TY - CONF A1 - Charmi, Amir T1 - Application of deep learning for structural health monitoring of a composite overwrapped pressure vessel undergoing cyclic loading N2 - Structural health monitoring (SHM) using ultrasonic-guided waves (UGWs) enables continuous monitoring of components with complex geometries and provides extensive information about their structural integrity and their overall condition. Composite overwrapped pressure vessels (COPVs) used for storing hydrogen gases at very high pressures are an example of a critical infrastructure that could benefit significantly from SHM. This can be used to increase the periodic inspection intervals, ensure safe operating conditions by early detection of anomalies, and ultimately estimate the remaining lifetime of COPVs. Therefore, in the digital quality infrastructure initiative (QI-Digital) in Germany, an SHM system is being developed for COPVs used in a hydrogen refueling station. In this study, the results of a lifetime fatigue test on a Type IV COPV subjected to many thousands of load cycles under different temperatures and pressures are presented to demonstrate the strengths and challenges associated with such an SHM system. During the cyclic testing up to the final material failure of the COPV, a sensor network of fifteen surface-mounted piezoelectric (PZT) wafers was used to collect the UGW data. However, the pressure variations, the aging process of the COPV, the environmental parameters, and possible damages simultaneously have an impact on the recorded signals. This issue and the lack of labeled data make signal processing and analysis even more demanding. Thus, in this study, semi-supervised, and unsupervised deep learning approaches are utilized to separate the influence of different variables on the UGW data with the final aim of detecting and localizing the damage before critical failure. T2 - 11th European Workshop on Structural Health Monitoring CY - Potsdam, Germany DA - 10.06.2024 KW - Anomaly detection KW - Damage localization KW - Deep learning KW - Structural health monitoring KW - Ultrasonic-guided waves PY - 2024 AN - OPUS4-60745 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - El Moutaouakil, H. A1 - Fuchs, C. A1 - Savli, E. A1 - Heimann, Jan A1 - Prager, Jens A1 - Moll, J. A1 - Tschöke, K. A1 - Márquez Reyes, O. A1 - Schackmann, O. A1 - Memmolo, V. A1 - Schneider, T. T1 - Acquiring a Machine Learning Data Set for Structural Health Monitoring of Hydrogen Pressure Vessels at Operating Conditions using Guided Ultrasonic Waves N2 - Hydrogen is an energy source of increasing importance. As hydrogen is very reactive to air and needs to be stored under high pressure, it is crucial to provide safe transportation and storage. Therefore, structural health monitoring, based on guided ultrasonic waves and machine learning methods, is used for Composite Overwrapped Pressure Vessels (COPVs) containing hydrogen. To acquire data that allows robust detection of COPV defects, there are two main process parameters to consider. These are the pressurization of the vessel and the temperature conditions at the vessel. This paper will focus on the derivation of a design of experiment (DoE) from the needs of various validation scenarios (e.g. concerning pressure, temperature or excitation frequency). Practical limitations must be considered as well. We designed experiments with multiple reversible damages at different positions. A network of 25 transducers, structured as five rings with five sensors in one line, is installed on a vessel. Guided ultrasonic waves are used via the pitch-catch procedure, which means that the transducers act pairwise as transmitter and receiver in order to measure all transmitterreceiver combinations. This leads to 600 signal paths, recorded by a Verasonics Vantage 64 LF data acquisition system. Finally, the influences of temperature and pressure within the acquired data set are going to be visualized. T2 - 11th European Workshop on Structural Health Monitoring CY - Potsdam, Germany DA - 10.06.2024 KW - Composite Overwrapped Pressure Vessel KW - Hydrogen KW - Guided Ultrasonic Waves KW - Data Acquisition KW - Pressurization KW - Machine Learning PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-607472 DO - https://doi.org/10.58286/29754 SN - 1435-4934 SP - 1 EP - 8 AN - OPUS4-60747 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Gleim, Tobias T1 - Experimental And Numerical Analyses For The Evaluation Of Heat Fluxes Of A Fire Reference Test N2 - Packages for the transport of high-level radioactive material are designed to endure severe accidents. To obtain approval, these transport packages must adhere to the specification-based criteria of the IAEA SSR-6 [1]. To ensure compliance with these requirements, specific mechanical and thermal tests need to be appointed with respect to the package type. Typically, IAEA SSR-6 [1] prescribes mechanical tests followed by a thermal fire test as part of a cumulative test sequence. To approve the fire test, BAM uses a reference package representing the original package in its outer geometry for characterizing the actual fire and its impact on the package. This serves a dual purpose: it allows the precise adjustment of experimental parameters for the package design to be approved, and it provides input parameters for thermomechanical simulations, cf. [2]. With the help of this methodology for characterizing boundary conditions of the package, temperature evolutions within the reference package can be studied in a Finite-Element Analyses (FEA). This helps to compare the experiments with the numerical simulations on the case of the reference package, but also serves at the same time for preliminary simulations with the package design to be approved. The thermal test consists of a 30-minute fully engulfing 800°C pool fire or an equally severe fire, e.g. a propane gas fire. The fire reference test is performed prior to the regulatory fire test with the package design to be approved. The fire reference package in the described case is a closed sheet 316L steel cylinder with a wall thickness of 10 mm, a length of 182 mm, and a diameter of 102 mm. The package was instrumented with thermocouples and filled with heat resistant insulating material. T2 - ASME PVP 2024 CY - Bellevue, WA, USA DA - 28.07.2024 KW - Experimental KW - Numerical KW - Heat Flux KW - Reference Test PY - 2024 AN - OPUS4-60847 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Gleim, Tobias T1 - Safety Aspects for Transport Containers with regard to Ageing and Battery Accident Scenarios N2 - In Germany, the search for a final repository for highly radioactive material is currently based on the assumption that interim storage will take considerably longer than was anticipated. At that time, authorization procedures assumed that interim storage would be brief, until the containment systems could be placed in a final repository. For today's new approvals and extensions, the IAEA (International Atomic Energy Agency) regulations for the transport of radioactive material require an assessment of all components and component groups with regard to ageing. To assess the safety requirements not only over the previously envisaged periods but also over long durations, numerous individual parts and component groups must be examined and evaluated for ageing and interactions between materials. The metal seals of a double lid sealing system, for example, are critical components that must be studied with respect to ageing. In a containment system for radioactive material, metal seals must not only undergo classic ageing, but also withstand mechanical influences and radiation over extended periods. In addition to assessments by the applicants, BAM must also independently analyze and evaluate these ageing mechanisms as part of its sovereign mandate. Another challenge in both new approvals and extensions is the assessment of transport regarding changes in the state of the art, which are not synchronously assessed in the regulations. In transporting radioactive material, a classic oil fire has been assumed in a hypothetical accident scenario from the development of the regulations to the present day. Due to the rapid development of propulsion technologies in recent years, such as battery or hydrogen-powered vehicles, investigations must be conducted in the revision process of the IAEA regulations to assess the impact of these new technologies on safety assessments. It is important for the member states of the IAEA to know whether new technologies are covered by the regulations or if changes are necessary to continue issuing international licenses. By focusing on batteries from the material to the cell to the module and the application, BAM contributes to the evaluation of batteries at every step of the chain. In addition to the safety of current and new battery technologies, BAM also endeavors to address issues of compositional trace and sustainable energy materials. T2 - MSD: Leaf CY - Livermore, CA , USA DA - 07.08.2024 KW - Safety Aspects KW - Ageing KW - Accident Scenarios KW - Battery PY - 2024 AN - OPUS4-60851 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Naster, Maximilian T1 - Experimental and Numerical Analyses for the Evaluation of Hydrogen as an Energy Source for Thermal Testing of Transport Packages of Radioactive Material N2 - In this paper we present a new hydrogen-based test rig for an ongoing feasibility study of using hydrogen as an energy source for the thermal testing of transport packages containing radioactive materials. The test rig will be capable of combusting hydrogen for a wide range of different burner geometries, mass flows and if necessary hydrogen blends. As this type of fire test according to the IAEA boundary conditions does not yet exist, a large number of preliminary investigations, safety assessments and calculations must be carried out in order to develop a viable concept for hydrogen fires. In the first step of the feasibility study, the temperature, structure, and radiation of various hydrogen flames are surveyed. In future works, the results will make it possible to design burner frames that are suitable for fire reference tests in order to make comparisons with pool and propane fires used in assessment procedures today. In parallel comparative numerical simulations are conducted to model the thermal behaviour of hydrogen flames using the software package Ansys®. On the one hand, the numerical simulations support the experiments by providing an overview of numerous parameters and the measuring range; on the other hand, they will help with the design of the burner frame in future work. This paper gives an overview in the design and capabilities of the test rig. Furthermore, the results of the parameter studies show that burner geometry and mass flow provide a significant design margin for the thermal shape of the hydrogen flames. In addition, the results of the initial numerical calculations will be used to determine the necessary sensors, the positions, and their operating range. Only the optimal interaction allows a controlled system that permits user-defined hydrogen fires. T2 - PVP2024, Pressure Vessels & Piping Conference CY - Bellevue, Washington, USA DA - 29.07.2024 KW - Hydrogen KW - Fire KW - IAEA Regulations KW - CFD KW - Burner PY - 2024 AN - OPUS4-60855 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Vlassopoulos, Efstathios A1 - Dagan, Ron A1 - Fiorito, Luca A1 - Herm, Michel A1 - Jansson, Peter A1 - Kromar, Marjan A1 - Király, Márton A1 - Leppanen, Jaakko A1 - Feria Marquez, Francisco A1 - Metz, Volker A1 - Papaioannou, Dimitrios A1 - Herranz, Luis Enrique A1 - Rochman, Dimitri A1 - Schillebeeckx, Peter A1 - Seidl, Marcus A1 - Hernandez Solis, Augusto A1 - Stankovskiy, Alexey A1 - Alvarez Velarde, Francisco A1 - Verwerft, Marc A1 - Rodriguez Villagra, Nieves A1 - Wiss, Thierry A1 - Zencker, Uwe A1 - Žerovnik, Gasper T1 - EURAD Work Package 8 Deliverable 8.2 Updated State-of-the-Art Report N2 - The state-of-the-art (SOTA) report offers an overview of the status of knowledge in the area of spent nuclear fuel (SNF) characterisation and assessment during the pre-disposal phase using several numerical and experimental approaches and methodologies. A review on characterisation of SNF properties in terms of source term and inventory assessment (neutron, gamma-ray emission, decay heat, radionuclide inventory, and elemental content) and in terms of out-of-core fuel performance (cladding performance and fuel integrity in view of the safety criteria for SNF interim storage, transport and canister packaging) is presented. This updated SOTA report provides the progress made in the spent fuel characterisation (SFC) work package as part of the European Joint Programme on Radioactive Waste Management (EURAD), documents the identified technical gaps, and provides recommendations for future work. The report is expected to be used by all EURAD colleagues in their national programmes as a key resource for knowledge management programmes and to contribute to demonstrating and documenting the state-of-the-art. KW - Radioactive waste management KW - Spent fuel characterisation KW - Extended interim storage KW - Predisposal PY - 2024 UR - https://www.ejp-eurad.eu/publications/d82-updated-state-art-report SP - 1 EP - 182 AN - OPUS4-61218 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Grunewald, Thomas T1 - Entzündung von wasserstoffhaltigen Atmosphären durch mechanisch erzeugte Funken N2 - In einer Forschungskooperation zwischen BG-RCI und der Bundesanstalt für Materialforschung und -prüfung (BAM) wurde im Rahmen des Forschungsvorhabens „HySpark“ untersucht, wie sich die Zündwahrscheinlichkeit von verschiedenen, metallischen Werkstoffpaarungen in unterschiedlichen Methan-Wasserstoff-Gemischen verhält. Es bestehen signifikante Unterschiede in der Zündwahrscheinlichkeit durch mechanisch erzeugte Schlagvorgänge zwischen den ver¬schiedenen Metallen bzw. Stählen und insbesondere zwischen den einzelnen Brenngas/Luft-Gemischen. Mechanisch erzeugte Schlagfunken stellen in explosionsgefährdeten Bereichen eine potentielle Zündquelle dar, oft in Verbindung mit der Zündquelle „heiße Oberflächen“. Eine Vielzahl von mechanischen und reaktionskinetischen Einflüssen verursacht dabei eine komplexe Interaktion von Parametern, von deren Auswirkung auf die Zündwahrscheinlichkeit bislang wenig bekannt ist. Die statistisch erfassten Eigenschaften von Schlagfunken in verschiedenen Untersuchung der BAM lassen auf stochastische Prozesse schließen, bei denen die Anzahl der durch einen Schlagprozess abgetrennten Partikel und deren Oxidationsverhalten sowie die Höhe der kinetischen Schlagenergie entscheidenden Einfluss auf die Zündwahrscheinlichkeit hat /L4/; /L5/. Werkzeuge sind keine Geräte oder Schutzsysteme im Sinne der Richtlinie 2014/34/EU /L1/. Deshalb ist es nicht möglich, Werkzeuge in Übereinstimmung mit dieser Richtlinie zu zertifizieren. Trotzdem müssen die Materialien für solche Werkzeuge bestimmte Mindestanforderungen gemäß TRGS 723 /L2/ erfüllen. Die TRGS 723 Abschnitt 5.15 fordert den Nachweis der Funkenfreiheit der verwendeten Werkstoffpaarung bei Verwendung in explosionsgefährdeten Berei¬chen. Der Nachweis der Erfül¬lung dieser Anforderungen ist durch Zertifizierungen im sogenannten „gesetzlich nicht geregelten“ Bereich möglich. Die BAM bietet diese Zertifizierung im Rahmen ihres Zertifizierungsprogrammes 2.8 „Funkenarme Werkzeuge“ an /L3/. Bei der Gefährdungsbeurteilung für den Gebrauch von Werkzeugen im explosionsgefährdeten Bereich müssen mechanisch erzeugte Funken oder heiße Reibflächen, die bei mechanischen Schlagvorgängen durch den Einsatz von Werkzeugen oder Geräten bzw. Maschinen entstehen können, müssen als Zündquelle gesondert betrachtet werden. Üblicherweise wird die Mindestzündenergie bzw. die Explosionsgruppe auch für die Beurteilung der Zündwirksamkeit von mechanischen Schlägen für Brenngase herangezogen [6]. Während Schlagvorgänge als Zündquelle für explosionsfähige Atmosphären der Explosionsgruppe IIA in vielen Fällen weniger relevant sind, werden sie besonders bei Vorhandensein einer explosionsfähigen Atmosphäre der Explosionsgruppe IIC als sehr wirksame Zündquelle angesehen, die berücksichtigt werden muss. Entsprechend wird in der TRGS 723 [6] sowie der DIN EN ISO 80079-36 [21] als Schutzmaßnahme z.B. die Verwendung von funkenarmen Werkzeugen aus nicht gehärtetem schwer oxidierbarem Nicht-Eisen-Metall genannt, wobei die mögliche kinetische Schlagenergie unter 60 J bleiben und die Funkenfreiheit für die jeweils vorliegende mögliche Werkstoffpaarung (Werkstück, Stützen, Boden usw.) nachgewiesen sein muss. Manche Hersteller von Werkzeugen, die für den Einsatz in explosionsgefährdeten Bereichen vorgesehen sind, nennen ihre Werkzeuge „funkenfrei“. Die Bezeichnung wird missverständlicher Weise abgeleitet aus dem englischen „non sparking tools“. Die Bezeichnung funkenarme Werkzeuge, „low sparking tools“, trifft eher zu, denn es gibt tatsächlich keine funkenfreien, metallischen Werkzeuge. Denn es ist immer eine Frage mit welcher kinetischen Energie und gegen welchen weiteren potentiellen Schlagpartner/Werkstoff die funkenarmen Werkzeuge geschlagen werden. Üblicherweise werden Werkzeuge für den industriellen Einsatz aus hochlegierten Chromstählen hergestellt. Mit steigender kinetischer Schlagenergie und sinken¬der Zündenergie der Brenngas-Luft-Atmosphäre im explosionsgefährdeten Be¬reich, steigt die Zündwahrscheinlichkeit im Falle von Schlag- oder Reibbeanspru¬chung deutlich. Funkenarme Werkzeuge für den Einsatz in explosionsgefährdeten Bereichen wer¬den überwiegend aus speziellen Nichteisen-Metalllegierungen (NE-Metall) her¬stellt. Die beiden großen Werkstoffsorten zur Herstellung von funkenarmen Werkzeugen sind Aluminium-Bronze und Kupfer-Aluminium. Für diese beiden Werkstoffe und deren mögliche Schlagpartner gibt es bisher nur wenige umfassenden Untersuchungen mit Aussagen zur Zündwahrscheinlichkeit. T2 - 18. Essener Explosionsschutztage, Haus der Technik e.V. (HdT), Außeninstitut der RWTH Aachen, Veranst.-Nr. VA24-00428-050-E CY - Essen, Germany DA - 24.09.2024 KW - Mechanisch erzeugte Funken KW - Schlagfunken KW - Schleiffunken KW - Reibfunken KW - Nichtelektrische Funken KW - Mechanischer Explosionsschutz KW - Nichtelektrischer Explosionsschutz KW - Funkenarme Werkzeuge KW - Funkenfreie Werkzeuge KW - Ex-Werkzeuge PY - 2024 AN - OPUS4-61120 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eichner, Lukas T1 - LUKAS’ JACKET: A test structure for model and monitoring based lifetime management of offshore jacket support structures N2 - The goal of the experiments is to demonstrate that systems like three-dimensional jackets possess redundancies that, despite the reduced fatigue life of individual components, enable reliable operation if an appropriate maintenance concept is in place. In practice, individual potentially faulty components in the structure have been handled conservatively so far. To move away from this approach, methods and strategies in the field of life cycle management that enable economically optimal and reliable operation must be transferred from scientific research to practice. Experiments are the preferred method to establish the proof of concept. To realistically simulate the operational lifetime of a jacket structure through an experiment, cyclic loads must be applied to the structure to replicate typical fatigue processes. To ensure that the test structure is not a "disposable product" and can undergo multiple test cycles, the experimental concept includes system-level and component-level tests. The latter are conducted on removable joints. These elements at the nodes of the structure have been manufactured in multiple variations, both to potentially contain mentioned flaws and to undergo more load cycles individually than the main structure. Once the removable joint is sufficiently pre-damaged and thus the reduced remaining fatigue life is established, the element is inserted into the overall structure. The defined maintenance strategy is then implemented on the entire system. This strategy consists of structural health monitoring (SHM), inspections, and repairs. At defined intervals, cyclic loading is interrupted to apply dynamic loads. Using the installed monitoring system and coupled operational modal analysis (OMA), the modal parameters of the structure are determined, which can help identify potential system damage. Optimal sensor placement (OSP) can be determined based on a maximum value of information (VoI) across the entire pre-posterior predicted service life. For detailed investigations at the hotspots, inspections are conducted using non-destructive methods, among others. Overall global and local information about the structure's condition is gathered these methods, which are then incorporated into models describing the structure through Bayesian updating. This allows for initial system identification based on different system responses and later updating of the predicted parameters of analytical and numerical models. Utilizing the updated models, decisions regarding maintenance actions, such as further inspections or repairs, are made, which are subject to uncertainties. The probabilistic models enable a reliability- and risk-based maintenance strategy, where, for example, maximum failure rates can act as triggers for maintenance actions. These decisions are relevant for the planned duration of the simulated operational lifetime, as well as for potential lifetime extensions, which are currently of significant importance in practice. Optimizing the maintenance strategy for the operational lifetime of the structures with these methods will lead to a higher utility of the offshore wind farm. The work associated with the test structure encompasses a variety of topics (including fatigue, damage detection and identification, reliability, Bayesian updating, system identification, SHM, maintenance planning, decisions under uncertainties), which are integrated through corresponding models and methods. All these models have been and are being applied in the numerical accompaniment of the experiments. By applying them to a structure that includes the relevant locations and aspects of real-world structures, both well-functioning and suboptimal parts of the established framework will be revealed. T2 - 20th EAWE PhD Seminar on Wind Energy CY - Visby, Sweden DA - 23.09.2024 KW - Offshore Jacket Support Structure KW - Test Structure KW - Fatigue KW - Lifetime Management KW - Structural Health Monitoring PY - 2024 AN - OPUS4-61146 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Chaudhuri, Somsubhro A1 - Stamm, Michael A1 - Lapšanská, Ivana A1 - Lançon, Thibault A1 - Osterbrink, Lars A1 - Driebe, Thomas A1 - Hein, Daniel A1 - Harendt, René T1 - Infrared Thermography of Turbulence Patterns of Operational Wind Turbine Rotor Blades Supported With High‐Resolution Photography: KI‐VISIR Dataset N2 - With increasing wind energy capacity and installation of wind turbines, new inspection techniques are being explored to examine wind turbine rotor blades, especially during operation. A common result of surface damage phenomena (such as leading edge erosion) is the premature transition of laminar to turbulent flow on the surface of rotor blades. In the KI-VISIR (Künstliche Intelligenz Visuell und Infrarot Thermografie—Artificial Intelligence-Visual and Infrared Thermography) project, infrared thermography is used as an inspection tool to capture so-called thermal turbulence patterns (TTPs) that result from such surface contamination or damage. To complement the thermographic inspections, high-resolution photography is performed to visualise, in detail, the sites where these turbulence patterns initiate. A convolutional neural network (CNN) was developed and used to detect and localise turbulence patterns. A unique dataset combining the thermograms and visual images of operational wind turbine rotor blades has been provided, along with the simplified annotations for the turbulence patterns. Additional tools are available to allow users to use the data requiring only basic Python programming skills. KW - Thermography KW - Thermografie KW - Wind energy KW - Leading edge erosion KW - KI PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-615772 DO - https://doi.org/10.1002/we.2958 IS - e2958 SP - 1 EP - 9 PB - Wiley AN - OPUS4-61577 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hicke, Konstantin T1 - Fibre Optic Sensors (Division 8.6) N2 - Fiber optic sensing technology being researched and developed at BAM and its numerous applications/ use cases is presented briefly after a short introductory part on the fundamentals of (distributed) fiber optic sensing. T2 - BAM - RCNDE (UK) Webinar CY - Online meeting DA - 13.11.2024 KW - Distributed fiber optic sensing KW - Structural health monitoring KW - Condition monitoring KW - DAS KW - Embedded fiber optic sensors PY - 2024 AN - OPUS4-61643 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kardjilov, Nikolay T1 - Neutron Thermo Tomography N2 - This study presents an investigation of the neutron transmission signal as a function of martensitic steel sample temperature and phase transformation during a welding process. A theoretical description that includes the Debye-Waller factor was used to describe the temperature influence on the neutron cross-sections. Neutron imaging using a monochromatic beam helps to observe transmission variations related to the martensitic-austenitic phase transformations before the Bragg-edge and to the material temperature above the Bragg-edge. In-situ neutron imaging of welding experiments show the distribution of the phase transformation and of the temperature in bulk steel samples. The performed finite element modelling of expected temperature distributions shows good agreement with the obtained experimental data. T2 - Neutron Wavelength-Dependent Imaging Workshop (NEUWAVE-12) CY - Lund, Sweden DA - 01.09.2024 KW - Neutron Imaging KW - Energy Selective KW - Neutron Thermo Tomography PY - 2024 AN - OPUS4-61265 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schneider, Ronald T1 - Impulsvortrag: Ermüdungslebensdauerbewertung mittels Informationen aus Monitoring und Inspektionen N2 - Kontext: Ermüdungsbeanspruchte Tragstrukturen von Windenergieanlagen, Bestimmung der Ermüdungsbeanspruchungen und -zuverlässigkeit auf der Grundlage von Simulationen aus dem Design unter Berücksichtigung von Modellunsicherheiten, Aktualisierung der Ermüdungsbeanspruchungen und -zuverlässigkeit auf der Grundlage von globalen Monitoring- und lokalen Inspektionsinformationen aus dem Betrieb unter Berücksichtigung von Modell- und Messunsicherheiten T2 - 3. Verbundtreffen ReNEW CY - Berlin, Germany DA - 05.09.2024 KW - Modellunsicherheiten KW - Windenergie KW - Ermüdungslebensdauer KW - Tragstrukturen KW - Monitoring KW - Inspektionen PY - 2024 AN - OPUS4-61427 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wille, Frank T1 - Tightness Verification Procedures of welded Lids for Encapsulations for Damaged Spent Nuclear Fuel in the Design Approval Process of Dual-Purpose Cask N2 - Damaged spent nuclear fuel (DSNF) can be loaded in Germany in dual-purpose casks (DPC) for transport and interim storage. Therefore, special encapsulations are needed to guarantee a safe handling and a reliable tight closure. These encapsulations must be durable and leak-tight for a possible long interim storage term and the transport thereafter. Because components inside the package containment like these special encapsulations are not accessible within periodical inspections of the DPC. Due to the general design of DPCs for standard fuel assemblies, specific requirements needed to be considered for the design of the special encapsulations for DSNF to ensure the loading in existing package designs. Especially the content of the encapsulations with damaged spent nuclear fuel must be avoided to enter in the inner space of the DPC, due to the possible higher amount of corrosive and radioactive material as well as greater quantities of water, which can be trapped in defect fuel rods. The main difference of the e T2 - ASME PVP 2024 CY - Bellevue, WA, USA DA - 28.07.2024 KW - Tightness verification KW - Weld seams KW - Drop tests KW - Encapsulations for damaged spent nuclear fuel KW - Helium leak tests PY - 2024 AN - OPUS4-61353 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hahn, Sarah-K. T1 - Second Life Verwendungen - Untersuchungen und erste Erfahrungen mit einem Ausbildungsdemonstrator N2 - Der Vortrag gibt zunächst einen Themeneinstieg in den Bereich der Second-Life-Batterien sowie rechtliche und technische Grundlagen zu Lebenszyklus und Alterung. Im Weiteren werden experimentelle Ergebnisse aus Versuchen zum thermischen Durchgehen mit Batteriemodulen aus dem BMBF-Vorhaben SEE-2L vorgestellt. Darüber hinaus wird ein eigens entwickelter Ausbildungsdemonstrators vorgestellt, welcher einen wesentlichen Baustein des Ergebnistransfers aus dem Vorhaben darstellt. T2 - Brände von Lithium-Ionen Batterien in Elektrofahrzeugen kontrollieren, eindämmen und vorbeugen CY - Essen, Germany DA - 25.04.2024 KW - Auswirkungsbetrachtungen KW - Elektrische Energiespeicher KW - Lithium-Ionen-Batterie KW - Stationäre Energiespeicher KW - Thermisches Durchgehen PY - 2024 AN - OPUS4-60187 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tschirschwitz, Rico T1 - Sicherheit stationärer elektrischer Energiespeicher – Ergebnisse aus dem Projekt SEE-2L N2 - Einleitend wird im Vortrag das Aktivitätsfeld Elektrische Energiespeicher und -umwandlung vorgestellt sowie eine kurze Einführung in die Terminologie der elektrischen Energiespeicher gegeben. Im Folgenden wird das BMBF-Vorhaben SEE-2L vorgestellt. Hier wird der Schwerpunkt auf die Entwicklung und den Aufbau eines Großversuchsstand für das thermische Durchgehen von Lithium-Batterien auf Modul- und Batterieebene gelegt. Darüber hinaus werden die Ergebnisse einer ersten Versuchsserie vorgestellt. Zum Abschluss wird ein kurzer Ausblick zu weiteren anstehenden Versuchen gegeben. T2 - Behörden-Erfahrungsaustausch Anlagensicherheit 2024 CY - Berlin, Deutschland DA - 03.06.2024 KW - Auswirkungsbetrachtungen KW - Elektrische Energiespeicher KW - Lithium-Ionen-Batterie KW - Stationäre Energiespeicher KW - Thermisches Durchgehen PY - 2024 AN - OPUS4-60190 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hahn, Sarah-K. T1 - Sicherheit elektrochemischer Energiespeicher – Ergebnisse aus dem Projekt SEE-2L N2 - Die Transformation der Energienutzung von konventionellen zu erneuerbaren Quellen führt dazu, dass zukünftig mehr Energie effizient zwischengespeichert werden muss. Eine Möglichkeit der elektrochemischen Zwischenspeicherung bieten Lithium-Ionen-Batterien. Hierfür können ausgemusterte Automobilantriebsbatterien verwendet werden. Erfüllen sie die hohen Anforderungen des mobilen Bereichs nicht mehr, haben sie oftmals noch eine ausreichende Kapazität und Leistungsfähigkeit für die stationäre Zwischenspeicherung. Neben der Verwendung der Batterien im größeren Maßstab, z.B. bei Energieversorgern, werden durch den vermehrten Einsatz von Photovoltaik-Anlagen in Ein- und Mehrfamilienhäusern verstärkt Zwischenspeicher für Privathaushalte nachgefragt. Dies birgt auch für Einsatzkräfte neue Herausforderungen in der Gefahrenabwehr. Im vom Bundesministerium für Bildung und Forschung (BMBF) geförderten Verbundprojekt „SEE-2L – Sicherheit elektrochemischer Energiespeicher in Second Life Anwendungen“ wurden Versuche mit Second Life Modulen durchgeführt. Verbundpartner im Projekt waren neben der vfdb die Otto-von-Guericke-Universität Magdeburg und die Bundesanstalt für Materialforschung und -prüfung. Zudem war das Institut der Feuerwehr Nordrhein-Westfalen eingebunden. Die durchgeführten Versuche bilden eine Grundlage für die Einordnung der Batteriespeicher, z.B. aus Sicht des baulichen Brandschutzes, zur Methodik der Brandbekämpfung oder zur Risikobewertung hinsichtlich der Prozess- und Anlagensicherheit. Im Beitrag werden die Versuchsergebnisse vorgestellt und Ansätze für deren Anwendung gezeigt. Um die gewonnenen Erkenntnisse zu vermitteln, wurde im Projekt zudem ein Schulungskonzept für Einsätze mit Lithium-Ionen-Technologien erarbeitet, das im Beitrag präsentiert wird. Es besteht aus theoretischen und praktischen Anteilen, sodass bei den Feuerwehren praxisnah aus- bzw. fortgebildet werden kann. T2 - vfdb-Jahresfachtagung CY - Magdeburg, Ger DA - 06.05.2024 KW - Auswirkungsbetrachtungen KW - Elektrische Energiespeicher KW - Lithium-Ionen-Batterie KW - Stationäre Energiespeicher KW - Thermisches Durchgehen PY - 2024 AN - OPUS4-60192 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Tschirschwitz, Rico A1 - Bernardy, Christopher T1 - Aufbau eines Großversuchsstandes sowie Realisierung von Brandversuchen mit elektrischen Energiespeichern im Bereich bis 500 kWh - Schlussbericht zum Teilvorhaben BAM, Teil I: Kurzbericht N2 - Der Abschlussbericht stellt die wesentlichen Arbeitsschritte und Ergebnisse des Teilvorhabens der BAM im BMBF-Vorhaben SEE-2L vor. Im Rahmen dieses Vorhabens wurde auf dem Testgelände Technische Sicherheit (BAM TTS) ein Großversuchsstand für das thermische Durchgehen von Lithium-Batterien auf Modul- und Batterieebene entwickelt und aufgebaut. Im Zuge des Projektes konnte eine erste Versuchsserie zu den Auswirkungen des thermischen Durchgehens von Batteriemodulen durchgeführt werden. Der Abschlussbericht umfasst zwei Teile, im Teil I den Kurzbricht und im Teil II die eingehende Darstellung. KW - Thermisches Durchgehen KW - Auswirkungsbetrachtungen KW - Elektrische Energiespeicher KW - Stationäre Energiespeicher KW - Lithium-Ionen-Batterie PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-600676 DO - https://doi.org/10.2314/KXP:1887873864 N1 - Das Projekt SEE-2L ist ein drittmittelfinanziertes Verbundvorhaben des BMBF, Förderkennzeichen 13N15493, Projektlaufzeit 01.02.2021 - 30.04.2023. SP - 1 EP - 20 PB - Technische Informationsbibliothek (TIB) CY - Hannover AN - OPUS4-60067 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hahn, Sarah-K. A1 - Saupe, Alexander A1 - Tschirschwitz, Rico A1 - Bernardy, Christopher A1 - Janßen, Marvin A1 - Amano, Kofi Owusu Ansah A1 - Krause, Ulrich T1 - Sicherheit elektrochemischer Energiespeicher – Ergebnisse aus dem Projekt SEE-2L N2 - Die Transformation der Energienutzung von konventionellen zu erneuerbaren Quellen führt dazu, dass zukünftig mehr Energie effizient zwischengespeichert werden muss. Eine Möglichkeit der elektrochemischen Zwischenspeicherung bieten Lithium-Ionen-Batterien. Hierfür können ausgemusterte Automobilantriebsbatterien verwendet werden. Erfüllen sie die hohen Anforderungen des mobilen Bereichs nicht mehr, haben sie oftmals noch eine ausreichende Kapazität und Leistungsfähigkeit für die stationäre Zwischenspeicherung. Neben der Verwendung der Batterien im größeren Maßstab, z.B. bei Energieversorgern, werden durch den vermehrten Einsatz von Photovoltaik-Anlagen in Ein- und Mehrfamilienhäusern verstärkt Zwischenspeicher für Privathaushalte nachgefragt. Dies birgt auch für Einsatzkräfte neue Herausforderungen in der Gefahrenabwehr. Im vom Bundesministerium für Bildung und Forschung (BMBF) geförderten Verbundprojekt „SEE-2L – Sicherheit elektrochemischer Energiespeicher in Second Life Anwendungen“ wurden Versuche mit Second Life Modulen durchgeführt. Verbundpartner im Projekt waren neben der vfdb die Otto-von-Guericke-Universität Magdeburg und die Bundesanstalt für Materialforschung und -prüfung. Zudem war das Institut der Feuerwehr Nordrhein-Westfalen eingebunden. Die durchgeführten Versuche bilden eine Grundlage für die Einordnung der Batteriespeicher, z.B. aus Sicht des baulichen Brandschutzes, zur Methodik der Brandbekämpfung oder zur Risikobewertung hinsichtlich der Prozess- und Anlagensicherheit. Im Beitrag werden die Versuchsergebnisse vorgestellt und Ansätze für deren Anwendung gezeigt. Um die gewonnenen Erkenntnisse zu vermitteln, wurde im Projekt zudem ein Schulungskonzept für Einsätze mit Lithium-Ionen-Technologien erarbeitet, das im Beitrag präsentiert wird. Es besteht aus theoretischen und praktischen Anteilen, sodass bei den Feuerwehren praxisnah aus- bzw. fortgebildet werden kann. T2 - 70. Jahresfachtagung der vfdb CY - Magdeburg, Deutschland DA - 06.05.2024 KW - Auswirkungsbetrachtungen KW - Elektrische Energiespeicher KW - Lithium-Ionen-Batterie KW - Stationäre Energiespeicher KW - Thermisches Durchgehen PY - 2024 SN - 978-3-9360-5038-7 SP - 645 EP - 657 PB - vfdb, Vereinigung zur Förderung des Deutschen Brandschutzes e.V. CY - Münster AN - OPUS4-60068 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kowalski, Kurt A1 - Hulshoff, S.J. A1 - Ströer, P. A1 - Withag, J. A1 - Genot, A. A1 - Morgans, A.S. A1 - Bake, Friedrich A1 - Venner, K. A1 - Sanders, M.P.J. A1 - Hirschberg, Lionel T1 - Entropy-patch choked-nozzle interaction: quasi-steady-modeling-regime limits probed N2 - Indirect combustion noise due to the interaction of flow inhomogeneities with a choked combustion-chamber exit is an important cause of combustion instability in solid rocket motors. Moreover, it is believed to be an issue in electrical-power generation turbines and aero-engines. If these flow inhomogeneities are essentially characterized by the fluid having a locally appreciablydifferent thermodynamic state, the acoustic response engendered by its interaction with the combustion-chamber exit is commonly referred to as entropy noise. In this paper, dedicated numerical-simulation results of entropy-patch choked-nozzle interactions are presented. Two types of entropy patches were considered: rectangular slugs and circular spots. Moreover, analytical-model-based analysis, of said simulation results, is presented. Based on said analysis, the authors posit the existence of three modeling regimes: the quasi-steady-modeling regime, the blended-physical-effects regime, and the inertial-modeling regime. T2 - 30th AIAA/CEAS Aeroacoustics Conference (2024) CY - Rome, Italy DA - 04.06.2024 KW - Entropy-Nozzle Interaction KW - Indirect Combustion Noise KW - Entropy Noise PY - 2024 SN - 978-1-62410-720-7 DO - https://doi.org/10.2514/6.2024-3113 SP - 1 EP - 23 AN - OPUS4-60174 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Albakri, Bashar A1 - Turski Silva Diniz, Analice A1 - Benner, Philipp A1 - Muth, Thilo A1 - Nakajima, Shinichi A1 - Favaro, Marco A1 - Kister, Alexander ED - Hillman, Robert T1 - Machine learning-assisted equivalent circuit identification for dielectric spectroscopy of polymers N2 - Polymers have become indispensable across fields of application, and understanding their structure–property relationships and dynamic behaviour is essential for performance optimization. Polymer membranes, particularly ion exchange membranes, play a crucial role in renewable energy conversion technologies, fuel cells, solar energy conversion, and energy storage. In this context, broadband dielectric spectroscopy (BDS) offers a powerful, non-destructive approach to investigate the electrical response and relaxation dynamics of polymers. These properties are investigated by parametrizing the system’s impedance response in terms of a network of circuit elements, i.e. the electrical equivalent circuit (EEC), whose impedance resembles the one of the system under investigation. However, the determination of the EEC from BDS data is challenging due to system complexity, interdependencies of circuit elements, and researcher biases. In this work, we propose a novel approach that incorporates a convolutional neural network (CNN) model to predict the EEC topology. By reducing user bias and enhancing data analysis, this approach aims to make BDS accessible to both experienced users and those with limited expertise. We show that the combination of machine learning and BDS provides valuable insights into the dynamic behaviour of polymer membranes, thus facilitating the design and characterization of tailored polymers for various applications. We also show that our model outperforms state-of-the-art machine learning methods with a top-5 accuracy of around 80% for predicting the circuit topology and a parameter fitting error as low as 0.05%. KW - Polymer membranes KW - Electrochemical impedance spectroscopy KW - Broadband dielectric spectroscopy KW - Deep learning KW - Machine learning KW - Equivalent circuit PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-602138 DO - https://doi.org/10.1016/j.electacta.2024.144474 SN - 0013-4686 VL - 496 SP - 1 EP - 13 PB - Elsevier Ltd. AN - OPUS4-60213 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Quercetti, Thomas A1 - Feldkamp, Martin A1 - Gleim, Tobias A1 - Musolff, Andre A1 - Werner, Jan A1 - Wille, Frank T1 - Enhancement of the BAM Fire Test Stand for Testing a Large Transport Package for Radioactive Materials N2 - Packages for the transport of spent nuclear fuel are designed to endure severe accidents. To obtain approval, these transport packages must adhere to the specification-based criteria of the international transport regulations SSR-6 of the International Atomic Energy Agency (IAEA). To ensure compliance with these requirements, specific mechanical and thermal tests need to be addressed with respect to the package type. Typically, SSR-6 prescribes a mechanical test followed by a thermal fire test as part of different testing scenarios. To approve the latter test of the sequence, BAM performs calorimeter tests in advance with so-called fire reference packages for characterizing the actual fire and its impact on the package to be tested. Packages are designed with different geometry sizes depending on their purpose. For previous tests, the implemented test setups in the fire test stand were sufficiently dimensioned and could cover all requirements in this respect. However, to cover additional testing needs in the future, BAM is expanding the test setup for the purpose of testing significantly larger packages. In previous test setups one ring burner for propane surrounding the test specimen was sufficient. The limiting size in this configuration was the design height of the transport package to be tested. According to the thermal test of the IAEA-Regulations [1], a 30-minute fully engulfing 800°C pool fire or an equally severe fire, e.g., propane gas fire, must be applied to the transport package. Possible adjustments such as nozzle cross-section and propane mass flow can be adjusted to a certain extent. Further modifications, to cover significantly higher and larger packages all-around with a fully engulfing fire, must be accomplished with an additional, second burner ring. Both burner rings had the same dimensions and were mounted on top of each other at different heights to create a significantly larger volume of fire that completely engulfs the package including its impact limiter. To meet the IAEA regulatory boundary conditions, the enhanced fire test stand with the second burner ring is tested with a large fire reference package and will then be used for real-size transport packages after all parameters are successfully met. This fire reference package represents the external geometry of a generic transport cask for radioactive material and is equipped with numerous temperature sensors to record temperature curves at the interior wall surfaces. T2 - RAMTrans 2024 CY - London, United Kingdom DA - 14.05.2024 KW - Fire testing KW - Full-scale KW - Transport package PY - 2024 SP - 1 EP - 7 AN - OPUS4-60253 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Quercetti, Thomas T1 - Enhancement of the bam fire test stand for testing a large transport package for radioactive materials N2 - Packages for the transport of spent nuclear fuel are designed to endure severe accidents. To obtain approval, these transport packages must adhere to the specification-based criteria of the international transport regulations SSR-6 of the International Atomic Energy Agency (IAEA). To ensure compliance with these requirements, specific mechanical and thermal tests need to be addressed with respect to the package type. Typically, SSR-6 prescribes a mechanical test followed by a thermal fire test as part of different testing scenarios. To approve the latter test of the sequence, BAM performs calorimeter tests in advance with so-called fire reference packages for characterizing the actual fire and its impact on the package to be tested. Packages are designed with different geometry sizes depending on their purpose. For previous tests, the implemented test setups in the fire test stand were sufficiently dimensioned and could cover all requirements in this respect. However, to cover additional testing needs in the future, BAM is expanding the test setup for the purpose of testing significantly larger packages. In previous test setups one ring burner for propane surrounding the test specimen was sufficient. The limiting size in this configuration was the design height of the transport package to be tested. According to the thermal test of the IAEA-Regulations [1], a 30-minute fully engulfing 800°C pool fire or an equally severe fire, e.g., propane gas fire, must be applied to the transport package. Possible adjustments such as nozzle cross-section and propane mass flow can be adjusted to a certain extent. Further modifications, to cover significantly higher and larger packages all-around with a fully engulfing fire, must be accomplished with an additional, second burner ring. Both burner rings had the same dimensions and were mounted on top of each other at different heights to create a significantly larger volume of fire that completely engulfs the package including its impact limiter. To meet the IAEA regulatory boundary conditions, the enhanced fire test stand with the second burner ring is tested with a large fire reference package and will then be used for real-size transport packages after all parameters are successfully met. This fire reference package represents the external geometry of a generic transport cask for radioactive material and is equipped with numerous temperature sensors to record temperature curves at the interior wall surfaces. T2 - RAMTrans 2024 CY - London, United Kingdom DA - 14.05.2024 KW - Fire testing KW - Full-scale KW - Transport package PY - 2024 AN - OPUS4-60255 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Möglichkeiten zur Optimierung von schweißbedingten Beanspruchungen durch Einsatz von LTT-Zusatzwerkstoffen N2 - Der Vortrag gibt einen Überblick zum Thema Low Transformation Temperature (LTT) Zusatzwerkstoffe. Es wird gezeigt, wie mit einem Experiment unter Nutzung von Sychrotronstrahlung das Phänomen der Umwandlungsplastizität untersucht werden kann. T2 - 12. Vollversammlung des SFB 1120: Summer School 2024 CY - Steinfeld (Kall), Germany DA - 11.06.2024 KW - Eigenspannungen KW - LTT-Zusatzwerkstoffe KW - Hochfester Stahl PY - 2024 AN - OPUS4-60259 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Griesche, Axel T1 - Crystallographic phase transformations and corresponding temperature distributions during gtaw of supermartensitic stainless steel visualized by nbei N2 - We investigated the phase transformations during butt-welding of supermartensitic steel plates with help of Neutron-Bragg-Edge Imaging (NBEI). Gas tungsten arc welding (GTAW) was used with a motorized torch allowing for automated weldments. The austenitization in the heat affected zone (HAZ) could be clearly visualized at λ = 0.39 nm, a wavelength smaller than the Bragg edge wavelengths of both austenite and martensite. The re-transformation into the martensitic phase during cooling was clearly detected. However, we observed an unexpected additional change in transmission at λ = 0.44 nm, a wavelength larger than the wavelength of the Bragg edges of both the martensitic and austenitic phases. We attribute this change to the Deybe-Waller-Factor that describes the temperature dependence of coherent scattering at a crystal lattice. The observed two-dimensional attenuation map corresponds well with a temperature distribution modelling by software macros in ANSYS [3]. Here, the absolute temperature values could be achieved by calibrating the modelled attenuation with help of a thermocouple placed at the steel plate. This allows in return for a direct two-dimensional temperature reading based on the Debye-Waller-relation between neutron attenuation and sample temperature. T2 - WCNR-12 CY - Idaho Falls, Id, USA DA - 02.06.2024 KW - Neutron KW - Radiography KW - Welding PY - 2024 AN - OPUS4-60242 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tschirschwitz, Rico T1 - Sicherheit elektrochemischer Energiespeicher - Ergebnisse aus dem Projekt SEE-2L N2 - Im Rahmen des BMBF-Vorhabens SEE-2L wurde auf dem Testgelände Technische Sicherheit (BAM TTS) ein Großversuchsstand für das thermische Durchgehen von Lithium-Batterien auf Modul- und Batterieebene entwickelt und aufgebaut. Im Zuge des Projektes konnte eine erste Versuchsserie zu den Auswirkungen des thermischen Durchgehens von Batteriemodulen durchgeführt werden. Im Vortrag werden die wesentlichen Ergebnisse der Versuche vorgestellt. T2 - Magdeburg-Köthener Brandschutz- und Sicherheitstagung CY - Magdeburg, Germany DA - 14.03.2024 KW - Auswirkungsbetrachtungen KW - Elektrische Energiespeicher KW - Lithium-Ionen-Batterie KW - Stationäre Energiespeicher KW - Thermisches Durchgehen PY - 2024 AN - OPUS4-60143 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Li, Guiping A1 - Liu, Ye A1 - Schultz, Thorsten A1 - Exner, Moritz A1 - Muydinov, Ruslan A1 - Wang, Hui A1 - Scheurell, Kerstin A1 - Huang, Jieyang A1 - Szymoniak, Paulina A1 - Pinna, Nicola A1 - Koch, Norbert A1 - Adelhelm, Philipp A1 - Bojdys, Michael J. T1 - One‐Pot Synthesis of High‐Capacity Sulfur Cathodes via In‐Situ Polymerization of a Porous Imine‐Based Polymer N2 - AbstractLithium‐ion batteries, essential for electronics and electric vehicles, predominantly use cathodes made from critical materials like cobalt. Sulfur‐based cathodes, offering a high theoretical capacity of 1675 mAh g−1 and environmental advantages due to sulfur's abundance and lower toxicity, present a more sustainable alternative. However, state‐of‐the‐art sulfur‐based electrodes do not reach the theoretical capacities, mainly because conventional electrode production relies on mixing of components into weakly coordinated slurries. Consequently, sulfur‘s mobility leads to battery degradation—an effect known as the “sulfur‐shuttle”. This study introduces a solution by developing a microporous, covalently‐bonded, imine‐based polymer network grown in situ around sulfur particles on the current collector. The polymer network (i) enables selective transport of electrolyte and Li‐ions through pores of defined size, and (ii) acts as a robust host to retain the active component of the electrode (sulfur species). The resulting cathode has superior rate performance from 0.1 C (1360 mAh g−1) to 3 C (807 mAh g−1). Demonstrating a high‐performance, sustainable sulfur cathode produced via a simple one‐pot process, our research underlines the potential of microporous polymers in addressing sulfur diffusion issues, paving the way for sulfur electrodes as viable alternatives to traditional metal‐based cathodes. KW - In-situ polymerization KW - Sulfur cathodes PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-604215 DO - https://doi.org/10.1002/anie.202400382 SN - 1433-7851 SP - 1 EP - 11 PB - Wiley VHC-Verlag AN - OPUS4-60421 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lu, Xin A1 - Hicke, Konstantin A1 - Krebber, Katerina T1 - Distributed fiber optic sensing for monitoring of underground facilities N2 - Distributed fiber optic sensing (DFOS) technique is a promising and robust non-destructive testing tool that can seamlessly acquire environmental conditions over large scales. Therefore, it has found extensive applications in structural health monitoring. Its appeal for monitoring underground facilities lies in the intrinsic properties of the optical fiber, such as immunity to magnetic interference, small size, chemical inertia, etc. This paper provides a concise overview of DFOS applications in underground facility monitoring. Following a brief introduction to the workingbnprinciple of the DFOS technique, various examples are provided to demonstrate how distributed fiber sensors contribute to monitoring underground facilities. The paper presents unpublished field test results with an emphasis in the energy sector, including monitoring gas storage facilities, geothermal reservoir exploration, and ground movement detection. Furthermore, the paper identifies several directions for enhancing the DFOS system. T2 - SPIE Photonics Europe CY - Strasbourg, France DA - 07.04.2024 KW - Structure health monitoring KW - Geothermal borehole KW - Distributed fiber optic sensing KW - Ground movement KW - Leakage detection PY - 2024 DO - https://doi.org/10.1117/12.3023571 SN - 0277-786X VL - 13001 SP - 1 EP - 10 PB - SPIE AN - OPUS4-60384 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Weber, Mike T1 - Consequences of an Imperfectly Mounted Reinforcement Cage in a Cylindrical Concrete Container During Mechanical Specimen Tests N2 - In 2007 the license for the German Konrad repository for low and intermediate level radioactive waste was finally confirmed. Since then, the site is improved, prepared and equipped for the currently planned start of waste package emplacement in 2029. Bundesanstalt fuer Materialforschung und -pruefung is regularly contracted by the Bundesgesellschaft für Endlagerung as the responsible authority for waste product control, waste container design testing, and waste package acceptance. In this context BAM is mainly responsible for design testing of various container types including the evaluation of quality assurance measures for container manufacturing. In addition to general requirements concerning container design, the casks have to withstand specific mechanical load scenarios. Drop tests from different heights under consideration of the most damaging drop orientation and a stacking test are two examples for necessary safety demonstrations. If the containers are made from concrete the reinforcement has the function to absorb tensile forces the concrete is not able to withstand by its own. Because of manufacturing imperfections of cylindrical concrete containers manufactured already decades ago, the reinforcement cages are not always exactly, asymmetrically positioned when they were poured. This inspired BAM to perform various ABAQUS® finite-element (FE) simulations by using the example of a simplified cylindrical container design with generic dimensions. On the basis of the calculated tensile and compressive stress distributions suggestions are derived on how a cylindrical concrete container with an imperfectly placed reinforcement cage has to be oriented for a drop or stacking test to ensure the most damaging test scenario. T2 - RAMTRANS 2024 CY - London, United Kingdom DA - 14.05.2024 KW - Finite-element-analysis KW - Container design testing procedure KW - Reinforced concrete containers KW - Drop test KW - Stacking test KW - Imperfectly mounted reinforcement cage PY - 2024 AN - OPUS4-60120 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Gleim, Tobias A1 - Feldkamp, Martin A1 - Quercetti, Thomas A1 - Musolff, André A1 - Werner, Jan A1 - Wille, Frank T1 - Enhancement of Fire Test Stand Performance at Test Site of BAM: Installation and Evaluation of an Augmented System with a Fire Reference Package N2 - Packages for the transport of radioactive material are designed to en-dure severe accidents. Packages for the transportation of radioactive material must demonstrate that the package can withstand certain prescribed tests from the IAEA Regulations [1]. In addition to mechanical tests, a thermal test in form of a fire test must be carried out. As packages to be tested at BAM are signifi-cantly larger than previous package designs, BAM has expanded an existing fire test stand. A modular concept is chosen, which means that the arrangement of the burner nozzles can be adapted to the test specimen. The dimensions of the burner rings, the type, the orientation and the number of burner nozzles can be varied depending on the test specimen. In addition, various pumps can be used to set the corresponding mass flow. With the help of a calorimeter test, the fire test stand can be qualified for a specific size of packages regarding the boundary conditions of the IAEA Regulations [1]. Due to the typically wood filled impact limiters in German package designs, a fire test is necessary, as experiments have shown that possible openings that occurred during a mechanical test contributed to the igni-tion of the wood filled impact limiters within the prescribed 30 minutes of the IAEA Regulations [1]. From a series of experiments, two experiments are pre-sented to show the possibilities to obtain different temperatures and temperature rates in the test specimen. In addition to sensor data, the heat flux into the package is calculated to verify that the IAEA boundary conditions are satisfied. In addition to the temperature data, other data such as wind speed and wind direction are also recorded to explain subsequent effects in the measurement data in a comprehen-sible manner. T2 - Wood & Fire Safety 2024 CY - Strbske Pleso, Slowakei DA - 13.05.2024 KW - IAEA Regu-lations KW - Fire Test Stand KW - Accident Scenario KW - Fire Qualification PY - 2024 UR - https://link.springer.com/book/9783031591761 SN - 978-3-031-59176-1 SN - 978-3-031-59179-2 SN - 978-3-031-59177-8 DO - https://doi.org/10.1007/978-3-031-59177-8_22 VL - 1 SP - 189 EP - 197 PB - Springer Cham AN - OPUS4-60101 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Gleim, Tobias T1 - Enhancement of Fire Test Stand Performance at Test Site of BAM: Installation and Evaluation of an Augmented System with a Fire Reference Package N2 - Packages for the transport of radioactive material are designed to en-dure severe accidents. Packages for the transportation of radioactive material must demonstrate that the package can withstand certain prescribed tests from the IAEA Regulations [1]. In addition to mechanical tests, a thermal test in form of a fire test must be carried out. As packages to be tested at BAM are signifi-cantly larger than previous package designs, BAM has expanded an existing fire test stand. A modular concept is chosen, which means that the arrangement of the burner nozzles can be adapted to the test specimen. The dimensions of the burner rings, the type, the orientation and the number of burner nozzles can be varied depending on the test specimen. In addition, various pumps can be used to set the corresponding mass flow. With the help of a calorimeter test, the fire test stand can be qualified for a specific size of packages regarding the boundary conditions of the IAEA Regulations [1]. Due to the typically wood filled impact limiters in German package designs, a fire test is necessary, as experiments have shown that possible openings that occurred during a mechanical test contributed to the igni-tion of the wood filled impact limiters within the prescribed 30 minutes of the IAEA Regulations [1]. From a series of experiments, two experiments are pre-sented to show the possibilities to obtain different temperatures and temperature rates in the test specimen. In addition to sensor data, the heat flux into the package is calculated to verify that the IAEA boundary conditions are satisfied. In addition to the temperature data, other data such as wind speed and wind direction are also recorded to explain subsequent effects in the measurement data in a comprehen-sible manner. T2 - Wood & Fire Safety 2024 CY - Štrbské Pleso, Slovakia DA - 13.05.2024 KW - Fire Test Stand KW - Accident Scenario KW - Fire Qualification KW - IAEA Regu-lations PY - 2024 UR - https://link.springer.com/book/9783031591761 AN - OPUS4-60104 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rolle, Annette A1 - Neumeyer, Tino A1 - Ballheimer, Viktor A1 - Wille, Frank T1 - Investigations of Aged Metal Seals for Transport Package Safety Assessment N2 - Acceptable limits for activity release from transport casks for high-level radioactive material specified in the IAEA regulations must be kept by the integrity of cask body and the cask sealing system. BAM as the German competent authority for mechanical, thermal and containment assessment of packages liable for approval verifies the activity release compliance with the regulatory limits. The specification of conservative package design leakage rates is one of the most important aspects in assessment. Metal seals of the Helicoflex® Type are usually used to ensure the required package tightness for both, storage, and transport of the cask before and after storage. Due to the long-term use the seal behavior is influenced by temperature and time. The mechanical and thermal loadings associated with the routine, normal and accident conditions of transport specified in the regulations can have a significant effect on the leak tightness of the sealing system. Whereas the safety for application of new, non- aged Helicoflex® seals is verified sufficiently, there are still technical data gaps concerning the efficiency of aged Helicoflex® seals. BAM performed experiments to learn more about the sealing efficiency of aged Helicoflex® seals with Aluminum and Silver outer jackets. The seals were compressed in test-flanges and for artificial ageing the complete flange systems were stored in an oven for several month at a high temperature. After this ageing procedure the flanges were opened completely, the seals were moved a little to vary the contact area, and the flanges were compressed again. During the compression and decompression tests after the aging, load-deformation characteristics of the seals, and leakage rates were measured. With these tests a load situation was simulated, which can occur in the regulatory drop test of the cask: Under high impact loads the bolted lid can lift a little for a short moment, allowing a little movement of the seal, so that the contact area can change before compressing again. Details about test conditions and first results will be presented in the poster. T2 - RAMTrans 2024, 12th Internatiopnal Conference on the Transport , Storage and Disposal of Radioactive Materials CY - London, UK DA - 15.05.2024 KW - Seals KW - Ageing KW - Radioaktiv PY - 2024 AN - OPUS4-60112 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Feldkamp, Martin A1 - Gleim, Tobias A1 - Quercetti, Thomas A1 - Wille, Frank T1 - Combustion Chamber Design for Encapsulated Wood-Component Testing N2 - Heavy-weight packages for the safe transport of radioactive material are equippedwith impact limiters often built ofwood-filled steel sheet structures to fulfil the requirements of the International Atomic Energy Agency (IAEA) regulations. The requirements definemechanical tests followed by a thermal test, including criteria ensuring the package design’s ability to withstand severe accidents and provide a high level of technical safety. Impact limiters are a package component mainly designed for the packages to withstand severe mechanical accident scenarios. In drop tests the impact limiters absorb the kinetic energy during impact of the package. The package must then - with its pre-damaged impact limiters - endure a thermal test defined precisely in the IAEA regulations as a 30-min fully engulfing 800 °C-fire. After the fire, a wood-filled impact limiter may continue to release thermal energy from an ongoing combustion process, defining relevant package temperatures. The energy flow from a possible burning impact limiter to the package is important for the safety evaluation of transport packages. To investigate the combustion behaviour of densely packed layers of spruce wood, encapsulated in pre-damaged cylindrical metal enclosures, a test set-up has been realised. The set-up consists of a combustion chamber to perform these tests under defined boundary conditions. The temperature development of the test specimens will be observed fromoutside with a thermographic imager, with HD-Cameras, and the mass loss will be measured during the entire test. Airflow conditions in the combustion chamber are analysed using Computational Fluid Dynamics (CFD) calculations in OpenFOAM. The planned combustion test setup is described. T2 - Wood & Fire Safety 2024 CY - Štrbské Pleso, Slovakia DA - 12.05.2024 KW - Fire KW - Combustion KW - Smouldering PY - 2024 SN - 978-3-031-59176-1 SN - 978-3-031-59179-2 SN - 978-3-031-59177-8 DO - https://doi.org/10.1007/978-3-031-59177-8 SP - 215 EP - 222 PB - Springer Nature Switzerland AG CY - Gewerbestrasse 11, 6330 Cham, Switzerland AN - OPUS4-60226 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Feldkamp, Martin T1 - Combustion Chamber Design for Encapsulated Wood-Component Testing N2 - eavy-weight packages for the safe transport of radioactive material are equippedwith impact limiters often built ofwood-filled steel sheet structures to fulfil the requirements of the International Atomic Energy Agency (IAEA) regulations. The requirements definemechanical tests followed by a thermal test, including criteria ensuring the package design’s ability to withstand severe accidents and provide a high level of technical safety. Impact limiters are a package component mainly designed for the packages to withstand severe mechanical accident scenarios. In drop tests the impact limiters absorb the kinetic energy during impact of the package. The package must then - with its pre-damaged impact limiters - endure a thermal test defined precisely in the IAEA regulations as a 30-min fully engulfing 800 °C-fire. After the fire, a wood-filled impact limiter may continue to release thermal energy from an ongoing combustion process, defining relevant package temperatures. The energy flow from a possible burning impact limiter to the package is important for the safety evaluation of transport packages. To investigate the combustion behaviour of densely packed layers of spruce wood, encapsulated in pre-damaged cylindrical metal enclosures, a test set-up has been realised. The set-up consists of a combustion chamber to perform these tests under defined boundary conditions. The temperature development of the test specimens will be observed fromoutside with a thermographic imager, with HD-Cameras, and the mass loss will be measured during the entire test. Airflow conditions in the combustion chamber are analysed using Computational Fluid Dynamics (CFD) calculations in OpenFOAM. The planned combustion test setup is described. T2 - Wood & Fire Safety 2024 CY - Štrbské Pleso, Slovakia DA - 12.05.2024 KW - IAEA KW - Combustion Chamber KW - Smouldering KW - Wood PY - 2024 AN - OPUS4-60227 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Barretto, T. A1 - Gentes, S. A1 - Braun, J. A1 - Averin, Anton A1 - Lecompagnon, Julien A1 - Stroncik, N. T1 - Automated non-destructive internal corrosion detection on radioactive drums (ZIKA) N2 - The aim of the ZIKA research project, funded by the BMBF funding program FORKA (FKZ:15S9446 A-C), is the automated detection of internal corrosion of radioactive drums using non-destructive testing (NDT). The newly gained findings will be combined with research results from the previous project EMOS (FKZ:15S9420), which dealt with the external damage of drums. Using NDT, internal corrosion and possible internal sources of damage can be identified before they become a safety-relevant issue. However, if internally sourced damages can be seen externally, the integrity of the damaged drum is no longer guaranteed, which has significant consequences. Therefore, early detection before integrity failure is of particular importance for interim storage facilities with low- and medium-level radioactive waste drums. T2 - Kerntechnik 2024 CY - Leipzig, Germany DA - 11.06.2024 KW - Corrosion detection KW - Non-destructive testing KW - Automated inspection system PY - 2024 SP - 1 EP - 5 AN - OPUS4-60322 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zencker, Uwe A1 - Völzke, Holger T1 - Brittle Failure Limits of Spent Fuel Claddings Subjected to Long-Term Dry Interim Storage Conditions N2 - The mechanical properties of spent fuel claddings can be adversely affected under the conditions of long-term dry interim storage, so that the failure limits may be reached in case of mechanical loads during handling or transport after storage. Pre-storage drying and the early stage of interim storage can expose the cladding to higher temperatures and higher tensile hoop stresses than those associated with in-reactor operation and pool storage. During slow cooling of a cladding tube under internal pressure, radial hydrides may precipitate in zirconium-based cladding alloys. This can lead to embrittlement of the material and sudden failure of the cladding integrity under mechanical stress. In order to prevent brittle failure, numerical methods are being developed to predict the mechanical behaviour and identify limiting conditions. Experimental investigations, numerical analyses and evaluation methods are discussed. An established experimental method for characterising cladding materials is the Ring Compression Test (RCT). Some test results on irradiated cladding tubes after operation in pressure water reactors are publicly available. However, it is helpful to carry out studies on unirradiated surrogate claddings with similar material properties to reduce the effort associated with irradiated samples in hot cells and to perform material tests with a wider range of parameters. On the basis of such experimental data, load-displacement curves have been numerically analysed for a selection of cladding materials. Radial hydrides can cause a sample to break suddenly due to fracture even at low deformation. Noticeable load drops in the RCT are caused by unstable crack propagation through the radial hydride network. The failure mechanism is quasi-cleavage in the hydrides and micro-void nucleation, growth, and coalescence in the zirconium matrix, with ductile tearing patches connecting adjacent hydrides. The cohesive zone approach was used to simulate the failure process taking into account the radial hydride morphology. The developed method can adequately describe both the deformation and failure behaviour of irradiated as well as unirradiated claddings of zirconium-based alloys with radial hydrides under RCT conditions. Limiting conditions can be expressed in terms of fracture energy and cohesive strength. T2 - IAEA International Conference on the Management of Spent Fuel from Nuclear Power Plants - Meeting the Moment CY - Vienna, Austria DA - 10.06.2024 KW - Ageing Management KW - Cladding Embrittlement KW - Extended Storage KW - Ring Compression Test KW - Spent Nuclear Fuel PY - 2024 SP - 1 EP - 10 AN - OPUS4-60323 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zencker, Uwe T1 - Brittle Failure Limits of Spent Fuel Claddings Subjected to Long-Term Dry Interim Storage Conditions N2 - The mechanical properties of spent fuel claddings can be adversely affected under the conditions of long-term dry interim storage, so that the failure limits may be reached in case of mechanical loads during handling or transport after storage. Pre-storage drying and the early stage of interim storage can expose the cladding to higher temperatures and higher tensile hoop stresses than those associated with in-reactor operation and pool storage. During slow cooling of a cladding tube under internal pressure, radial hydrides may precipitate in zirconium-based cladding alloys. This can lead to embrittlement of the material and sudden failure of the cladding integrity under mechanical stress. In order to prevent brittle failure, numerical methods are being developed to predict the mechanical behaviour and identify limiting conditions. Experimental investigations, numerical analyses and evaluation methods are discussed. An established experimental method for characterising cladding materials is the Ring Compression Test (RCT). Some test results on irradiated cladding tubes after operation in pressure water reactors are publicly available. However, it is helpful to carry out studies on unirradiated surrogate claddings with similar material properties to reduce the effort associated with irradiated samples in hot cells and to perform material tests with a wider range of parameters. On the basis of such experimental data, load-displacement curves have been numerically analysed for a selection of cladding materials. Radial hydrides can cause a sample to break suddenly due to fracture even at low deformation. Noticeable load drops in the RCT are caused by unstable crack propagation through the radial hydride network. The failure mechanism is quasi-cleavage in the hydrides and micro-void nucleation, growth, and coalescence in the zirconium matrix, with ductile tearing patches connecting adjacent hydrides. The cohesive zone approach was used to simulate the failure process taking into account the radial hydride morphology. The developed method can adequately describe both the deformation and failure behaviour of irradiated as well as unirradiated claddings of zirconium-based alloys with radial hydrides under RCT conditions. Limiting conditions can be expressed in terms of fracture energy and cohesive strength. T2 - IAEA International Conference on the Management of Spent Fuel from Nuclear Power Plants - Meeting the Moment CY - Vienna, Austria DA - 10.06.2024 KW - Ageing Management KW - Cladding Embrittlement KW - Extended Storage KW - Ring Compression Test KW - Spent Nuclear Fuel PY - 2024 AN - OPUS4-60324 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Gleim, Tobias T1 - Potential Effects of Battery and Hydrogen Fires regarding Regulatory Requirements N2 - Introduction and Necessity of the Investigation The IAEA regulations for the safe transport of radioactive material (IAEA SSR-6) define the safety requirements for different package types and consider different transport conditions. The accident conditions of transport specify different mechanical and thermal tests based on investigations of real accident scenarios. Considering the rapid development of new boundary conditions of transport such as electric mobility and the use of hydrogen as energy source for trucks and other kind of vehicles, potential effects of battery and hydrogen fires in transport accidents should be investigated. The aim is to evaluate the existing test requirements developed and derived decades ago, whether they are covering the current transport situation. This concept paper will briefly present the reasons for detailed investigations as bases for a coordinated research project under the roof of the IAEA. T2 - Technical Exchange IRSN – BAM Transport & Storage of Packages for Radioactive Material CY - Berlin, Germany DA - 04.06.2024 KW - Fire KW - Battery KW - Hydrogen KW - IAEA Regulations PY - 2024 AN - OPUS4-60338 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Naster, Maximilian T1 - Hydrogen Fire Testing N2 - In this presentation we present a new hydrogen-based test rig for an ongoing feasibility study of using hydrogen as an energy source for the thermal testing of transport packages containing radioactive materials. The test rig will be capable of combusting hydrogen for a wide range of different burner geometries, mass flows and if necessary hydrogen blends. As this type of fire test according to the IAEA boundary conditions does not yet exist, a large number of preliminary investigations, safety assessments and calculations must be carried out in order to develop a viable concept for hydrogen fires. In the first step of the feasibility study, the temperature, structure, and radiation of various hydrogen flames are surveyed. In future works, the results will make it possible to design burner frames that are suitable for fire reference tests in order to make comparisons with pool and propane fires used in assessment procedures today. In parallel comparative numerical simulations are conducted to model the thermal behaviour of hydrogen flames using the software package Ansys®. On the one hand, the numerical simulations support the experiments by providing an overview of numerous parameters and the measuring range; on the other hand, they will help with the design of the burner frame in future work. This paper gives an overview in the design and capabilities of the test rig. Furthermore, the results of the parameter studies show that burner geometry and mass flow provide a significant design margin for the thermal shape of the hydrogen flames. In addition, the results of the initial numerical calculations will be used to determine the necessary sensors, the positions, and their operating range. Only the optimal interaction allows a controlled system that permits user-defined hydrogen fires. T2 - Technical Exchange IRSN – BAM Transport & Storage of Packages for Radioactive Material CY - Berlin, Germany DA - 04.06.2024 KW - Hydrogen PY - 2024 AN - OPUS4-60341 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Best practice: How to work with a mobile diffractometer N2 - Beginning with a general overview about resdiual stress determination by X-ray diffraction, the presentation is focussing on some does and dont's when working with a portable diffractometer. T2 - European Conference on Residual Stresses 11 - Tutorial 1: Residual stresses in additive manufacturing CY - Prague, Czech Republic DA - 03.06.2024 KW - Residual stress KW - X-ray diffraction PY - 2024 AN - OPUS4-60287 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Saeed, Hasan A1 - Chaudhuri, Somsubhro A1 - De Waele, Wim T1 - Experimental evaluation of the short and long fatigue crack growth rate of S355 structural steel offshore monopile weldments in air and synthetic seawater N2 - Welded steel structures used in the offshore wind industry are exposed to harsh marine environments, which can result in corrosion-induced fatigue damage. Of particular concern is the heat affected zone (HAZ) of welded joints, a region known for its altered microstructure and mechanical properties, which can significantly influence the initiation and propagation of fatigue cracks. This study investigates the short and long fatigue crack growth rates, and the effect of seawater exposure, for the HAZ in S355 steel weldments. Single-edge notch bend (SENB) specimens are used, with a shallow notch in the HAZ. A series of specimens is immersed in synthetic seawater that is continuously circulated at a controlled temperature to assess the synergistic effects of corrosion and fatigue. The experimental method integrates a novel application of front face strain compliance for monitoring short cracks, alongside an extended back-face strain compliance approach for monitoring long crack propagation. It is concluded that the short fatigue crack growth rate of the HAZ is 2.7 to 3.5 times higher in seawater as compared to air. As the crack propagates and enters into the long crack regime, the ratio decreases to 2.2 times at the transition point of the two-stage crack growth curve and further decreases to 1.5 times when the notch advances towards fracture. The findings indicate that the fatigue crack growth rates documented in standards tend to be on the conservative side. This study significantly enriches the fatigue crack growth data available in literature, which will contribute to a more accurate lifetime assessment offshore wind turbine structures. KW - Fatigue crack growth rate KW - Short crack KW - Offshore monopile foundation KW - Corrosion fatigue PY - 2024 DO - https://doi.org/10.1016/j.apor.2024.104063 VL - 149 SP - 1 EP - 17 PB - Elsevier Ltd. AN - OPUS4-60691 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Mehri Sofiani, F. A1 - Tacq, J. A1 - Elahi, S.A. A1 - Chaudhuri, Somsubhro A1 - De Waele, W. T1 - A hybrid probabilistic-deterministic framework for prediction of characteristic size of corrosion pits in low-carbon steel following long-term seawater exposure N2 - A hybrid deterministic-probabilistic framework is presented that combines in-situ measurements and numerical analysis to predict the characteristic size of corrosion pits over extended periods of exposure to seawater. A probabilistic model, informed by corrosion current density and temperature data, applies a sampling method to a range of overpotential values to reflect the surface deterioration in terms of pitting. The model is calibrated and validated with pit size data obtained from corroded coupons. Results reveal a positively skewed truncated lognormal distribution of pit depths which implies a higher prevalence of smaller pit depths, corroborated both experimentally and numerically. KW - Pitting corrosion KW - Offshore structures KW - Probabilistic analysis KW - Potentiodynamic polarisation PY - 2024 DO - https://doi.org/10.1016/j.corsci.2024.112039 VL - 232 SP - 1 EP - 15 PB - Elsevier Ltd. AN - OPUS4-60693 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Chaudhuri, Somsubhro T1 - Passive infrared thermography as an inspection tool for operational wind turbine rotor blades N2 - The growing wind energy infrastructure presents a significant challenge in the maintenance and operation of wind turbines (WT) and their intricate components. An important aspect of WT maintenance is the inspection of wind turbine rotor blades (WTB) to ensure the overall health and safety of the turbine. This inspection process involves both visual and mechanical examinations of the blades to identify any indicators of damage or wear that could compromise their performance and, consequently, the structural integrity of the entire WT system. The complexity of WTBs is compounded by their ever-expanding dimensions, exceeding 100 meters in length for 16 MW WT systems, and their multi-material composition. Within this context, passive infrared thermography emerges as a potential alternative to conventional contact- or proximity-based inspection methods. Unlike active thermography, passive thermography uses solar radiation and ambient temperature variation for thermal contrast, eliminating the need for traditional heat lamps, flash, or laser-based techniques. A novel inspection method has been developed to semi-autonomously assess wind turbine blades (WTBs) while the wind turbine (WT) is operational, from ground level. This approach leverages optimal thermal contrast, which depends on prevailing weather conditions during field measurements, enabling the visualization of both external and internal features of the WTBs through post-processing techniques. In this study, thermal data obtained through passive thermography is compared with contemporaneous visual imagery to definitively classify observed features in thermal images as either surface or sub-surface features. This analysis, coupled with corresponding weather conditions, provides valuable insights into the capabilities and limitations of the inspection technique. Additionally, finite-element-based (FE) thermal simulations of a WTB section are employed to parametrically assess the influence of weather conditions, beyond those observed during field measurements, based on a validated model. In addition, the thermal images also consist of thermal signatures of leading-edge turbulence due to possible leading-edge erosion in WTBs. These are primarily vortices, and their shape and size depend on the morphology of the damage as well as the rotational speed of the WTBs. The inspections are accompanied by automatic data evaluation of the thermal signatures. To improve the precision of erosion damage identification, a fully convolutional network (FCN) is employed, trained, and tested using over 1000 annotated thermographic blade images. Additionally, the study introduces strategies for grouping smaller damage indications and simplification rules based on realistic thermal imaging resolutions. As leading-edge erosion could potentially lead to annual energy production (AEP) losses, this technique could prove to be a powerful tool in establishing the presence of damage and the resulting AEP loss. T2 - 20th World Conference on Non-Destructive Testing CY - Incheon, South Korea DA - 27.05.2024 KW - Non-destructive testing KW - Thermografie KW - Wind turbine rotor blades KW - Windenergie Anlage Rotorblätter KW - Thermography PY - 2024 AN - OPUS4-60695 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zencker, Uwe T1 - Fracture Mechanics Analysis of Spent Fuel Claddings during Long-Term Dry Interim Storage N2 - The European Joint Programme on Radioactive Waste Management (EURAD) is working on Spent Fuel Characterization (SFC) in its work package (WP) 8. Inspired by the EURAD activities, the International Atomic Energy Agency (IAEA) established an international Coordinated Research Project (CRP) on SFC. The EURAD WP SFC participants are collaborating as a team on the IAEA CRP on SFC. The EURAD WP SFC project consists of four tasks. Task 3 investigates the behaviour of nuclear fuel and cladding after discharge. The aim of these activities is to understand and describe the evolution of the cladding-pellet system and its ageing under conditions of extended interim storage, transportation and emplacement in a final disposal system. At the Third Research Coordination Meeting on Spent Fuel Characterization, BAM as contributor to Task 3 reported on the activities and status of its research work. T2 - IAEA 3rd Research Coordination Meeting of the Coordinated Research Project on Spent Fuel Characterization CY - Cockermouth, UK DA - 01.07.2024 KW - Nuclear fuel KW - Cladding KW - Discharge PY - 2024 AN - OPUS4-60668 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zencker, Uwe A1 - Gaddampally, Mohan Reddy A1 - Völzke, Holger T1 - Failure Analysis on Irradiated Claddings Subjected to Long-Term Dry Interim Storage N2 - Long-term dry interim storage may adversely affect the mechanical properties of spent fuel rods, possibly resulting in a reduced resilience during handling or transport after storage. The cladding is the first barrier for the spent fuel pellets. An established method for characterising the cladding material is the ring compression test (RCT), in which a small, cylindrical sample of the cladding tube is subjected to a compressive load. Radial hydrides may precipitate in zirconium-based alloys (Zircaloy) under pre-storage drying and during slow cooling, which result in embrittlement of the cladding material and eventually a possible sudden failure of cladding integrity under additional mechanical loads. The focus of the presented research is on the development of appropriate nu-merical methods for predicting the mechanical behaviour and identification of limiting conditions to prevent brittle fracture of Zircaloy claddings. A modelling approach based on cohesive zones is ex-plained which is able to reproduce the propagation of cracks initiated at radial hydrides in the zir-conium matrix. The developed methods are applied to defueled samples of cladding alloy ZIRLO®, which were subjected to a thermo-mechanical treatment to reorient existing circumferential hy-drides to radial hydrides. A selected sample showing sudden load drops during a quasi-static ring compression test is analysed by means of fracture mechanics for illustrative purposes. Based on the developed fracture mechanics approach, not only the deformation behaviour but also the fail-ure behaviour of irradiated as well as unirradiated Zircaloy claddings with radial hydrides under RCT loading conditions can be adequately described. T2 - 27th International Conference on Structural Mechanics in Reactor Technology - SMiRT 27 CY - Yokohama, Japan DA - 03.03.2024 KW - Cladding Embrittlement KW - Cohesive Zone Modelling KW - Ring Compression Test KW - Spent Nuclear Fuel PY - 2024 SP - 1 EP - 8 AN - OPUS4-60671 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zencker, Uwe T1 - Failure Analysis on Irradiated Claddings Subjected to Long-Term Dry Interim Storage N2 - Long-term dry interim storage may adversely affect the mechanical properties of spent fuel rods, possibly resulting in a reduced resilience during handling or transport after storage. The cladding is the first barrier for the spent fuel pellets. An established method for characterising the cladding material is the ring compression test (RCT), in which a small, cylindrical sample of the cladding tube is subjected to a compressive load. Radial hydrides may precipitate in zirconium-based alloys (Zircaloy) under pre-storage drying and during slow cooling, which result in embrittlement of the cladding material and eventually a possible sudden failure of cladding integrity under additional mechanical loads. The focus of the presented research is on the development of appropriate nu-merical methods for predicting the mechanical behaviour and identification of limiting conditions to prevent brittle fracture of Zircaloy claddings. A modelling approach based on cohesive zones is ex-plained which is able to reproduce the propagation of cracks initiated at radial hydrides in the zir-conium matrix. The developed methods are applied to defueled samples of cladding alloy ZIRLO®, which were subjected to a thermo-mechanical treatment to reorient existing circumferential hy-drides to radial hydrides. A selected sample showing sudden load drops during a quasi-static ring compression test is analysed by means of fracture mechanics for illustrative purposes. Based on the developed fracture mechanics approach, not only the deformation behaviour but also the fail-ure behaviour of irradiated as well as unirradiated Zircaloy claddings with radial hydrides under RCT loading conditions can be adequately described. T2 - 27th International Conference on Structural Mechanics in Reactor Technology - SMiRT 27 CY - Yokohama, Japan DA - 03.03.2024 KW - Cladding Embrittlement KW - Cohesive Zone Modelling KW - Ring Compression Test KW - Spent Nuclear Fuel PY - 2024 AN - OPUS4-60672 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Nietzke, Jonathan T1 - Mechanische Eigenschaften von additiv gefertigtem AISI 316L unter Wasserstoffatmosphäre N2 - Wasserstoff führt zu einer Degradation der mechanischen Eigenschaften vieler Stähle. In dieser Arbeit wurde dieser Effekt in additiv hergestelltem AISI 316L (1.4404) mithilfe von in-situ SSRT-Versuchen untersucht. T2 - BMDK / Forschungsseminar Otto-von-Guericke-Universität Magdeburg CY - Magdeburg, Germany DA - 11.12.2024 KW - Wasserstoff KW - AISI 316L KW - 1.4404 KW - SSRT PY - 2024 AN - OPUS4-62166 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Amano, Kofi Owusu Ansah T1 - Thermal runaway characteristics and gas emission from sodium-ion cells – impact of state of charge level N2 - Like lithium batteries, sodium batteries can also undergo thermal runaway. In a series of tests, 30 thermal runaway tests were carried out with sodium battery cells. The tests were carried out both in nitrogen and in air with different SOCs. The presentation shows the main results of these tests. T2 - 7th International Battery Production Conference (IBPC) CY - Braunschweig, Germany DA - 27.11.2024 KW - Consequneces KW - Electrical Energy Storage KW - Sodium-ion battery KW - Gas release KW - SIB PY - 2024 AN - OPUS4-62178 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Grimault de Freitas, Tomás T1 - Closing the gaps towards the Standardisation of the Hollow Specimen Method for Tests in High-Pressure Hydrogen Gas N2 - Metallic materials, mainly steels, are the most commonly used structural materials in various components throughout the hydrogen supply chain. Ensuring their sustainable and safe use in hydrogen technologies is a crucial factor in the development of the hydrogen economy. This is particularly important since hydrogen can promote crack formation and ultimately lead to premature failure in these materials when combined with mechanical load. This process is commonly known as Hydrogen Embrittlement and can occur in a large number of steels used for the hydrogen technologies.[1] Extensive materials qualification is required for the rapid implementation of hydrogen technologies, however, most accepted, and standardised test methods for determining the effect of gaseous hydrogen on metallic materials describe complex and costly procedures (e.g. in-situ autoclave technique) that are only available to a very limited extent worldwide. The hollow specimen technique is a simple and economical method that has the potential to overcome the limitations of the current methods and complement them for qualifying metallic materials under high-pressure hydrogen gas. Unlike the conventional autoclave technique, this method requires significantly lower amounts of hydrogen, resulting in fewer safety measures and no need for complex equipment or a specialised laboratory. The technique's low investment and testing costs, simple operation, and shorter testing time make it an optimal for widespread use around the world, thereby increasing the output of results. Initial studies have demonstrated the feasibility of assessing hydrogen effects in metallic materials using the hollow specimen technique. This led to the establishment of an ISO committee to standardise the method, however, there are open questions that currently prevent the technique from being standardised for hydrogen testing. These open questions relate to specimen geometry, inner hole surface and gas quality and are being addressed in the TransHyDE - H2HohlZug project. The aim of the project is to systematically address and close the gaps towards the standardisation of this technique for tests in hydrogen. The project is divided into four work packages. First, the elastic-plastic behaviour of a hollow tensile specimen is compared with that of a conventional solid tensile specimen of identical external dimensions using finite element methods (3D-FEM) and subsequently validated by experimental results. In the second, the influence of the inner hole surface quality of the specimen on the hydrogen effects is evaluated. Five different methods of producing the inner axial hole were chosen to ensure different average roughness values and residual stresses (drilling vs. EDM), and also to ensure a good representation of the more common and easily accessible processes (drilling and reaming) to the more complex ones (EDM and honing). Next, the influence of gas purity (different compositions) and purging process (different routines) is evaluated. Finally, an optimal specimen geometry, inner hole production process, gas quality and purging process are proposed from each working package and its reproducibility and repeatability is evaluated in a round robin with national and international partners. This contribution presents the structure and milestones of the project, followed by initial results regarding the influence of different manufacturing and finishing processes on the inner hole surface of the hollow specimen and its response to hydrogen effects. T2 - MPA Seminar 2024 - Materials, Processes, Applications CY - Stuttgart, Germany DA - 08.10.2024 KW - Hydrogen KW - Hydrogen Embrittlement KW - Tensile Test KW - High-Pressure Gaseous Hydrogen KW - Hollow Specimen Technique KW - Standardisation KW - TransHyDE KW - H2HohlZug PY - 2024 AN - OPUS4-61286 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eisermann, R. A1 - Esterl, F. A1 - Schuchardt, M. A1 - Breithaupt, Mathias A1 - Plath, R. T1 - Distributed acoustic/vibration sensing: Towards advanced transformer condition monitoring N2 - A novel method for transformer vibration monitoring using intensity-based distributed acoustic/vibration sensing (DAS/DVS) is presented. Fibre optic sensors were fully integrated into an oil-filled medium voltage distribution transformer. Opencircuit in-situ measurements were carried out using a single and three-phase supply with an electrical power of up to 30 kVA. Spectral analysis of the mechanical vibrations were performed by measuring the frequency response of the transformer using plain fibre- and transducer-based DVS approaches. The results were compared with the spectra of a microphone mounted on the outside of the transformer housing and the electrical measurements on the high voltage side. Using the fibre optic DVS based monitoring we were able to detect changes in operating power and frequency. Further it could be shown, that it is possible to identify anomalous behaviour such as electrical/mechanical noise sources using the determined vibration spectra. T2 - 2024 IEEE International Conference on High Voltage Engineering and Applications (ICHVE) CY - Berlin, Germany DA - 18.08.2024 KW - Distributed acoustic sensing KW - DAS KW - Transformer monitoring PY - 2024 DO - https://doi.org/10.1109/ICHVE61955.2024.10676084 SP - 1 EP - 4 PB - IEEE CY - New York City, New York, USA AN - OPUS4-61798 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Román Healy Corominas, Francesco Piccolo T1 - Sulfur Spillover on Carbon Materials and its Relevance for Metall-Sulfur Solid-State Batteries N2 - Lithium-sulfur batteries are commonly assembled using a composite material containing porous carbon and sulfur as the cathode. While much work has been done on the design of such high performance composites, the interaction between sulfur and carbon is poorly unterstood. Here we provide further evidence that sulfur and porous carbon undergo a spontaneous reaction at room temperature, recently described as "sulfur spillover". Thermal measurements, XRD, XAS and EPR are used to provide insight into the interaction energy and structure of sulfur after spillover. We also show that the effect may cause a loss in cell voltage by about 70 mV. T2 - 11th Workshop Lithium-Sulfur Batteries CY - Dresden, Germany DA - 11.11.2024 KW - Sulfur Spillover KW - Metal-Sulfur Solid-State Batteries KW - TAM IV KW - XRD KW - XAS KW - EPR PY - 2024 AN - OPUS4-61736 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -