TY - CONF A1 - Brunner-Schwer, Christian T1 - How innovative welding technology can speed up the wind tower manufacturing process eightfold N2 - In the wind industry, a great deal of welding is required for the manufacture of foundation structures, floating platforms and towers. The poster illustrates how this welding process can be realised much more efficiently with the help of electromagnetic weld pool backing. T2 - Wind Europe Annual Event 2024 CY - Bilbao, Spain DA - 20.03.2024 KW - Schweißen KW - Laserschweißen KW - Windeneergie PY - 2024 AN - OPUS4-60604 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kardjilov, Nikolay T1 - Neutron Thermo Tomography N2 - This study presents an investigation of the neutron transmission signal as a function of martensitic steel sample temperature and phase transformation during a welding process. A theoretical description that includes the Debye-Waller factor was used to describe the temperature influence on the neutron cross-sections. Neutron imaging using a monochromatic beam helps to observe transmission variations related to the martensitic-austenitic phase transformations before the Bragg-edge and to the material temperature above the Bragg-edge. In-situ neutron imaging of welding experiments show the distribution of the phase transformation and of the temperature in bulk steel samples. The performed finite element modelling of expected temperature distributions shows good agreement with the obtained experimental data. T2 - Neutron Wavelength-Dependent Imaging Workshop (NEUWAVE-12) CY - Lund, Sweden DA - 01.09.2024 KW - Neutron Imaging KW - Energy Selective KW - Neutron Thermo Tomography PY - 2024 AN - OPUS4-61265 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Möglichkeiten zur Optimierung von schweißbedingten Beanspruchungen durch Einsatz von LTT-Zusatzwerkstoffen N2 - Der Vortrag gibt einen Überblick zum Thema Low Transformation Temperature (LTT) Zusatzwerkstoffe. Es wird gezeigt, wie mit einem Experiment unter Nutzung von Sychrotronstrahlung das Phänomen der Umwandlungsplastizität untersucht werden kann. T2 - 12. Vollversammlung des SFB 1120: Summer School 2024 CY - Steinfeld (Kall), Germany DA - 11.06.2024 KW - Eigenspannungen KW - LTT-Zusatzwerkstoffe KW - Hochfester Stahl PY - 2024 AN - OPUS4-60259 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Griesche, Axel T1 - Crystallographic phase transformations and corresponding temperature distributions during gtaw of supermartensitic stainless steel visualized by nbei N2 - We investigated the phase transformations during butt-welding of supermartensitic steel plates with help of Neutron-Bragg-Edge Imaging (NBEI). Gas tungsten arc welding (GTAW) was used with a motorized torch allowing for automated weldments. The austenitization in the heat affected zone (HAZ) could be clearly visualized at λ = 0.39 nm, a wavelength smaller than the Bragg edge wavelengths of both austenite and martensite. The re-transformation into the martensitic phase during cooling was clearly detected. However, we observed an unexpected additional change in transmission at λ = 0.44 nm, a wavelength larger than the wavelength of the Bragg edges of both the martensitic and austenitic phases. We attribute this change to the Deybe-Waller-Factor that describes the temperature dependence of coherent scattering at a crystal lattice. The observed two-dimensional attenuation map corresponds well with a temperature distribution modelling by software macros in ANSYS [3]. Here, the absolute temperature values could be achieved by calibrating the modelled attenuation with help of a thermocouple placed at the steel plate. This allows in return for a direct two-dimensional temperature reading based on the Debye-Waller-relation between neutron attenuation and sample temperature. T2 - WCNR-12 CY - Idaho Falls, Id, USA DA - 02.06.2024 KW - Neutron KW - Radiography KW - Welding PY - 2024 AN - OPUS4-60242 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Best practice: How to work with a mobile diffractometer N2 - Beginning with a general overview about resdiual stress determination by X-ray diffraction, the presentation is focussing on some does and dont's when working with a portable diffractometer. T2 - European Conference on Residual Stresses 11 - Tutorial 1: Residual stresses in additive manufacturing CY - Prague, Czech Republic DA - 03.06.2024 KW - Residual stress KW - X-ray diffraction PY - 2024 AN - OPUS4-60287 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Nietzke, Jonathan T1 - Mechanische Eigenschaften von additiv gefertigtem AISI 316L unter Wasserstoffatmosphäre N2 - Wasserstoff führt zu einer Degradation der mechanischen Eigenschaften vieler Stähle. In dieser Arbeit wurde dieser Effekt in additiv hergestelltem AISI 316L (1.4404) mithilfe von in-situ SSRT-Versuchen untersucht. T2 - BMDK / Forschungsseminar Otto-von-Guericke-Universität Magdeburg CY - Magdeburg, Germany DA - 11.12.2024 KW - Wasserstoff KW - AISI 316L KW - 1.4404 KW - SSRT PY - 2024 AN - OPUS4-62166 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Grimault de Freitas, Tomás T1 - Closing the gaps towards the Standardisation of the Hollow Specimen Method for Tests in High-Pressure Hydrogen Gas N2 - Metallic materials, mainly steels, are the most commonly used structural materials in various components throughout the hydrogen supply chain. Ensuring their sustainable and safe use in hydrogen technologies is a crucial factor in the development of the hydrogen economy. This is particularly important since hydrogen can promote crack formation and ultimately lead to premature failure in these materials when combined with mechanical load. This process is commonly known as Hydrogen Embrittlement and can occur in a large number of steels used for the hydrogen technologies.[1] Extensive materials qualification is required for the rapid implementation of hydrogen technologies, however, most accepted, and standardised test methods for determining the effect of gaseous hydrogen on metallic materials describe complex and costly procedures (e.g. in-situ autoclave technique) that are only available to a very limited extent worldwide. The hollow specimen technique is a simple and economical method that has the potential to overcome the limitations of the current methods and complement them for qualifying metallic materials under high-pressure hydrogen gas. Unlike the conventional autoclave technique, this method requires significantly lower amounts of hydrogen, resulting in fewer safety measures and no need for complex equipment or a specialised laboratory. The technique's low investment and testing costs, simple operation, and shorter testing time make it an optimal for widespread use around the world, thereby increasing the output of results. Initial studies have demonstrated the feasibility of assessing hydrogen effects in metallic materials using the hollow specimen technique. This led to the establishment of an ISO committee to standardise the method, however, there are open questions that currently prevent the technique from being standardised for hydrogen testing. These open questions relate to specimen geometry, inner hole surface and gas quality and are being addressed in the TransHyDE - H2HohlZug project. The aim of the project is to systematically address and close the gaps towards the standardisation of this technique for tests in hydrogen. The project is divided into four work packages. First, the elastic-plastic behaviour of a hollow tensile specimen is compared with that of a conventional solid tensile specimen of identical external dimensions using finite element methods (3D-FEM) and subsequently validated by experimental results. In the second, the influence of the inner hole surface quality of the specimen on the hydrogen effects is evaluated. Five different methods of producing the inner axial hole were chosen to ensure different average roughness values and residual stresses (drilling vs. EDM), and also to ensure a good representation of the more common and easily accessible processes (drilling and reaming) to the more complex ones (EDM and honing). Next, the influence of gas purity (different compositions) and purging process (different routines) is evaluated. Finally, an optimal specimen geometry, inner hole production process, gas quality and purging process are proposed from each working package and its reproducibility and repeatability is evaluated in a round robin with national and international partners. This contribution presents the structure and milestones of the project, followed by initial results regarding the influence of different manufacturing and finishing processes on the inner hole surface of the hollow specimen and its response to hydrogen effects. T2 - MPA Seminar 2024 - Materials, Processes, Applications CY - Stuttgart, Germany DA - 08.10.2024 KW - Hydrogen KW - Hydrogen Embrittlement KW - Tensile Test KW - High-Pressure Gaseous Hydrogen KW - Hollow Specimen Technique KW - Standardisation KW - TransHyDE KW - H2HohlZug PY - 2024 AN - OPUS4-61286 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Brunner-Schwer, Christian T1 - Von der Young Professional-Förderung zum Start-up der WeldNova GmbH N2 - Das Unterpulverschweißen (UP) ist das Lichtbogenschweißverfahren mit der höchsten Abschmelzrate. Beim Schweißen von dicken Blechen ist dieses Verfahren jedoch besonders für die Wurzellage von Nachteil. Voll-ständiges Umschmelzen ohne extremen Wurzeldurchhang oder ein Austropfen der Schmelze ist ohne weitere Hilfsmittel schwer zu erreichen. Aus diesem Grund werden Pulver-, Kupfer-, keramische Badstützen oder Ble-che zur Vermeidung des Wurzeldurchhangs verwendet. Bei der Verwendung von Kupfer- oder Keramikstützen beeinflusst beispielsweise die Diffusion chemischer Elemente in die Schweiß- oder Schmelzlinie die mecha-nischen Eigenschaften der Schweißnaht. All diese Badstützen erfordern zusätzliche Schritte zur Vorbereitung und Entfernung sowie zur Reinigung der Schweißwurzel. Die Verwendung einer elektromagnetischen Bad-stütze hat dagegen viele Vorteile. Der Magnet kommt nicht mit dem Werkstück in Kontakt, sodass ein zusätz-licher Schritt des Entfernens nicht erforderlich ist. Versuche mit Laserstrahlschweißen oder Laserhybrid-schweißen haben bereits erstmalig gezeigt, dass Blechdicken bis 30 mm einlagig einseitig geschweißt werden können und zusätzlich ein Spalt oder Kanterversatz von bis zu 2 mm überbrückt werden können. In dieser Arbeit wird die elektromagnetische Badstütze für den UP-Prozess eingesetzt. Die Wurzellage wird an 15 mm dicken Blechen mit einer Spaltgröße von 2 mm geschweißt. Die Verwendung eines elektromagnetischen Sys-tems stellt hier sicher, dass die Schmelze nach oben gedrückt und in Position gehalten wird. Ferner kann die Schweißtiefe entsprechend den magnetischen Parametern angepasst werden. Dieses Verfahren kann die Produktivität im Schweißbereich von vielen Betrieben deutlich steigern und Kosten gleichzeitig senken und kann dazu beitragen, diese Arbeitsplätze in Deutschland zu sichern. T2 - DVS CONGRESS 2024 Große Schweißtechnische Tagung CY - Erfurt, Germany DA - 16.09.2024 KW - Hochleistungs-Lichtbogenschweißen KW - Unterpulverschweißen PY - 2024 AN - OPUS4-62038 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Brunner-Schwer, Christian T1 - Hochleistungslaserhybridschweißen von dickwandigen Stählen – potenzielle Anwendungen in der Windenergieindustrie N2 - Das Laserstrahl-Lichtbogen-Hybridschweißverfahren kombiniert Laserstrahl- und Lichtbogenschweißverfahren in einem gemeinsamen Schmelzbad. Das Verfahren wurde Ende der 70er Jahre entwickelt, um die Synergieeffekte der Schweißprozesse effektiv zu nutzen. Durch die hohe Strahlungsintensität des Laserstrahls werden hohe Einschweißtiefen erreicht. Es ist möglich, die Anzahl der Schweißlagen zu reduzieren und somit die thermische Belastung des Grundwerkstoffes zu senken, da der Wärmeeintrag verringert wird. Die Überbrückung von Spalten und Kantenversatz kann durch die Zufuhr eines geschmolzenen Zusatzdrahtes durch das MSG-Verfahren erreicht werden. Der Zusatzdraht kann zudem das metallurgische Gefüge positiv beeinflussen. Daher ist das Laser-Hybridschweißverfahren ideal für das einlagige Schweißen von Dickblechen und wird bereits erfolgreich in der Schiffbauindustrie zum Schweißen von Blechen mit einer Dicke von bis zu 15 mm verwendet. Obwohl Hochleistungslaser heutzutage bereits im Multi-Kilowatt-Bereich verfügbar sind, sind sie für den industriellen Einsatz nur auf Stahlbleche mit einer Dicke von max. 15 mm geeignet. Hohe Abkühlgeschwindigkeiten, gravitationsbedingtes Austropfen beim einlagigen Schweißen von Dickblechen, Prozessinstabilitäten bei höheren Laserleistungen und Schweißnahtimperfektionen wie Rissbildung sind einige Faktoren, die den Einsatz von Laser-Hybridschweißtechnologien aktuell begrenzen. Ohne eine Badstütze ist eine Verringerung der Schweißgeschwindigkeit und somit der Abkühlgeschwindigkeit aufgrund unzulässiger Wurzelüberhöhungen oder gravitationsbedingtem Austropfen nicht möglich. Bei herkömmlichen Badstützen ist es allerdings erforderlich, dass sie mechanisch befestigt und die Wurzel entfernt oder nachbearbeitet werden muss. In dieser Arbeit wird als Alternative das innovative Konzept der elektromagnetischen Schweißbadsicherung vorgestellt und die Fähigkeiten dieses Verfahrens erläutert. T2 - 21. Tagung Schweißen in der maritimen Technik und im Ingenieurbau CY - Hamburg, Germany DA - 24.04.2024 KW - Schweißen KW - Laserschweißen KW - Behälterbau PY - 2024 AN - OPUS4-62039 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Brunner-Schwer, Christian T1 - Auf dem Weg zum einlagigen Schweißen von dickwandigen Bauteilen – Prozesse, Potenziale, Beispiele N2 - Bislang kommt das Laserstrahlschweißen bzw. Laserhybridschweißen hauptsächlich bei Dickblechen mit einer Wandstärke von bis zu 15 mm zum Einsatz. Für Anwendungen über 20 mm war dieses Verfahren aufgrund einiger Herausforderungen bisher nur bedingt realisierbar. Die von der Ausgründung WeldNova GmbH der Bundesanstalt für Materialforschung und -prüfung (BAM) entwickelte Schweißbadsicherung ermöglicht nun ein einlagiges Schweißen von bis zu 40 mm Wandstärken mit einer Laserleistung von bis zu 20 kW. T2 - 52. Sondertagung Schweißen im Anlagen und Behälterbau 2024 CY - Munich, Germany DA - 12.03.2024 KW - Schweißen KW - Laserschweißen KW - Windeneergie PY - 2024 AN - OPUS4-62042 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Nietzke, Jonathan T1 - H2HohlZug: Standardisation of a New, Cost-effective Method for Material Characterisation for the Hydrogen Economy N2 - The feasibility of the method for slow strain tensile tests has been demonstrated in several studies, leading to the establishment of the ISO/TC 164/SC 1/WG 9 ISO committee for its standardisation. Questions have emerged during this process, that currently prevent the method from being standardised for hydrogen testing. These questions relate to specimen geometry, specimen manufacturing and gas quality and are being systematically addressed in the TransHyDE-H2HohlZug project. T2 - TrasnsHyDE Abschlusskonferenz CY - Berlin, Germany DA - 25.03.2025 KW - Hydrogen KW - Hydrogen Embrittlement KW - High-Pressure Gaseous Gas KW - Hollow Specimen Technique KW - TransHyDE KW - H2HohlZug PY - 2025 AN - OPUS4-62823 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Florian, Camilo T1 - Influence of oxidation in the formation and performance of laser-induced periodic surface structures N2 - The fabrication of laser-induced periodic surface structures (LIPSS) has been reported for metallic, semiconductor and dielectric materials when irradiated with linearly polarized ultrashort laser pulses. Different sets of processing parameters have been identified and extensively studied, allowing the use of LIPSS for applications in medicine, tribology and surface wetting to name a few. One important parameter that is often not considered is the laser-induced oxidation that is produced especially when oxidation prone materials are irradiated in air environment. This surface oxidation can potentially influence the final structures size, shape and orientation and modify their functionality in some specific applications. In this work, we first study the influence of the laser-induced oxidation layer on the formation of LIPSS by characterizing the response of the oxidation prone hard-coating material chromium nitride. Moreover, we employ complementary surface and depth-profiling analytic techniques to reveal morphological, chemical and structural features of different types of surface structures and LIPSS produced on titanium-based substrates. Finite-difference time-domain (FDTD) calculations finally explain how this superficial oxidation layer promotes the formation of a new type of low spatial frequency LIPSS. Also, we measure the depth-extent of the different oxides formed and demonstrate its beneficial influence for friction reduction and wear resistance applications. T2 - SPIE Photonics West Conference, Symposium "Laser-Based Micro- and Nano-Processing XVI" CY - San Francisco, CA, USA DA - 22.01.2022 KW - Laser-induced periodic surface structures (LIPSS) KW - Oxidation KW - Femtosecond laser KW - Laser processing KW - Finite-difference time-domain calculations (FDTD) PY - 2022 AN - OPUS4-54322 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Bonse, Jörn A1 - Spaltmann, Dirk T1 - Editorial: Special issue "Laser-induced periodic surface nano- and microstructures for tribological applications" N2 - Laser material processing is an emerging technology that generates surface functionalities on the basis of optical, mechanical, or chemical properties. In the form of laser surface texturing (LST), it has attracted a remarkable amount of research to tailor surface properties towards various tribological applications. The main advantages of this single-step, laser-based technology are the contactless machining, featuring a high flexibility, efficiency, and speed, along with the excellent quality of the processed products. LST can be applied precisely localized to sub-micrometric areas, but, via laser beam scanning, it is also feasible for structuring large surface areas at the square meter size. This Special Issue focuses on the latest developments concerning the tribological performance of laser-generated periodic surface nano- and microstructures and their applications. This includes the laser-based processing of different surface patterns, such as “self-organized” laser-induced periodic surface structures (LIPSS, ripples), grooves, micro-spikes, hierarchical hybrid nano-/micro-structures, microfeatures generated by direct laser interference patterning (DLIP), or even dimples or other topographic geometries shaped by direct laser modification or ablation. The applications of these periodically nano- and micro-patterned surfaces may improve the lubricated or non-lubricated tribological performance of surfaces in conformal and even non-conformal contact through a reduction of wear, a variation of the coefficient of friction, altered load carrying capacity, etc., resulting in energy saving, improved reliability, increased lifetimes as well as durability, leading in turn to extended maintenance intervals/reduced down-time. This can be beneficial in terms of bearings, gears, engines, seals, cutting tools, or other tribological components. Fundamental aspects addressed may involve the investigation of the relevant physical and chemical effects accompanying the laser-generated nano- and microscale topographies, such as alterations of the material structures, the hardness, superficial oxidation, the role of additives contained in lubricants, surface wettability, micro-hydrodynamic effects, etc. For this Special Issue we aim to attract both academic and industrial researchers and would like to provide a bridge between research in the fields of tribology and laser material processing in order to foster the current knowledge and present new ideas for future applications and new technologies. KW - Laser-induced periodic surface structures (LIPSS) KW - Tribology KW - Applications KW - Wear KW - Friction PY - 2020 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-505948 DO - https://doi.org/10.3390/lubricants8030034 SN - 2075-4442 VL - 8 IS - 3 SP - 34, 1 EP - 34, 3 PB - MDPI CY - Basel AN - OPUS4-50594 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bonse, Jörn T1 - Surface oxidation accompanying the formation of various types of femtosecond laser-generated surface structures on titanium alloy N2 - Different types of laser-generated surface structures, i.e., Laser-induced Periodic Surface Structures (LIPSS, ripples), Grooves, and Spikes are generated on titanium and Ti6Al4V surfaces by means of femtosecond (fs) laser scan processing (790 nm, 30 fs, 1 kHz) in ambient air. Morphological, chemical and structural properties of the different surface structures are characterized by various surface analytical techniques, including scanning electron microscopy (SEM), X-ray diffraction (XRD), Glow discharge optical emission spectroscopy (GD-OES), and depth-profiling Auger electron spectroscopy (AES). It is revealed that the formation of near-wavelength sized LIPSS is accompanied by the formation of a graded oxide extending several tens to a few hundreds of nanometers into depth. GD-OES performed on other superficial fs-laser generated structures produced at higher fluences and effective number of pulses per spot area such as periodic Grooves and irregular Spikes indicate even thicker graded oxide layers. These graded layers may be suitable for applications in prosthetics or tribology. T2 - E-MRS Spring Meeting 2021 CY - Online meeting DA - 31.05.2021 KW - Laser-induced periodic surface structures (LIPSS) KW - Titanium alloy KW - Oxidation KW - Glow-discharge optical emission spectroscopy PY - 2021 AN - OPUS4-52749 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN ED - Bonse, Jörn ED - Spaltmann, Dirk T1 - Laser-induced periodic surface nano- and microstructures for tribological applications N2 - This book is a reprint collection of articles from the Special Issue published online in the open access journal Lubricants. KW - Laser-induced periodic surface structures (LIPSS) KW - Friction KW - Wear KW - Applications PY - 2020 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-516611 UR - https://www.mdpi.com/books/pdfview/book/3130 SN - 978-3-03943-523-4 SN - 978-3-03943-524-1 SP - 1 EP - 180 PB - MDPI CY - Basel AN - OPUS4-51661 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kunz, C. A1 - Bonse, Jörn A1 - Spaltmann, Dirk A1 - Neumann, C. A1 - Turchanin, A. A1 - Bartolomé, J. F. A1 - Müller, F. A. A1 - Gräf, S. T1 - Tribological performance of metal-reinforced ceramic composites selectively structured with femtosecond laser-induced periodic surface structures N2 - The impact of femtosecond (fs) laser-induced periodic surface structures (LIPSS) on tribological properties was investigated for metal-reinforced ceramic composites (Al2O3-ZrO2-Nb). For this purpose, the metallic niobium (Nb) phase was selectively structured with LIPSS in an air environment with different values of the fs-laser peak fluence by near-infrared fs-laser radiation (λ = 1025 nm, τ = 300 fs, frep = 1 kHz), taking advantage of the different light absorption behavior of ceramic and metal. The tribological performance was evaluated by reciprocating sliding tests in a ball-on-disc configuration using Ringer's solution as lubricant. The surfaces were characterized before and after laser irradiation by optical microscopy, scanning electron microscopy, atomic force microscopy, X-ray photoelectron spectroscopy, energy dispersive X-ray spectroscopy and by measuring the contact angle with Ringer's solution. The LIPSS formation resulted in an increased wetting of the surface with the lubricant. Moreover, the selectively structured composite surfaces revealed a coefficient of friction significantly reduced by a factor of ~3 when compared to the non-irradiated surface. Furthermore, the formation of a laser-induced oxidation layer was detected with NbO as the most prominent oxidation state. Selectively structured composites with outstanding mechanical properties and enhanced tribological performance are of particular interest for biomedical applications. KW - Laser-induced periodic surface structures (LIPSS) KW - Femtosecond laser ablation KW - Ceramic matrix composites KW - Tribology PY - 2020 DO - https://doi.org/10.1016/j.apsusc.2019.143917 SN - 0169-4332 SN - 1873-5584 VL - 499 IS - 1 SP - 143917 PB - Elsevier B.V. CY - Amsterdam AN - OPUS4-49255 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Nietzke, Jonathan A1 - Konert, Florian T1 - Experimental and numerical characterization of hydrogen diffusion in thick-walled submerged arc welded joint of S420G2+M offshore steel grade N2 - Offshore wind turbines are an important goal in national energy strategies worldwide. Foundation structures are manufactured from submerged arc welded (SAW) plates with thicknesses up to 200 mm. In that connection, high-strength steels like the S420G2+M are more and more applied offering the possibility for increased stability and load-bearing capacity of the foundations. These offshore steel grades can show a susceptibility for delayed hydrogen assisted cold cracking of the weld joints. For that purpose, a minimum waiting time (MWT) of up to 48 h (dependent on applied standards) is recommended before non-destructive testing is allowed and conducted. But this concept is based on older steel grades that have been used for three or more decades. Nowadays, the metallurgical improvements (clean steels, proper rolling, and heat treatment) of base materials and well as welding consumables must be anticipated. Hence, the MWT concept should be critically discussed as it is assumed to be very conservative. For that reason, the focus of this study was to investigate the diffusion behavior in S420G2+M steel and its multi-layer SAW joint. Electrochemical permeation experiments were carried at room temperature. Boundary conditions were anticipated in terms of using different sample thicknesses. From the experimental data, hydrogen diffusion coefficients and absorbed diffusible hydrogen concentrations had been calculated. It was shown that hydrogen diffusion in the base material is increased compared to the weld metal. In addition, the sample thickness had a significant on the calculated diffusion coefficients. The minimum and maximum diffusion coefficients had been used for numerical modelling of the hydrogen diffusion in the welding joint. It became clear that a MWT must be always regarded together with a critical initial diffusible hydrogen concentration for the evaluation of a possible delayed cracking as diffusion times were mostly > 48 h due to the thick plates. T2 - 4th International Conference on Metals and Hydrogen - Steely & Hydrogen 2022 CY - Ghent, Belgium DA - 11.10.2022 KW - Hydrogen KW - Submerged arc welding KW - Minimum Waiting Time KW - Cold Cracking KW - Offshore steel grade PY - 2022 AN - OPUS4-56008 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - LTT-Zusatzwerkstoffe zur Optimierung von Schweißeigenspannungen N2 - Der Vortrag gibt eine Einführung zum Thema LTT-Zusatzwerkstoffe. Anhand experimenteller Befunde werden die Mechanismen erläutert und die Auswirkungen auf die Schweißeigenspannungen verdeutlicht. T2 - 1. LTT-Workshop des ISF RWTH Aachen CY - Aachen, Germany DA - 11.05.2022 KW - LTT-Zusatzwerkstoff KW - Hochfester Stahl KW - Eigenspannungen KW - Martensit KW - Phasenumwandlung PY - 2022 AN - OPUS4-56267 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Griesche, Axel T1 - The debye waller factor for temperature distribution determination in NBEI experiments: a case study for GTAW N2 - We could show in GTAW experiments with steel samples that the attenuation of neutron transmission underneath the welding torch due to the Debye-Waller-effect correlates well with sample temperatures obtained by FE numerical simulations. This would allow principally to determine sample temperatures by measuring the neutron beam attenuation. T2 - ITMNR-9 CY - Buenos Aires, Argentina DA - 17.10.2022 KW - Debye waller factor KW - GTAW KW - Temperature distribution determination PY - 2022 AN - OPUS4-56150 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael T1 - Repair welding of pressurized in-service hydrogen pipelines - A review on current challenges and strategies N2 - As energy carrier of the future, green hydrogen can make a decisive contribution to a sustainable energy supply. Particularly important is the decarbonization of heavy industry. Therefore, a reliable supply of hydrogen must be guaranteed. A hydrogen pipeline grid can achieve this purpose. In Europe concrete plans for a hydrogen pipeline grid already exist, as the so called “European Hydrogen backbone”. As building a completely new pipeline grid is economically not justifiable, a dual-way strategy of repurposing natural gas (NG) pipelines and newly built pipelines is intended. Long distance pipeline grids require regular maintenance and repairs. For natural gas (NG) pipelines in-service welding is state of the art. Concepts such as hot-tapping (drilling into pressurized pipelines) and “stoppling” (sealing off pipeline sections after installing bypasses or pressure relieves) allow the repair of damaged pipeline sections or the installation of new branches without shutting the pipeline down, which in most cases isn’t possible from an economic standpoint. The EIGA 121/14 guideline already pointed out in 2014 that “a hydrogen hot-tap shall not be considered a routine procedure”. This shows that the determination of the transferability of these repair concepts to hydrogen pipelines is of utmost importance. Due to the degrading effects of hydrogen on mechanical proper-ties, commonly referred to as “hydrogen embrittlement” it is necessary to understand and investigate the occurring effects. In the special case of repair welding on in-service hydrogen pipelines an increased hydro-gen uptake due to a large heat input and microstructural changes in the material needs to be considered. Therefore, material degradation must be investigated to determine whether modifications of repair procedures are necessary to ensure a reliable and safe hydrogen transportation via pipelines. For this reason, this paper gives an overview on existing weld repair concepts and its risks and limitations in terms of hydrogen absorption and possible embrittlement effects when transferred to hydrogen pipelines. The complexity lies in a large variety of materials (low alloyed steels), pipeline diameters and corresponding welded joints. The material compatibility of materials in used (repurposed NG-pipelines) and new condition must be investigated. Particularly for repurposed/used pipelines the effect of a pre-matured/corroded inner surface and sometimes insufficient documentation of the material “history” needs to be considered. An overview on ongoing and completed R&D-projects with respect to repair concepts for hydrogen pipelines and hydrogen effects on pipeline materials is given. The focus hereby lies on possible methods of material testing and modeling. Its current difficulties, limits and possible solution will be discussed. T2 - IIW Intermediate Meeting, Com. II-A CY - Incheon, Republic of Korea DA - 12.03.2024 KW - Hydrogen KW - Repair welding KW - Pipelines KW - In-service PY - 2024 AN - OPUS4-59674 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael T1 - Combined effect of heating rate and restraint condition on stress relief cracking susceptibility during PWHT of thick-walled Cr-Mo-V steel submerged arc welded joints N2 - Contemporary steels creep-resistant steels like the 13CrMoV9-10 are used as thick plates e.g., for applications in hydrocrackers. The large plate thickness requires high efficiency welding processes like submerged arc welding (SAW) and a mandatory post weld heat treatment (PWHT). The PWHT-parameters stem from a combination of empirical knowledge and traditional experiments on free shrinking (FS) welds. In that connection, the formation of so-called stress-relief cracking (SRC) must be anticipated. The SRC susceptibility of a welded component is a complex combination and interaction of com-ponent specific, thermal, and metallurgical factors. Many of which have to date not been conclusively researched. For example, it is well known that SRCs develop during PWHT due to formation and growth of carbides on prior austenite grain boundaries, resulting in a significant hardness increase (secondary hardening) and toughness decrease. This leads to a high SRC susceptibility of the coarse grain heat-affected zone (CGHAZ) of the last weld bead during PWHT. This is intensified in case of high residual stresses from the component-specific, structurally induced stiffness. In combination with multi-layer welding this leads to a multiaxial stress distribution. Nonetheless, the combined effect of PWHT and high-residual stresses on the SRC formation is merely unknown. For that reason, this study presents the effect of different heating rates in conjunction with a certain component stiffness. For that reason, SAW joints of 13CrMoV9-10 steel were investigated under FS and defined external restraint condition. T2 - IIW Intermediate Meeting, Com. II-A CY - Incheon, Republic of Korea DA - 12.03.2024 KW - Stress relief cracking KW - Welding KW - Post weld heat treatment KW - Submerged arc welding KW - Cr-Mo-V steel KW - Creep-resisting steel PY - 2024 AN - OPUS4-59673 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael A1 - Kannengießer, Thomas T1 - Call for interested people to contribute to series of comprehensive papers on welding and joining of components for sustainable energy systems N2 - Joining and welding technologies are of high importance for the manufacturing of components and parts used in sustainable energy generation, conversion, and transport. In that connection, offshore and on-shore installed wind turbines are of high interest for the generation of electrical energy as well as photo-voltaic systems (solar cells). The electricity can be either directly transported or conversed via power-to-gas e.g., to hydrogen. In that scope, electrolyzer up to MW-range are of interest as well as the conver-sion back to electricity via fuel cells. In addition, hydrogen is a key element of the decarburization of in-dustries as well as the mobility sector encompassing sea, air and land transportation driven by hydrogen or its derivates. Well-known examples cover the direct reduction of iron ore to replace the conventional blast furnace process up to gas turbines or fuel cells for home-end use. All mentioned technologies re-quire reliable components, which are to a high extend dependent on joining and especially welding pro-cessing of materials. Especially, the (petro-) chemical industry has many years of experience with both materials used in hydrogen applications. The challenge is e.g., the transition to mass production of sys-tem components of electrolyzers/fuel cells and for distribution grids. At this point, the scalability of cur-rently applied joining processes often limits the economic efficiency, whereas especially laser welding or additive manufacturing will be of high interest. In that connection, it is very important to provide answers by joint research of universities, institutes, and industrial companies. Very often, solutions are already available and “just” have to be investigated and adapted for the new application, like repair welding of NG pipelines. For that reason, we want to set up a series of comprehensive papers with the aforementioned title. The idea is to get an in-depth but manageable overview of the importance of joining technologies in sustaina-ble energy generation, conversion, and transport encompassing current processes, limitations, and fur-ther perspectives. In that connection, the additive manufacturing is gaining more and more attention. If applicable, current challenges in the adaption or creation of new standards/regulations shall be addressed. T2 - IIW Intermediate Meeting, Com. II-A CY - Incheon, Republic of Korea DA - 12.03.2024 KW - Hydrogen KW - Welding KW - Comprehensive study KW - Component manufatcturing KW - Additive manufacturing PY - 2024 AN - OPUS4-59676 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Liepold, Philipp T1 - CTS Testing of High-Strength Filler Materials N2 - Controlled Thermal Severity (CTS) tests are known for applicatying high restraint intensity to fillet welds. Due to two different variations of the test it was possible to apply different amounts of restraint intensity to high-strength GMAW fillet welds at a high level of restraint. The results show the effect of heat input, filler material and restraint intensity on solidification cracking susceptibility. T2 - DIN Sitzung NA 092-00-05 GA „Zerstörende Prüfung von Schweißverbindungen“ (DVS AG Q 4/Q 4.1) CY - Berlin, Germany DA - 20.03.2024 KW - CTS PY - 2024 AN - OPUS4-59773 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Eigenspannungsabbau mittels LTT - Schweißzusätzen unter Berücksichtigung der Nahtgeometrie N2 - Der Vortrag befasst sich mit der gezielten Einbringung zusätzlicher LTT-Lagen zur Erzeugung von Druckeigenspannungen in ermüdungskritischen Bereichen von konventionellen Schweißverbindungen. Dies ermöglicht eine wirtschaftliche Lösung, ohne die Integrität der Schweißverbindungen zu beeinträchtigen. Dazu wurden Längssteifen aus hochfestem Stahl in der ersten Lage mit konventionellem Schweißzusatzwerkstoff mittels Metall-Lichtbogenschweißen geschweißt. Anschließend wurde ein Chrom-Nickel-legierter LTT-Schweißzusatz auf die Stirnseiten der Steifen aufgebracht. Durch Variation der Schweißparameter konnten verschiedene Schweißnahtgeometrien des LTT-Zusatzwerkstoffs analysiert werden. T2 - NA 092-00-05 GA "Gemeinschaftsarbeitsausschuss NAS/NMP: Zerstörende Prüfung von Schweißverbindungen (DVS AG Q 4/Q 4.1) CY - Berlin, Germany DA - 20.03.2024 KW - LTT KW - Eigenspannungen KW - hochfester Stahl PY - 2024 AN - OPUS4-59752 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Investigation of hot cracking susceptibility via Modified Varestraint Transvarestraint testing of high-strength filler material N2 - MVT testing was conducted in Transvarestraint mode in multiple welding conditions and under a range of bending speeds. The materials observed were high strength filler metals used in GTAW namely DIN EN ISO 16834-A G 69 4 M21 Mn3Ni1CrMo (G69), 16834-A G 89 6 M21 Mn4Ni2CrMo (G89 6), 16834-A G 89 5 M21 Mn4Ni2,5CrMo (G89 5) and a filler wire 18276-A T 89 4 ZMn2NiCrMo M M21 1 H5 (T89). For evaluation light optical microscope pictures were used. Pixels containing cracks were manually segmented using a self-written program. Out of the segmented images data including crack length, position and area can be calculated for every crack. The results show dependencies of solidification cracking on the test parameters. T2 - IIW Intermediate Meeting Comission II-C CY - Incheon, Republic of Korea DA - 12.03.2024 KW - Solidification cracking KW - High strength steel KW - Varestraint test PY - 2024 AN - OPUS4-59749 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schröder, Nina T1 - Ti and Nb influence on the HAZ microstructures of weld-simulated high strength structural steel S690QL N2 - High-strength low-alloyed (HSLA) steels with yield strength / proof stress ≥ 600 MP are the basis of modern light-weight steel constructions. Indeed, the economic and ecological benefits strongly depend on their processability in terms of welding. In this context, he use of highly productive welding processes, suitable welding consumables is of vital interest and requires a fundamental understanding of the microstructural changes in the HSLA steel and especially the heat-affected zone (HAZ) of the welded joint. Microalloying elements, such as Ti or Nb, are essential to achieve the desired mechanical properties. In this context, the underlying standards such as EN 10025-6 only specify maximum values, resulting in different manufacturer customized microalloy concepts. Furthermore, even small deviations can have a drastic effect expressed by an excessive hardening or softening despite identical welding conditions and filler metal. The reason is the different thermal stability of the Ti and Nb-related precipitates (typically carbides or carbon nitrides). As a result, it is difficult (or even impossible) to adequately predict the weldability. Against this background, different microalloying routes with varying Ti and Nb contents for a S690QL reference grade were systematically investigated in terms of lab-cast alloys close to realistic chemical compositions. To investigate the influence of the welding heat input on the HAZ microstructure formation, physical simulations were carried with specified peak temperatures and cooling times (by a dilatometer, see Fig. 1a). The focus was the identification of the occurring phase transformations during cooling and the final HAZ microstructure, see Fig. 1b. In this context, a double welding cycle was simulated to further identify the behavior of the so-called intercritical HAZ (where softening is likely to occur) in case of the common multi-layer welding for thick plates, see Fig. 1c. The results showed: (1) microalloying has significant influence on the formation of the individual HAZ dependent on (2) the thermal stability of the Ti or Nb-precipitates and (3) synergistic effects of further elements such as Mo and their effect on phase transformations in the HAZ. The results represent a microstructure-based validation of welding processing of such HSLA-steels e.g. in terms of preferred microalloy and weld heat input combinations. T2 - MaterialsWeek/SteelInnovation 2025 CY - Frankfurt am Main, Germany DA - 02.04.2025 KW - HSLA KW - Dilatometry KW - Microalloying elements KW - HAZ-Softening KW - Digital Image Correlation (DIC) PY - 2025 AN - OPUS4-62938 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael T1 - Simulation der Wasserstoffverteilung in UP-geschweißten Grobblechen als Bewertungstool für die Kaltrissanfälligkeit von Offshorestrukturen N2 - Gründungsstrukturen für Offshore-Windkraftanlagen bestehen in der Regel aus hochfesten Stahlgrobblechen, die im UP-Verfahren geschweißt werden, durch den u.U. größere Mengen an Wasserstoff eingebracht werden können. Die große Blechdicke führt zudem zu langen Diffusionswegen und einer verlängerten Diffusionszeit für den Wasserstoff. Infolgedessen kann sich der Wasserstoff in Bereichen mit hoher mechanischer Spannung und Dehnung ansammeln und daher zu einer verzögerten Kaltrissbildung führen. Aufgrund der verzögerten Diffusion muss daher eine Mindestwartezeit von bis zu 48 h eingehalten werden, bevor eine zerstörungsfreie Prüfung durchgeführt wird. Darüber hinaus ist die Beurteilung möglicher Kaltrissstellen sehr komplex. Es wurde daher ein numerisches Modell zur Abbildung einer bauteilähnlichen Schweißnahtprüfung entwickelt. Dazu wurde das Temperaturfeld während des Schweißens und der anschließenden Abkühlung experimentell bestimmt und numerisch simuliert. Auf dieser Grundlage wurde Diffusionsmodell zur numerischen Simulation der zeitlich-örtlichen Wasserstoffkonzentration erstellt. Mit diesem Modell wurden zwei Anwendungsfälle simuliert: (1) Veränderung der Wasserstoffverteilung als Funktion des Temperaturzyklus während des Mehrlagenschweißens und (2) für das Wartezeitintervall ≤ 48 h. Ein Vorteil des Diffusionsmodells ist die Simulation einer normierten Konzentration, d.h. zwischen „0“ (kein Wasserstoff) und „1“ (max. Konzentration), die auf experimentell ermittelte Wasserstoffkonzentrationen skaliert werden kann. T2 - 6. Symposium Materialtechnik CY - Clausthal-Zellerfeld, Germany DA - 20.02.2025 KW - Gründungsstrukturen KW - Offshore KW - Kaltrissbildung KW - Wasserstoff KW - Numerische Simulation PY - 2025 AN - OPUS4-62616 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hübner, Martin A1 - Reichel, Levin A1 - Schröpfer, Dirk A1 - Kromm, Arne A1 - Kannengießer, Thomas T1 - Modern welding processes for optimising repair welds on high strength offshore steels N2 - The successful energy transition in Germany will require offshore wind turbines with outputs >10 MW in the future. To achieve these high outputs, turbines far from coast are required with large subsea jacket structures (30 m up to 50 m) and tall towers (up to 200 m). High-strength steels with a yield strength up to 500 MPa and wall thicknesses up to 150 mm are increasingly being used for these structures. This plac-es high demands on welding manufacturing, especially for high-strength offshore steels. During the manu-facturing process detected defects by NDT require localized repair of welds by gouging and rewelding. Due to a lack of investigations, there are no repair concepts and information in standards and guidelines, par-ticularly for high-strength thick plate joints made of high-strength offshore steels. However, these are ur-gently needed to enable manufacturers, especially SMEs, to carry out safe and economical repairs. There-fore, BAM started the FOSTA project P1629 (IGF 01IF22746N) to investigate the stress-optimized repair (local gouging and welding) of high-strength thick plate joints made of offshore grades in the yield strength range off 355 to 460 MPa and similar weld metal with controlled high-performance GMAW pro-cesses and optimized narrow gouging grooves. The experimental analyses take into account the complex interaction of process, material, and design-related influences on the formation of weld induced stresses and the special microstructure of high-strength fine-grain structural steels. Welding-related material degra-dation and crack-critical residual tensile stresses need to be avoided to ensure high component safety and performance. A reduction in residual stress in the presence of high restraint conditions can be achieved by adapted heat control (if no disassembly measures are possible). The repair process involves manual thermal gouging, which allows the groove configuration to be modi-fied. Modern welding processes using high frequency arc control provide deep root penetration and focused energy input capable of welding narrow seams. A comparison was made between the traditional weld con-figuration with a wide 45° groove and transition arc welding and a narrow 30° groove with modern welding process. Even in the case of free shrinkage specimens, the narrow groove weld exhibits a significant reduc-tion of residual stresses, cf. Figure 1, especially in the HAZ and toward the adjacent base material. This can be attributed to the lower weld metal volume needed and the reduction of heat input per layer due to the controlled arc process. For the purposes of this comparison, the same weld seam build-up (but different number of layers) has been applied to both seam configurations. Note that in industrial application (manu-al welding), the wider groove would be welded with several off-center weld beads with conventional weld-ing process. In this analysis this would cause asymmetric effects regarding the residual stress state, diffi-cult to compare to each other. Component-related welding experiments on special testing equipment, adapted process and heat control concepts along with variable groove configurations will be developed and recommendations for guidelines elaborated. This is the prerequisite for fully utilizing the strength potential of high-strength steels and making a valuable contribution to the energy transition in Germany, especially for steel-processing SMEs. T2 - IIW Intermediate Meeting CII CY - Trollhättan, Sweden DA - 10.03.2025 KW - Repair welding KW - Gouging KW - Residual stress KW - Offshore wind turbines KW - High-strength steels PY - 2025 AN - OPUS4-62743 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hübner, Martin A1 - Kromm, Arne A1 - Kannengießer, Thomas A1 - Dittmann, Florian A1 - Varfolomeev, Igor T1 - Untersuchung der Ermüdungsfestigkeit von LTT-geschweißten Längssteifen mit variierender Nahtausführungen N2 - Low Transformation Temperature (LTT) Schweißzusätze erzeugen während der Abkühlung Druckeigenspannungen in die Schweißnaht und Wärmeeinflusszone durch eine Volumenexpansion, wodurch die Ermüdungsfestigkeit erhöht werden kann. Um das Potential dieser neuartigen Schweißzusätze besser zu quantifizieren, wurden konventionelle Längssteifen als Probenkörper verwendet, welche an den Stirnseiten mit einer LTT-Zusatznaht geschweißt wurden. Durch Variation der Schweißparameter konnten unterschiedliche Nahtformen realisiert werden. Es konnte, je nach Nahtausführung, eine Erhöhung der Ermüdungsfestigkeit bei 2 Millionen Lastwechsel von 64 MPa bis 100 MPa in Gegensatz zu konventionellen Proben festgestellt werden. Somit sind LTT-Zusätze grundsätzlich geeignet, um die Ermüdungsfestigkeit zu erhöhen. T2 - Frühjahrssitzung 2025 des Fachausschusses Eigenspannungen der AWT CY - Karlsruhe, Germany DA - 07.04.2025 KW - LTT (Low Transformation Temperature) KW - Eigenspannungen KW - Ermüdungsfestigkeit KW - Aufmischung PY - 2025 AN - OPUS4-62930 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hübner, Martin A1 - Kromm, Arne A1 - Kannengießer, Thomas A1 - Dittmann, Florian A1 - Varfolomeev, Igor T1 - Wechselwirkung zwischen Nahtgestaltung und Ermüdungsfestigkeit in LTT-geschweißten Längssteifen N2 - Schweißzusätze mit niedriger Martensitstarttemperatur (Low Transformation Temperature, LTT) induzieren während der Abkühlphase infolge einer volumeninduzierten Martensitumwandlung Druckeigenspannungen in der Schweißnaht sowie in der angrenzenden Wärmeeinflusszone (WEZ). Diese Spannungen können zu einer signifikanten Erhöhung der Ermüdungsfestigkeit führen. Zur quantitativen Bewertung des Potenzials dieser innovativen Werkstoffe wurden konventionelle Längssteifen als Versuchsproben herangezogen, bei denen an den Stirnseiten Schweißnähte unter Verwendung von LTT-Zusatzwerkstoffen appliziert wurden. Durch gezielte Variation der Schweißparameter konnten unterschiedliche Nahtgeometrien realisiert werden. In Abhängigkeit von der Nahtausführung zeigte sich bei einer Belastungszahl von 2 Millionen Zyklen eine Steigerung der Ermüdungsfestigkeit im Bereich von 64 MPa bis 100 MPa im Vergleich zu Referenzproben mit herkömmlichen Schweißzusätzen. Die Ergebnisse belegen, dass der Einsatz von LTT-Schweißzusätzen grundsätzlich geeignet ist, die Ermüdungsfestigkeit geschweißter Strukturen zu verbessern. T2 - Din Sitzung: Gemeinschaftsarbeitsausschuss NAS/NMP, Zerstörende Prüfung von Schweißverbindungen CY - Online meeting DA - 20.03.2025 KW - LTT (Low Transformation Temperature) KW - Eigenspannungen KW - Ermüdungsfestigkeit KW - high-strength steels PY - 2025 AN - OPUS4-62929 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Fey, Gero T1 - Dilatometer-based welding simulation: CCT-Diagram and investigation of heat-affected zones in pipeline steels N2 - Presentation of the research project “Hydrogen-dependent mechanical properties of the weld microstructure of low-alloy steels for long-distance gas pipelines” and the present results at the Young Professionals International Conference (YPIC) of the International Institute of Welding (IIW) T2 - 2nd Online Young Welding Professional International Conference - YPIC2025 CY - Online meeting DA - 06.02.2025 KW - Pipeline steel KW - CCT KW - Dilatometry KW - Heat-affected zone PY - 2025 AN - OPUS4-62583 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Fey, Gero T1 - Dilatometerbasierte Schweißsimulation: ZTU-Diagramme und Untersuchung der Wärmeeinflusszonen in Pipelinestählen N2 - Präsentation des Forschungsprojekts "Wasserstoffabhängige mechanische Eigenschaften der Schweißnahtgefüge niedriglegierter Stähle für Ferngasleitungen" und der bisherigen Ergebnisse auf der 28. Konferenz aller Werkstofftechnischen und Materialwissenschaftlichen Studiengänge (KaWuM) an der TU Ilmenau. T2 - 28. Konferenz aller Werkstofftechnischen und Materialwissenschaftlichen Studiengänge CY - Ilmenau, Germany DA - 07.11.2024 KW - ZTU-Diagramm KW - Wärmeeinflusszone KW - WEZ KW - Dilatometer KW - Pipelinestahl PY - 2024 AN - OPUS4-62418 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael T1 - Fügetechnik für Wasserstofftechnologien: Ausgewählte Themen und Herausforderungen N2 - Die Präsentation fasst die Bedeutung der Fügetechnik für Wasserstofftechnologien im Rahmen der Arbeiten für einer Studie (DVS-Berichte Nr. 373) mit besonderer Berücksichtigung der Normung und Regelwerkssetzung zusammen. T2 - Sitzung des DIN-Gemeinschaftsarbeitsausschusses NA 092 00 05 GA, NAS/NMP: Zerstörende Prüfung von Schweißverbindungen CY - Online meeting DA - 10.03.2022 KW - Wasserstoff KW - Fügetechnik KW - Schweißen KW - Wasserstofftechnologien KW - Bedeutung PY - 2022 AN - OPUS4-54447 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael T1 - Reliable hydrogen determination in metallic materials and their weld joints: Parameters and challenges N2 - In the course of tomorrow's hydrogen-based energy transition, the construction of the corresponding infrastructure will play a central role. The majority of materials used to date are typically welded for component fabrication. In that context, steels are widely applied and can be prone to hydrogen embrittlement. This includes the classical delayed cold cracking during welding processing as well as embrittlement phenomena during operation. For the evaluation of any hydrogen effect on, for example, the mechanical properties of a welded metallic material, the hydrogen content must be precisely determined. In the case of welds, for example, according to ISO 3690, this is the isothermal carrier gas hot extraction (CGHE). CGHE is based on accelerated hydrogen degassing due to thermal activation of hydrogen at elevated temperatures. In addition to the pure quantification of hydrogen, thermal desorption analysis (TDA) with varied heating rates can be used to determine and evaluate the bonding state at microstructural defects in the material. For both techniques, experimental and measurement influences have to be considered, which have a great effect on the result. For CGHE, for example, ISO 3690 suggests different sample geometries as well as minimum extraction times. The present study summarizes results and experiences of numerous investigations with different sample temperatures and geometries (ISO 3690 type B and cylindrical TDA samples) regarding: the influence of the sample surface (polished/welded), measurement accuracies depending on the sample volume as well as the insufficient monitoring of the effect of the PI controller on the extraction temperature. In particular, a deviating extraction temperature to the set temperature, can significantly falsify the measurement results. Based on the results, methods are shown to quickly reach the desired extraction temperature without having to physically interfere with the measurement equipment. This serves to substantially improve the reliability of hydrogen measurement through increased signal stability and accelerated hydrogen desorption. In general, an independent temperature measurement with dummy samples for the selected heating procedure is advisable to exclude possible unwanted temperature influences already before the measurement. In addition (and way more important), the methods described can be transferred directly to industrial applications. T2 - 47th MPA-Seminar CY - Stuttgart, Germany DA - 10.10.2023 KW - Hydrogen assisted cracking KW - Carrier gas hot extraction KW - Welding KW - ISO 3690 KW - Metals PY - 2023 AN - OPUS4-58677 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Engelking, Lorenz T1 - Herstellung beanspruchungsgerechter Oberflächen durch Kombination innovativer additiver und abtragender Fertigungsschritte an hochbelasteten Komponenten N2 - In vielen Anwendungen werden aufgrund zunehmender Anforderungen an den Widerstand gegenüber hohen, kombinierten mechanischen, tribologischen, thermischen und korrosiven Beanspruchungen Hochleistungsle¬gierungen eingesetzt. Den vielfach komplexen Bauteilstrukturen, herausfordernden Fertigungseigenschaften und der Erhöhung der Ressourceneffizienz lässt sich heute mit der additiven Fertigung (AM) begegnen, dem oftmals noch unzureichende Kenntnisse über die resultierende Homogenität und Anisotropie der speziellen Gefüge und den damit verbundenen Eigenschaften entgegensteht. Viele Anwendungen benötigen zudem definierte Oberflächen mit hohen Anforderungen an die Oberflächenintegrität, dem durch komplementären Einsatz von additiven und abtragenden Fertigungsschritten Rechnung getragen wird. Hochleistungslegierungen auf der Basis von Nickel oder Kobalt sind infolge der niedrigen Wärmeleitfähigkeit verbunden mit hoher Festigkeit und Zähigkeit äußerst herausfordernd mit Blick auf eine wirtschaftliche Zerspanung mit geometrisch bestimmter Schneide. Ein Vorhaben (IGF-Nr. 20.979 N/DVS-Nr. 1.3211) der BAM und TU Clausthal/ISAF befasst sich mit der Lösung dieser Problemstellung durch gezielte Beeinflussung des Gefüges mittels Modifikation der Schweißzusatzwerkstoffe und den Einsatz des ultraschallunterstützten Fräsens (US), bei gleichzeitiger Sicherstellung der geforderten Eigenschaften der untersuchten Werkstoffe. Es werden die Ergebnisse der Mikrostruktur und der Zerspanbarkeit der Modifikationen der MSG-Schweißung der FeNi36-Referenzlegierung mit 0,4 Gew.-% Zr und der Modifikationen der MSG-Schweißung der CoCr-Referenzlegierung mit 1 Gew.-% Zr sowie Hf vorgestellt. Abschließend werden aus den Ergebnissen Handlungsempfehlungen abgeleitet. T2 - Sitzung der Arbeitsgruppe (AG) V 12 „Additive Fertigung“ CY - Online meeting DA - 15.11.2023 KW - Legierungsmodifikation KW - Ultraschallunterstütztes Fräsen KW - Additive Fertigung KW - Oberflächenintegrität PY - 2023 AN - OPUS4-58859 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hübner, Martin T1 - Hybrider Einsatz von LTT-Schweißzusatzwerkstoffen N2 - LTT (Low Transformation Temperature) - Schweißzusätze stellen eine Alternative zur Verfügung, um die Schwingfestigkeit in Schweißnähten zu erhöhen. Ziel dieses Vortages ist es zum einem die Thematik der LTT - Schweißzusätze, insbesondere in hybrider Ausführung zu erläutern, Zum anderen werden die Ergebnisse der Vorversuche präsentiert. T2 - BMDK CY - Magdeburg, Germany DA - 25.10.2023 KW - LTT (Low Transformation Temperature) KW - Martensitstarttemperatur KW - Baustähle KW - Eigenspannungen KW - Aufmischung PY - 2023 AN - OPUS4-58690 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael A1 - Kannengießer, Thomas T1 - Fügetechnik in Wasserstofftechnologien - Forschungsbedarf für die Branche (Kurzversion) N2 - Die Studie gibt einen kurzen Überblick über die jetzige Bedeutung der Fügetechnik in Wasserstofftechnologien und über zukünftige Forschungsbedarfe für die Branche in den einzelnen Technologiefeldern Wasserstofferzeugung, -speicherung, -transport und -nutzung. Fügetechnologien haben dabei wesentliche Bedeutung für die erfolgreiche Umsetzung von technischen Komponenten der Wasserstofftechnologien. Die Schwerpunkte bzw. Forschungsbedarfe ergeben sich bspw. durch die Erstellung neuer Infrastruktur für Wasserstoffspeicherung und -transport sowie durch Umnutzung der bestehenden Erdgasinfrastruktur. Bei der Wasserstofferzeugung und -anwendung wird z.B. die Entwicklung effiziente Massenproduktionsmethoden von Elektrolyseuren und Brennstoffzellen einen wichtigen Meilenstein bilden und laserbasierte Fügetechnologien sind hier zum Teil schon etabliert. Die additive Fertigung nimmt dabei eine Querschnittsposition ein und besitzt hohes Anwendungspotential für die Zukunft z.B. für die Fertigung von Komponenten in Gasturbinen. Aus den technischen Fragestellungen und Forschungsbedarfen ergeben sich zudem Herausforderungen für die notwendige Neu- und Weiterentwicklung von technischen Regelwerken und Normen und den Eingang in die Aus- und Weiterbildung von fügetechnischem Fachpersonal. T2 - DVS Congress 2021 CY - Online meeting DA - 14.09.2021 KW - Wasserstoff KW - Fügetechnik KW - Forschung KW - Werkstoff KW - Bedarf PY - 2021 SN - 978-3-96144-146-4 VL - 371 SP - 612 EP - 624 PB - DVS Media GmbH CY - Düsseldorf AN - OPUS4-53370 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schröder, Nina A1 - Rhode, Michael A1 - Kannengießer, Thomas T1 - Experimentelle Bestimmung und thermodynamische Modellierung des Ausscheidungsverhaltens in der WEZ eines S690QL bei unterschiedlichen Mikrolegierungsrouten N2 - Für eine signifikante Festigkeitssteigerung von vergüteten, hochfesten Feinkornbaustählen mit einer Normstreckgrenze > 690 MPa, ist die Zugabe von Mikrolegierungselementen, wie Nb und Ti, unerlässlich. Die Normvorgaben zur chemischen Zusammensetzung dieser Stähle (bspw. in DIN EN 10025-6) geben zur Erzielung der vorgeschriebenen Eigenschaften dabei oft nur Grenzgehalte für die Hersteller vor. Die Wirkung der Legierungselemente bzw. ihrer Karbide und/oder Nitride ist teilweise komplett konträr, insbesondere bei Auflösung und Wiederausscheidung in der WEZ bei identischem Schweißzusatz. Somit wird eine adäquate Vorhersage der Chargenabhängigkeit hinsichtlich der Schweißeignung und des Tragverhaltens der Schweißverbindung erschwert. Zuzüglich können moderne Schweißprozesse, wie MSG mit modifiziertem Sprühlichtbogen (mod. SLB) durch ihre hohe Wärmeeinwirkung die Phasenumwandlung in der Wärmeeinflusszone negativ beeinflussen. Eine unerwünschte Eigenschaft ist dabei die Erweichung (engl.: softening) der WEZ, wie auch u.U. der gegenteilige Effekt der Aufhärtung (engl.: hardening). Vor diesem Hintergrund werden im Rahmen eines DFG-Vorhabens systematisch Mikrolegierungsrouten mit variierenden Ti- und Nb-Gehalten des hochfesten und vergüteten Feinkornbaustahls S690QL untersucht. Dazu wird das MAGSchweißen mit mod. SLB verwendet, welches durch hohe Abschmelzleistung gekennzeichnet ist und schmalere Fugenöffnungswinkel (α = 30°) ermöglicht. An diesen Schweißungen wird der Effekt der metallurgischen Zusammensetzung in Kombination mit hoher Wärmeeinwirkung auf die Ausbildung einer kritischen WEZ-Gefügezone mit Erweichung und/oder exzessiver Aufhärtung untersucht. Ein besonderes Augenmerk wird auf die Phasenumwandlungen und das Ausscheidungsverhalten im Gefüge der Wärmeeinflusszone gelegt. Neben umfangreichen metallographischen Untersuchungen einzelner WEZ-Bereiche wurden, unter Variation der chemischen Zusammensetzung, thermodynamische Phasenberechnungen mittels ThermoCalc durchgeführt. Hierdurch wird ein Verständnis zur Phasentransformation und Ausscheidungswachstum und -auflösung während des Schweißens in Abhängigkeit von Temperatur und Abkühlbedingungen geschaffen. Das Ziel ist es, mittels erster Untersuchungen den Einfluss der Wärmeeinwirkung auf die Gefügeausbildung in der WEZ zu zeigen. Insbesondere wird hier auf die Auswirkung der unterschiedlichen Mikrolegierungskonzepte (Ti oder Nb) geachtet. T2 - DVS CONGRESS 2022 - Große Schweißtechnische Tagung CY - Koblenz, Germany DA - 19.09.2022 KW - WEZ-Erweichung KW - Hochfester Feinkornbaustahl KW - ThermoCalc KW - Thermodynamische Simulation KW - Mikrolegierungselemente KW - Modifizierter Sprühlichtbogen PY - 2022 SN - 978-3-96144-189-1 SN - 978-3-96144-190-7 VL - 382 SP - 131 EP - 137 PB - DVS Media GmbH CY - Düsseldorf AN - OPUS4-55834 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Neumann, Martin A1 - Gleim, Tobias A1 - Gradt, Thomas T1 - Friction coefficients for wood-wood and wood-steel high pressure contact under temperatures between -40 °C and 90 °C N2 - Wood is widely used in impact limiters of Transport casks for radioactive material. Encapsulated by an outer and inner Steel structure, spruce wood is offen applied in layers of altemating direction. The friction at the interfaces between these layers is of crucial importance for the impact and energy absorption e.g., at an accidental impact of a cask against a hard component. In order to get detailed Information for corresponding numerical calculations, in this study the friction coefficient for the combinations wood-wood and wood-steel was measured in the temperature ränge between -40 °C and 90 °C according to the relevant stress conditions for such casks. Results show decreasing friction with increasing temperature, ranging from 0.43 at -40 °C to 0.22 for 90 °C for wood-steel combinations and from 0.3 at -40 °C to 0.24 at 90 °C to for a wood-wood combination. KW - Wood KW - Friction KW - Transport cask KW - Radioactive material PY - 2023 DO - https://doi.org/10.24053/TuS-2023-0007 SN - 0724-3472 VL - 70 IS - 2 SP - 5 EP - 12 PB - expert verlag AN - OPUS4-57787 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Quackatz, Lukas T1 - Measurement of hydrogen concentration in steel using Laser-induced Breakdown spectroscopy (LIBS) N2 - Currently, the ISO 3690 standard requires a thermal activation of the diffusible hydrogen in weld metal for the subsequent ex situ concentration measurement by TDS. Laser-induced breakdown spectroscopy (LIBS) would offer a time and spatially resolved, almost non-destructive, measurement of hydrogen at surfaces. We could already show that this analysis technique allows for highly accurate in situ measurements of chemical compositions of e.g. Mn, Cr and Ni during welding e.g. in the melt pool, the weld metal or the heat affected zone. For quantitative LIBS measurements of hydrogen in steel, certified reference materials with different hydrogen concentrations were used for calibration. There is a significant problem in welding steels: A critical combination of diffusible hydrogen, hardness microstructure and weld residual stresses can cause cold cracks to form in the weld microstructure. We investigated hydrogen in steels, which was loaded either electrochemically or with high-pressure hydrogen gas. Subsequently, various experiments were conducted to verify the feasibility of hydrogen measurements with LIBS. For example, depth profiles of hydrogen distribution could be obtained. Furthermore, samples were water jet cut and a line scan was made over the cross section to obtain a spatially resolved representation of the hydrogen. Total hydrogen concentrations were determined using carrier gas hot extraction. Our results show that LIBS is a promising technique for time and spatially resolved measurement of hydrogen in steels. T2 - IIW Annual Assembly 2023 CY - Singapore DA - 16.07.2023 KW - LIBS KW - Hydrogen measurement KW - Welding KW - Stainless steel PY - 2023 AN - OPUS4-57989 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Increasing the Significance of Varestraint Tests through Improved Crack Evaluation N2 - The contribution describes a newly developed software tool for crack identification and selection in Modified Varestraint Transvarestraint (MVT) testing. From the digital crack information, in addition to the classical results, such as Total Crack Length (TCL) and Maximum Crack Length (MCL), advanced evaluations can be applied, taking into account the loading and welding parameters. A numerical parameter study is conducted to demonstrate how the isolated variation of individual welding and loading parameters, affects the crack lengths that can potentially be expected based on the machine specifics. An alternative crack criterion is presented that evaluates the crack formation in relation to the machine behavior. Some examples demonstrate the possibilities and limitations of the approach. The criterion can be used to compare and transfer the results of different varestraint test variants. T2 - IIW Annual Assembly, Comission II-C CY - Singapore DA - 17.07.2023 KW - Solidification cracking KW - Varestraint-Test PY - 2023 AN - OPUS4-57984 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schröder, Nina T1 - Local strain behaviour by digital image correlation of cross weld tensile specimens of high strength steel with two different Ti microalloying routes N2 - Microalloying elements such as Nb and Ti play a decisive function in achieving the desired mechanical strength of quenched and tempered, high-strength fine-grain structural steels with a nominal yield strength ≥ 690 MPa. The current specifications for the chemical composition only provide manufacturers with upper limits. However, even minor deviations in the alloy concept can have a significant impact on the mechanical properties. Consequently, accurate prediction of weldability and the integrity of welded joints becomes difficult or even impossible due to differences in composition and the resulting microstructures. Undesirable consequences include a possible softening of the heat-affected zone (HAZ) or, conversely, hardening effects. In view of these challenges, various microalloying strategies with different Ti and Nb contents are being systematically investigated for the first time using specially developed laboratory casting alloys. Each alloying route is based on the common S690QL, maintaining both the chemical composition and the heat treatment parameters. To analyse the weldability, three-layer welds were performed using gas metal arc welding (GMAW) and critical microstructures, such as areas of the heat-affected zone (HAZ) that exhibit significant softening or hardening, were identified. The effect of the softened HAZ region on failure was evaluated using transverse tensile specimens. Digital image correlation (DIC) is used to image changes in local strains in different HAZ regions in situ. Using a specially developed mirror system, the local strains of the microstructure zones on the top and bottom of the weld are recorded simultaneously. This makes it possible to analyse how the weld seam geometry (e.g., V-seam) influences the strain gradients. In addition, the analysis of the local deformation helps to understand the effects of the softened HAZ on the global strain, the fracture constriction, the fracture position, and the overall fracture behavior T2 - The 77th IIW Annual Assembly and International Conference on Welding and Joining CY - Rhodos, Greece DA - 07.07.2024 KW - HSLA KW - Digital Image Correlation KW - Microalloy KW - GMAW KW - HAZ KW - Cross-weld tensile test PY - 2024 AN - OPUS4-60794 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Westin, Elin T1 - Assessing ferrite content in duplex stainless weld metal: WRC '92 predictions vs. practical measurements N2 - The weldability of stainless steels is largely controlled by the chemical composition, and alloys with ferritic or ferritic-austenitic solidification show the highest resistance to hot cracking. As the resulting phase balance also affects the final properties, it may be beneficial to both foresee and measure the weld metal ferrite content. The WRC ’92 constitution diagram is currently the most accurate prediction tool available, but it does not take the cooling rate into consideration and the precision may be less accurate for stainless steels with high ferrite numbers (FN). This study aims to assess the reliability of the WRC ’92 diagram for weld metals with FN > 50. The chemical composition was altered through gas tungsten arc welding (GTAW) of UNS S32205 with ER347 filler wire that had been PVD-coated with either niobium (Nb), copper (Cu), nickel (Ni), manganese (Mn), carbon (C), or silicon (Si). The actual ferrite content was evaluated using image analysis, FERITSCOPE® and X-ray diffraction (XRD). While predictions from the WRC ’92 diagram were deemed acceptable for Ni, Si, and Mn, notable deviations were observed for Nb, Cu, and C. The FeriteScope exhibited a consistent trend with image analysis, albeit with slightly higher FN values, wider scatter, and the conversion factor from FN to vol.-% is open for discussion. The lowest accuracy and largest spread were obtained using non-contact XRD, rendering it unsuitable for ferrite measurements of welds. These findings underscore the need for improved prediction tools and appropriate measurement methods for assessing ferrite content in duplex weld metals. T2 - Annual Assembly and International Conference CY - Rhodes, Greece DA - 07.07.2024 KW - Duplex steel KW - Ratio austenite / ferrite KW - WRC diagram PY - 2024 AN - OPUS4-60771 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Liepold, Philipp T1 - Einfluss des Einspanngrades auf die Bildung von Erstarrungsrissen in Überlappverbindungen hochfester Stähle N2 - Im Vortrag werden Ergebnisse aus Versuchen mit dem Controlled Thermal Severity (CTS)-Test vorgestellt, der für sehr stark eingespannte Kehlnähte bekannt ist. Niedriglegierte Schweißungen an hochfesten Stählen sind nicht anfällig für Erstarrungsrissbildung. Unter dem besonderen Einfluss eines hohen Einspanngrades wurde die Erstarrungsrissneigung durch Abmessen der Rissflächen als Funktion der Schweißparameter und des Einspanngrades für vier hochfeste Schweißzusätze im MAG-Schweißen untersucht. Die Tests zeigen, dass sowohl eine Erhöhung des Einspanngrades als auch eine Änderung der Schweißparameter (hinsichtlich Streckenenergie und Geschwindigkeit) zu mehr Erstarrungsrissfläche führen. Besonders die Kombination aus sehr hohem Einspanngrad und hoher Streckenenergie plus hoher Schweißgeschwindigkeit sollte im Sinne der Erstarrungsrissminimierung vermieden werden. T2 - DVS-Congress CY - Erfurt, Germany DA - 16.09.2024 KW - CTS KW - Kehlnähte KW - Erstarrungsrisse PY - 2024 AN - OPUS4-61068 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Liepold, Philipp T1 - Investigation of Solidification cracking susceptibility via Modified Varestraint Transvarestraint testing of high-strength filler material N2 - The Modified Varestraint Transvarestraint test is a local variant of the globally used Varestraint test. With these tests, measuring solidification cracking susceptibility as a function of welding parameters is possible. A wide range of welding parameters for four high-strength steel filler wires, including three solid wires and one-flux cored metal wire, were tested. All wires do show a very low solidification cracking susceptibility, regardless of the paramaters. On a low level, it could be shown that solidification cracking susceptibility increases with heat input and welding speed. T2 - IIW Annual Assembly CY - Rhodos, Greece DA - 07.07.2024 KW - MVT KW - Varestraint KW - Transvarestraint KW - Solidification cracking PY - 2024 AN - OPUS4-60684 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Liepold, Philipp T1 - Investigation of restraint intensity influence on solidification cracking of high-strength filler materials in fillet welds via CTS testing N2 - Testing of highly restraint high-strength fillet welds with regards to solidification cracking susceptibility. The Controlled Thermal Severity test was used to apply a high amount of strain to solidifying welds. Test welds were cut and observed under an optical light microscope. A clear positive correlation between restraint intensity and measured crack sizes, as well as heat input and measured crack sized could be observed. T2 - IIW Annual Assembly CY - Rhodos, Greece DA - 07.07.2024 KW - CTS KW - Solidification cracking KW - Hot cracking KW - High-strength steel PY - 2024 AN - OPUS4-60682 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hübner, Martin T1 - Residual stress reduction using LTT welding consumables with focus on the weld geometry N2 - Low Transformation Temperature (LTT) welding consumables represent an innovative approach to realize compressive residual stress in weld and HAZ. LTT welding consumables use the volume-expanding martensitic phase transformation near room temperature to generate compressive residual stress during cooling. This article focusses on the weld geometry of LTT welding consumables and their influence on residual stress reduction. For this purpose, LTT layers were additionally applied to the front sides of conventionally welded longitudinal stiffeners. By varying parameters such as offset and welding speed, different weld geometries could be realized. These were analyzed for geometric parameters, chemical composition and residual stress using X-ray diffraction and fatigue testing. While the chemical composition was only slightly influenced by parameters changes, a clear influence was observed regarding to weld geometry and residual stress. The conventionally weld was characterized by tensile residual stress of ≈350 MPa at the weld toe, the additional LTT weld bead exhibits compressive and tensile residual stress of ≈-150MPa to ≈+150MPa depending to the parameter variation. T2 - International Institut of Welding 2024 CY - Rhodos, Greece DA - 07.07.2024 KW - LTT (Low Transformation Temperature) KW - Residual stress KW - Fatigue strength KW - High-strength steels PY - 2024 AN - OPUS4-60825 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Fey, Gero T1 - Nachbildung der Schweißgefüge von Pipelinestählen durch Dilatometerversuche: ZTU-Diagramme und Wärmeeinflusszonen im Fokus N2 - This study investigates the suitability of low-alloy pipeline steels for hydrogen transportation, focusing on the development of weld microstructures. Previous research has been limited by a deficiency in the understanding of how different microstructural components respond to trapped hydrogen. By developing Continuous Cooling Transformation (CCT) diagrams through dilatometry analysis, this study explores the impact of t8/5-cooling times (the time between 800 °C and 500 °C) on the microstructure and mechanical properties of the HAZ compared to the base material. The findings provide valuable insights into how cooling times influence transformation temperatures and microstructure development, which, in turn, affect hydrogen diffusion and absorption. These findings establish a foundation for future investigations into hydrogen's impact on weld microstructures, including experimental studies, with the aim of optimizing welding practices and enhancing resistance to hydrogen-assisted cracking. Ultimately, this research contributes to improving the safety and reliability of hydrogen transportation systems in commonly used industrial pipeline steels. T2 - Forschungsseminar am Institut für Werkstoff- und Fügetechnik der Otto-von-Guericke-Universität Magdeburg CY - Magdeburg, Germany DA - 18.06.2025 KW - Pipelinestahl KW - ZTU KW - WEZ KW - L555ME KW - X80M KW - Dilatometrie PY - 2025 AN - OPUS4-63751 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Fey, Gero T1 - Thermophysically Simulated Weld HAZ and CCT Diagram of High Strength Low Alloy Pipeline Steel N2 - This study investigates the suitability of low-alloy pipeline steels for hydrogen transportation, focusing on the development of weld microstructures. Previous research has been limited by a deficiency in the understanding of how different microstructural components respond to trapped hydrogen. By developing Continuous Cooling Transformation (CCT) diagrams through dilatometry analysis, this study explores the impact of t8/5-cooling times (the time between 800 °C and 500 °C) on the microstructure and mechanical properties of the HAZ compared to the base material. The findings provide valuable insights into how cooling times influence transformation temperatures and microstructure development, which, in turn, affect hydrogen diffusion and absorption. These findings establish a foundation for future investigations into hydrogen's impact on weld microstructures, including experimental studies, with the aim of optimizing welding practices and enhancing resistance to hydrogen-assisted cracking. Ultimately, this research contributes to improving the safety and reliability of hydrogen transportation systems in commonly used industrial pipeline steels. T2 - 78th IIW Annual Assembly & International Conference on Welding and Joining CY - Genoa, Italy DA - 22.06.2025 KW - Pipeline steel KW - CCT KW - HAZ KW - Dilatometry KW - Welding KW - L485ME KW - X70M PY - 2025 AN - OPUS4-63752 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Fey, Gero T1 - Unter Druck gesetzt: Die unterschätzte Bedeutung des In-Service-Schweißen an druckführenden, in Betrieb befindlicher H2-Ferngasleitungen N2 - Wasserstoff gilt als Energieträger für die Erreichung der Klimaziele und einer nachhaltigen zukünftigen Energieversorgung. Für den notwendigen Transport des Wasserstoffs in großem Maßstab und über weite Entfernungen ist eine zuverlässige Pipeline-Infrastruktur erforderlich. Umfassende weltweite Forschungsprojekte deuten auf die allgemeine Kompatibilität der verwendeten überwiegend ferritischen Stähle für die vorgesehenen Betriebsbedingungen von bis zu 60 °C bei 100 bar Wasserstoff hin. Dies ist jedoch nicht direkt übertragbar auf schweißtechnische Reparatur- und Wartungsarbeiten an im Betrieb befindlichen Pipelines. Ein im Erdgasnetz etabliertes Verfahren stellt das „Hot-Tapping“ dar, bei dem eine unter Druck stehende Pipeline im Betrieb angebohrt wird. Hierfür kommt ein an die Rohrleitung geschweißtes Formstück zum Einsatz, das die Montage der Bohr-/Lochschneidemaschine ermöglicht. In den Richtlinien EIGA 121/14 bzw. AIGA 033/14 wird darauf hingewiesen, dass das Anbohren von Wasserstoffleitungen kein Routineverfahren darstellt: “[…] a hydrogen hot-tap shall not be considered a routine procedure […]“. Dieser Aussage liegt unter anderem zugrunde, dass das Anschweißen des Formstücks an das Rohr und alle zu erwartenden Wärmebehandlungen vor und nach dem Schweißen eine lokale Temperaturerhöhung verursachen. Insbesondere auch an der Rohrinnenfläche, die dem Wasserstoff ausgesetzt ist. Diese erhöhten Temperaturen begünstigen die Absorption und Diffusion von Wasserstoff in das Material. Besonders zu beachten ist außerdem die lokal auftretende kurzzeitige Austenitisierung des Materials, die eine lokal stark erhöhte Wasserstoffkonzentration verursachen kann. Aus den genannten Gründen gibt diese Studie einen kurzen Überblick über die derzeit weltweit verfügbaren Forschungsprojekte zum Schweißen von Wasserstoff-Pipelines im Betrieb. Vorgestellt werden unter anderem erste Ergebnisse des Kooperationsforschungsprojektes H2SuD, das derzeit an der BAM bearbeitet wird. T2 - DVM-Workshop "Werkstoffe für die Wasserstoffinfrastruktur – von der Werkstoffentwicklung bis zum Einsatz im Bauteil" CY - Berlin, Germany DA - 21.05.2025 KW - Pipeline KW - Schweißen KW - Wasserstoff KW - In-Service Welding KW - Reparaturschweißen PY - 2025 AN - OPUS4-63749 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Fey, Gero T1 - Ermittlung wasserstoffabhängiger, mechanischer Eigenschaften der Schweißnahtgefüge niedriglegierter Stähle für Ferngasleitungen N2 - This study investigates the suitability of low-alloy pipeline steels for hydrogen transportation, focusing on the development of weld microstructures. Previous research has been limited by a deficiency in the understanding of how different microstructural components respond to trapped hydrogen. By developing Continuous Cooling Transformation (CCT) diagrams through dilatometry analysis, this study explores the impact of t8/5-cooling times (the time between 800 °C and 500 °C) on the microstructure and mechanical properties of the HAZ compared to the base material. The findings provide valuable insights into how cooling times influence transformation temperatures and microstructure development, which, in turn, affect hydrogen diffusion and absorption. These findings establish a foundation for future investigations into hydrogen's impact on weld microstructures, including experimental studies, with the aim of optimizing welding practices and enhancing resistance to hydrogen-assisted cracking. Ultimately, this research contributes to improving the safety and reliability of hydrogen transportation systems in commonly used industrial pipeline steels. T2 - DVM-Workshop "Werkstoffe für die Wasserstoffinfrastruktur – von der Werkstoffentwicklung bis zum Einsatz im Bauteil" CY - Berlin, Germany DA - 21.05.2025 KW - Pipelinestahl KW - Dilatometrie KW - ZTU KW - WEZ PY - 2025 AN - OPUS4-63750 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bernardy, Christopher A1 - Konert, Florian A1 - Popiela, Bartosz A1 - Sarif, Raduan T1 - H2Safety@BAM: Competence Center for safe hydrogen technologies N2 - Presentation of the competence center H2Safety@BAM at the European PhD Hydrogen Conference 2024 in Ghent, Belgium. T2 - European PhD Hydrogen Conference 2024 (EPHyC2024) CY - Ghent, Belgium DA - 20.03.2024 KW - H2safety KW - Hydrogen KW - Safety KW - Competence center PY - 2024 AN - OPUS4-59756 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Erxleben, Kjell A1 - Kaiser, Sebastian A1 - Rhode, Michael A1 - Kannengiesser, Thomas A1 - Kromm, Arne T1 - In-service and repair welding of pressurized hydrogen pipelines–a review on current challenges and strategies N2 - Hydrogen is the energy carrier for a sustainable future without fossil fuels. As this requires a reliable transportation infrastructure, the conversion of existing natural gas (NG) grids is an essential part of the worldwide individual national hydrogen strategies, in addition to newly erected pipelines. In view of the known effect of hydrogen embrittlement, the compatibility of the materials already in use (typically low-alloy steels in a wide range of strengths and thicknesses) must be investigated. Initial comprehensive studies on the hydrogen compatibility of pipeline materials indicate that these materials can be used to a certain extent. Nevertheless, the material compatibility for hydrogen service is currently of great importance. However, pipelines require frequent maintenance and repair work. In some cases, it is necessary to carry out welding work on pipelines while they are under pressure, e.g., the well-known tapping of NG grids. This in-service welding brings additional challenges for hydrogen operations in terms of additional hydrogen absorption during welding and material compatibility. The challenge can be roughly divided into two parts: (1) the possible austenitization of the inner piping material exposed to hydrogen, which can lead to additional hydrogen absorption, and (2) the welding itself causes an increased temperature range. Both lead to a significantly increased hydrogen solubility in the respective materials compared to room temperature. In that connection, the knowledge on hot tapping on hydrogen pipelines is rare so far due to the missing service experiences. Fundamental experimental investigations are required to investigate the possible transferability of the state-of-the-art concepts from NG to hydrogen pipeline grids. This is necessary to ensure that no critical material degradation occurs due to the potentially increased hydrogen uptake. For this reason, the paper introduces the state of the art in pipeline hot tapping, encompassing current research projects and their individual solution strategies for the problems that may arise for future hydrogen service. Methods of material testing, their limitations, and possible solutions will be presented and discussed. KW - In-service KW - Welding KW - Hydrogen pipeline KW - Review PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-638847 DO - https://doi.org/10.1007/s40194-025-02127-x SN - 0043-2288 SP - 1 EP - 24 PB - Springer Science and Business Media LLC AN - OPUS4-63884 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Liepold, Philipp A1 - Kromm, Arne A1 - Kannengießer, Thomas T1 - A Force Based Determination of Hot Cracking Susceptibility N2 - Two high-strength, low-alloy Gas Metal Arc Welding (GMAW) wires were evaluated for their susceptibility to Solidification Cracking (SC) using a modified version of the Transverse Motion Weldability (TMW) test. In theoriginal TMW test, the Transverse Displacement Speed (TDS) is varied iteratively, and crack lengths are measured in each iteration. The modified version eliminates the need for multiple runs by continuously reducing the TDS over a single run. Rather than emphasizing crack lengths, this method assesses the reaction force to the TDS, thereby determining a Critical TDS (CTDS). This critical point directly correlates with the cessation of SC growth. CTDS values were measured under a range of welding parameters, thereby demonstrating the influence of Welding speed and arc energy (U × I/welding speed) on SC susceptibility for the tested filler metals. The CTDS data obtained from this testing method have the potential to provide valuable insights for practical applications in the field. KW - Force based KW - Neural Network KW - TRS PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-640140 DO - https://doi.org/10.5781/JWJ.2025.43.4.10 SN - 2466-2100 VL - 43 IS - 4 SP - 447 EP - 457 AN - OPUS4-64014 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael A1 - Czeskleba, Denis A1 - Irfan, Muhammad Dary A1 - Wandtke, Karsten A1 - Kaiser, Sebastian A1 - Kannengießer, Thomas T1 - Wasserstoffdiffusion in hochfesten UP-Schweißverbindungen – einfacher als gedacht N2 - Hochfeste Baustähle werden im modernen Stahlbau aus wirtschaftlichen und konstruktiven Gründen zunehmend eingesetzt, z. B. im Gebäude-, Anlagen- oder Mobilkranbau. Durch den Einsatz von Stählen mit höheren 690 MPa) können durch die Reduzierung der Wanddicke erhebliche Gewichtsreduzierungen und geringere Verarbeitungskosten erreicht werden, insbesondere bei der Verwendung des Unterpulverschweißen (UP) durch seine hohe Abschmelzleistung. Aufgrund ihrer speziellen Mikrostruktur haben hochfeste Stähle eine begrenzte Duktilität und sind anfälliger für wasserstoffunterstützte Kaltrisse (HACC). Darüber hinaus führen große mittels UP geschweißter Blechdicken zu hohen Schweißeigenspannungen und langen Diffusionswegen für z.B. durch den Schweißprozess eingebrachten Wasserstoff. Abgesicherte Diffusionskoeffizienten für UP-Schweißungen dieser Festigkeitsklasse sind als Grundlage für die Abschätzung des Zeitintervalls einer möglichen verzögerten Kaltrissbildung oder für Nachwärmung zur Wasserstoffreduktion nur sehr begrenzt verfügbar. Aus diesem Grund wurden experimentelle Versuche zur mikrostruktur-spezifischen Diffusion in S690-Schweißungen durchgeführt. Dazu wurde ein thermomechanisch (TM) gewalzter bzw. vergüteter (QL) Zustand dieses Werkstoffs betrachtet, sowie das jeweilige charakteristische Schweißgut und WEZ. Dazu wurden den Schweißmikrostrukturen lokal Proben entnommen und über Permeations- bzw. Warmauslagerungsversuche die gefügespezifische Diffusion von Raumtemperatur bis 400°C charakterisiert. Im Gegensatz zu bekannten Effekten des Wärmebehandlungszustandes der Grundwerkstoffe auf die Diffusion in MSGSchweißverbindungen, zeigten die Wasserstoffdiffusionskoeffizienten über alle untersuchten Gefügezustände keine signifikanten Unterschiede, insbesondere nicht für die lokale WEZ diverser, untersuchter Streckenergiebereiche. Aus praktischer Anwendersicht können daher dickwandige UP-Verbindungen hinsichtlich einer verzögerten Wasserstoffdiffusion nur anhand der einfach ermittelbaren Diffusionskoeffizienten für den Grundwerkstoffkoeffizient beurteilt werden. Zudem zeigte sich, dass der unterschiedliche Walz- und Wärmebehandlungszustand (TM vs. QL) in UP-Schweißnähten eine untergeordnete Rolle für die Wasserstoffdiffusion und damit für die mögliche Zeitverzögerung der Kaltrissbildung hat. Ergänzende numerische Simulationen der Wasserstoffverteilung bestätigten das Verhalten. T2 - DVS Congress 2025 CY - Essen, Germany DA - 16.09.2025 KW - Unterpulverschweißen KW - Wasserstoffdiffusion KW - Wasserstoffunterstützte Kaltrissbildung KW - Wasserstoffrisse PY - 2025 SN - 978-3-96144-299-7 DO - https://doi.org/10.53192/DVSC20250330 VL - 401 SP - 330 EP - 340 PB - DVS Media GmbH CY - Düsseldorf AN - OPUS4-64132 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Erxleben, Kjell T1 - Component test for the assessment of in-service welding on/onto pressurized hydrogen pipelines N2 - Hydrogen is seen as the energy carrier of the future. Therefore a reliable infrastructure to transport hydrogen in a large scale is needed. A so called European hydrogen backbone out of long distance transmission pipelines is planned by European countries to create a hydrogen transport infrastructure. Due to economic reasons this will be achieved by new build pipelines such as repurposed natural Gas (NG) pipelines, converted to hydrogen useage. A general suitability for hydrogen service of low alloyed pipeline steel, as it is used for NG service today, is given. But in case of necessary in-service welding procedures in terms of e.g. hot-tapping and stoppling, the risk of a critical hydrogen uptake into the pipe materials due to much higher temeperatures while welding and the possibility of hydrogen embrittlement (HE) needs to be closely investigated. The presentation gives an overview of the current H2-SuD project, investigating the feasability of in-service welding on future hydrogen pipelines. Therefore, component-like demonstrators were developed to test (I) the additional hydrogen uptake due to in-service welding under hydrogen pressure and (II) to measure the temperature field due to different welding parameters and demonstrator geometries, especially on the inner pipe wall surface. Collected data will be used to validate a numerical simulation of the thermal field and additionally the hydrogen diffusion in the pipeline material. T2 - Presentation at The University of Manchester CY - Manchester, United Kingdom DA - 12.09.2025 KW - In-service KW - Hydrogen KW - Pipeline KW - Welding PY - 2025 AN - OPUS4-64129 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kaiser, Sebastian T1 - Wasserstoffdiffusion in hochfesten UP-Schweißverbindungen - einfacher als gedacht N2 - Hochfeste Baustähle werden im modernen Stahlbau aus wirtschaftlichen und konstruktiven Gründen zunehmend eingesetzt, z. B. im Gebäude-, Anlagen- oder Mobilkranbau. Durch den Einsatz von Stählen mit höheren 690 MPa) können durch die Reduzierung der Wanddicke erhebliche Gewichtsreduzierungen und geringere Verarbeitungskosten erreicht werden, insbesondere bei der Verwendung des Unterpulverschweißen (UP) durch seine hohe Abschmelzleistung. Aufgrund ihrer speziellen Mikrostruktur haben hochfeste Stähle eine begrenzte Duktilität und sind anfälliger für wasserstoffunterstützte Kaltrisse (HACC). Darüber hinaus führen große mittels UP geschweißter Blechdicken zu hohen Schweißeigenspannungen und langen Diffusionswegen für z.B. durch den Schweißprozess eingebrachten Wasserstoff. Abgesicherte Diffusionskoeffizienten für UP-Schweißungen dieser Festigkeitsklasse sind als Grundlage für die Abschätzung des Zeitintervalls einer möglichen verzögerten Kaltrissbildung oder für Nachwärmung zur Wasserstoffreduktion nur sehr begrenzt verfügbar. Aus diesem Grund wurden experimentelle Versuche zur mikrostruktur-spezifischen Diffusion in S690-Schweißungen durchgeführt. Dazu wurde ein thermomechanisch (TM) gewalzter bzw. vergüteter (QL) Zustand dieses Werkstoffs betrachtet, sowie das jeweilige charakteristische Schweißgut und WEZ. Dazu wurden den Schweißmikrostrukturen lokal Proben entnommen und über Permeations- bzw. Warmauslagerungsversuche die gefügespezifische Diffusion von Raumtemperatur bis 400°C charakterisiert. Im Gegensatz zu bekannten Effekten des Wärmebehandlungszustandes der Grundwerkstoffe auf die Diffusion in MSGSchweißverbindungen, zeigten die Wasserstoffdiffusionskoeffizienten über alle untersuchten Gefügezustände keine signifikanten Unterschiede, insbesondere nicht für die lokale WEZ diverser, untersuchter Streckenergiebereiche. Aus praktischer Anwendersicht können daher dickwandige UP-Verbindungen hinsichtlich einer verzögerten Wasserstoffdiffusion nur anhand der einfach ermittelbaren Diffusionskoeffizienten für den Grundwerkstoffkoeffizient beurteilt werden. Zudem zeigte sich, dass der unterschiedliche Walz- und Wärmebehandlungszustand (TM vs. QL) in UP-Schweißnähten eine untergeordnete Rolle für die Wasserstoffdiffusion und damit für die mögliche Zeitverzögerung der Kaltrissbildung hat. Ergänzende numerische Simulationen der Wasserstoffverteilung bestätigten das Verhalten. T2 - DVS Congress 2025 CY - Essen, Germany DA - 16.09.2025 KW - Unterpulverschweißen KW - Wasserstoffdiffusion KW - Wasserstoffunterstützte Kaltrissbildung KW - Wasserstoffrisse PY - 2025 AN - OPUS4-64130 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael T1 - Numerical simulation of weld heat input effect on microstructure and hydrogen diffusion in thick-walled S690 submerged arc welded joints N2 - High-strength, low-alloy (HLSA) steels such as S690 are an attractive option for heavy industries such as offshore wind turbines and peripheral equipment due to their combination of excellent mechanical properties and weldability. The construction of these thick-walled structures requires highly efficient welding processes such as submerged arc welding (SAW). However, SAW presents challenges related to delayed hydrogen assisted cold cracking (HACC). Despite its importance, the effect of different diffusion coefficients on the cold cracking susceptibility of different microstructures within SAW-welded S690 steels is not fully understood. For this reason, the present study focuses on comparing the cold cracking susceptibility of thermomechanically rolled (TM) or quenched and tempered (QL) variants of S690 steel. SAW was performed on specimens of both steel grades to produce weldments consisting of weld metal, heat-affected zone (HAZ), and base metal. Electrochemical hydrogen permeation tests (ISO 17081) were performed to determine the microstructure specific coefficients. Using the obtained coefficients, a numerical model was developed to identify the time- and microstructure-dependent local hydrogen diffusion and its influence on the distribution within the welds. The results showed that the TM grade exhibited slightly accelerated hydrogen diffusion compared to the QL grade, which is beneficial for hydrogen reduction and increases the HACC resistance. However, the further simulations with different ply sequences showed that the welding heat input (i.e. welding ply sequence) had a significantly higher effect on hydrogen accumulation. Specifically, increased welding heat input and increased thicknesses decrease hydrogen diffusivity. For this reason, microstructure-specific hydrogen diffusion played a minor role in thick-layer SAW joints compared to the need to control the welding parameters (layer sequence, individual layer thickness, welding heat input). T2 - FEMS Euromat 2025 - 18th European Congress and Exhibition on Advanced Materials and Processes CY - Granada, Spain DA - 15.09.2025 KW - Hydrogen assisted cracking KW - Welding KW - High strength steels KW - Numerical simulation KW - Electrochemical permeation PY - 2025 AN - OPUS4-64158 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael T1 - Hydrogen trap characterization in 200 and 1,000 bar charged CoCrNi medium entropy alloy compared to steel AISI 316L N2 - Multiple principal element alloys (MPEAs) represent a new class of metallic materials. MPEAs, such as the CoCrNi medium entropy alloy (MEA), have attracted considerable research attention as potential materials to replace, for example, austenitic steels in high-pressure hydrogen environments. Due to the relatively new alloy concept, studies on the specific hydrogen diffusion and trapping behavior of high-pressure hydrogen-charged CoCrNi MEAs are rare so far. For this reason, a CoCrNi-MEA was investigated and compared to an austenitic stainless steel, AISI 316L. Both materials were subjected to high pressure hydrogen loading for two different pressures: 200 bar and 1,000 bar. After charging, thermal desorption analysis (TDA) was used with three heating rates from 0.125 K/s to 0.500 K/s to clarify the specific hydrogen desorption and trapping behavior. To the best of our knowledge, this study is the first to characterize hydrogen diffusion and trapping in 1,000 bar high-pressure charged CoCrNi. For this purpose, the underlying TDA spectra were analyzed in terms of peak deconvolution into a metallurgically justifiable number of defined peaks. The individual peak temperatures and activation energies “EA” were calculated. The following conclusions can be drawn from the results obtained: (1) Exposure to 200 bar or 1,000 bar leads to an increase in hydrogen absorption, regardless of the material investigated, expressed by a significantly increased desorption rate at 1,000 bar. However, the effusion peaks typically occur only at high temperatures. The (2) TDA showed that a four-peak deconvolution scenario was sufficient to describe the trapping behavior and the "EA" indicated the dominance of irreversible traps. In addition, the average trapping energy is higher than in the 316L. The (3) charge pressure related hydrogen solubility was in the order of: CoCrNi-MEA < 316L for both pressures and (4) charging at 1000 bar results in an average concentration of 49 wt.ppm (CoCrNi-MEA) and > 75 wt.ppm (316L). In summary, the CoCrNi-MEA was characterized by a reduced solubility, but very deep entrapment compared to the 316L. For this reason, further application potentials of the MEA may arise. T2 - FEMS Euromat 2025 - 18th European Congress and Exhibition on Advanced Materials and Processes CY - Granada, Spain DA - 15.09.2025 KW - Medium entropy alloy KW - Hydrogen KW - Trapping KW - Diffusion KW - High-pressure charging PY - 2025 AN - OPUS4-64160 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael T1 - Effect of Ti and Nb on hydrogen trapping in welded S690 HSLA steel and effect on delayed cold cracking N2 - Fine-grain, high-strength, low-alloy (HSLA) structural steels with yield strengths > 600 MPa are now the state of the art in construction applications such as mobile cranes and civil engineering. HSLA grades derive their strength from a combination of specific heat treatment and the underlying chemical composition. In this context, Ti or Nb are essential to obtain a fine-grained microstructure as well as the necessary carbides or nitrides for precipitation strengthening. In this context, the specific effect of Ti or Nb-rich compounds on hydrogen trapping and diffusion is well known for special laboratory cast alloys, but unknown for realistic steel compositions. For this reason, a series of S690Q-based alloys were synthesized, close to a real steel composition, but with well controlled Ti or Nb additions in different amounts. Specimens were obtained from these alloys by electrochemical discharge machining (EDM). The specimens were tested using the well-established electrochemical permeation technique. From the experimental results, the hydrogen diffusion coefficients and the analytical subsurface hydrogen concentration were calculated. In addition, the hydrogen trapping behavior at elevated temperatures was interpreted by thermal desorption analysis (TDA) using different heating rates of hydrogen charged samples. The results showed that in contrast to metallurgically "pure" laboratory cast alloys, realistic chemical compositions were similar in their hydrogen trapping behavior, despite some small differences. All investigated steel grades exhibited shallow and reversible hydrogen trapping, regardless of their chemical composition. Of course, the experiments only allowed the calculation of effective diffusion coefficients and trapping energies, which represent an average of the entire microstructure. Nevertheless, HSLA steels are typically joined by arc welding, which includes the risk of delayed hydrogen assisted cracking. From the point of view of welding practice, however, a more or less identical hydrogen diffusion behavior means that no special "metallurgically specific", justifiable measures need to be considered, despite the well-established processes such as "soaking" or dehydrogenation heat treatment. Of course, a closer look at the heat-affected zone (HAZ) or the weld metal of the specific welds is necessary. However, especially in the case of thick-walled welds, it is assumed that the weld metal and HAZ are similar to the base material due to the multi-layer welding, which results in multiple annealing cycles of the weld metal and HAZ. T2 - FEMS Euromat 2025 - 18th European Congress and Exhibition on Advanced Materials and Processes CY - Granada, Spain DA - 15.09.2025 KW - Hydrogen assisted cracking KW - HSLA KW - Diffusion KW - Electrochemical permeation PY - 2025 AN - OPUS4-64156 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael T1 - Component test for the assessment of in-service welding on/onto pressurized hydrogen pipelines N2 - Hydrogen is the energy carrier of tomorrow and requires a reliable large-scale transport infrastructure. In addition to new pipelines, the conversion of existing natural gas (NG) pipeline grids is an essential part. The transport of hydrogen is fundamentally different from that of NG, as hydrogen can be absorbed into the pipeline material. Given the effects of hydrogen embrittlement, the material compatibility (low alloy steels in a wide range of strengths and thicknesses) must be investigated. However, pipelines e.g. require maintenance or the need for installation of additional outlets with the necessity of welding on/onto the pipelines while they are still in service, i.e. with gas flow under high pressure, such as the well-known "hot tapping". This in-service welding poses challenges for hydrogen operations. The challenge can be roughly divided into the possible austenitization of the inner pipe material exposed to hydrogen, the welding itself, which causes an increased temperature range. Both lead to a significant increase in hydrogen solubility and diffusivity compared to room temperature. In addition, possible surface reactions of the present iron oxides (e.g. magnetite or hematite) with the hot hydrogen should be considered. In this context, the knowledge of hydrogen pipelines is scarce due to the lack of operational experience. Fundamental experimental investigations are required to investigate the transferability from NG to hydrogen pipeline grids. For this reason, the present study presents a specially designed mock-up / demonstrator concept for the realistic assessment of the welding process conditions. The mock-up was designed to allow in-situ temperature measurement during the welding process as well as ex-post sample extraction for quantification of the absorbed hydrogen concentration. For safety reasons, the required volume of pressurized hydrogen was limited by inserting a solid cylinder to ensure a 1 cm thick layer of hydrogen gas. Welding experiments on the DN60 and DN200 pressurized mock-ups showed the possibility of safe welding on or onto pressurized hydrogen pipelines. Indeed, the austenitizing temperature was reached on the inner surface of the pipeline, especially on thinner-walled pipelines, using current welding parameter recommendations. This corresponded to an increased hydrogen uptake in the welded area of several ppm. From this point of view, the suggested component concept is a viable strategy for the screening of several materials and welding parameter combinations under realistic operational conditions. T2 - FEMS Euromat 2025 - 18th European Congress and Exhibition on Advanced Materials and Processes CY - Granada, Spain DA - 15.09.2025 KW - In-service welding KW - Pipeline KW - Hydrogen KW - Component test PY - 2025 AN - OPUS4-64159 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schaumann, P. A1 - Schürmann, K. A1 - Pittner, Andreas A1 - Rethmeier, Michael T1 - Experimental investigations on the fatigue resistance of automatically welded tubular X-joints for jacket support structures N2 - The development within the offshore wind sector towards more powerful turbines combined with increasing water depth for new wind parks is challenging both the designer as well as the manufacturer of bottom fixed support structures. Besides XL-monopiles, the market developed an innovative and economic jacket support structure which is based on automatically manufactured tubular joints combined with standardized pipes. Besides the improvements for a serial manufacturing process the automatically welded tubular joints show a great potential in terms of fatigue resistance e.g. due to a smooth weld geometry without sharp notches. However, these benefits are not considered yet within the fatigue design process of automatically manufactured jacket substructures according to current standards due to the lack of suitable S-N curves. Therefore, 32 axial fatigue tests on single and double-sided automatically welded tubular X-joints have been performed to determine a new hot spot stress related S-N curve. Based on these constant amplitude fatigue tests a new S-N curve equal to a FAT 126 curve was computed which implicitly includes the benefits of the automatically welding procedure. T2 - EERA Deep Wind 2020 CY - Trondheim, Norway DA - 15.01.2020 KW - Notch stress approach KW - Fatigue tests KW - Automated manufacturing KW - Tubular X-joints KW - Structural stress approach PY - 2020 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-518509 DO - https://doi.org/10.1088/1742-6596/1669/1/012022 VL - 1669 SP - 012022 PB - IOP Publishing Ltd AN - OPUS4-51850 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mielentz, Frank A1 - Stolpe, Heiko A1 - Effner, Ute A1 - Behrens, Matthias A1 - Bernstein, Thomas A1 - Niederleithinger, Ernst T1 - Entwicklung einer Bohrlochsonde für Ultraschalluntersuchungen an Abschlussbauwerken in Endlagern N2 - Für die Qualitätssicherung von Abschlusswerken für Endlager wird eine Ultraschall-Bohrlochsonde entwickelt. Mithilfe dieser Sonde, die aus einer Vielzahl von einzelnen koppelmittelfreien Ultraschall-Punktkontaktprüfköpfen besteht, soll die Rissfreiheit der Versuchsbauwerke überprüft werden. Ein erster Prototyp der Sonde wurde mit einem kommerziellen Ultraschallgerät betrieben und bestand aus 12 Transversalwellen-Punktkontaktprüfköpfen von denen jeweils sechs als Sender und sechs als Empfänger parallelgeschaltet waren. Um den erzeugten Schalldruck der Bohrlochsonde zu steigern, wurde bei der Neuentwicklung die Prüfkopfanzahl erhöht und zusätzlich die laufzeitgesteuerte Anregung der einzelnen Prüfköpfe vorgesehen. Für die Anregung der Prüfköpfe mit programmierten Zeitverzögerungen wurde ein neuartiger mehrkanaliger Sender für bipolare Rechtecksignale entwickelt. Durch die Entwicklung der Bohrlochsonde soll eine dynamische Anpassung der Prüfkopf-Apertur sowie eine Fokussierung des Schallfeldes in Abhängigkeit der zu untersuchenden Tiefe erfolgen. Mithilfe entsprechender Anregungsfunktionen kann das Schallfeld der Bohrlochsonde unterschiedlich geformt werden, z. B. ist auch ein Schwenken des fokussierten Schallbündels möglich. Dadurch wird das erfasste Prüfvolumen begrenzt und auf diese Weise das Signal-Störverhältnis der Empfangssignale verbessert. In Kombination mit SAFT-Rekonstruktionsrechnungen wird durch eine optimierte Abstrahlcharakteristik der Sonde mit einem hohen Schalldruck unter verschiedenen Winkeln eine verbesserte Signalqualität und damit eine erhöhte Aussagesicherheit der Ergebnisse in der Objektabbildung erwartet. T2 - DGZfP-Jahrestagung 2021 CY - Online meeting DA - 10.05.2021 KW - Abdichtbauwerk KW - Bohrlochsonde KW - Ultraschall-Echoverfahren KW - Verschlussbauwerk KW - Zerstörungsfreie Prüfung KW - Ultraschall-Messtechnik PY - 2021 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-526746 UR - https://jahrestagung.dgzfp.de/portals/jt2021/bb176/inhalt/poster.htm SN - 978-3-947971-18-3 VL - 176 SP - 1 EP - 7 PB - Deutsche Gesellschaft für Zerstörungsfreie Prüfung (DGZfP) CY - Berlin AN - OPUS4-52674 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Gook, Sergej A1 - El-Batahgy, Abdel-Monem A1 - Gumenyuk, Andrey A1 - Biegler, Max A1 - Rethmeier, Michael T1 - Application of Hybrid Laser Arc Welding for Construction of LNG Tanks Made of Thick Cryogenic 9% Ni Steel Plates N2 - Hybrid laser-arc welding (HLAW) was applied for butt welding of 14.5 mm thick plates of ferritic cryogenic steel X8Ni9 containing 9% Ni, which is used for manufacturing storage and transport facilities of liquefied natural gas (LNG). The weld seam formation and the achievable metallurgical and mechanical properties of the hybrid welds were investigated experimentally for two types of filler wire, an austenitic wire dissimilar to the base metal (BM) and an experimentally produced matching ferritic wire. Safe penetration and uniform distribution of the austenitic filler metal in the narrow hybrid weld could only be achieved in the upper, arcdominated part of the weld. The pronounced heterogeneous distribution of the austenitic filler metal in the middle part and in the root area of the weld could not ensure sufficient notched impact toughness of the weld metal (WM). As a result, a decrease in the impact energy down to 17±3 J was observed, which is below the acceptance level of ≥34 J for cryogenic applications. In contrast, the use of a matching ferritic filler wire resulted in satisfactory impact energy of the hybrid welds of up to 134±52 J at the concerned cryogenic temperature of -196 °C. The obtained results contribute to an important and remarkable conversion in automated manufacturing of LNG facilities. In other words, the results will help to develop a new laser-based welding technology, where both quality and productivity are considered.The efficiency of the developed welding process has been demonstrated by manufacturing a prototype where a segment of the inner wall of large size LNG storage tank was constructed. In this concern, hybrid laser arc welding was conducted in both horizontal (2G) and vertical (3G) positions as a simulation to the actual onsite manufacturing. The prototype was fabricated twice where its quality was confirmed based on non-destructive and destructive examinations. KW - Hardness KW - Hybrid Laser arc Welding KW - 9% Ni Steel KW - Fusion zone size KW - Microstructure KW - Tensile Strength KW - Impact Absorbed Energy PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-586080 DO - https://doi.org/10.1007/s40516-023-00229-2 SP - 1 EP - 22 PB - Springer Nature AN - OPUS4-58608 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Gumenyuk, Andrey A1 - Üstündağ, Ömer A1 - Pelz, Till A1 - Bakir, Nasim A1 - Gerhards, Benjamin A1 - Schleser, Markus A1 - Rethmeier, Michael T1 - Single pass laser vacuum welding of thick steel plates using electromagnetic support N2 - The increasing demand for renewable energy produced by offshore wind turbines goes along with an increased demand in the production of offshore wind turbine foundations, so called “monopiles”, which are made by joining thick metal sheets. The industrial standard of multi-layer submerged arc welding (SAW) for joining of thick metal sheets is the current bottleneck in the production of monopiles. A possible increase in productivity by the implementation of high-power laser welding in a newly developed mobile vacuum chamber (MoVac) and an electromagnetic root support is the subject of this study. Single run butt welds are performed in flat position on S355 mild steel of thicknesses up to 80 mm using a disc laser system with 1030 nm wavelength and a maximum output of 60 kW. The laser optic is fixed on the MoVac-System which is held and manipulated by an articulated robot. KW - Laser beam welding KW - Laser welding with mobile vacuum PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-612068 DO - https://doi.org/10.1016/j.procir.2024.08.145 VL - 124 SP - 418 EP - 423 PB - Elsevier BV AN - OPUS4-61206 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eissel, A. T1 - Modification of Co Cr alloys to optimize of additively welded microstructures and subsequent surface finishing N2 - Cobalt chromium alloys are often used in turbine and plant construction. This is based on their high thermal and mechanical stress resistance as well as their high wear resistance to corrosive and abrasive loads. However, cobalt is a cost-intensive material that is difficult to machine. Moreover, increasingly complex structures and the optimisation of resource efficiency also require additive manufacturing steps for the production or repair of components in many sectors. Concerning inhomogeneity and anisotropy of the microstructure and properties as well as manufacturing-related stresses, a lot of knowledge is still necessary for the economic use of additive welding processes in SMEs. As a result of the high stresses on the components and requirements for a high surface quality, a complementary use of additive and machining manufacturing processes is necessary. Thereby, Co–Cr alloys are extremely challenging for machining with geometrically defined cutting edges because of their low thermal conductivity combined with high strength and toughness. An approach to solve this problem is to refine and homogenise the microstructure. This is achieved by modifying the alloy with elements zirconium and hafnium, which are added up to a maximum of 1 wt.-%. A reduction of the process forces and stresses on the tool and work piece surface is also achievable via hybrid milling processes. There are already studies on the combined use of additive and machining manufacturing processes based on laser technology. However, knowledge based on powder and wire-based arc processes is important, as these processes are more widespread. Furthermore, the effects on the surface zone of additively manufactured components by hybrid finish milling have not yet been a subject of research. The results show that the structural morphology could be significantly influenced with the addition of zirconium and hafnium. T2 - 74th IIW Annual Assembly CY - Online meeting DA - 12.07.2021 KW - Modification of structural morphology KW - Co–Cr-alloy KW - Plasma-transferred arc welding KW - Ultrasonic-assisted milling PY - 2021 AN - OPUS4-56670 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wilhelm, Eugen A1 - Mente, Tobias A1 - Rhode, Michael T1 - Waiting time before NDT of welded offshore steel grades under consideration of delayed hydrogen-assisted cracking N2 - Offshore wind turbines (OWT) are a major goal of the energy strategy of Germany encompassing the increase of the installed wind power. OWT components are manufactured from welded steel plates with thicknesses up to 200 mm. The underlying standards and technical recommendations for construction of OWTs encompass specifications of so-called minimum waiting time (MWT) before non-destructive testing of the weld joints is allowed. Reason is the increased risk of time-delayed hydrogen assisted cold cracking as hydrogen diffusion is very slow due to the very thick plates. The strict consideration of those long MWT up to 48 h during the construction of OWTs leads to significant financial burden (like disproportionately high costs for installer ships as well as storage problems (onshore)). In this study, weld joints made of S355 ML were examined in comparison with the offshore steel grade S460 G2+M. The aim was to optimize, i.e., reduce, the MWT before NDT considering varied heat input, hydrogen concentration and using self-restraint weld tests. This would significantly reduce the manufacturing time and costs of OWT construction. To quantify the necessary delay time until hydrogen-assisted cold cracks appear, acoustic emission analysis was applied directly after welding for at least 48 h. KW - Hydrogen KW - Welding KW - Cracking KW - Offshore KW - Steel PY - 2021 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-524959 DO - https://doi.org/10.1007/s40194-020-01060-5 SN - 0043-2288 VL - 65 SP - 947 EP - 959 PB - Springer Nature AN - OPUS4-52495 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Richter, Tim T1 - Residual stresses in near-component specimens of a high and a medium entropy alloy due to tig and friction stir welding N2 - The new alloying concept of multi-element systems with defined entropy (HEA - High Entropy Alloy or MEA - Medium Entropy Alloy) is gaining increasing importance in materials research. Significantly improved properties or combinations of properties are shown by some HEA/MEA-systems, which have the potential to substitute conventional alloys such steels and are therefore promising for a wide range of applications, e.g., overcome of the trade-off between high strength and ductility. Thus, primarily the production and resulting microstructures of HEA as well as properties have been investigated so far. Furthermore, processing is a main issue to transfer HEA systems from the laboratory to real components, e.g., for highly stressed components. Since welding is the most important joining process for metals, it is crucial to investigate the influence of welding processing on these material properties to guarantee component integrity. Welding leads to residual stresses, which significantly affect the component integrity. Only a very few studies on the effect of welding on residual stresses in HEA and MEA weld joints are available so far. Hence, the focus of this study is the residual stress formation and distribution in a CoCrFeMnNi HEA and ternary CoCrNi MEA using two different welding processes: Tungsten Inert Gas (TIG) welding and soldi-state Friction Stir Welding (FSW). As a pathway for application of HEA in this investigation for the first time residual stress analyses in realistic near-component specimens were performed. The residual stresses were determined by X-ray diffraction (XRD) on the surfaces of top and root weld side. The results were correlated with the local welding microstructures. The results show that both FSW and TIG generate significant tensile residual stresses on the weld surfaces in and transverse to the welding direction. In the case of FSW of the CoCrFeMnNi HEA, the longitudinal residual stresses are in the range of the yield strength of approx. 300 MPa in the weld zone. T2 - OVGU-Kolloquium (BMDK des IWF) CY - Online meeting DA - 19.05.2022 KW - High Entropy Alloy KW - Welding KW - Residual stresses KW - Microstructure PY - 2022 AN - OPUS4-56671 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Richter, Tim A1 - Rhode, Michael T1 - Hydrogen embrittlement and mechanical properties of 9 % Cr P92 steel and P91 weld metal N2 - Martensitic 9 %-Cr steels like P91 and P92 can show an increased susceptibility to delayed hydrogen assisted cracking. The focus of this study was the microstructure and heat treatment effect on the mechanical properties of P92 base material and P91 multi-layer weld metal in both as-welded and post weld heat treated (PWHT) condition. Tensile tests with hydrogen free reference samples and electrochemically hydrogen charged samples were carried out, the mechanical properties were assessed and supported by dedicated fractographic analysis. In addition, hydrogen and microstructure dependent fracture criteria were calculated. All investigated microstructures showed a hydrogen influenced degradation of the mechanical properties compared to the hydrogen free reference samples. In that connection, the as welded martensitic P91 weld metal had the highest degree of degradation in presence of hydrogen. The P91 PWHT weld metal and the P92 base material had comparable properties. From that point of view, a significantly increased risk for hydrogen assisted cold cracking during welding fabrication of P91 weld joints must be considered before any heat treatment is conducted. T2 - IIW Annual Assembly, Meeting of Commission IX-C CY - Tokyo, Japan DA - 21.07.2022 KW - Creep-resistant steel KW - Mechanical properties KW - Hydrogen assisted cracking KW - Weld joint KW - Degradation PY - 2022 AN - OPUS4-55462 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Konert, Florian A1 - Nietzke, Jonathan T1 - H2 Safety at BAM - Eine Kurzvorstellung N2 - Zusammenfassend wird dem Teilnehmerkreis, bestehend aus Industrievertretern, vorgestellt, welche Aktivitäten die BAM im Bereich Wasserstoff auszeichnen. Ein spezielles Augenmerk liegt hierbei auf dem Kompetenzfeld "MatCom". T2 - 8. SITZUNG DER „EXPERTENGRUPPE WASSERSTOFF“ (EG-H2) des IGV e.V. CY - Online meeting DA - 17.02.2022 KW - H2 KW - Wasserstoff KW - Materialkompatibilität KW - Werkstoffkompatibilität PY - 2022 AN - OPUS4-54367 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Drexler, Andreas A1 - Konert, Florian T1 - Hydrogen Solubility in Steels – What is the Role of Microstructure? N2 - Hydrogen gas plays a key role in the European energy transition strategy. When transmitting and storing compressed hydrogen gas, safety is one of the most important conditions. With increasing hydrogen pressure and temperature, more hydrogen is absorbed by the steel components, such as pipelines or valves, and may lead to embrittlement. Although, a deep understanding of microstructure on the hydrogen solubility in steels is missing. Classical Sieverts’ law is only valid at high temperatures and low gas pressures. For that purpose, new theory is presented, which explains the role of microstructure on hydrogen solubility. Hydrogen trapping at microstructural defects is a thermally activated mechanism and causes an increase of the hydrogen solubility with decreasing temperatures. This mechanism has to be considered in cryogenic applications, such liquid or compressed hydrogen storage. T2 - EPRI Workshop on Hydrogen Embrittlement 2024 CY - Oxford, UK DA - 23.06.2024 KW - Hydrogen KW - Sieverts’ law KW - Hydrogen solubility in steels KW - Hydrogen trapping PY - 2024 AN - OPUS4-60477 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Konert, Florian T1 - Evaluating X65 pipeline steel using the hollow specimen technique N2 - This presentation describes the usability of the hollow tensile specimen technique for in-situ material testing in a hydrogen atmosphere. In addition, the presentation provides an outlook on the methodology for investigating the suitability of pipeline steels and their weld seams for hydrogen operation. T2 - EPHyC 2024 CY - Ghent, Belgium DA - 19.03.2024 KW - Hydrogen embrittlement KW - Hollow specimen technique KW - Pipeline steel KW - SSRT PY - 2024 AN - OPUS4-59746 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Fey, Gero T1 - Thermophysically Simulated Weld HAZ and CCT Diagram of� High Strength Low Alloy Pipeline Steel N2 - Kurzvorstellung der laufenden Projekte "Wasserstoffabhängige mechanische Eigenschaften der Schweißnahtgefüge niedriglegierter Stähle für Ferngasleitungen" und "Praktikable Prüfung geschweißter Ferngasleitungen aus niedrig-legierten Stählen für den sicheren Transport von Wasserstoff" mit kurzem Ergebnisstand und zukünftiger Versuchsplanung/Outlook T2 - Sitzung des NA 092-00-05 GA "Gemeinschaftsarbeitsausschuss NAS/NMP: Zerstörende Prüfung von Schweißverbindungen (DVS AG Q 4/Q 4.1)" CY - Online meeting DA - 20.03.2025 KW - ZTU-Diagramm KW - CCT KW - WEZ KW - Dilatometry KW - Pipeline Steel PY - 2025 AN - OPUS4-63107 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hübner, Martin T1 - Einfluss der Nahtgeometrie auf den Eigenspannungsabbau unter Verwendung von Low Transformation Temperature (LTT) – Schweißzusätzen N2 - Low Transformation Temperature (LTT)-Schweißzusätze stellen einen innovativen Ansatz zur Erhöhung der Ermüdungsfestigkeit geschweißter Konstruktionen dar. LTT-Schweißzusätze zeichnen sich durch eine martensitische Phasenumwandlung nahe der Raumtemperatur aus, welche Druckeigenspannungen in der Schweißnaht und der Wärmeeinflusszone (WEZ) generieren. Dieser Vortrag fokussiert sich auf die gezielte Einbringung zusätzlicher LTT-Lagen an ermüdungskritischen Stellen von konventionell geschweißten Verbindungen. Dies ermöglicht eine ökonomische Anwendung, ohne dass die Schweißnahtintegrität zu stark beeinflusst wird. Die Auswirkungen zusätzlicher LTT-Lagen wurden anhand geschweißter Längssteifen aus hochfestem Stahl hinsichtlich der chemischen Zusammensetzung und der Eigenspannungen untersucht. Unter Variation der Schweißgeschwindigkeit und Abstand zur konventionellen Naht konnten 3 unterschiedliche Nahtausführungen des Chrom-Nickellegierten LTT-Zusatzes bewertet werden. Die chemische Zusammensetzung wurde mittels OES-Analysen untersucht. Dabei stellte heraus, dass die Aufmischung in allen Varianten sehr ähnlich war trotz teils unterschiedlicher LTT-Volumina. Härtebestimmungen ergaben in allen 3 Varianten eine ähnliche Härte. Daraus lässt sich annehmen, dass die Martensitstarttemperatur bei allen Nahtvarianten ähnlich ist. Röntgenografische Eigenspannungsmessungen belegen, dass die Eigenspannungen am versa-genskritischen Nahtübergang bei Einsatz von LTT-Schweißzusätzen deutlich abgesenkt werden. Während die konventionelle Schweißnaht Zugeigenspannungen von ca. 350 MPa aufweist, können an den LTT-Nähten teilweise Druckeigenspannungen von bis zu -150 MPa nachgewiesen werden. Je höher der Abstand zur konventionellen Naht und je größer das eingebrachte LTT-Volumen ist, umso stärker sind die Eigenspannungsreduzierungen am Nahtübergang. Da in allen 3 Varianten eine ähnliche Martensitstarttemperatur angenommen werden kann, ist somit die Geometrische Komponente der LTT-Zusatzlage ein entscheidender Faktor für die Eigenspannungsreduzierung. T2 - AWT FA 13 CY - Wolfsburg, Germany DA - 19.03.2024 KW - Chemische Zusammensetzung, KW - LTT KW - Nahtgeometrie KW - Eigenspannungen PY - 2024 AN - OPUS4-60135 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Residual stress reduction using LTT welding consumables with focus on the weld geometry N2 - This article focuses on the selective placement of additional LTT layers to generate compressive residual stresses in fatigue-critical areas of conventional weld joints. This enables an economical solution without effecting the integrity of welded joints. For this, longitudinal stiffeners made of high-strength steel were gas metal arc welded using conventional welding consumable in the first layer. Afterwards, a chromium-nickel alloyed LTT welding consumable was deposit on front sides of the stiffeners. By varying the welding parameters, different weld geometries of the LTT filler metal could be analyzed. The effects of additional LTT layers were investigated with regards to residual stresses, microstructure and strength. X-ray residual stresses measurements show that the residual stresses at the failure critical weld toe are significantly reduced by using additional LTT layers. While the conventional weld is characterized by tensile residual stresses, compressive residual stresses can be detected at the LTT weld. The level of residual stresses is influenced by the geometry of the LTT layer. Additional LTT layers with a high offset to the conventional weld generate more compressive residual stress in the HAZ than with a low offset. Therefore, the weld geometry has a considerable impact on the residual stress profile. T2 - IIW Intermediate Meeting Comission II-A CY - Incheon, Republic of Korea DA - 12.03.2024 KW - LTT KW - Residual stress KW - High strength steel PY - 2024 AN - OPUS4-59747 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Scharf-Wildenhain, R. A1 - Hälsig, A. A1 - Hensel, J. A1 - Wandtke, Karsten A1 - Schröpfer, Dirk A1 - Kromm, Arne A1 - Kannengießer, Thomas T1 - Einfluss von Wärmeführung und Bauteildesign auf die Eigenschaften und fertigungsbedingten Beanspruchungen additiv geschweißter hochfester Feinkornbaustähle N2 - Hochfeste Feinkornbaustähle verfügen über großes Potenzial für gewichtsoptimierte, effiziente Strukturen in vielen modernen Stahlkonstruktion. Weitere Effizienzsteigerungen können durch additives Fertigen sowie bionische Bauweisen erreicht werden. Hochfeste Zusatzwerkstoffe für additives MSG-Schweißen (engl.: Wire Arc Additive Manufacturing, WAAM) sind bereits von den Schweißzusatzherstellern lieferbar. Eine breite industrielle Anwendung insbesondere für KMU ist aufgrund fehlender quantitativer Erkenntnisse und Richtlinien bezüglich schweißbedingter Beanspruchungen und Bauteilsicherheit während der Herstellung und des Betriebs derzeit stark limitiert. In einem gemeinsamen Forschungsprojekt (FOSTA-P1380/IGF21162BG) der BAM und der TU Chemnitz werden daher die mit Eigenspannungsausbildung und der Gefahr einer Kaltrissbildung verbundenen prozess- und werkstoffbedingten sowie konstruktiven Einflüsse beim WAAM hochfester Stähle untersucht. Der vorliegende Beitrag fokussiert die Analyse der Auswirkungen von Schweißwärmeführung und Design der WAAM-Bauteile auf die Abkühlbedingungen, Gefüge, mechanisch-technologischen Eigenschaften und Eigenspannungen. Hierfür werden geometrisch definierte Probenkörper (Hohlquader) vollautomatisiert mit einem speziellen, hochfesten WAAM-Massivdraht (Streckgrenze >790 MPa) geschweißt. Die Wärmeführung und Probenabmessungen werden innerhalb eines statistischen Versuchsplans variiert. Die Schweißwärmeführung wird dabei so eingestellt, dass die t8/5-Abkühlzeiten im empfohlenen Verarbeitungsbereich (ca. 5 s bis 20 s) sichergestellt sind. Hierzu ließen sich über zusätzliche thermo-physikalische Umformsimulationen mittels Dilatometer die komplexen Wärmezyklen abbilden und die resultierende Zugfestigkeit des Schweißgutes bestimmen. Das WAAM-Schweißen komplexer Geometrien mit variierenden Schweißwärmeführungen und geometrischen Verhältnissen bzw. Wanddicken bedingt neben den Auswirkungen auf die Abkühlbedingungen, Abkühlzeiten und Gefüge deutliche Einflüsse auf die konstruktiven Steifigkeitsverhältnisse beim Schweißen. Es zeigen sich anhand der Schweißexperimente signifikante Auswirkungen durch Probenskalierung und Wärmeeinbringung auf die resultierenden lokalen Eigenspannungen. Die Folge können ungünstige Bauteileigenschaften und risskritische Zugeigenspannungen sein. T2 - DVS Congress 2022 CY - Koblenz, Germany DA - 19.09.2022 KW - MAG-Schweißen KW - Additive Fertigung KW - Eigenspannungen KW - Hochfester Stahl KW - Kaltrisssicherheit KW - Wärmeführung KW - Windenergie PY - 2022 SN - 978-3-96144-189-1 VL - 382 SP - 737 EP - 745 PB - DVS Media GmbH CY - Düsseldorf AN - OPUS4-56719 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schröder, Nina A1 - Rhode, Michael A1 - Kannengießer, Thomas T1 - Mikrolegierungseinfluss auf das Ausscheidungsverhalten und die mechanischen Eigenschaften geschweißter hochfester Baustähle N2 - Mikrolegierungselemente, wie Nb und Ti, sind für die signifikante Festigkeitssteigerung von vergüteten, hochfesten Feinkornbaustählen mit einer Nominalstreckgrenze ≥ 690 MPa unerlässlich. Normvorgaben zur chemischen Zusammensetzung geben dabei nur obere Grenzwerte für die Hersteller vor. Weiterhin wirken sich bereits kleine Abweichungen in der Legierungsroute teilweise drastisch auf die mechanischen Eigenschaften aus. Somit wird eine adäquate Vorhersage der Schweißeignung und der Integrität der Schweißverbindung aufgrund der variierenden Mikrogefüge erschwert bis unmöglich. Unerwünschte Nebeneffekte sind die mögliche Erweichung der Wärmeeinflusszone (WEZ) als auch der gegenteilige Effekt der Aufhärtung. Vor diesem Hintergrund werden erstmals systematisch die unterschiedlichen Mikrolegierungsrouten mit variierenden Ti und Nb-Gehalten an Versuchsschmelzen untersucht. Die Stahlgüte S690QL bildet dabei die Grundlage der chemischen Zusammensetzung sowie der entsprechenden Wärmebehandlung. Zur Untersuchung der jeweiligen Schweißeignung wurden Dreilagen-Schweißungen mittels moderner MAG-Hochleistungsschweißprozesse durchgeführt und kritische Gefügebereiche mit hoher Erweichung/Aufhärtung identifiziert. Der Fokus der analytischen Betrachtungen lag hier auf der Identifikation der Phasenumwandlungen beim Abkühlen und auf dem metallurgischen Ausscheidungsverhalten. Zusätzlich wurden isotherme und nicht-isotherme Phasenberechnungen mit der Software Thermo-Calc durchgeführt. Mechanisch-technologische Untersuchungen zur Kerbschlagzähigkeit mittels Kerbschlagbiegeversuchen durchgeführt wurden, bestätigen dabei die Ergebnisse der thermodynamischen Simulation bezüglich des Ausscheidungsverhaltens während der Temperatur-Zeit Schweißzyklen. Daraus lässt sich der Einfluss der Wärmeeinwirkung beim Schweißen auf die Gefügeausbildung in der WEZ und der korrespondierenden mechanischen Eigenschaften qualitativ beschreiben. T2 - DVS Congress 2023 Große Schweißtechnische Tagung CY - Essen, Germany DA - 11.09.2023 KW - WEZ-Erweichung KW - Mikrolegierungseinflüsse KW - Hochfester Feinkornbaustahl KW - Kerbschlagzähigkeit PY - 2023 SN - 978-3-96144-230-0 VL - 389 SP - 218 EP - 225 PB - DVS Media GmbH CY - Düsseldorf AN - OPUS4-59419 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schröder, Nina T1 - Einfluss unterschiedlicher Mikrolegierungsrouten eines S690QL auf das Ausscheidungsverhalten in der WEZ N2 - Mikrolegierungselementen, wie Nb und Ti sind für eine signifikante Festigkeitssteigerung von vergüteten, hochfesten Feinkornbaustählen mit einer Nominalstreckgren-ze ≥ 690 MPa unerlässlich. Normvorgaben zur chemischen Zusammensetzung dieser Stähle geben zur Erzielung der vorgeschriebenen Eigenschaften dabei oft nur Grenzgehalte für die Hersteller vor. Die Wirkung der Mikrolegierungselemente bzw. ihrer Karbide und/oder Nitride ist teilweise komplett konträr, insbesondere bei Auflösung und Wiederausscheidung in der WEZ bei identischem Schweißzusatz. Somit wird eine adäquate Vorhersage der Chargenabhängigkeit hinsichtlich der Schweißeignung und des Tragverhaltens der Schweißverbindung erschwert. Eine unerwünschte Eigenschaft ist dabei die Erweichung der WEZ, wie auch u.U. der gegenteilige Effekt der Aufhärtung. T2 - 5. Symposium Materialtechnik CY - Clausthal-Zellerfeld, Germany DA - 23.02.2023 KW - Divergente Ausbildung der Wärmeeinflusszone KW - Hochfester vergüteter Feinkornbaustahl KW - Thermodynamische Simulation KW - Mikrolegierungseinfluss PY - 2023 AN - OPUS4-58004 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael T1 - Combined effect of heating rate and restraint condition on stress relief cracking susceptibility during PWHT of thick walled Cr Mo V steel submerged arc welded joints N2 - Contemporary steels creep-resistant steels like the 13CrMoV9-10 are used as thick plates e.g., for applications in hydrocrackers. The large plate thickness requires high efficiency welding processes like submerged arc welding (SAW) and a mandatory post weld heat treatment (PWHT). The PWHT-parameters stem from a combination of empirical knowledge and traditional experiments on free shrinking (FS) welds. In that connection, the formation of so-called stress-relief cracking (SRC) must be anticipated. The SRC susceptibility of a welded component is a complex combination and interaction of com-ponent specific, thermal, and metallurgical factors. Many of which have to date not been conclusively researched. For example, it is well known that SRCs develop during PWHT due to formation and growth of carbides on prior austenite grain boundaries, resulting in a significant hardness increase (secondary hardening) and toughness decrease. This leads to a high SRC susceptibility of the coarse grain heat-affected zone (CGHAZ) of the last weld bead during PWHT. This is intensified in case of high residual stresses from the component-specific, structurally induced stiffness. In combination with multi-layer welding this leads to a multiaxial stress distribution. Nonetheless, the combined effect of PWHT and high-residual stresses on the SRC formation is merely unknown. For that reason, this study presents the effect of different heating rates in conjunction with a certain component stiffness. For that reason, SAW joints of 13CrMoV9-10 steel were investigated under FS and defined external restraint condition. T2 - 77th IIW Annual Assembly and International Conference, Meeting of Commission II-A CY - Ixia, Rhodes, Greece DA - 07.07.2024 KW - Stress relief cracking KW - Submerged arc welding KW - Post weld heat treatment KW - Cr-Mo-V steel PY - 2024 AN - OPUS4-60675 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wandtke, Karsten T1 - Einfluss der Prozessführung auf den Eigenspannungszustand beim WAAM-Schweißen hochfester Stahlbauteile N2 - Hochfeste Feinkornbaustähle verfügen über großes Potenzial für gewichtsoptimierte, effiziente Strukturen in vielen modernen Stahlkonstruktion. Weitere Effizienzsteigerungen können durch additives Fertigen sowie bionische Bauweisen erreicht werden. Hochfeste Zusatzwerkstoffe für additives MSG-Schweißen (engl.: Wire Arc Additive Manufacturing, WAAM) sind bereits von den Schweißzusatzherstellern lieferbar. Eine breite industrielle Anwendung insbesondere für KMU ist aufgrund fehlender quantitativer Erkenntnisse und Richtlinien bezüglich schweißbedingter Beanspruchungen und Bauteilsicherheit während der Herstellung und des Betriebs derzeit stark limitiert. In einem gemeinsamen Forschungsprojekt (FOSTA-P1380/IGF21162BG) der BAM und der TU Chemnitz werden daher die mit Eigenspannungsausbildung und der Gefahr einer Kaltrissbildung verbundenen prozess- und werkstoffbedingten sowie konstruktiven Einflüsse beim WAAM hochfester Stähle untersucht. Der vorliegende Beitrag fokussiert die Analyse der Auswirkungen von Schweißwärmeführung und Design der WAAM-Bauteile auf die Abkühlbedingungen, Gefüge, mechanisch-technologischen Eigenschaften und Eigenspannungen. Hierfür werden geometrisch definierte Probenkörper (Hohlquader) vollautomatisiert mit einem speziellen, hochfesten WAAM-Massivdraht (Streckgrenze >790 MPa) geschweißt. Die Wärmeführung und Probenabmessungen werden innerhalb eines statistischen Versuchsplans variiert. Die Schweißwärmeführung wird dabei so eingestellt, dass die t8/5-Abkühlzeiten im empfohlenen Verarbeitungsbereich (ca. 5 s bis 20 s) sichergestellt sind. Hierzu ließen sich über zusätzliche thermo-physikalische Umformsimulationen mittels Dilatometer die komplexen Wärmezyklen abbilden und die resultierende Zugfestigkeit des Schweißgutes bestimmen. Das WAAM-Schweißen komplexer Geometrien mit variierenden Schweißwärmeführungen und geometrischen Verhältnissen bzw. Wanddicken bedingt neben den Auswirkungen auf die Abkühlbedingungen, Abkühlzeiten und Gefüge deutliche Einflüsse auf die konstruktiven Steifigkeitsverhältnisse beim Schweißen. Es zeigen sich anhand der Schweißexperimente signifikante Auswirkungen durch Probenskalierung und Wärmeeinbringung auf die resultierenden lokalen Eigenspannungen. Die Folge können ungünstige Bauteileigenschaften und risskritische Zugeigenspannungen sein. Im Rahmen der Normungssitzung werden praktikable Verarbeitungsempfehlungen basierend auf den Erkenntnissen des Vh. mit Vertretern aus Industrie und Forschung diskutiert. T2 - NA 092-00-05 GA: Gemeinschaftsarbeitsausschuss NAS/NMP: Zerstörende Prüfung von Schweißverbindungen (DVS AG Q 4/Q 4.1) CY - Online meeting DA - 10.03.2022 KW - MAG-Schweißen KW - Additive Fertigung KW - Eigenspannungen KW - Hochfester Stahl KW - Kaltrisssicherheit KW - Wärmeführung KW - Windenergie PY - 2022 AN - OPUS4-56722 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schröder, Nina T1 - Auswirkungen von Titan und Niob auf das metallurgische Schweißverhalten von hochfesten Feinkornbaustählen und deren mechanischen Eigenschaften N2 - Mikrolegierungselemente wie Nb und Ti sind entscheidend für die erwünschte mechanische Festigkeit von vergüteten Feinkornbaustählen mit einer Nennstreckgrenze von ≥ 690 MPa. Aktuelle Spezifikationen geben lediglich Obergrenzen für die chemische Zusammensetzung vor, allerdings können geringfügige Abweichungen erhebliche Auswirkungen auf die mechanischen Eigenschaften haben. Die Vorhersage der Schweißbarkeit und Integrität von Schweißverbindungen stellt aufgrund der variierenden Zusammensetzung und Mikrostrukturen Herausforderungen dar. Unerwünschte Effekte wie Erweichung der Wärmeeinflusszone (WEZ) oder Verfestigung können auftreten. Um dies zu untersuchen, wurden verschiedene Mikrolegierungsrouten mit variierenden Ti- und Nb-Gehalten an Laborschmelzen erforscht. Die Basis jeder Route entsprach der üblichen S690QL in Zusammensetzung und Wärmebehandlung. Dreilagenschweißungen wurden mittels Metallaktivgasschweißens (MAG) durchgeführt, um kritische Gefügebereiche zu identifizieren. Die Analyse konzentrierte sich auf Phasenumwandlungen während der Abkühlung und metallurgisches Ausscheidungsverhalten. Die mechanischen Eigenschaften der Schweißnähte wurden durch Zugversuche ermittelt. Die Ergebnisse zeigen einen bedeutenden Einfluss der Mikrolegierungsroute und Schweißwärmezufuhr auf die Ausscheidungskinetik, trotz insgesamt guter Schweißbarkeit der Werkstoffe. T2 - Bacheloranden-, Masteranden-, Doktoranden Kolloquium CY - Magdeburg, Germany DA - 17.01.2024 KW - WEZ-Erweichung KW - Hochfester Feinkornbaustahl KW - Digital Image Correlation KW - Querzugversuch KW - Mikrolegierungseinfluss PY - 2024 AN - OPUS4-59420 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Einfluss spanender Bearbeitungsschritte auf die Eigenspannungen additiv gefertigter Komponenten aus hochfestem Stahl N2 - Diese Studie konzentriert sich auf den Einfluss der Bearbeitung auf die Eigenspannungen und den Verzug von WAAM-Proben. Definierte Proben wurden vollautomatisch mit einem speziellen WAAM-Massivdraht (Streckgrenze >820 MPa) mit unterschiedlichen geometrischen Designs geschweißt. Der Eigenspannungszustand vor und nach dem Abtrennen der AM-Struktur von der Substratplatte wurde mittels Röntgenbeugung an der Probenoberfläche analysiert und durch 3D-Verformungsanalysen mittels Photogrammetrie ergänzt. Die Ergebnisse zeigen einen signifikanten Einfluss der Geometrie auf die Relaxation und Umverteilung der Eigenspannungen. T2 - NA 092-00-05 GA "Gemeinschaftsarbeitsausschuss NAS/NMP: Zerstörende Prüfung von Schweißverbindungen (DVS AG Q 4/Q 4.1) CY - Berlin, Germany DA - 20.03.2024 KW - DED-arc KW - Eigenspannungen KW - Hochfester Stahl PY - 2024 AN - OPUS4-59753 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Eissel, A. A1 - Engelking, Lorenz A1 - Treutler, K. A1 - Schröpfer, Dirk A1 - Wesling, V. A1 - Kannengießer, Thomas ED - da Silva, L. F. M. ED - Martins, P. A. F. ED - Reisgen, U. T1 - Nickel-Iron-Alloy Modification to Enhance Additively Welded Microstructure for Subsequent Milling N2 - The aerospace industry uses nickel–iron alloys, e.g., FeNi36, to create moulding tools for composite materials, since these alloys have a low coefficient of thermal expansion. Nickel–iron alloys are hard-to-cut materials. The moulding tools are large in size and involve complex structures, making them cost-intensive and difficult to manufacture. Thus, the focus is set on additive manufacturing, which can additionally enable the repair of components in order to eliminate local defects. However, the process usually results in a heterogeneous microstructure and anisotropic mechanical properties. As there is a high demand for a precise and exact fit of the precision moulds and the surface quality, the welded components must be subsequently machined. Additionally, inhomogeneous microstructure may lead to unstable cutting forces and conditions. Consequently, a modification of the microstructure morphology is achieved through specific alloy modifications in order to stabilise and improve the subsequent machining process. Therefore, titanium and zirconium are chosen as modification elements with a maximum 1% weight percent and are added to nickel–iron alloy powder. The elements are alloyed, and build-up welded by plasma-transferred-arcwelding. The resulting microstructure morphology of the welded wall structure and the machining properties are then determined. It can be shown that titanium has a significant effect on the structural morphology of the welded layers, as well as on the machining. KW - Alloy modification KW - Alloy 36 KW - Plasma-transferred arc welding KW - Ultrasonic-assisted milling KW - Surface integrity PY - 2022 SN - 978-3-030-95463-5 DO - https://doi.org/10.1007/978-3-030-95463-5_6 SP - 85 EP - 99 PB - Springer CY - Cham AN - OPUS4-55484 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Increasing the Significance of Varestraint Tests through Improved Crack Evaluation N2 - It was found that there is a systematic dependence of the crack growth on the welding parameters as well as on the load. Decreasing welding speeds with simultaneously higher heat input promote crack formation with increasing strain rate. Based on the results, a new crack criterion was finally selected which allows an extended assessment of the material behavior during the MVT-test. The threshold introduced can quantify the dependencies of the crack formation on the welding and testing parameters, which could not be comprehensively described with the conventional evaluation. In principle, the evaluation routine can also be transferred to other Varestraint or externally loaded hot cracking tests. T2 - IIW Intermediate Meeting Comission II-c CY - Garching, Germany DA - 06.03.2023 KW - Solidification cracking KW - Varestraint-Test PY - 2023 AN - OPUS4-57131 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael T1 - Quantitative Bestimmung von Wasserstoff durch Heißgasextraktion: Erfahrungen und Grenzen N2 - Die Trägergas-Heißextraktion (TGHE) mit Warmauslagerung (d.h. ohne Schmelzen der Proben) ist eine häufig angewandte Technik zur Bestimmung von Wasserstoff, u.a. für Schweißverbindungen aber auch allgemein für Metalle geeignet. Die TGHE basiert auf der beschleunigten Wasserstoffausgasung aufgrund der thermischen Aktivierung bei erhöhten Temperaturen. Die Norm ISO 3690 schlägt hierzu verschiedene Probengeometrien sowie die erforderliche Mindestextraktionszeit in Abhängigkeit der Temperatur vor. Die vorliegende Präsentation fasst die Ergebnisse und Erfahrungen zahlreicher Testläufe an der BAM der letzten 15 Jahre mit unterschiedlichen Probentemperaturen, Geometrien, etc. zusammen, die die Wasserstoffbestimmung beeinflussen können. Dabei handelt es sich insbesondere um die Bewertung des Absorptionskoeffizienten für Infrarotstrahlung der Probenoberfläche, die begrenzte Empfindlichkeit von WLD im Vergleich zum MS, die Temperaturmessung, u.v.m. Zusammenfassend lässt sich sagen, dass die Temperatur die treibende Kraft der TGHE ist. Es werden Vorschläge zur Verbesserung der Zuverlässigkeit der Wasserstoffbestimmung gemacht, die von der Stabilität des Wasserstoffsignals während der Extraktion und der Auswertung der aufgezeichneten Daten abhängt. Im Allgemeinen ist eine unabhängige Temperaturmessung mit Dummy-Proben für die weitere Datenanalyse nützlich, insbesondere wenn diese Daten für die Berechnung der Einfangkinetik verwendet werden. T2 - Herbstsitzung des DGM Arbeitskreises "Materialprüfung unter Wasserstoff" CY - Dortmund, Germany DA - 19.11.2024 KW - Wasserstoff KW - Trägergasheißextraktion KW - Messung KW - Massenspektrometrie KW - Schweißen PY - 2024 AN - OPUS4-61721 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schröpfer, Dirk T1 - Residual stress formation in DED-arc manufactured high strength steel components N2 - Additive manufacturing (AM) processes enable the efficient production of advanced constructions. New developments in topology optimization are leading to weight-optimized designs of increasing complexity. Direct energy deposition processes (DED) such as wire and arc-based additive manufacturing are an important method of additive manufacturing. The wire filler metals enable a wide range of materials, while the arc process provides a high deposition rate compared to laser and powder-based processes. Combined with the use of high-strength steels, the thickness of walls or components can be significantly reduced in the context of lightweight construction, which results in significant savings in energy, costs, time and resources. Suitable high-strength steel filler metals are commercially available for DED-arc AM processes. However, guidelines and quantitative knowledge about welding stresses and cold cracking issues during component production and service are lacking. This limits the industrial application considerably. In a joint project of BAM and Chemnitz University of Technology, the main influences and complex interactions of material, production process, design and processing steps on the residual stress level are investigated. The aim is to develop processing recommendations and a cold cracking test for economical processing and stress-related design of high-strength steels with DED-arc. This study focuses on residual stress analysis by neutron diffraction (ND) and X-ray diffraction (XRD) on defined test specimens. The ND analysis were performed at the Paul Scherrer Institute- Villigen, Switzerland (PSI) and the XRD analysis at BAM. The study shows a quantitative and qualitative comparison of the residual stress magnitudes and distribution between the component bulk (ND) and surface (XRD) analyses. The ND analysis reveals that in DED-arc AM walls the residual stresses dominate in the direction of welding and are negligibly small in each case transverse to the direction of welding. The topology of the analyzed residual stresses shows almost identical residual stress maps compared to XRD. In addition, the residual stresses are significantly influenced by the solid phase transformation of the material due to low cooling times and less post heat treatment cycles of following AM layers in the area of the top layer. T2 - IIW Intermediate Meeting C-II/CIX CY - Munich, Germany DA - 06.03.2023 KW - Additive manufacturing KW - High strength steel KW - Residual stress PY - 2023 AN - OPUS4-59307 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Scharf-Wildenhain, R. A1 - Hälsig, A. A1 - Hensel, J. A1 - Wandtke, Karsten A1 - Schröpfer, Dirk A1 - Kannengießer, Thomas T1 - Heat control and design‑related effects on the properties and welding stresses in WAAM components of high‑strength structural steels N2 - Commercial high-strength fller metals for wire arc additive manufacturing (WAAM) are already available. However, widespread industrial use is currently limited due to a lack of quantitative knowledge and guidelines regarding welding stresses and component safety during manufacture and operation for WAAM structures. In a joint research project, the process- and material-related as well as design infuences associated with residual stress formation and the risk of cold cracking are being investigated. For this purpose, reference specimens are welded fully automated with defned dimensions and systematic variation of heat control using a special, high-strength WAAM fller metal (yield strength>790 MPa). Heat control is varied by means of heat input (200–650 kJ/m) and interlayer temperature (100–300 °C). The ∆t8/5 cooling times correspond with the recommendations of fller metal producers (approx. 5–20 s). For this purpose, additional thermo-physical forming simulations using a dilatometer allowed the complex heat cycles to be reproduced and the resulting ultimate tensile strength of the weld metal to be determined. Welding parameters and AM geometry are correlated with the resulting microstructure, hardness, and residual stress state. High heat input leads to a lower tensile stress in the component and may cause unfavorable microstructure and mechanical properties. However, a sufciently low interlayer temperature is likely to be suitable for obtaining adequate properties at a reduced tensile stress level when welding with high heat input. The component design afects heat dissipation conditions and the intensity of restraint during welding and has a signifcant infuence on the residual stress. These complex interactions are analyzed within this investigation. The aim is to provide easily applicable processing recommendations and standard specifcations for an economical, appropriate, and crack-safe WAAM of high-strength steels. KW - GMA welding KW - Additive manufacturing KW - Residual stresses KW - High-strength steel KW - Cold cracking safety KW - Heat control KW - Wind energy PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-567397 DO - https://doi.org/10.1007/s40194-022-01450-x SN - 1878-6669 VL - 2022 SP - 1 EP - 11 PB - Springer CY - Berlin AN - OPUS4-56739 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Eissel, A. A1 - Engelking, Lorenz A1 - Gustus, R. A1 - Treutler, K. A1 - Wesling, V. A1 - Schröpfer, Dirk A1 - Kannengießer, Thomas T1 - Alloy modification for additive manufactured Ni alloy components—part I: effect on microstructure and hardness of Invar alloy N2 - Alloy 36 (1.3912), also known as “Invar,” is an alloy with 36% nickel. The alloy has a remarkably low thermal expansion coefficient in certain temperature ranges. This peculiarity is called the invar effect, which was discovered in 1896 by the Swiss physicist Charles Édouard Guillaume. Therefore, it is used in applications in which dimensional stability is critical, such as molding tools for composite materials in aerospace, automotive applications, or liquified natural gas (LNG) cargo tanks. Moreover, increasingly complex structures and the optimization of resource efficiency also require additive manufacturing steps for the production or repair of components. Additively manufactured components have a heterogeneous microstructure and anisotropic mechanical properties. In addition, the manufactured components require subsequent machining surface finishing, like finish milling, to achieve their final contour. Nickel iron alloys are difficult to machine. Additionally, inhomogeneous microstructure may lead to unstable cutting forces and conditions. In part I of this investigation, the initial alloy 36 is modified with the elements Ti, Zr, and Hf up to a maximum of 0.33 wt.-%. The influence of the modification elements on the microstructure as well as on the hardness of the AM components is examined. Furthermore, one modification is applied to metal arc welding process and investigated. Part II focuses on the effect of the alloy modifications on machinability as well as on the surface integrity of plasma-transferred-arc-welded (PTA) and finish milled invar components. T2 - 75th IIW Annual Assembly CY - Tokyo, Japan DA - 17.07.2022 KW - Alloy modification KW - Alloy 36 KW - Plasma-transferred arc welding PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-571777 DO - https://doi.org/10.1007/s40194-023-01510-w SN - 0043-2288 SP - 1 EP - 9 PB - Springer CY - Heidelberg AN - OPUS4-57177 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Engelking, Lorenz A1 - Eissel, A. A1 - Schröpfer, Dirk A1 - Treutler, K. A1 - Kannengießer, Thomas A1 - Wesling, V. T1 - Optimisation of surface residual stresses using ultrasonic‑assisted milling for wire‑arc additive manufactured Ni alloy components N2 - Nickel alloys are cost intensive materials and generally classified as difficult-to-cut material. However, machining of these materials is needed especially in case of alloy 36 (1.3912), which is commonly used in mould construction for the production of fibre-reinforced composites. With regard to repair, modification and manufacturing of such components, additive manufacturing offers significant economic advantages. Nevertheless, subsequent machining steps are needed to achieve the final component contour and defined surface conditions. Dependent on the material and machining process conditions, detrimental tensile residual stresses may be the result on the machined surface, having negative impact on the component performance and safety. In this investigation, machining experiments were carried out on wire arc additive manufactured components made of alloy 36, varying the cutting speed and the feed rate. In addition, the conventional milling process (CM) was compared with a modern, hybrid machining process, the ultrasonic-assisted milling (US). The cutting forces and the surface-near residual stresses were analysed using X-ray diffraction. A significant improvement of the machinability as well as the surface integrity by using the ultrasonic assistance was observed, especially at low cutting speeds. The CM induced mainly tensile residual stresses, the US mainly compressive residual stresses. KW - Surface integrity KW - Ultrasonic-assisted milling KW - Additive manufacturing KW - Ni alloy KW - Alloy 36 PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-575246 DO - https://doi.org/10.1007/s00170-023-11326-z SN - 1433-3015 VL - 126 IS - 9 SP - 4191 EP - 4198 PB - Springer Nature AN - OPUS4-57524 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Schröpfer, Dirk A1 - Becker, Amadeus A1 - Kannengießer, Thomas T1 - Kurzdarstellung der Projektergebnisse: Beanspruchungsgerechte Reparatur von Schweißverbindungen bei der Fertigung von Bauteilen aus hochfesten Feinkornbaustählen N2 - Bei der Montage von Stahlkonstruktionen kommt es trotz anforderungsgerechter schweißtechnischer Fertigung vereinzelt zur Detektion von unzulässigen Unregelmäßigkeiten im Schweißbereich. In einem Forschungsprojekt (FOSTA P1311) wurden Untersuchungen durchgeführt und Kenntnisse erarbeitet, um mittelfristig vor allem KMU beanspruchungsgerechte Reparaturkonzepte zur Verfügung zu stellen. Damit können letztlich Schäden und zumeist teure Nacharbeiten verhindert und eine verbesserte Ausnutzung des hohen Festigkeitspotentials hochfester Stähle erreicht werden. Gerade KMU können mit Blick auf die Kosten für Fertigung, Schweißarbeit und Material von den Erkenntnissen beim Einsatz hochfester Stähle, die für eine effiziente Realisierung der Energiewende in Deutschland notwendig sind, profitieren. KW - MAG-Schweißen KW - Hochfester Stahl KW - Eigenspannungen KW - Thermisches Ausfugen KW - Reparaturschweißen KW - Gefügedegradation PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-555822 SP - 1 EP - 2 PB - Bundesanstalt für Materialforschung und -prüfung (BAM) CY - Berlin AN - OPUS4-55582 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Rhode, Michael A1 - Kromm, Arne A1 - Mente, Tobias A1 - Brackrock, Daniel A1 - Czeskleba, Denis A1 - Kannengießer, Thomas T1 - Component test for the assessment of delayed hydrogen-assisted cracking in thick-walled SAW joints for offshore applications N2 - Offshore wind turbines continuously increase in size and weight and demand adequate offshore foundations concepts like monopiles, tripods, or jackets. These components are typically constructed using submerged arc welding (SAW) with high-strength thick steel plates like the S420ML. During welding, the occurrence of delayed hydrogen-assisted cracking (HAC) must be anticipated. HAC is a critical combination of the local hydrogen concentration within a susceptible microstructure under certain mechanical load, i.e., the occurring (welding) residual stresses. The welding sequence of the thick-walled plates complicates the residual stress distribution due to the necessary repeated thermal cycling, i.e., welding seam/layer deposition to fill the joint. For that purpose, SAW with two-wire-technique was used to weld a specially designed and prototype-like mock-up of a real component with a thickness of 50 mm, filled with over 20 passes and a seam length of 1000 mm. Additional welded stiffeners simulated the effect of a high restraint, to achieve critical HAC conditions. The necessity of a minimum waiting time (MWT) before the NDT can be conducted (to exclude HAC) was critically verified by the application of ultrasonic testing of the welded joint at different time-steps of the NDT of up to 48 h after the completion welding. The residual stresses were determined by a robot XRD goniometer. Tensile residual stresses up to the yield limit are found both in the weld metal and in the heat-affected zone. Numerical modeling allowed the qualitative estimation of the hydrogen diffusion in the weld. No noticeable HAC occurrence was identified and confirms the high cracking resistance of the investigated material. Finally, the applicability of the MWT concept should be critically discussed. KW - Hydrogen KW - Cold cracking KW - Minimum Waiting Time KW - Offshore steel grade KW - Component test PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-591981 DO - https://doi.org/10.1007/s40194-023-01658-5 SP - 1 EP - 15 PB - Springer Science and Business Media LLC AN - OPUS4-59198 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kromm, Arne A1 - Thomas, Maximilian A1 - Kannengießer, Thomas A1 - Gibmeier, Jens T1 - On the interpretation of Varestraint and Transvarestraint hot cracking test results N2 - The Varestraint test and its variant Transvarestraint are one of the most widely used techniques for evaluating a material solidification cracking sensitivity during welding. The result of such tests is a crack length which is proportional to the material’s cracking susceptibility. Nevertheless, the welding and load parameters can unintentionally influence the crack length, which in some cases can distort the material evaluation. An approach is described as to how these effects can be assessed with the aid of a digital crack analysis. The crack lengths are compared position-dependently with their possible propagation due to the weld pool movement during continuous loading. The index derived from this can be used by the operator to evaluate his test parameters. In addition, a comparison of the results of different Varestraint setups is made possible. Alongside experimental results, a numerical sensitivity analysis is presented on how individual welding and loading parameters can affect the crack lengths. KW - Varestraint test KW - Solidification cracking KW - Weldability PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-595089 DO - https://doi.org/10.1007/s40194-024-01706-8 SN - 0043-2288 SP - 1 EP - 13 PB - Springer Science and Business Media LLC AN - OPUS4-59508 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Quackatz, Lukas A1 - Griesche, Axel A1 - Nietzke, Jonathan A1 - Kannengießer, Thomas T1 - In situ measurement of hydrogen concentration in steel using laser‑induced breakdown spectroscopy (LIBS) N2 - The ISO 3690 standard “Determination of hydrogen content in arc weld metal” requires a thermal activation of the diffusible hydrogen in a piece of weld metal for the subsequent ex situ concentration measurement by carrier gas hot extraction CGHE or thermal desorption spectroscopy (TCD). Laser-induced breakdown spectroscopy (LIBS) offers a time and spatially resolved, almost non-destructive, in situ measurement of hydrogen at surfaces without sample preparation. We measured hydrogen in steels, which were charged either electrochemically or by high-pressure hydrogen gas, and compared the results. Further, the feasibility of quantitative hydrogen line scan measurements with LIBS was demonstrated by measuring hydrogen at water jet cut surfaces. The hydrogen concentrations measured with the help of LIBS were compared with CGHE measurements. It was observed that hydrogen can be reliably measured with LIBS for concentrations larger than 2 wt.-ppm. The maximum hydrogen concentration achieved using electrochemical charging was 85.1 ppm. The results show that LIBS is a promising technique for time- and spatially resolved measurements of hydrogen in steels. T2 - IIW Annual Assembly 2023 CY - Singapore KW - LIBS KW - Hydrogen measurement KW - Welding KW - Stainless steel KW - Diffusible hydrogen PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-593664 DO - https://doi.org/10.1007/s40194-023-01677-2 SP - 1 EP - 9 PB - Springer AN - OPUS4-59366 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wandtke, Karsten ED - Becker, Amadeus ED - Schröpfer, Dirk ED - Kromm, Arne ED - Kannengießer, Thomas ED - Scharf-Wildenhain, R. ED - Hälsig, A. ED - Hensel, J. T1 - Residual Stress Evolution during Slot Milling for Repair Welding and Wire Arc Additive Manufacturing of High-Strength Steel Components N2 - High-strength steels offer potential for weight optimization due to reduced wall thicknesses in modern constructions. Additive manufacturing processes such as Wire Arc Additive Manufacturing (WAAM) enable the resource-efficient production of structures. In the case of defects occurring in weld seams orWAAM components due to unstable process conditions, the economical solution is local gouging or machining and repair welding. It is important to understand the effects of machining steps on the multiaxial stress state in conjunction with the design-related shrinkage restraints. Research into how welding and slot milling of welds andWAAM structures affects residual stresses is still lacking. For this reason, component-related investigations with high-strength steels with yield strengths ≥790 MPa are carried out in our research. In-situ digital image correlation (DIC) and ex-situ X-ray diffraction (XRD) were used to analyze the stresses and strains induced on specimens during and after milling. The systematic analyses revealed a significant interaction of the stiffness and microstructure of the specimens with the initial residual stresses induced by welding. Subsequent repair welds can result in significantly higher residual stresses. KW - High strength steels KW - Additive manufacturing KW - Residual stress KW - Repair welding KW - Ditigtal image correlation PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-593515 DO - https://doi.org/10.3390/met14010082 VL - 14 IS - 1 SP - 1 EP - 11 PB - MDPI CY - Basel AN - OPUS4-59351 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schröder, Nina A1 - Rhode, Michael A1 - Kannengießer, Thomas T1 - Thermodynamic prediction of precipitations behaviour in HAZ of a gas metal arc welded S690QL with varying Ti and Nb content N2 - For a significant increase in the strength of high-strength fine-grained structural steels with a nominal yield strength ≥690 MPa, the addition of microalloying elements such as Nb and Ti is required. The standard specifications for the chemical composition of these steels (e.g., in EN 10025-6) often only give the manufacturer limit contents to achieve the defined properties. The effect of the alloying elements in the heat affected zone (HAZ) is sometimes completely contrary. This makes it difficult to adequately predict the batch dependency regarding weldability and the load-bearing behaviour of the welded joint. Three different micro-alloyed steels of the grade S690QL were produced on a laboratory scale, focusing on different Nb and Ti contents. To investigate the tempering effect, these were gas metal arc welded in three layers. In addition to metallographic investigations of individual HAZ areas, thermodynamic phase calculations were carried out using Thermo-Calc, following variations in the chemical composition. This provides an understanding of phase transformation, precipitation growth, and dissolution during welding as a function of temperature and cooling conditions. The results show a divergent metallurgical behaviour in the HAZ of the three different micro-alloyed steels. Thereby, the Ti micro-alloyed grade showed a strong softening of the HAZ in contrast to the Nb micro-alloyed grade. This can be attributed to a contrary precipitation behaviour during welding. KW - High-strength structural steel KW - Gas metal arc welding KW - HAZ-softening KW - Microalloying influences KW - Thermodynamic simulation PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-579988 DO - https://doi.org/10.1007/s40194-023-01550-2 SN - 0043-2288 SP - 1 EP - 10 PB - Springer AN - OPUS4-57998 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wandtke, Karsten A1 - Schröpfer, Dirk A1 - Scharf-Wildenhain, R. A1 - Hälsig, A. A1 - Kromm, Arne A1 - Kannengießer, Thomas A1 - Hensel, J. T1 - Fertigungsbedingte Beanspruchungen und Kaltrisssicherheit in generativ gefertigten Bauteilen aus hochfesten Feinkornbaustählen - Kurzdarstellung der Projektergebnisse, FOSTA P1380 N2 - Die Verwendung hochfester Feinkornbaustähle hat für viele Anwendungen des Stahlbaus ein großes Potenzial für gewichtsoptimierte, effiziente Strukturen mit ho-her mechanischer Beanspruchbarkeit. Weitere Zugewinne an Effizienz sind durch generative Fertigungsschritte sowie bionische Bauweisen erzielbar. Hierzu stehen bereits kommerzielle hochfeste drahtförmige Zusatzwerkstoffe für formgebendes MSG-Schweißen zur Verfügung. Dem Einsatz stehen noch fehlende quantitative Aussagen zu den fertigungsbedingten Beanspruchungen und der Bauteilsicherheit während Herstellung und Betrieb im Wege. Dies betrifft insbesondere prozess- sowie materialbedingte Einflüsse und die konstruktive Schrumpfbehinderung verbunden mit der Ausbildung hoher Zugeigenspannungen und damit zusammenhängenden Kaltrissbildung. Hierfür wurden im Projekt detaillierte und anwenderbezogene Kenntnisse zu den komplexen Wechselwirkungen zwischen Schweißprozess und Wärmeführung während der Fertigung, der metallurgischen Vorgänge und insbesondere der vorliegenden konstruktiven Einflüsse auf die entstehenden Eigenspannungen erarbeitet, um ein frühzeitiges Bauteilversagen aufgrund eines hohen fertigungsbedingten Beanspruchungsniveaus bis hin zu einer Rissbildung während der Fertigung sicher zu vermeiden. Gleichzeitig wurden die Einflüsse auf die mechanisch-technologischen Gütewerte systematisch analysiert. Zudem wurden die Auswirkungen trennender Verfahren durch Entfernen der Substratplatte sowie durch die spanende Bearbeitung der Vorformlinge zu Endbauteilgeometrien geklärt, da diese unmittelbar den Eigenspannungszustand beeinflussen und deutlichen Verzug der Bauteile auslösen. Für das generative Schweißen konnten Verarbeitungsempfehlungen sowie Normenvorgaben erarbeitet werden. Dies hilft insbesondere KMU eine wirtschaftliche, beanspruchungsgerechte und risssichere generative Fertigung von Bauteilen aus hochfesten Feinkornbaustählen zu ermöglichen. KW - MAG-Schweißen KW - Additive Fertigung KW - Eigenspannungen KW - Kaltrisssicherheit KW - Hochfester Stahl PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-582198 N1 - Das IGF-Vorhaben IGF-Nr. 21162 BG (P 1380) "Fertigungsbedingte Beanspruchungen und Kaltrisssicherheit in generativ gefertigten Bauteilen aus hochfesten Feinkornbaustählen" der Forschungsvereinigung Stahlanwendung e. V. wurde über die AiF im Rahmen des Programms zur Förderung der Industriellen Gemeinschaftsforschung (IGF) vom Bundesministerium für Wirtschaft und Klimaschutz aufgrund eines Beschlusses des Deutschen Bundestages gefördert. SP - 1 EP - 2 PB - Bundesanstalt für Materialforschung und -prüfung (BAM) CY - Berlin AN - OPUS4-58219 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schröpfer, Dirk A1 - Witte, Julien A1 - Kromm, Arne A1 - Kannengießer, Thomas T1 - Stresses in repair welding of high-strength steels—part 1: restraint and cold cracking risk N2 - AbstractThe sustainable and resource-efficient production of wind energy plants requires the use of modern high-strength fine-grain structural steels. This applies to both foundation and erection structures, like mobile or ship cranes. During the assembly of steel structures, unacceptable defects can occasionally be found in the weld area. In most cases, the economical solution would be local thermal gouging of the affected areas and re-welding. Due to the high shrinkage restraint of the joint groove in the overall structure, the superposition of global and local welding-induced stresses may lead to crack formation and component failure, particularly in interaction with the degradation of the microstructure and mechanical properties of high-strength steels during the repair process. However, manufacturers hardly have any information about these issues and there is a lack of recommendations and guidelines to take these safety-relevant aspects into account in adequate repair concepts. The aim of this research is to derive recommendations for repair concepts appropriate to the stresses and materials involved providing a basis for standards and guidelines to avoid cold cracking, damage and expensive reworking especially for high-strength steels. Part 1 of this study involves systematic investigations of influences of shrinkage restraint during repair welding of two high-strength steels S500MLO for offshore application and S960QL for mobile crane structures. The quantification of the shrinkage restraint of repair weld joints was achieved by means of experimental and numerical restraint intensity analysis. In welding experiments with self-restrained slot specimens, restraint intensity and introduction of hydrogen via the welding arc using anti spatter spray were varied systematically to analyse the effect on welding result, residual stresses and cold cracking. It could be shown that increasing restraint intensities result in significantly higher transverse residual stress levels. In the case of hydrogen introduction S500MLO showed no cold cracking independent of the restraint conditions. However, S960QL was found to be considerably cold cracking sensitive if hydrogen is introduced. With increasing restraint intensity length and number of cold cracks increases significantly. Part 2 [1] of this study is focussed on microstructure and residual stresses due to gouging and stress optimization via adequate heat control parameters in repair welding. KW - Metals and Alloys KW - Mechanical Engineering KW - Mechanics of Materials PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-595212 DO - https://doi.org/10.1007/s40194-024-01691-y SN - 0043-2288 SP - 1 EP - 13 PB - Springer Science and Business Media LLC AN - OPUS4-59521 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schröder, Nina A1 - Rhode, Michael A1 - Kannengießer, Thomas T1 - Influence of microalloying on precipitation behavior and notch impact toughness of welded high‑strength structural steels N2 - Microalloying elements such as Nb and Ti are essential to increase the strength of quenched and tempered high-strength low alloy (HSLA) structural steels with nominal yield strength ≥ 690 MPa and their welded joints. Standards such as EN 10025–6 only specify limits or ranges for chemical composition, which leads to variations in specific compositions between steel manufacturers. These standards do not address the mechanical properties of the material, and even small variations in alloy content can significantly affect these properties. This makes it difficult to predict the weldability and integrity of welded joints, with potential problems such as softening or excessive hardening of the heat-affected zone (HAZ). To understand these metallurgical effects, previous studies have investigated different microalloying routes with varying Ti and Nb contents using test alloys. The high-strength quenched and tempered fine-grained structural steel S690QL is the basic grade regarding chemical composition and heat treatment. To evaluate weldability, three-layer welds were made using high-performance MAG welding. HAZ formation was investigated, and critical microstructural areas were identified, focusing on phase transformations during cooling and metallurgical precipitation behavior. Isothermal thermodynamic calculations for different precipitations were also carried out. Mechanical properties, especially Charpy notch impact toughness, were evaluated to understand the influence of different microalloys on the microstructure of the HAZ and mechanical properties. KW - High-strength structural steel KW - Gas metal arc welding KW - HAZ-softening KW - Notch impact toughness KW - Microalloying influences KW - Thermodynamic simulation PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-608548 DO - https://doi.org/10.1007/s40194-024-01827-0 SN - 0043-2288 SP - 1 EP - 13 PB - Springer AN - OPUS4-60854 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Willeke, Maraike A1 - Giese, Marcel A1 - Lorenz, Swenja A1 - Treutler, Kai A1 - Schröpfer, Dirk A1 - Wesling, Volker A1 - Kannengießer, Thomas T1 - Effect of alloy modification on the wear protection coatings made of Ni- and Co-based materials and surface machinability via ultrasonic milling process N2 - AbstractWear-resistant coatings are required for highly efficient and economical steel components in equipment, process, and power plant engineering to withstand high corrosive, tribological, thermal, and mechanical stresses. Co-alloys are used as wear-resistant coatings for steel components, tailored to the specific application. The substitutability of Co alloys with Ni-based wear protection systems, in addition to price and supply uncertainties, is facilitated by the combination of innovative welding and machining processes such as ultrasonic-assisted milling. The aim of the study is to improve the machinability of two different hard-facing alloys while maintaining the same wear protection potential. Therefore, the wear-resistant alloys NiMoCrSi (Colmonoy C56) and CoMnCrSi (Tribaloy T400) were modified by the alloying additions Nb, Hf, and Ti and then applied to a carbon-manganese steel S355 using the plasma transfer arc (PTA) welding process. The influence of the alloying additions on the microstructure as KW - Wear resistance KW - Co-based alloy KW - Ni-based alloy KW - PTA welding process KW - Ultrasonic assisted milling process PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-623931 DO - https://doi.org/10.1007/s00170-024-14955-0 SN - 0268-3768 SP - 1 EP - 17 PB - Springer Science and Business Media LLC AN - OPUS4-62393 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Quackatz, Lukas A1 - Westin, Elin Marianne A1 - Griesche, Axel A1 - Kromm, Arne A1 - Kannengießer, Thomas A1 - Treutler, Kai A1 - Wesling, Volker A1 - Wessman, Sten T1 - Assessing ferrite content in duplex stainless weld metal: WRC ‘92 predictions vs. practical measurements N2 - AbstractThe weldability of stainless steels is largely controlled by the chemical composition, and alloys with ferritic or ferritic-austenitic solidification show the highest resistance to hot cracking. As the resulting phase balance also affects the final properties, it may be beneficial to both foresee and measure the weld metal ferrite content. The WRC ‘92 constitution diagram is currently the most accurate prediction tool available, but it does not take the cooling rate into consideration and the precision may be less accurate for stainless steels with high ferrite numbers (FNs). This study aims to assess the reliability of the WRC ‘92 diagram for weld metals with FN  50. The chemical composition was altered through gas tungsten arc welding (GTAW) of UNS S32205 with ER347 filler wire that had been coated using physical vapor deposition (PVD) with either niobium (Nb), copper (Cu), nickel (Ni), manganese (Mn), carbon (C), or silicon (Si). The actual ferrite content was evaluated using image analysis, FeriteScope and X-ray diffraction (XRD). While predictions from the WRC ‘92 diagram were deemed acceptable for Ni, Si, and Mn, notable deviations were observed for Nb, Cu, and C. The FeriteScope exhibited a consistent trend with image analysis, albeit with slightly higher FN values, wider scatter, and the conversion factor from FN to vol% is open for discussion. The lowest accuracy and largest spread were obtained using non-contact XRD, rendering it unsuitable for ferrite measurements of welds. These findings underscore the need for improved prediction tools and appropriate measurement methods for assessing ferrite content in duplex weld metals. KW - Duplex stainless steel KW - Welding KW - Phase balance KW - Microscopy KW - Microstructure PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-618777 DO - https://doi.org/10.1007/s40194-024-01878-3 SN - 1878-6669 VL - 69 IS - 1 SP - 31 EP - 45 PB - Springer CY - Berlin AN - OPUS4-61877 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -