm Horstwalde KW - Structural Health Monitoring KW - Belastungsversuch KW - Modalanalyse KW - Schwingungsdynamik KW - Finite Elemente Simulation PY - 2022 SN - 978-3-18-092379-6 SN - 978-3-18-102379-2 DO - https://doi.org/10.51202/9783181023792-265 SN - 0083-5560 VL - 2379 SP - 265 EP - 284 PB - VDI-Verlag CY - Düsseldorf AN - OPUS4-55472 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eichner, Lukas A1 - Schneider, Ronald A1 - Simon, Patrick A1 - Baeßler, Matthias T1 - Optimal sensor placement for vibration-based structural health monitoring obtained via value of information analysis as part of a digital structural integrity management of offshore structures N2 - A digital structural integrity management of offshore structures enables an optimized planning of inspections and repairs with risk-based methods. In a risk-based approach, the inspection and repair strategy that minimizes the expected lifetime costs consisting of the expected inspection, repair and failure costs is determined. In addition to inspections, information on the structural condition can be continuously obtained by monitoring the vibration response of the structural system. Changes in the vibration characteristics quantified in terms of modal properties can be an indication of structural damage. In risk-based inspection and repair planning, the effect of monitoring results is determined via Bayesian updating of the structural condition and reliability. This information should be applied to inform decisions on inspections and may result in a reduced inspection effort. The benefit of continuously monitoring the structural health can be quantified in terms of the value of information, which corresponds to the difference between the expected lifetime costs with and without monitoring. In this work, we demonstrate in a numerical example how an optimized sensor placement for a vibration-based structural health monitoring system can be determined by maximizing the value of information. T2 - 3rd International Conference on Health Monitoring of Civil & Maritime Structures (HeaMES 2022) CY - Online meeting DA - 08.06.2022 KW - Structural Health Monitoring KW - Value of Information KW - Offshore Wind Energy KW - Optimal Sensor Placement KW - Bayesian System Identification PY - 2022 UR - https://www.researchgate.net/publication/362569906_Optimal_sensor_placement_for_vibration-based_structural_health_monitoring_obtained_via_value_of_information_analysis_as_part_of_a_digital_structural_integrity_management_of_offshore_structures SN - 978-1-8383226-7-0 SP - 23 EP - 32 AN - OPUS4-55465 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eichner, Lukas T1 - Optimal sensor placement for vibration-based structural health monitoring obtained via value of information analysis as part of a digital structural integrity management of offshore structures N2 - A digital structural integrity management of offshore structures enables an optimized planning of inspections and repairs with risk-based methods. In a risk-based approach, the inspection and repair strategy that minimizes the expected lifetime costs consisting of the expected inspection, repair and failure costs is determined. In addition to inspections, information on the structural condition can be continuously obtained by monitoring the vibration response of the structural system. Changes in the vibration characteristics quantified in terms of modal properties can be an indication of structural damage. In risk-based inspection and repair planning, the effect of monitoring results is determined via Bayesian updating of the structural condition and reliability. This information should be applied to inform decisions on inspections and may result in a reduced inspection effort. The benefit of continuously monitoring the structural health can be quantified in terms of the value of information, which corresponds to the difference between the expected lifetime costs with and without monitoring. In this work, we demonstrate in a numerical example how an optimized sensor placement for a vibration-based structural health monitoring system can be determined by maximizing the value of information. T2 - 3rd International Conference on Health Monitoring of Civil & Maritime Structures (HeaMES 2022) CY - Online meeting DA - 08.06.2022 KW - Bayesian System Identification KW - Offshore Wind Energy KW - Optimal Sensor Placement KW - Structural Health Monitoring KW - Value of Information PY - 2022 AN - OPUS4-55473 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eichner, Lukas A1 - Gerards, Paul A1 - Herrmann, Ralf A1 - Schneider, Ronald A1 - Hille, Falk A1 - Baeßler, Matthias T1 - A framework for data and structural integrity management for support structures in offshore wind farms based on building information modelling N2 - Support structures of wind turbines in German offshore wind farms are regularly inspected. Currently, inspection outcomes are generally not systematically recorded. This prevents their consistent handling and processing, which is a key requirement to enable an efficient structural integrity management. As part of the DiMoWind-Inspect project, a data model and reference designation system for such inspection results is developed to facilitate their identification, localization, quantification, tracing and linking throughout the lifetime of a wind farm and beyond. The inspection results together with structural health monitoring results and information on repairs form the basis for assessing and predicting the structural condition, estimating the remaining lifetime, and planning of future inspections, structural health monitoring, and repairs. As a basis for developing a digital structural integrity management, a generic framework is proposed in this paper, which describes the stakeholders, data, models, processes and workflows of the integrity management of support structures in offshore wind farms and their interrelations. The framework adopts a building information modelling approach to describe the information relevant to the structural integrity management. The central digital space of the framework is a common data environment. An implementation of the framework will enable a digital structural integrity management in which inspection, structural health monitoring, repair, assessment and planning outcomes generated throughout the life cycle of a wind farm can be consistently collected, managed, shared and processed by the relevant shareholders. T2 - 8th International Symposium on Reliability Engineering and Risk Management CY - Hannover, Germany DA - 04.09.2022 KW - Offshore wind energy KW - support structures KW - structural health monitoring KW - building information modelling KW - structural integrity management PY - 2022 DO - https://doi.org/10.3850/978-981-18-5184-1_MS-04-161-cd SP - 111 EP - 117 PB - Research Publishing CY - Singapore AN - OPUS4-55656 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eichner, Lukas T1 - A framework for data and structural integrity management for support structures in offshore wind farms based on building information modelling N2 - Support structures of wind turbines in German offshore wind farms are regularly inspected. Currently, inspection outcomes are generally not systematically recorded. This prevents their consistent handling and processing, which is a key requirement to enable an efficient structural integrity management. As part of the DiMoWind-Inspect project, a data model and reference designation system for such inspection results is developed to facilitate their identification, localization, quantification, tracing and linking throughout the lifetime of a wind farm and beyond. The inspection results together with structural health monitoring results and information on repairs form the basis for assessing and predicting the structural condition, estimating the remaining lifetime, and planning of future inspections, structural health monitoring, and repairs. As a basis for developing a digital structural integrity management, a generic framework is proposed in this paper, which describes the stakeholders, data, models, processes and workflows of the integrity management of support structures in offshore wind farms and their interrelations. The framework adopts a building information modelling approach to describe the information relevant to the structural integrity management. The central digital space of the framework is a common data environment. An implementation of the framework will enable a digital structural integrity management in which inspection, structural health monitoring, repair, assessment and planning outcomes generated throughout the life cycle of a wind farm can be consistently collected, managed, shared and processed by the relevant shareholders. T2 - 8th International Symposium on Reliability Engineering and Risk Management CY - Hannover, Germany DA - 04.09.2022 KW - Offshore wind energy KW - Support structures KW - Building information modelling KW - Structural health monitoring KW - Structural integrity maintenance PY - 2022 AN - OPUS4-55651 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Richter, Anja T1 - Reducing Escherichia coli adhesion to PET by modulating spatial periods of laser-induced surface nanoripples N2 - Using nanofiber-like cell appendages, secreted proteins and sugars, bacteria can establish initial surface contact followed by irreversible adhesion and the formation of multicellular biofilms. Here, the stabilizing extracellular biofilm matrix together with physiological changes on the single cell level leads to an increased resilience towards harsh environmental conditions, antimicrobials, the host immune response and established cleaning procedures. Persistent microbial adhesion on e.g., medical implants, in water supply networks or food-processing industry is often associated with chronic inflammation, nosocomial and foodborne infections, enhanced biofouling and product contamination. To prevent persistent microbial colonization, antibacterial surface strategies often target the initial steps of biofilm formation and impede adhesion of single cells before a mature biofilm is being formed. While chemical coatings have been widely used, their restricted biocompatibility for eukaryotic cells and attenuated antibacterial-effects due to compound release limit their areas of application and alternative strategies focus on modified surfaces topographies to impede bacterial adhesion. In this work, we used ns-UV laser treatment (wavelength 248 nm and a pulse duration of 20 ns) to generate laser-induced periodic surface structures (LIPSS) with different submicrometric periods ranging from ~210 to ~610 nm on commercial poly(ethylene terephthalate) (PET) foils. Following structurally and chemically analyses, PET samples were subjected to bacterial colonization studies with Escherichia coli TG1, a bacterial test strain with a strong biofilm formation capacity due to the formation of nanofiber-like cell-appendages (pili). Bacterial adhesion tests revealed that E. coli repellence decisively depends on the spatial periods of the LIPSS with the strongest reduction (~91%) in cell adhesion observed for LIPSS periods of 214 nm. Scanning electron microscopy and additional biofilm studies using a pili-deficient E. coli TG1 strain revealed the importance of extracellular appendages in the bacterial repellence observed here, thus, pointing out new antibiotics-free strategies for antibacterial surfaces by impeding nanofiber-mediated bacterial adhesion. T2 - E-MRS Spring Meeting 2022 CY - Online meeting DA - 30.05.2022 KW - Laser-induced periodic surface structures (LIPSS) KW - Bacterial adhesion tests KW - Bacteria repellent surfaces KW - Polymer foils KW - E. coli PY - 2022 AN - OPUS4-54930 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kruschwitz, Sabine A1 - Munsch, Sarah Mandy T1 - Potential automatisierter NMR-Messungen zur Ermittlung von Hydratationseigenschaften - ein Vergleich mit Vicat- und Wärmeflusskalorimetrie-Ergebnissen N2 - Es werden Ergebnisse von 1H-NMR-Relaxometrie-Messungen an Salzbeton und einem alkali-aktivierten Material, die im Rahmen des Themenfeldprojektes Seal Waste Safe durchgeführt werden, vorgestellt. Dabei wird die zeitliche Entwicklung von ausgewählten Merkmalen der ermittelten T2-Relaxationszeitenverteilungen während der Hydratation betrachtet. Als Referenz zur Identifikation von charakteristischen Hydratationsereignissen dienen der Vicat-Nadeleindringversuch und Wärmeflusskalorimetrie. T2 - Online-Workshop „Dauerhafte Verschlussbauwerke für Endlager“ CY - Online meeting DA - 14.02.2022 KW - NMR-Relaxometrie KW - Alkali-aktiviertes Material KW - Salzbeton KW - Seal Waste Safe PY - 2022 AN - OPUS4-54945 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Baeßler, Matthias T1 - Dynamisches Verhalten und Überwachung des Großen Fallturms der BAM in Horstwalde N2 - Falltürme sind Bauwerke, die als Versuchsanlagen sehr speziellen, impulsartigen Belastungen ausgesetzt sind. Am Fallturm auf dem Testgelände Technische Sicherheit (TTS) der BAM wurde bei Routineinspektionen eine Abnahme der strukturellen Integrität in Form von Vorspannungsverlusten in den Bolzen der Stahlverbindungen festgestellt. Um ein Verständnis für die zugrundeliegenden Trag- und Schädigungsmechanismen zu erlangen, wurde ein umfassendes Structural Health Monitoring (SHM) System geplant und am Bauwerk installiert unter Nutzung von digitalen Bauwerksmodellen. Für die Auslegung des Überwachungssystems, insbesondere aber zur Unterstützung der Untersuchung des Schädigungsprozesses, wurden Finite-Elemente-Modelle erstellt. Um sicherzustellen, dass die FE-Modelle das reale Tragwerksverhalten mit ausreichender Genauigkeit abbilden, mussten sie jedoch in Bezug auf die gemessenen Antworten des Tragwerks kalibriert werden. Der vorliegende Beitrag beschreibt experimentelle und numerische Untersuchungen zur Identifizierung des strukturellen Systems des Stahlrohrgitterturms in Vorbereitung einer Überwachungskampagne. Die Auswertung von gemessenen Schwingungen unter ambienter Anregung ermöglichte die Identifizierung der Eigenfrequenzen mehrerer globaler Schwingungsmoden des Fallturms. Zur Modellvalidierung wurde zunächst eine Sensitivitätsanalyse durchgeführt, um die Parameter mit dem größten Einfluss zu ermitteln. Anschließend wurde ein evolutionärer Algorithmus (EA) zur Optimierung nach dem Prinzip der Minimierung der Differenzen zwischen gemessenen und simulierten charakteristischen Antworten eingesetzt. Das aktualisierte Modell wurde schließlich an der dynamischen Reaktion der Turmstruktur infolge einer realen Falltest-induzierten Stoßbelastung validiert. Die Ergebnisse zeigten eine gute Übereinstimmung zwischen numerischen und experimentellen Ergebnissen. N2 - Drop test towers are structures subjected to very specific dynamic loadings. At the drop test tower at the Test Site Technical Safety (TTS) of BAM routine inspections revealed a decline of structural integrity in form of loss of pretension in bolts of structural steel connections. To get an understanding about the underlying damage mechanisms as well as to assure the structural safety in operation, a multifaceted Structural Health Monitoring (SHM) system was planned and installed at the structure with the help of digital models. For planning the monitoring system but especially for supporting the investigation of the damaging process finite element models are deployed. Though, to ensure the capability of the FE model to reproduce the real structural behavior in sufficient accuracy, it needs to be calibrated in respect to measured responses of the structure. The present contribution describes experimental and numerical investigations to identify the structural system of the steel tube lattice tower in preparation of the monitoring campaign. An ambient vibration test allowed the identification of the natural frequencies of several global vibrational modes of the drop test tower. For model updating first a sensitivity analysis is applied to identify the most influencing parameter. In succession a genetic algorithm was applied for optimization in the sense of minimization of the difference between measured and simulated characteristic responses. The updated model is finally validated on the dynamic response of the tower structure to a real drop test induced impact loading. The results showed a good agreement between numerical and experimental results though the robustness of the simulation should be improved by more sophisticated numerical modelling. T2 - 7. VDI-Fachtagung Baudynamik CY - Würzburg, Germany DA - 27.04.2022 KW - Großer Fallturm Horstwalde KW - Structural Health Monitoring KW - Belastungsversuch KW - Modalanalyse KW - Schwingungsdynamik KW - Finite Elemente Simulation PY - 2022 AN - OPUS4-55470 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Nietzke, Jonathan A1 - Konert, Florian T1 - Experimental and numerical characterization of hydrogen diffusion in thick-walled submerged arc welded joint of S420G2+M offshore steel grade N2 - Offshore wind turbines are an important goal in national energy strategies worldwide. Foundation structures are manufactured from submerged arc welded (SAW) plates with thicknesses up to 200 mm. In that connection, high-strength steels like the S420G2+M are more and more applied offering the possibility for increased stability and load-bearing capacity of the foundations. These offshore steel grades can show a susceptibility for delayed hydrogen assisted cold cracking of the weld joints. For that purpose, a minimum waiting time (MWT) of up to 48 h (dependent on applied standards) is recommended before non-destructive testing is allowed and conducted. But this concept is based on older steel grades that have been used for three or more decades. Nowadays, the metallurgical improvements (clean steels, proper rolling, and heat treatment) of base materials and well as welding consumables must be anticipated. Hence, the MWT concept should be critically discussed as it is assumed to be very conservative. For that reason, the focus of this study was to investigate the diffusion behavior in S420G2+M steel and its multi-layer SAW joint. Electrochemical permeation experiments were carried at room temperature. Boundary conditions were anticipated in terms of using different sample thicknesses. From the experimental data, hydrogen diffusion coefficients and absorbed diffusible hydrogen concentrations had been calculated. It was shown that hydrogen diffusion in the base material is increased compared to the weld metal. In addition, the sample thickness had a significant on the calculated diffusion coefficients. The minimum and maximum diffusion coefficients had been used for numerical modelling of the hydrogen diffusion in the welding joint. It became clear that a MWT must be always regarded together with a critical initial diffusible hydrogen concentration for the evaluation of a possible delayed cracking as diffusion times were mostly > 48 h due to the thick plates. T2 - 4th International Conference on Metals and Hydrogen - Steely & Hydrogen 2022 CY - Ghent, Belgium DA - 11.10.2022 KW - Hydrogen KW - Submerged arc welding KW - Minimum Waiting Time KW - Cold Cracking KW - Offshore steel grade PY - 2022 AN - OPUS4-56008 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - LTT-Zusatzwerkstoffe zur Optimierung von Schweißeigenspannungen N2 - Der Vortrag gibt eine Einführung zum Thema LTT-Zusatzwerkstoffe. Anhand experimenteller Befunde werden die Mechanismen erläutert und die Auswirkungen auf die Schweißeigenspannungen verdeutlicht. T2 - 1. LTT-Workshop des ISF RWTH Aachen CY - Aachen, Germany DA - 11.05.2022 KW - LTT-Zusatzwerkstoff KW - Hochfester Stahl KW - Eigenspannungen KW - Martensit KW - Phasenumwandlung PY - 2022 AN - OPUS4-56267 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Griesche, Axel T1 - The debye waller factor for temperature distribution determination in NBEI experiments: a case study for GTAW N2 - We could show in GTAW experiments with steel samples that the attenuation of neutron transmission underneath the welding torch due to the Debye-Waller-effect correlates well with sample temperatures obtained by FE numerical simulations. This would allow principally to determine sample temperatures by measuring the neutron beam attenuation. T2 - ITMNR-9 CY - Buenos Aires, Argentina DA - 17.10.2022 KW - Debye waller factor KW - GTAW KW - Temperature distribution determination PY - 2022 AN - OPUS4-56150 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Gleim, Tobias T1 - Fracture Mechanical Investigations on a Welding Seam of a Thick-Walled Transport Package N2 - Untersuchung einer Schweißnaht mit verschiedenen Codes. Vergleiche von experimentellen und numerischen Ergebnissen T2 - Technical Exchange IRSN – BAM: Transport & Storage of Packages for Radioactive Material CY - Cadarache, France DA - 13.10.2022 KW - Drop test KW - Fracture initiation KW - Transport package PY - 2022 AN - OPUS4-56055 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael T1 - Fügetechnik für Wasserstofftechnologien: Ausgewählte Themen und Herausforderungen N2 - Die Präsentation fasst die Bedeutung der Fügetechnik für Wasserstofftechnologien im Rahmen der Arbeiten für einer Studie (DVS-Berichte Nr. 373) mit besonderer Berücksichtigung der Normung und Regelwerkssetzung zusammen. T2 - Sitzung des DIN-Gemeinschaftsarbeitsausschusses NA 092 00 05 GA, NAS/NMP: Zerstörende Prüfung von Schweißverbindungen CY - Online meeting DA - 10.03.2022 KW - Wasserstoff KW - Fügetechnik KW - Schweißen KW - Wasserstofftechnologien KW - Bedeutung PY - 2022 AN - OPUS4-54447 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schröder, Nina A1 - Rhode, Michael A1 - Kannengießer, Thomas T1 - Experimentelle Bestimmung und thermodynamische Modellierung des Ausscheidungsverhaltens in der WEZ eines S690QL bei unterschiedlichen Mikrolegierungsrouten N2 - Für eine signifikante Festigkeitssteigerung von vergüteten, hochfesten Feinkornbaustählen mit einer Normstreckgrenze > 690 MPa, ist die Zugabe von Mikrolegierungselementen, wie Nb und Ti, unerlässlich. Die Normvorgaben zur chemischen Zusammensetzung dieser Stähle (bspw. in DIN EN 10025-6) geben zur Erzielung der vorgeschriebenen Eigenschaften dabei oft nur Grenzgehalte für die Hersteller vor. Die Wirkung der Legierungselemente bzw. ihrer Karbide und/oder Nitride ist teilweise komplett konträr, insbesondere bei Auflösung und Wiederausscheidung in der WEZ bei identischem Schweißzusatz. Somit wird eine adäquate Vorhersage der Chargenabhängigkeit hinsichtlich der Schweißeignung und des Tragverhaltens der Schweißverbindung erschwert. Zuzüglich können moderne Schweißprozesse, wie MSG mit modifiziertem Sprühlichtbogen (mod. SLB) durch ihre hohe Wärmeeinwirkung die Phasenumwandlung in der Wärmeeinflusszone negativ beeinflussen. Eine unerwünschte Eigenschaft ist dabei die Erweichung (engl.: softening) der WEZ, wie auch u.U. der gegenteilige Effekt der Aufhärtung (engl.: hardening). Vor diesem Hintergrund werden im Rahmen eines DFG-Vorhabens systematisch Mikrolegierungsrouten mit variierenden Ti- und Nb-Gehalten des hochfesten und vergüteten Feinkornbaustahls S690QL untersucht. Dazu wird das MAGSchweißen mit mod. SLB verwendet, welches durch hohe Abschmelzleistung gekennzeichnet ist und schmalere Fugenöffnungswinkel (α = 30°) ermöglicht. An diesen Schweißungen wird der Effekt der metallurgischen Zusammensetzung in Kombination mit hoher Wärmeeinwirkung auf die Ausbildung einer kritischen WEZ-Gefügezone mit Erweichung und/oder exzessiver Aufhärtung untersucht. Ein besonderes Augenmerk wird auf die Phasenumwandlungen und das Ausscheidungsverhalten im Gefüge der Wärmeeinflusszone gelegt. Neben umfangreichen metallographischen Untersuchungen einzelner WEZ-Bereiche wurden, unter Variation der chemischen Zusammensetzung, thermodynamische Phasenberechnungen mittels ThermoCalc durchgeführt. Hierdurch wird ein Verständnis zur Phasentransformation und Ausscheidungswachstum und -auflösung während des Schweißens in Abhängigkeit von Temperatur und Abkühlbedingungen geschaffen. Das Ziel ist es, mittels erster Untersuchungen den Einfluss der Wärmeeinwirkung auf die Gefügeausbildung in der WEZ zu zeigen. Insbesondere wird hier auf die Auswirkung der unterschiedlichen Mikrolegierungskonzepte (Ti oder Nb) geachtet. T2 - DVS CONGRESS 2022 - Große Schweißtechnische Tagung CY - Koblenz, Germany DA - 19.09.2022 KW - WEZ-Erweichung KW - Hochfester Feinkornbaustahl KW - ThermoCalc KW - Thermodynamische Simulation KW - Mikrolegierungselemente KW - Modifizierter Sprühlichtbogen PY - 2022 SN - 978-3-96144-189-1 SN - 978-3-96144-190-7 VL - 382 SP - 131 EP - 137 PB - DVS Media GmbH CY - Düsseldorf AN - OPUS4-55834 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Emamverdi, Farnaz A1 - Yin, Huajie A1 - Smales, Glen Jacob A1 - Harrison, W. J. A1 - Budd, P. M. A1 - Böhning, Martin A1 - Schönhals, Andreas T1 - Polymers of intrinsic microporosity - Molecular mobility and physical aging revisited by dielectric spectroscopy and X‑ray scattering N2 - Polymers of intrinsic microporosity (PIMs) are promising candidates for the active layer in gas separation membranes due to their high permeability and reasonable permselectivity. These appealing properties originate from a microporous structure as a result of inefficient segment packing in the condensed state due to a combination of a ladder-like rigid backbone and sites of contortion. However, this class of polymers suffers from a significant decrease in the permeability with time due to physical aging, whereby typically, the permselectivity increases. The initial microporous structures approach a denser state via local rearrangements, leading to the reduction of the permeability. Hence, a detailed characterization of the molecular mobility in such materials can provide valuable information on physical aging. In this work, the dielectric behavior of PIM-1 films and their behavior upon heating (aging) were revisited by isothermal frequency scans during different heating/cooling cycles over a broad temperature range between 133 and 523 K (−140 to 250 °C). In addition, the obtained results were compared with data of samples that were annealed at ambient temperatures over different time scales. Multiple dielectric processes were observed: several relaxation processes due to local fluctuations and a Maxwell−Wagner−Sillars polarization effect related to the microporosity. The temperature dependence of the rates of all processes follows the Arrhenius law where the estimated activation energy depends on the nature of the process. The influence of the thermal history (aging) on the processes is discussed in detail. KW - Polymers of intrinsic microporosity PY - 2022 DO - https://doi.org/10.1021/acs.macromol.2c00934 VL - 55 SP - 7340 EP - 7350 PB - American Chemical Society CY - Washington, DC AN - OPUS4-55485 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Villajos Collado, José Antonio T1 - Experimental volumetric hydrogen uptake determination at 77 K of commercially available metal-organic framework materials N2 - Storage is still limiting the implementation of hydrogen as an energy carrier to integrate the intermittent operation of renewable energy sources. Among different solutions to the currently used compressed or liquified hydrogen systems, physical adsorption at cryogenic temperature in porous materials is an attractive alternative due to its fast and reversible operation and the resulting reduction in storage pressure. The feasibility of cryoadsorption for hydrogen storage depends mainly on the performance of the used materials for the specific application, where metal-organic frameworks or MOFs are remarkable candidates. In this work, gravimetric and volumetric hydrogen uptakes at 77 K and up to 100 bar of commercially available MOFs were measured since these materials are made from relatively cheap and accessible building blocks. These materials also show relatively high porous properties and are currently near to large-scale production. The measuring device was calibrated at different room temperatures to calculate an average correction factor and standard deviation so that the correction deviation is included in the measurement error for better comparability with different measurements. The influence of measurement conditions was also studied, concluding that the available adsorbing area of material and the occupied volume of the sample are the most critical factors for a reproducible measurement, apart from the samples’ preparation before measurement. Finally, the actual volumetric storage density of the used powders was calculated by directly measuring their volume in the analysis cell, comparing that value with the maximum volumetric uptake considering the measured density of crystals. From this selection of commercial MOFs, the materials HKUST-1, PCN-250(Fe), MOF-177, and MOF-5 show true potential to fulfill a volumetric requirement of 40 g·L−1 on a material basis for hydrogen storage systems without further packing of the powders. KW - Hydrogen adsorption KW - Commercial metal-organic frameworks KW - Hydrogen uptake reproducibility KW - Volumetric uptake KW - Packing density PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-542215 DO - https://doi.org/10.3390/c8010005 SN - 2311-5629 VL - 8 IS - 1 SP - 1 EP - 14 PB - MDPI CY - Basel AN - OPUS4-54221 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tuma, Dirk T1 - High-pressure density data of hydrogen-containing natural gases for the extension of equation-of-state models N2 - This presentation reports new density data of hydrogen-containing natural gas mixtures between 250 and 350 K and up to pressures of 20 MPa. T2 - 11th International GAS Analysis Symposium & Exhibition CY - Paris, France DA - 17.05.2022 KW - Hydrogen-containing natural gas KW - Density data KW - Equation of state PY - 2022 AN - OPUS4-56433 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -