TY - CONF A1 - Bonse, Jörn T1 - Ultrakurzpulslaser induzierte Oxidschichten zur Reduktion von Reibung und Verschleiß auf Metalloberflächen N2 - Die Reduktion von Reibung und Verschleiß in technischen Systemen bietet ein großes Potenzial zur Reduktion von CO2-Emissionen. Dieser Beitrag diskutiert die Erzeugung und tribologische Charakterisierung von Ultrakurzpuls-generierten Nano- und Mikrostrukturen auf Metallen (Stahl, Titan). Besonderes Augenmerk wird dabei auf die Rolle der laserinduzierten Oxidschicht im Zusammenspiel mit verschleißreduzierenden Additiven in ölbasierten Schmiermitteln gerichtet. T2 - Workshop "Nachhaltigkeit durch Tribologische Schichten" - Europäische Forschungsgesellschaft Dünne Schichten e.V. CY - Karlsruhe, Germany DA - 17.05.2022 KW - Laser-induzierte periodische Oberflächenstrukturen KW - Reibungsreduktion KW - Verschleißreduktion KW - Oberflächenmodifikation KW - Oxidation KW - Additive PY - 2022 AN - OPUS4-54849 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Trappe, Volker T1 - Dynamic mechanical analysis of epoxy-matrix cross linking measured in-situ using an elastomer container N2 - A new patented dynamic mechanical analysis (DMA) is presented, where the tensile, bending- or torsional stiffness of a media can be characterized in-situ during the phase transition from liquid to solid. An epoxy system, e.g. Hexion L285/H287, is filled into an elastomer container, such as a silicone tube. This can be mounted into a conventional DMA and, based on a linear viscoelastic approach, the storage modulus (E’;G’), the loss modulus (E’’;G’’) and the loss angle tan(delta) can be measured at constant temperature as a function of time in order to investigate the liquid to sol-gel to solid transition. With this new method, the stiffness increase as a result of the cure process can be directly measured more precisely than with a rheometer in a shear plate set-up, because using an elastomer container gives a defined cross section for calculating the Young’s modulus. T2 - 20th European Conference on Composite Materials, ECCM20 CY - Lausanne, Switzerland DA - 26.06.2022 KW - Dynamic mechanical analysis (DMA) KW - Thermoset polymers KW - Cure process KW - Cross linking PY - 2022 AN - OPUS4-55213 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tschirschwitz, Rico T1 - Projekte und Aktivitäten zu Elektrischen Energiespeichern an der BAM N2 - Die Sicherheit von Lithiumbatterien ist ein entscheidender Punkt beim Ausbau der Elektromobilität. Der Beitrag gibt zunächst einen Überblick über das Aktivitätsfeld der elektrischen Energiespeicher an der BAM. Im weiteren werden sowohl die Projekte HaCLIB (Hazard Classification ofLithium-Ion Batteries) als auch SEE-2L (Sicherheit elektrochemischer Energiespeicher in 2nd-Life Anwendung) vorgestellt. Darüber hinaus werden noch die hoheitlichen Aufgaben der BAM im Bereich des Transports von kritisch defekten Batterien erläutert. T2 - Sitzung des ProcessNet-AA Reaktionstechnik sicherheitstechnisch schwieriger Prozesse (AA-RTSSP) der DECHEMA CY - Online meeting DA - 13.04.2022 KW - Stationäre Energiespeicher KW - Elektrische Energiespeicher KW - Auswirkungsbetrachtungen KW - EES PY - 2022 AN - OPUS4-54649 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bonse, Jörn T1 - Laser-Induced Periodic Surface Structures: when Maxwell meets Marangoni N2 - Laser-Induced Periodic Surface Structures (LIPSS, ripples) are a universal phenomenon and can be generated in a contactless, single-step process on almost any material upon irradiation of solids with intense laser radiation. Nowadays, processing rates of up to m^2/min are enabling new industrial applications in medicine, optics, tribology, biology, etc. Depending on the specific type of LIPSS, their structural sizes typically range from several micrometers down to less than 100 nanometers – far beyond the optical diffraction limit – while their orientations exhibit a clear correlation with the local polarization direction of the laser radiation. From a theoretical point of view, however, a controversial and vivid debate has emerged during the last two decades, whether LIPSS originate from electromagnetic effects (seeded already during the laser irradiation) – or whether they emerge from matter reorganization processes, i.e. distinctly after the laser irradiation. This presentation reviews the currently existent theories of LIPSS. A focus is laid on the historic development of the fundamental ideas, their corresponding mathematical descriptions and numerical implementations, along with a comparison and critical assessment of the different approaches. T2 - 16th International Conference on Laser Ablation (COLA 2021/22) CY - Matsue, Japan DA - 24.04.2022 KW - Laser-induced periodic surface structures (LIPSS) KW - Laser ablation KW - Theoretical modelling KW - Electromagnetic scattering KW - Hydrodynamics PY - 2022 AN - OPUS4-54716 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Baensch, Franziska T1 - Charakterisierung von Salzbeton und alkali-aktivierten Material basierend auf der Schallemissionsanalyse N2 - Nach einer kurzen Einführung in die Schallemissionsprüfung und -Analyse wird ein Versuchsstand vorgestellt, der im Rahmen des Themenfeldprojektes Seal Waste Safe installiert wurde. Schwerpunkt des Vortrages sind die Schallemissionsmessungen an einem 150 l Demonstrator aus Salzbeton und einem weiteren aus alkali-aktiviertem Material. Neben der konventionellen Schallemissionsanaylse mit Aktivitäts- und Intensitätsparametern der Zeitsignale, werden auch frequenzbasierte Parameter zur Analyse andiskutiert. N2 - After a brief introduction to acoustic emission testing and analysis, an experimental test setup is presented, which was part of the Seal Waste Safe project (internal BAM project 2019-2022). Herein, the acoustic emission measurements of a 150 l demonstrator made of salt concrete and another one made of alkali-activated material are focused. In addition to the conventional acoustic emission analysis regarding the activity and intensity parameters of the detected time signals, also frequency-based parameters were discussed for analysis. T2 - Dauerhafte Verschlussbauwerke für Endlager CY - Online meeting DA - 14.2.2022 KW - Acoustic Emission KW - Schallemission KW - Salzbeton KW - Alkali aktiviertes Material KW - Geopolymer PY - 2022 AN - OPUS4-54937 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Stamm, Michael A1 - Krankenhagen, Rainer T1 - Weather-dependent passive thermography of unheated wind turbine blades N2 - Up to now, the inspection of wind turbines with industrial climbers has been considered ”state of the art”. However, ever-larger wind turbines and advancing digitization make modern and automated inspection methods indispensable. Passive thermography can serve as such a digital and atomized method while it is well known for its applications in the inspection of buildings or electrical circuits. However, its application relies on thermal gradients in the inspected object such that a temperature contrast exists between damaged and sound areas. This also holds for unheated structures like rotor blades of wind turbines which show no intrinsic temperature gradient and can hardly be heated. Under certain weather conditions with sufficient solar loading and diurnal temperature variations, passive thermography is suitable for the in-service inspection of rotor blades. However, for a reliable use of passive thermography on ”thermal passive” components, the incorporation of these environmental conditions in the planning and evaluation of thermal inspections is crucial. Additionally, the complex inner structure of wind turbine blades in comparison to other objects and buildings require a specific method referencing the individual rotor blades to each other. This allows the distinction between the thermal response of design-specific structural features and damages or irregularities between the three blades. We show thermal signatures of damage in rotor blades and contrast them with structural characteristics by comparing the three blades. In addition to measurements in industrial environments, laboratory measurements are shown and compared to simulations. The long-term goal is to simulate the influence of different weather parameters and thus gain a better understanding of measurements in the field. The results shown here can be seen as one step towards industrial application. T2 - SPIE Defense + Commercial Sensing CY - Orlando, Florida, USA DA - 03.04.2022 KW - Passive thermography KW - Wind energy KW - FEM simulations PY - 2022 DO - https://doi.org/10.1117/12.2618740 VL - 12109 SP - 1 EP - 8 PB - Society of Photo-Optical Instrumentation Engineers (SPIE) AN - OPUS4-54943 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Stamm, Michael T1 - Weather-dependent passive thermography of unheated wind turbine blades N2 - Up to now, the inspection of wind turbines with industrial climbers has been considered ”state of the art”. However, ever-larger wind turbines and advancing digitization make modern and automated inspection methods indispensable. Passive thermography can serve as such a digital and atomized method while it is well known for its applications in the inspection of buildings or electrical circuits. However, its application relies on thermal gradients in the inspected object such that a temperature contrast exists between damaged and sound areas. This also holds for unheated structures like rotor blades of wind turbines which show no intrinsic temperature gradient and can hardly be heated. Under certain weather conditions with sufficient solar loading and diurnal temperature variations, passive thermography is suitable for the in-service inspection of rotor blades. However, for a reliable use of passive thermography on ”thermal passive” components, the incorporation of these environmental conditions in the planning and evaluation of thermal inspections is crucial. Additionally, the complex inner structure of wind turbine blades in comparison to other objects and buildings require a specific method referencing the individual rotor blades to each other. This allows the distinction between the thermal response of design-specific structural features and damages or irregularities between the three blades. We show thermal signatures of damage in rotor blades and contrast them with structural characteristics by comparing the three blades. In addition to measurements in industrial environments, laboratory measurements are shown and compared to simulations. The long-term goal is to simulate the influence of different weather parameters and thus gain a better understanding of measurements in the field. The results shown here can be seen as one step towards industrial application. T2 - Defense + Commercial Sensing 2022 CY - Orlando, Florida, USA DA - 3.4.2022 KW - Passive thermography KW - Wind energy KW - FEM simulations PY - 2022 UR - https://spie.org/defense-commercial-sensing/presentation/Weather-dependent-passive-thermography-of-unheated-wind-turbine-blades/12109-19?SSO=1 AN - OPUS4-54944 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wille, Frank T1 - CASTOR in Warteposition, aber bitte sicher. N2 - CASTOR-Behälter sollen den Auswirkungen schwerster Unfälle standhalten und müssen dabei ihre Sicherheitsfunktionen beibehalten. Dazu zählen der sichere Einschluss des radioaktiven Inventars mit nachgewiesener Behälterintegrität und -dichtheit, die ausreichende Abschirmung der radioaktiven Strahlung, die Ableitung der von den Brennelementen ausgehenden Wärme und der Ausschluss des Entstehens einer nuklearen Kettenreaktion, d.h. die Kritikalitätssicherheit sind zu gewährleisten. Zum Nachweis dieser Fähigkeiten werden die Behälter gegen Stoß, Aufprall, Durchstoßen, Feuer sowie beim Eintauchen in Wasser geprüft. Durch diese Tests werden Beanspruchungen aus potentiellen schweren Unfällen abdeckend simuliert. Die hierfür erforderlichen experimentellen Tests, aber auch die Prüfung und Entwicklung komplexer rechnerischer Simulationen des Behälterverhaltens unter Anwendung der Finite-Elemente-Methode erfolgen bei der Bundesanstalt für Materialforschung und -prüfung (BAM). Die Basis bildet das Regelwerk der Internationalen Atom- und Energieorganisation (IAEO) zum sicheren Transport von radioaktiven Stoffen, welches international harmonisierte Schutzziele und Prüfanforderungen definiert. Die seit 60 Jahren praktizierte stetige Weiterentwicklung der Sicherheitsanforderungen trägt aktuellen Erkenntnissen, Erfahrungen und Risikoanalysen Rechnung. Die Brennelementbehälter werden mechanischen Prüfungen sowie Brand- und Wasserdruckprüfungen unterzogen. Hierdurch wird nachgewiesen, dass sie den Auswirkungen eines schweren Unfalls standhalten können. Nur Behälter die zweifelsfrei die kumulativen mechanischen und thermischen Tests und auch die Wasserdruckprüfung mit Erfüllen aller Schutzziele bestehen, bekommen eine Zulassung, die es erlaubt die Behälter zu transportieren. KW - Kerntechnik KW - Radioaktive Stoffe KW - Transport KW - Zwischenlagerung KW - IAEA KW - Fallprüfung PY - 2022 DO - https://doi.org/10.26125/73hj-nz53 SN - 1611-9479 VL - 24 IS - 3 SP - 112 EP - 114 PB - Bunsen-Gesellschaft CY - Frankfurt AN - OPUS4-54856 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Amano, K. A1 - Hahn, S. A1 - Tschirschwitz, Rico A1 - Rappsilber, Tim A1 - Krause, U. T1 - An Experimental Investigation of Thermal Runaway and Gas Release of NMC Lithium-Ion Pouch Batteries Depending on the State of Charge Level N2 - In this study, 19 experiments were conducted with 25 pouch cells of NMC cathode to investigate thermal runaway and the release of gases from lithium-ion batteries (LIBs). Single cells, double cells, and a four-cell battery stack were forced to undergo thermal runaway inside an air-tight reactor vessel with a volume of 100 dm3 . The study involved two series of tests with two types of ignition sources. In the Series 1 tests, a heating plug was used to initiate thermal runaway in LIBs in the ranges of 80–89% and 90–100% SOC. In the Series 2 tests, a heating plate was used to trigger thermal runaway in LIBs in the ranges of 30–50%, 80–89%, and 90–100% SOC. Thermal runaway started at an onset temperature of 344 ± 5 K and 345 K for the Series 1 tests and from 393 ± 36 K to 487 ± 10 K for the Series 2 tests. Peak reaction temperatures ranged between 642 K and 1184 K, while the maximum pressures observed were between 1.2 bar and 7.28 bar. Thermal runaway induced explosion of the cells and lead to a rate of temperature increase greater than 10 K/s. The amounts of gases released from the LIBs were calculated from pressures and temperatures measured in the reactor. Then, the gas composition was analyzed using a Fourier transform infrared (FTIR) spectrometer. The highest gaseous production was achieved at a range of 90–100% SOC and higher battery capacities 72 L, 1.8 L/Ah (Series 1, battery stack) and 103 L, 3.2 L/Ah (Series 2, 32 Ah cell)). Among the gases analyzed, the concentration of gaseous emissions such as C2H4 , CH4 , and C2H6 increased at a higher cell capacity in both series of tests. The study results revealed characteristic variations of thermal behavior with respect to the type of ignition source used. KW - Lithium-ion batteries KW - Battery KW - Pouch cell KW - NMC Cathode KW - Thermal runaways PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-548601 DO - https://doi.org/10.3390/batteries8050041 VL - 8 IS - 5 SP - 1 EP - 16 PB - MDPI CY - Basel, Switzerland AN - OPUS4-54860 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ghafafian, Carineh T1 - Fully-reversed fatigue behavior of scarf joint repairs for wind turbine blade shell applications N2 - Due to manufacturing imperfections which can propagate to damage under in-service loads, wind turbine rotor blades, made primarily of glass fiber reinforced polymers (GFRP), often fail significantly before their design life. To enable a quick and cost-effective return to service, localized repairs can be executed by technicians in the field, directly accessing the blades by suspended roping. Scarf joint repairs, shown to be highly efficient with a smooth load transition across angled joint walls and a restored aerodynamic profile, are the focus of this study. The damage mechanisms of these structures were examined under fully-reversed mechanical cyclic loading with a load ratio R = -1, which was made possible on the coupon scale by a custom designed anti-buckling support. The number of cycles to failure were compared across load levels. While the scarf joint ratio was held constant at 1:50, known from industry and literature to be a good compromise between restored mechanical properties and repair size, the layup sequence was varied between small-to-large and large-to-small. Hereby the effect of the presence of resin pockets and fiber orientation mismatch between the parent and repair structure on the failure mechanism as well as fatigue strength of ±45° GFRP scarf joint repair structures was studied. Strain development across the joint length was measured to assess stiffness degradation in addition to the fatigue strength recovery of scarf joint structures with respect to pristine reference specimens. Grayscale analysis was used to monitor the damage state leading to fracture across the specimens. Post-mortem fractography analysis with light microscopy described the global failure mechanisms as well as local damage distribution within the structure, all of which provided insight to critical variables in scarf joint GFRP structures under fully-reversed mechanical cyclic loading, allowing for the tailoring of such repairs on wind turbine blade shells for maximum restoration of service life. T2 - 20th European Conference on Composite Materials (ECCM20) CY - Lausanne, Switzerland DA - 26.06.2022 KW - Glass fiber reinforced polymers KW - Scarf repairs KW - Fatigue PY - 2022 AN - OPUS4-55638 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Feldkamp, Martin A1 - Quercetti, Thomas A1 - Gleim, Tobias T1 - Temperature and Heat Flux Measurements in Fire Testing N2 - Packages for the transport of Spent Nuclear Fuel and high active radioactive waste are designed to withstand severe accidents. Specific mechanical and thermal tests are defined in the IAEA Regulations for the Safe Transport of Radioactive Materials in order to cover these hypothetical severe accidents. The thermal test mainly consists of a 30 minute fully engulfing fire. Components such as the package impact limiters can lead to supplementary energy release during the thermal test as they might continue burning after the fire phase. Local heat flux into the package can occur. Measurement of heat flux into the package is of importance to evaluate component temperatures and review their acceptance. The usability of heat flux sensors and temperature measurement equipment has to be tested to apply them in impact limiter fire testing. Further questions arise such as :“Is the infrared camera a useful tool to determine heat flux at the boundary surface?” T2 - Technical Exchange IRSN – BAM Transport & Storage of Packages for Radioactive Material CY - Berlin, Germany DA - 08.09.2021 KW - Heat flux sensor PY - 2021 AN - OPUS4-55659 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zekhnini, Khalid T1 - Corrosion testing in a laboratory container: Corrosion testing with artificial seawater and sediment N2 - Electricity generation by offshore wind turbine generators (WTG) is an important pillar of the energy transition. Corrosion processes on WTGs pose a particular challenge with regard to safe operation over longer periods of time due to the highly corrosive conditions in the offshore area. BAM is therefore conducting research to ensure a safe operation of the turbines over their intended service life to protect people and the environment. In a joint research project, different corrosion-relevant areas of a WTG foundation structure were specifically simulated in test basins within a laboratory container. The aim of the work was, on the one hand, the gravimetric and electrochemical determination of corrosion rates in the different areas of an WTG that are relevant for cathodic corrosion protection (CCP): Underwater and sediment zone as well as the transition area between these two zones. Also, targeted tests were carried out under CCP. In addition, investigations regarding calcareous deposition during CCP were carried out on idealized specimens under laboratory conditions to better assess its influence on the protection process. The investigations were carried out in a laboratory container with different basins, which were filled with sand as sediment and artificial seawater according to ISO 15711and connected via a closed water circuit. The poster at EURCORR 2022 provides an overview of the investigations and the most important results. It will be evaluated, if a simulation of offshore corrosion conditions is possible to a certain extent in an idealized system with artificial seawater and sediment. T2 - EUROCORR 2022 CY - Berlin, Germany DA - 28.08.2022 KW - Corrosion KW - Corrosion Testing KW - Artificial Sea Water KW - Laboratory Container PY - 2022 AN - OPUS4-55664 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hicke, Konstantin T1 - Distributed fiber optic sensing @BAM N2 - Research and developement activities of BAM regarding Distributed Fiber Optic Sensing are portrayed using exemplary previous and current projects. Shown results pertain to distributed acoustic sensing (DAS), distributed temperagture sensing (DTS) and distributed strain sensing (DSS). T2 - Seismic seminar FU Berlin (group Prof. Shapiro) CY - Online meeting DA - 15.09.2022 KW - Distributed fiber optic sensing KW - Distributed acoustic sensing KW - Distributed temperature sensing KW - Distributed strain sensing KW - Infrastructure monitoring PY - 2022 AN - OPUS4-55721 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schönhals, Andreas T1 - Inelastic and Quasielastic Neutron Scattering Experiments on Mircroporous Membranes for Green Separation processes N2 - Polymers with intrinsic microporosity are promising candidates for the active separation layer in gas separation membranes. These polymers are characterized by a high permeability and reasonable permselectivity. The reasonable permselectivity of these materials is somehow surprising because for microporous systems a more Knudsen-like diffusion is expected rather than a size dependent temperature activated sieving process. It was argued in the framework of a random gate model that molecular fluctuations on a time scale from ps to ns are responsible for the permselectivity. Here a series of microporous polynorbornenes with bulky SiMe3 side groups and a rigid backbone is considered which have different microporosities characterized by BET surface area values. First inelastic time-of-flight neutron scattering measurements were carried out to investigate the low frequency density of state (VDOS). The measured data show the characteristic low frequency excess contribution to the VDOS above the Debye sound wave level, generally known as the Boson peak in glass-forming materials. It was found that the maximum position of the Boson peak correlates with the BET surface area. For two selected comparable polynorbornenes elastic scans as well as QENS measurements by a combination of neutron time-of-flight and backscattering were carried out. A low temperature relaxation process was found for both polymers. This process was assigned to the methyl group rotation. It was analysed in terms of a jump diffusion in a three-fold potential. The analysis of the dependence of the elastic incoherent structure factor on the scattering vector yields the number of methyl groups which might be immobilized. T2 - QENS / WINS 2022 CY - San Sebastian, Spain DA - 23.05.2022 KW - Polymers of intrinsic Microporosity PY - 2022 AN - OPUS4-55673 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schönauer-Kamin, Daniela T1 - Powder-Aerosol deposited (PAD) calcium manganate as n-type thermoelectric material N2 - Currently, calcium manganate CaMnO3 and calcium cobaltite Ca3Co4O9 are being investigated as n-type resp. p-type semiconducting materials as oxidation- and temperature-resistant thermoelectric materials for oxide multilayer thermoelectric generators (TEGs). In order to manufacture multilayer TEGs, pressure-assisted sintering processes at high temperatures are necessary to achieve optimal thermoelectric material properties. To realize TEGs in planar film technology, another method to obtain dense ceramic layers directly from the synthesized starting powders without a subsequent high temperature step is emerging recently: the powder aerosol deposition (PAD) method. In the present work, it is investigated whether PAD is suitable to produce dense ceramic films from Sm-doped CaMnO3 and Ca3Co4O9 powders. The resulting thermoelectric properties are characterized as a function of temperature. CaMnO3 powder could successfully be processed by PAD with resulting layer thicknesses of 5- 6 µm without any high-temperature sintering steps of the films. The electrical conductivity and the Seebeck coefficient of the films were determined in-plane from room temperature to 600 °C in air. The results show a Seebeck coefficient of around -200 µV/K, which is comparable to results of pressed and sintered bars. At 400 °C, the electrical conductivity corresponds to the conductivity of the bar. At higher temperatures the conductivity is better than with the reference. Below 400°C, the electrical conductivity is somewhat lower than that of the reference sample, a mild thermal treatment of the PAD layer improves it. It is expected that the thermal conductivity of the PAD film will be lower compared to the bars due to the nano-crystalline film morphology. This should result in a significantly increased ZT value for the PAD layers and a higher efficiency of the TEG. The work shows that both CaMnO3 and Ca3Co4O9 can be successfully processed by PAD, and the PAD films show comparable thermoelectric properties. T2 - 18th European Conference on Thermoelectrics CY - Barcelona, Spanien DA - 14.09.2022 KW - Film depositition KW - Calcium cobaltite PY - 2022 AN - OPUS4-55771 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Stamm, Michael T1 - Towards automated passive thermography of wind turbine blades N2 - Up to now, the inspection of wind turbines by industrial climbers has been considered "state of the art". However, many aspects like ever-larger wind turbines, minimizing the risk for man and machine and the advancing digitalization make modern and automated inspection methods indispensable. A particular interest here is contactless and remote methods that can be used with drones instead of climbing robots. The work presented here contributes to the long-term goal of making autonomous and advanced inspections of wind turbine rotor blades using drones ready for industrial use. Besides visual inspection, only a few inspection methods are capable of non-contact inspection on an industrial scale. Passive thermography can serve as such a contactless and digital inspection method and is well known for its applications in the inspection of buildings or electrical circuits. It can even sense both near-surface and subsurface defects. The sensitivity to subsurface defects makes one advantage of thermography over visual inspections. As a digital inspection method, it is generally also more objective and offers more comparability. For example, defects and their extent can be easily monitored and compared over time. However, its industrial application relies on thermal gradients in the inspected object such that a temperature contrast exists between damaged and sound areas. This also applies to large unheated structures such as wind turbine rotor blades, which do not have an intrinsic temperature gradient and at the same time cannot be easily heated externally. Under certain weather conditions, a change of the environmental temperature or the solar loading conditions can provide the necessary thermal gradients to make passive thermography viable for the in-service inspection of rotor blades. For a reliable use of passive thermography on "thermal passive" components, the incorporation of these environmental conditions in the planning and evaluation of thermal inspections is crucial. Compared to many other objects and buildings, wind turbine blades have varying and often unknown complex internal structures depending on the model. A special method is therefore required, that can be used independently of the internal structure of the blades and that relates the individual thermograms of the three rotor blades to each other. This allows the distinction between the thermal response of design-specific structural features and damages or irregularities between the three blades. In this work we present thermal signatures of rotating in-service rotor blades taken under industrial relevant conditions. These thermograms show surface and subsurface damages and irregularities which we contrast with structural design features by referencing the three blades to each other. In addition, we examine the strong influence of different weather conditions on the inspection results. A direct comparison of measured results with inspection reports from industrial climbers serves as a benchmark. T2 - EERA DeepWind conference CY - Trondheim, Norway DA - 19.01.2022 KW - Thermography KW - Wind energy KW - Passve IR KW - Rotor blades KW - Maintenance PY - 2022 AN - OPUS4-55818 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Stamm, Michael T1 - Towards the in-service blade inspection by ground-based passive thermography N2 - Until today, the optical inspection of rotor blades by industrial climbers is considered state of the art. However, both more and larger rotor blades and the increasing digitalization of maintenance work make modern inspection methods increasingly necessary. In this context, passive thermography can serve as a useful digital technique for in-service inspection of wind turbine blades. Unlike active thermography, this inspection method does not require an active heat source but takes advantage of heating by the sun and diurnal temperature fluctuations. This allows inspections from the ground during operation and does not require shutting down the wind turbine. However, an inspection with passive thermography is highly weather dependent. Thus, the already weak thermal signatures formed due to internal structures and possible internal damage are only strong enough under certain weather conditions. To obtain meaningful inspection results despite the relatively small thermal differences between intact and defective components, three aspects are crucial: 1. Measurements should be taken at the time of optimum weather conditions. It must be kept in mind that different internal damage will be revealed by thermal signatures under different weather conditions. 2. The thermal signature of the rotor blades, including possible damages, must be simulated with FEM simulations. In this way, the influence of different weather conditions can be predicted but also understood in the aftermath. 3. The temperature differences between identically designed and assembled rotor blades must be considered to analyze variations between blades. This work will address all these aspects and show, based on field measurements under industrial conditions (exemplarily shown in figure 1), laboratory measurements and FEM simulations, which steps must be taken to establish passive thermography as an industrial inspection method. T2 - EERA SP7 Rotor Blade workshop CY - Roskilde, Denmark DA - 23.06.2022 KW - Thermography KW - Wind energy KW - Maintenance KW - Rotor blades KW - Passive IRT PY - 2022 AN - OPUS4-55819 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Junge, P. A1 - Stargardt, Patrick A1 - Kober, D. A1 - Greinacher, M. A1 - Rupprecht, C. T1 - Thermally Sprayed Al2O3 Ceramic Coatings for Electrical Insulation Applications N2 - Thermal spraying enables a fast and propelling way to additively deposit various ceramics as electric insulators, which are used in conditions where polymers are not suitable. Alumina (Al2O3) is among the most employed materials in the coating industry since it exhibits good dielectric properties, high hardness, high melting point while still being cost-effective. Various parameters (e.g. feedstock type, plasma gas mixture, plasma power) significantly influence the resulting coating in terms of microstructure, porosity, crystallinity, and degree of un-or molten particles. As a consequence, these parameters need to be investigated to estimate the impact on the electrical insulating properties of thermally sprayed alumina. This study focuses on the development of a novel electric insulation coating from Al2O3 feedstock powders deposited via atmospheric plasma spray (APS). The microstructure, porosity, and corresponding crystallographic phases have been analyzed with optical microscopy, XRD, and SEM images. To achieve an understanding of the parameters influencing the electrical insulation performance of the manufactured coatings, an in-depth analysis of the fundamental dielectric parameters e.g., DC resistance, breakdown strength, dielectric loss tangent, permittivity is presented. T2 - International Thermal Spray Conference and Exposition 2022 CY - Vienna, Austria DA - 04.05.2022 KW - Thermal Spray KW - Alumina KW - Dielectric properties PY - 2022 SP - 1 EP - 8 AN - OPUS4-55821 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Stamm, Michael T1 - In situ Charakterisierung von Reparaturen in GFK Schalenstrukturen mittels Lockin Thermografie und Felddehnungsmessungen N2 - Die tiefgreifende Reparatur von Faserverbundwerkstoffen stellt durch deren inneren Aufbau eine besondere Herausforderung dar, die unter anderem bei der Instandhaltung von Rotorblättern von Windkraftanlagen zum Tragen kommt. Um die Reparaturen von Rotorblattschalen zu untersuchen und zu optimieren, wurden an der BAM Sandwich-Schalenprüfkörper aus Glasfaserkunststoff (GFK) entwickelt. Nachdem in diese Schalenprüfkörper Modell-Reparaturen eingebracht wurden, werden zyklische mechanische Ermüdungsversuche bis zum Bruch durchgeführt. Vorrangiges Ziel ist es, den Einfluss verschiedener Reparaturvariablen auf die Ermüdungslebensdauer der Struktur zu verstehen, sowie die stabilste Reparaturmethode zu bestimmen. Während der zyklischen Lastversuche wurden regelmäßig in-situ Messungen mit einer Thermografie Kamera und einem optischen Felddehnungsmesssystem durchgeführt. Durch beide Messmethoden lassen sich Eigenschaften der Probekörper zeitlich und räumlich aufgelöst darstellen. Während die Felddehnungsmessungen Aufschluss über die Verformung an der Oberfläche geben, erfasst die thermische Inspektion Temperaturänderungen an der Oberfläche. Besonders die thermografischen Messwerte bilden hier das oberflächennahe Volumen ab, in dem sich Temperaturänderungen an der Oberfläche abzeichnen. Die Messergebnisse beider Systeme stellen also verschiede aber korrelierte Parameter dar. Denn die zyklische Belastung (Bewegung) ruft eine periodische Temperaturänderung im Bauteil hervor. Dieser so genannte Thermoeleastische Effekt kann durch eine Lockin-Analyse der Temperaturtransienten (Temperaturverläufe) nachgewiesen werden. Die räumliche Darstellung der thermischen Effekte lässt Rückschlüsse auf die tatsächliche Lastverteilung im Probekörpervolumen zu. Darüber hinaus führen nichtelastische Verformungen zu einer zusätzlichen Wärmefreisetzung, die durch geeignete Auswerteverfahren ebenfalls nachgewiesen werden können. Entsprechende Hot-Spots in der räumlichen Verteilung erlauben eine frühzeitige Erkennung besonders belasteter Bereiche lange vor dem eigentlichen Bauteil-Versagen. Das gestattet die Lokalisierung des Initial-Schadens, was mit der numerischen Spannungsanalyse korreliert werden kann und die Entwicklung und Bewertung verschiedener Reparaturstrategien. T2 - DGZfP Jahrestagung 2022 CY - Kassel, Germany DA - 23.05.2022 KW - Lockin Thermografie KW - GFK KW - NDT KW - ZfP PY - 2022 AN - OPUS4-55823 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bonse, Jörn T1 - Laser-induced Periodic Surface Structures (LIPSS): Mechanisms, Applications, and unsolved Problems N2 - Laser-induced Periodic Surface Structures (LIPSS, ripples) are a universal phenomenon and can be generated in a contactless, single-step process on almost any type of solid upon irradiation with intense laser pulses. They represent a (quasi-)periodic modulation of the surface topography in the form of a linear grating and are typically formed in a “self-ordered” way in the focus of a laser beam. Thus, they are often accompanying laser material processing applications. The structural sizes of LIPSS typically range from several micrometers down to less than 100 nanometers – far beyond the optical diffraction limit – while their orientations exhibit a clear correlation with the local polarization direction of the laser radiation. From a theoretical point of view, a controversial debate has emerged during the last decades, whether LIPSS originate from electromagnetic effects (seeded already during the laser irradiation) – or whether they emerge from matter-reorganization processes (distinctly after the laser irradiation). From a practical point of view, however, LIPSS represent a simple and robust way for the nanostructuring of solids that allows creating a wide range of different surface functionalities featuring applications in optics, tribology, medicine, energy technologies, etc. While the currently available laser and scanner technology already allows surface processing rates at the m^2/min level, industrial applications of LIPSS are sometimes limited by the complex interplay between the nanoscale surface topography and the specific surface chemistry. This typically manifests in difficulties to control the processing of LIPSS and in limitations to ensure the long-term stability of the created surface functions. This presentation reviews the currently existent theories of LIPSS. A focus is laid on the historic development of the fundamental ideas behind the LIPSS, their corresponding mathematical descriptions and numerical implementations, along with a comparison and critical assessment of the different approaches. Moreover, some unsolved scientific problems related to LIPSS are identified and the pending technological limitations are discussed. Hereby, it is intended to stimulate further research and developments in the field of LIPSS for overcoming these limitations and for supporting the transfer of the LIPSS technology into industry T2 - 10th International LIPSS Workshop 2022 CY - Orléans, France DA - 21.09.2022 KW - Laser-induced periodic surface structures (LIPSS) KW - Surface functionalization KW - Femtosecond laser processing KW - Time-resolved coherent scattering PY - 2022 AN - OPUS4-55814 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -