TY - CONF A1 - Tornaghi, M. L. A1 - Tsionis, G. A1 - Pegon, P. A1 - Molina, J. A1 - Peroni, M. A1 - Korzen, Manfred A1 - Tondini, N. A1 - Covi, P. A1 - Abbiati, G. A1 - Antonelli, M. A1 - Gilardi, B. T1 - Experimental study of braced steel frames subjected to fire after earthquake N2 - The EQUFIRE project aims to study the post-earthquake fire Performance of steel frame structures and is part of the Transnational Access activities of the SERA project (www.sera-eu.org) at the ELSA Reaction Wall of the European Commission - Joint Research Centre. As it has happened in many historical occasions, after an earthquake, earthquakeinduced rupture of gas piping, failure of electrical systems, etc. may trigger fire. The structural fire performance can deteriorate because the fire acts on a previously damaged structure. In addition, the earthquake may have damaged fire protection elements and the fire can spread more rapidly if compartmentation walls have failed. This is particularly relevant for steel structures as the high thermal conductivity of elements with small thickness entails quick temperature rise with consequent fast loss of strength and stiffness. EQUFIRE studied a four-storey three-bay steel frame with concentric bracings in the central bay. The structure was designed for reference peak ground acceleration equal to 0.186g, soil type B and type 1 elastic response spectrum according to Eurocode 8. Tests were performed at the ELSA Reaction Wall and at the furnace of the Federal Institute for Materials Research and Testing (BAM). The experimental activities at the ELSA Reaction Wall comprise pseudo-dynamic tests on a full-scale specimen of the first storey of the building, while the upper three storeys are numerically simulated. The aim is to study the response of the structure and fire protection elements, including their interaction, under the design earthquake and for different configurations: bare frame without fire protection, specimen with three fire protection solutions (conventional and seismic-resistant boards, and vermiculite sprayed coating) applied on the bracing and one column, and with conventional and seismic-resistant fire barrier walls built in the two external bays of the specimen. The testing programme at BAM included fire tests of five columns (two specimens without fire protection elements and three specimens with the types of fire protection mentioned above). Before the fire test, each column was subjected to a horizontal and vertical displacement history resulting from the seismic action. During the fire tests, the effect of the surrounding structure was simulated by limiting the axial thermal expansion. The experimental results will serve to study the response of structural and non-structural components to fire following earthquake scenarios, with a view to improving existing design guidelines and future standards. T2 - The 17th World Conference on Earthquake Engineering - 17WCEE CY - Meeting was canceled DA - 13.09.2020 KW - Fire following earthquake KW - Concentrically braced steel frames KW - Large-scale tests KW - Pseudo-dynamic testing KW - Substructuring PY - 2020 SP - 2i-0104-1 EP - 2i-0104-12 AN - OPUS4-51426 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - von Werder, Julia A1 - Gardei, André A1 - Hoppe, Johannes A1 - Meng, Birgit ED - Littmann, K. T1 - Funktionalisierung von Fasern für zementgebundene Materialien - ausgewählte Prüfmethoden N2 - Die geringe Zugfestigkeit von zementgebundenen Materialien kann durch die Zugabe von Fasern maßgeblich verbessert werden. Ziel eines gemeinsamen Verbundprojekts mit einem Industriepartner war die Erhöhung der Leistungsfähigkeit von kurzen Polymer- und Carbonfasern durch eine Verbesserung des Verbundes zwischen Faseroberfläche und Zementsteinmatrix. Von der IONYS AG wurde dazu eine spezielle Funktionalisierung entwickelt, die über eine Hydrophilisierung der Faseroberfläche eine chemische Anbindung an die Zementsteinmatrix gewährleistet. Aufgabe der BAM war es, die Effizienz der neuen Beschichtung bezüglich der Erhöhung der Nachrissbiegezugfestigkeit und der Reduzierung der Schwindrissbildung während der Erhärtungsphase zu quantifizieren. Die Ergebnisse zeigen, dass die Funktionalisierung die Neigung zur Schwindrissbildung für die Carbonfasern und in noch stärkerem Maße für die Polymerfasern reduziert. Eine Erhöhung der Nachrissbiegezugfestigkeit konnte dagegen nur für die deutlich steiferen Carbonfasern nachgewiesen werden. T2 - 10. Kolloquium Industrieböden CY - Esslingen, Germany DA - 03.03.2020 KW - Fibres KW - Cementitious materials KW - Shrinkage KW - Strain hardening PY - 2020 SN - 978-3-8169-3505-6 SP - 173 EP - 178 PB - expert Verlag GmbH CY - Tübingen AN - OPUS4-51915 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - von Werder, Julia A1 - Fontana, P. A1 - Hoppe, Johannes A1 - Bilgin, S. A1 - Meng, Birgit ED - Serrat, C. ED - Casas, J. R. ED - Gibert, V. T1 - Composite Facade Elements with Self-Cleaning Surface made of Ultra-High-Performance Concrete (UHPC) N2 - In the framework of the European project H-House various concrete façade elements were developed with the aim to ensure a long service life by combining a very durable material with self-cleaning properties. The façade elements presented are made of a shell of UHPC filled with blocks of aerated autoclaved concrete as insulating material. Self-cleaning properties were realized amongst others by imprinting a microstructure into the surface during casting. The paper focuses on selected technological aspects of the manufacturing process of prototypes which had to be performed in two concreting sections. Furthermore the challenges faced when upscaling the self-cleaning properties are addressed and the strategy to assess the self-cleaning properties by measuring the contact and the roll-off angel is presented. The results show that a successfull upscalaing process requires detailed planning and that the best results can often be achieved with a moderate work effort or material use. T2 - XV International Conference on Durability of Building Materials and Components (DBMC 2020) CY - Online meeting DA - 20.10.2020 KW - Ultra-High-Performance Concrete KW - Facade Elements KW - Self-Cleaning Properties KW - Adhesive Pull-Strength KW - Microstructure KW - Architectural Concrete PY - 2020 SN - 978-84-121101-8-0 SP - 1289 EP - 1297 PB - International Center for Numerical Methods in Engineering (CIMNE) CY - Spain AN - OPUS4-51967 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wiehle, Philipp A1 - Brinkmann, M. T1 - Tragfähigkeit von Lehmmauerwerk - Experimentelle und numerische Analyse T1 - Load-bearing capacity of earth masonry – An experimental and numerical analysis N2 - Die Bemessung von tragendem Lehmmauerwerk erfolgt in Deutschland auf Basis der Lehmbau Regeln. Das dort verankerte Nachweisverfahren beruht auf einem globalen Sicherheitskonzept, welches aus zuverlässigkeitstheoretischer Sicht nicht mehr dem Stand der Technik entspricht. Auf Grund dessen wird das Bemessungskonzept für Lehmmauerwerk vom Deutschen Institut für Bautechnik (DIBt) voraussichtlich 2023 außer Kraft gesetzt. Ein statischer Nachweis von tragenden Lehmbauten wäre in Deutschland dann ausschließlich mit einer Zustimmung im Einzelfall (ZiE) oder vorhabenbezogener Bauartgenehmigung (vBg) möglich. Beides ist mit erheblichem Mehraufwand und höheren Kosten verbunden, was für den Lehmmauerwerksbau einen entscheidenden Nachteil im Vergleich zum konventionellen Mauerwerksbau darstellt. Um eine unkomplizierte Praxisanwendung von Lehmmauerwerk zu ermöglichen, werden innerhalb eines Forschungsvorhabens, welches von der Bundesanstalt für Materialforschung und -prüfung (BAM), dem Institut für Massivbau der Technischen Universität Darmstadt sowie dem Ingenieurbüro ZRS durchgeführt wird, auf Basis der Produktnormen für Lehmsteine und Lehmmauermörtel Grundlagen für ein aktualisiertes Bemessungskonzept entwickelt. Im Rahmen des Projekts wird ebenfalls untersucht, inwiefern die Bemessungsregeln nach den vereinfachten Berechnungsmethoden für unbewehrtes Mauerwerk gemäß DIN EN 1996-3 / NA auf den Lehmmauerwerksbau übertragbar sind. Falls eine Anwendung des normativen Nachweisverfahrens bei Lehmmauerwerk möglich ist, wäre zukünftig eine Aufnahme von Lehmsteinen und Lehmmauermörtel in den nationalen Anhang des Eurocode 6 denkbar, was eine bedeutsame Erweiterung des Anwendungsbereichs von Lehmmauerwerk zur Folge hätte. Diverse wissenschaftliche Untersuchungen konnten zeigen, dass bemessungsrelevante Festigkeits- und Verformungseigenschaften von Lehmmauerwerksbaustoffen stark von der vorherrschenden Materialfeuchte abhängen, welche im hygroskopischen Wassergehaltsbereich im Wesentlichen von der relativen Luftfeuchte (RLF) bestimmt wird. Auch die Zwischenergebnisse des laufenden Forschungsvorhabens zur Entwicklung eines Bemessungskonzepts für Lehmmauerwerk ergaben eine deutlich erkennbare Abhängigkeit zwischen der Materialfeuchte und den relevanten Festigkeits- und Verformungseigenschaften. Eine detaillierte Kenntnis des feuchteabhängigen Materialverhaltens von Lehmsteinen, -mörtel und -mauerwerk ist zwingend erforderlich, um ein konsistentes und zuverlässiges Bemessungskonzept für Lehmmauerwerk zu entwickeln. Im Rahmen des laufenden Forschungsprojektes werden deshalb umfangreiche Versuche zum Drucktragverhalten von Lehmsteinen und -mörtel sowie Lehmmauerwerk nach Konditionierung bei unterschiedlichen RLF durchgeführt und analysiert. Weiterhin werden auf Basis der experimentellen Ergebnisse numerische Modelle kalibriert, welche die detaillierte Analyse der Biegedrucktragfähigkeit von Lehmmauerwerk ermöglichen. In diesem Beitrag werden zunächst die bisherigen Zwischenergebnisse bezüglich der experimentell ermittelten feuchteabhängigen Materialkennwerte von Lehmsteinen, -mörtel und -mauerwerk dargelegt. Darauf aufbauend werden numerische Untersuchungen zur Bestimmung der Systemtragfähigkeit von Lehmmauerwerk unter Feuchteeinflusses durchgeführt und erläutert. N2 - The structural design of load-bearing earthen masonry in Germany is based on the Lehmbau Regeln. The verification procedure outlined in these regulations is based on a global safety concept that no longer corresponds to the state of the art from a reliability theory perspective. As a result, the structural design concept for earthen masonry will most likely be discontinued by the German Institute for Building Technology (DIBt) in 2023. A structural verification of load-bearing earthen buildings would then only be possible in Germany with an approval for individual cases (ZiE) or a project-related permit type (vBg). Both methods are associated with considerable additional work and higher costs, which is a decisive disadvantage for earthen masonry construction compared to conventional masonry construction. In order to enable a straightforward practical application of earthen masonry, the Federal Institute for Materials Research and Testing (BAM), the Institute for Solid Construction of the Technical University of Darmstadt and ZRS Engineers are laying the groundwork for an updated structural design concept based on the product standards for earth blocks and earthen masonry mortar. The project will also investigate the extent to which the design rules based on the simplified calculation methods for unreinforced masonry according to DIN EN 1996-3 / NA can be transferred to earthen masonry construction. If the normative verification procedure can be applied to earthen masonry, it would be conceivable to include earth blocks and earthen masonry mortar in the national appendix of Eurocode 6 in the future, which would result in a significant expansion of the field of application of earthen masonry. Various scientific studies have shown that the strength and deformation properties of earthen masonry building materials relevant to structural design are strongly dependent on the prevailing material moisture level, which is essentially determined by the relative humidity (RH) in the hygroscopic water content range. The interim results of the current research project for the development of a structural design concept for earthen masonry also showed a clearly recognisable dependency between the material moisture level and the relevant strength and deformation properties. Detailed knowledge of the moisture-dependent material behaviour of earth blocks, earthen mortar and masonry is absolutely essential to developing a consistent and reliable structural design concept for earthen masonry. Within the framework of the current research project, extensive tests on the pressure load bearing capacity of earth blocks and earthen mortar as well as earthen masonry after conditioning at different RH levels are therefore being carried out and analysed. Furthermore, numerical models are being calibrated on the basis of the experiment results, which facilitate a detailed analysis of the bending pressure bearing capacity of earthen masonry. This paper presents, firstly, the interim results obtained so far concerning the experimentally determined moisture-dependent material characteristics of earth blocks, earthen mortar and masonry. Based on this material, numerical investigations for determining the system bearing capacity of earthen masonry under the influence of moisture are carried out and explained. T2 - LEHM 2020 CY - Weimar, Germany DA - 30.10.2020 KW - Lehm KW - Earth KW - Tragfähigkeit KW - Mauerwerk KW - Feuchte KW - Load-bearing KW - Moisture KW - Strength PY - 2020 SP - 1 EP - 12 PB - Dachverband Lehm CY - Weimar AN - OPUS4-53231 LA - mul AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Buchheim, Janine A1 - Recknagel, Christoph A1 - Wolter, Patrick A1 - Kittler-Packmor, Kai T1 - A new approach towards scientific evaluation and performance-related design of bituminous joint sealing materials and constructions N2 - While there is a permanent improvement of concrete pavement mixtures and pavement construction types over the last decades, the state-of-the-art joint sealing materials and joint constructions seem to stagnate on an antiquated empirical level. This status has been reaffirmed in the latest European standard. The consequences in the motorway network due to unsatisfying capability and durabilty of joint sealing systems are unacceptable. In addition, inadequate traffic performance (noise emissions, roll-over comfort) and traffic safety losses in the joint area of concrete pavements are existing challenges. These deficits and weaknesses reflect a demand for joint sealing materials and constructions whose approval requirements take functional aspects into account. Furthermore a sufficient analysis of decisive loads and a practice-oriented method to evaluate the requirements towards performance and durability is still missed. In this contribution decisive loads to German highways are analyzed. The design of test specimen for representative functional testing of joint sealing systems is discussed. The focus is on the geometry of the test specimens and the used concrete mixture. Finally, a new approach for a function-orientated test concept that considers representative load functions is presented. The potential of this approach to validate the durability and capability of various joint sealing systems is also presented using an example. T2 - RILEM International Symposium on Bituminous Materials CY - Online meeting DA - 08.06.2020 KW - Joint sealing KW - Expansion joint KW - Performance testing KW - Capability KW - Durability PY - 2020 SN - 978-3-030-46454-7 VL - 27 SP - 1 EP - 6 PB - Springer Nature AN - OPUS4-53488 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Erning, Johann Wilhelm T1 - Sprechen wir über Korrosion - aber richtig! N2 - Die Korrosion in ihren zahlreichen Erscheinungsformen beschäftigt Fachleute und Laien. Um-so wichtiger ist es, die einzelnen Phänomene korrekt und eindeutig zu benennen. Nur so kann man eine saubere Beschreibung der Korrosionsvorgänge erreichen und damit in der wörtlichen und schriftlichen Kommunikation richtig verstanden werden. An zahlreichen Beispielen wird der richtige und normgemäße Sprachgebrauch beschrieben. T2 - Korrosionsschutz in der maritimen Technik CY - Hamburg, Germany DA - 29.01.2020 KW - Korrosion KW - Nomenklatur PY - 2020 SN - 978-3-935406-72-7 SP - 7 EP - 11 AN - OPUS4-50327 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tian, H. A1 - Voigt, Marieke A1 - Lehmann, C. A1 - Meng, Birgit A1 - Stephan, D. ED - Middendorf, B. ED - Fehling, E. T1 - Composition and microstructure stability of cement compound under cyclic hydrothermal condition N2 - There have been many researches focused on the performance improvement of ultra-high performance concrete (UHPC) by autoclaving treatment. The goal of autoclaving is to increase the pozzolanic reaction, and to densify the cement stone and the transition zone which originates from the incorporation of supplementary cementitious materials (SCMs), such as silica fume, fly ash and blast furnace slag. Due to the superior properties, UHPC can also be utilized under high mechanical load and aggressive condition, for example, the fabrication of water tanks for thermal storage which is of great significance for saving energy and reducing CO2 emission. It is known that mineral stability of the hydration products of an inorganic binder is highly related to the temperature and pressure of the environment. A certain stable composition at room temperature, however, may undergo a phase transformation at high temperature and the performance decrease under this severe condition will generally be more severe. In this way, the rationale behind this deterioration under long-term hydrothermal condition involving many cycles and long duration has to be clarified, and then appropriate optimizing methods will be performed in order to obtain a kind of construction with high durability under aggressive environment. For this purpose, different types and amounts of SCMs are introduced into the standard mixture of UHPC and the phase compositions after autoclaving at 200 °C and 15.5 bar are determined by combined X-ray diffraction and scanning electron microscope. Mercury intrusion porosimeter is used to characterise the microstructure of the samples. In order to establish the relationship between microstructure and macroscopic properties, compressive and flexural strength are also investigated. T2 - HiPerMat 2020 CY - Kassel, Germany DA - 11.03.2020 KW - Hydrothermal treatment KW - UHPC KW - Composition PY - 2020 SN - 978-3-7376-0828-2 VL - 23 SP - 87 EP - 88 PB - Kassel University Press CY - Kassel AN - OPUS4-52375 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Voigt, Marieke A1 - von Werder, Julia A1 - Meng, Birgit ED - Middendorf, B. ED - Fehling, E. T1 - Microstructure analysis of thermally treated ultra high performance concrete in the context of the durability performance N2 - Ultra high performance concrete (UHPC) is known for its high compressive strength of more than 150 MPa and its high durability. Thermal treatment at 90°C can accelerate the strength development so that the 28-days-strength can be achieved immediately after the treatment and an additional increase up to 30 % in some cases. The reason for the strength development is an accelerated hydration of the clinker minerals and an intensified pozzolanic reaction leading to a denser microstructure. In previous research inhomogeneities in form of a zonation after unprotected thermal treatment were observed and analysed in respect to changes in the microstructure. This zonation is defined by a different microstructure in the core compared to the outer zone in the matter of porosity, mineral phase composition and a significant change in the potassium and sulphur concentration of the zones is measurable. To isolate different transport mechanisms responsible for these element distributions UHPC samples were thermally treated at 90 °C and the microstructure was investigated under dry conditions and after immersion in water to investigate the influence of dehydration during and rehydration after the thermal treatment on the microstructure. Through durability testing via water absorption, water vapour diffusion, permeability testing and sulfuric acid resistance transport mechanisms like diffusion, migration, capillary suction are under investigation in correlation with the microstructure analysis. For the microstructure analysis measurements with µXRF, mercury intrusion porosity, XRD and SEM were conducted. T2 - HiPerMat 2020 CY - Kassel, Germany DA - 11.03.2020 KW - UHPC KW - Thermal treatment KW - Zonation KW - Transport mechanism KW - Durability PY - 2020 SN - 978-3-7376-0828-2 DO - https://doi.org/10.17170/kobra-202002271026 VL - 23 SP - 151 EP - 152 PB - Kassel University Press CY - Kassel AN - OPUS4-52373 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - von Werder, Julia A1 - Bilgin, S. A1 - Hoppe, Johannes A1 - Fontana, P. A1 - Meng, Birgit ED - Middendorf, B. ED - Fehling, E. ED - Wetzel, A. T1 - Composite UHPC facade elements with self-cleaning surface: Aspects of technological manufacturing N2 - In the framework of the European collaborative project H-House, which was finished in 2017, large façade elements were developed consisting of a box shaped external shell of ultra-high-performance concrete (UHPC) with a functionalized surface and an insulation of autoclaved aerated concrete (AAC). The exposed concrete of the elements was further refined by adding self-cleaning properties to the surface through imprinting a microstructure in combination with chemical agents directly in the casting process. The paper focuses on selected technological aspects of the manufacturing process of large-scale prototypes. Presented are results of the upscaling process of functionalized surfaces from small specimen up to large UHPC composite facade elements produced for the construction of a demonstrator. T2 - 5th International Symposium on Ultra-High Performance Concrete and High Performance Construction Materials (HiPerMat 2020) CY - Kassel, Germany DA - 11.03.2020 KW - Ultra-High Performance Concrete KW - Facade Elements KW - Self-Cleaning Properties KW - Architectural Concrete PY - 2020 SN - 978-3-7376-0828-2 DO - https://doi.org/10.17170/kobra-202002271026 IS - 32 SP - 51 EP - 52 PB - kassel university press CY - Kassel AN - OPUS4-51908 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schmidt, Wolfram A1 - Olonade, K. A. A1 - Mbugua, R. N. A1 - Lenz, F. J. A1 - Tchetgnia Ngassam, I. T1 - Bio-Based Rheology Modifiers for High Performance Concrete – Possible Modes of Actions and Case Study for Cassava Starch in West Africa N2 - Polymers that help tailoring rheological properties during the casting process have become inevitable constituents for all kinds of high-performance concrete technologies. Due to lacking industries, these typically crude-oil based admixtures are not readily available in many parts of the world, which limits the implementation of more sustainable high-performance construction technologies in these regions. Alternative polymers, which often demand for less processing, can be derived from local plant-based resources. The paper provides experimental data of flow tests of cement pastes with polysaccharides from Triumfetta pendrata A. Rich, acacia gum and cassava without and in the presence of polycarboxylate ether superplasticizer. The flow tests are amended by observations of the zeta potentials and the hydrodynamic diameters in the presence of and without calcium ions in the dispersion medium. The results show that in the presence of and without calcium ions all polysaccharides provide negative zeta potentials, yet, they affect flowability and thixotropy in different ways. Cassava starch, acacia gum, and the gum of Triumfetta pendrata A. Rich qualified well for robustness improvement, strong stiffening, and additive manufacturing, respectively. The reason for the different effects can be found in their average sizes and size distribution. Due to the promising results, a flow chart for local value chains is derived on the example of yet unused cassava wastes, which can be converted in parallel. T2 - 3rd International Conference on the Application of Superabsorbent Polymers CY - Skukuza, South Africa KW - Admixtures KW - Polysaccharides KW - Rheology KW - Thixotropy KW - Concrete PY - 2020 SN - 978-3-030-33341-6 SN - 978-3-030-33342-3 DO - https://doi.org/10.1007/978-3-030-33342-3_17 SP - 158 EP - 166 PB - Springer AN - OPUS4-58404 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Stuff, Maria A1 - Rübner, Katrin A1 - Prinz, Carsten A1 - Rische, N. A1 - Chronz, M. A1 - Kühne, Hans-Carsten ED - Siegesmund, S. ED - Middendorf, B. T1 - Towards a better understanding of tuff stone deterioration N2 - Stone deterioration is the result of a complex interaction of external physical, chemical and biological forces with the mineralogical-petrophysical properties of the stone. With a better understanding of how these properties are linked to material behavior and durability, more effective measures for stone conservation can be developed. Studying these interactions in tuff is particularly complex due to the naturally high heterogeneity of tuff rocks. The first aim of a current research project is to combine the results of recent and older studies on tuff deterioration. Furthermore, the literature overview is complemented by our own investigation of Weibern and Ettringen tuff, with a focus on pore structure characteristics. T2 - STONE - 14th international congress on the deterioration and conservation of stone CY - Meeting was canceled DA - 07.09.2020 KW - Pore structure KW - Weathering KW - Weibern tuff KW - Ettringen tuff PY - 2020 SN - 978-3-96311-172-3 SP - 805 EP - 810 PB - Mitteldeutscher Verlag CY - Halle (Saale) AN - OPUS4-51549 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schwettmann, K. A1 - Stephan, D. A1 - Nytus, N. A1 - Radenberg, M. A1 - Weigel, Sandra T1 - Post carbon road - The endless cycle of bitumen reuse N2 - In Germany, the reuse of asphalt has a long tradition. Since the 1980s, the reclaimed asphalt has been recycled achieving a reuse rate of around 90% and thus a very high value in the last years. In the future, instead of the amount, the quality of the reclaimed asphalt will be more important because the recycled asphalt will be reused again and again. Thus, these asphalt mixes are in the second or even third cycle of reuse. Concerning this situation, the question arises if asphalt can be reused several times without any loss in quality. An important factor affecting the asphalt quality is the binder bitumen. During the production, construction and service life, the ageing of this binder occurs causing a hardening of the bitumen. To compensate this hardening, additives for the reclaimed asphalt in terms of rejuvenation agents (rejuvenators) gain in importance. With these rejuvenators, the physical properties of bitumen can be modified e.g. the hardness and the stiffness reduced. However, the mechanism of the rejuvenation agents and the effects of the bitumen chemistry are largely unknown because the composition of the products varies very strongly. But with growing knowledge about these mechanisms and effects of the rejuvenation agents, the chemical composition and thus the physical and ageing behavior of bitumen can be targeted modified by the use of suitable rejuvenators. In this work, the actual results of the project Postcarbone road should be presented including investigations about the chemical and physical mechanisms as well as the efficiency of different rejuvenators. Further, a model for the cyclic reuse of bitumen should be developed. Based on this model, the choice of a suitable rejuvenation agent for the considered bitumen or rather asphalt should be possible. The project Postcarbone road (392670763) is funded by the German Research Foundation (DFG). T2 - 7th Eurasphalt and Eurobitume Comgress CY - Online meeting DA - 15.06.2021 KW - Bitumen KW - Multiple ageing and rejuvenation KW - Conventional testing KW - DSR KW - BBR KW - FTIR KW - Asphaltene content KW - Column chromatography PY - 2021 SP - 1 EP - 14 AN - OPUS4-53490 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Weise, Frank A1 - Müller, U. A1 - Hüsken, Götz A1 - Gardei, Andre T1 - Begutachtung Berliner Tuffsteinfassaden - Turmruine der Kaiser-Wilhelm-Gedächtniskirche und Charlottenburger Tor N2 - Am Ende des 19. und zu Beginn des 20. Jahrhunderts wurden auch in Berlin vermehrt Bauwerke mit einer Fassadenverblendung aus Eifeler Tuffsteinen errichtet. Die Eifeler Tuffsteine zeichnen sich aufgrund ihrer hohen Porosität einerseits durch eine gute Verarbeitbarkeit aus. Andererseits sind sie nur schwach gebunden und besitzen deshalb eine geringe Verwitterungsbeständigkeit. T2 - Workshop Kulturguterhaltung - Vom Dampfkessel zu Nanomaterialien CY - Berlin, Germany DA - 17.11.2021 KW - Fassade KW - Tuffstein KW - Schalenbildung PY - 2021 SN - 2567-1251 VL - 3 SP - 107 EP - 123 PB - Druckerei G. Bohm CY - Berlin AN - OPUS4-54461 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - von Werder, Julia A1 - Simon, Sebastian A1 - Meng, Birgit T1 - Internal sulfate resistance of concrete N2 - If the amount of sulfate within the mix design for concrete is not balanced, ettringite formation which first controls solidification continues while the concrete is hardening. Ettringite forms by reaction of sulfate contained in the cement or in some admixture with calcium aluminate (C3A) as cement component. The “late primary ettringite formation” promotes an increase in volume within the hardened concrete leading to cracks. To analyze the effect of substituting part of ordinary Portland cement (OPC) by a treated brown coal fly ash mortar bars were tested according to ASTM C452. This test method was originally developed to extrapolate from the internal to external sulfate attack and is based on the idea that by testing a concrete mixture containing sulfate the process of deterioration is accelerated because it does not have to diffuse into the concrete before reaction first. In addition to the samples prescribed in ASTM C452 further samples in the size of the German SVA procedure were tested also designed for accessing the external sulfate resistance. The results show that while the replacement of 25 % of cement by brown coal fly ash leads to length changes around the limit defined by ASTM, the substitution of 50 % cement exceeded the limit by a multiple. The progress of expansion is the very similar for the two geometries tested. In-situ XRD measurements confirmed that while for pastes made of OPC the formation of ettringite is completed after 20 hours, this is not true for the mixtures containing the brown coal fly ash. In a different study the effect of hydrothermal treatment on the phase composition of ultra-high-performance concrete was analyzed. The results show that the sulfate and aluminate resulting from the decomposition of ettringite are bound into new phases. If this binding is permanent this might allow the larger use of sulfate bearing raw materials. T2 - EuroCoalAsh 2021 Conference CY - Online meeting DA - 02.11.2021 KW - Brown coal fly ash KW - Ettringite KW - Internal sulfate resistance KW - Test methods KW - In-situ XRD KW - Hydrothermal treatment PY - 2021 SP - 131 EP - 137 CY - Thessaloniki AN - OPUS4-54133 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Weise, Frank A1 - Patitz, G. A1 - Redmer, B. A1 - Hübner, M. T1 - Zerstörungsfreie Strukturaufklärung antiker Baudenkmäler des Pergamonmuseums N2 - Das Pergamonmuseum ist eines der am meisten besuchten Museen Berlins. Es wird seit etwa 20 Jahren im Rahmen des 1999 von der Stiftung Preußischer Kulturbesitz beschlossenen Masterplans Museumsinsel schrittweise grundhaft instandgesetzt und um einen weiteren Flügel ergänzt, der 2025 fertig gestellt sein soll. In diesem Kontext wurde auch kurz nach dem Beschluss des Masterplans eine Bauzustandsanalyse an den in Originalgröße in der Antikensammlung ausgestellten Baudenk¬ mälern durchgeführt. Allerdings stellte man dabei fest, dass herkömmliche Erkundungsverfahren wie die Bauaufnahme, die baugeschichtliche Untersu¬ chung, das Quellenstudium sowie die äußerliche Begutachtung nicht ausreichen, um die innere Struktur der antiken Baudenkmäler hinreichend zu charakterisieren. Deshalb wurde die BAM im Jahr 2003 von der ARGE Pfanner Pergamonmuseum beauftragt, in enger Zusammenarbeit mit zwei Ingenieurbüros, dem Ingenieurbüro Patitz (IGP) und der Gesellschaft für geophysikalische Unter¬ suchungen mbH (GGU) unter Hinzuziehung einer Restauratorin, die innere Struktur ausgewählter an¬ tiker Baudenkmäler zerstörungsfrei zu untersuchen. Das Ziel der zerstörungsfreien Strukturaufklärung zum inneren Aufbau der Bauteile war es, einerseits sicherheitsrelevante Informationen für die statische Nachweisführung bereitzustellen, sowie andererseits eine Planungsgrundlage für die eventuell erforder¬ liche Ertüchtigung der Baudenkmäler zu schaffen. Im Fokus der Untersuchungen standen dabei das Markttor von Milet und das Säulenjoch der Heiligen Halle am Markt von Priene1 • Im nachstehenden Beitrag werden exemplarisch die am Markttor von Milet durchgeführten Untersuchungen vorgestellt. T2 - Workshop Kulturguterhaltung - Vom Dampfkessel zu Nanomaterialien CY - Berlin, Germany DA - 17.11.2021 KW - Bauzustandsanalyse KW - Radar KW - Radiografie PY - 2021 SN - 2567-1251 VL - 3 SP - 47 EP - 57 PB - Druckerei G. Bohm CY - Berlin AN - OPUS4-54460 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Weise, Frank A1 - Fladt, Matthias A1 - Wieland, M. T1 - Internal water-repellent treatment - a novel strategy for mitigating alkali-aggregate reaction in concrete pavements N2 - To prevent future alkali-aggregate reaction (AAR) damage, which has occurred frequently in the Germanhighway network in recent years, a new regulation has been drafted. This regulation severely limits the use of alkali-sensitive aggregates by requiring that their suitability be verified by certified inspectors using newly developed AAR concrete tests that involve the external supply of alkali. This has led to a significant limitation in the number of aggregates usable for concrete pavements. A novel AAR avoidance strategy is now being pursued, which aims to enable the use of borderline alkali-sensitive aggregates through the application of an internal water-repellent treatment. The addition of water repellents during concrete production should significantly reduce the ingress of water and external de-icing salts into the concrete pavement, thus reducing the potential for AAR damage. This paper presents the results of laboratory tests to assess the suitability of this new AAR prevention strategy. Representative, highly AAR-susceptible road paving concrete made with an alkali- sensitive greywacke and various water repellents were used as the basis for these experiments. The tests for concrete suitability included determining the conventional fresh and hardened concrete properties as well as concrete prism tests with external alkaline supply. Building on these results, laser-induced breakdown spectroscopy (LIBS) analyses of de-icing-salt intrusion as well as microscopic examinations for verification of the AAR characteristics were carried out. The results of the AAR concrete tests with external alkaline supply support the conclusion that, when hydrophobic agents containing a suitable active ingredient are used, the AAR damage process in road paving concrete can be sufficiently prevented. T2 - 16th International Conference on Alkali-Aggregate Reaction in Concrete CY - Lisboa, Portugal DA - 31.05.2022 KW - Concrete pavements KW - Internal water-repellent treatment KW - Preventive measures KW - Testing for potential AAR PY - 2021 SN - 978-972-49-2315-4 VL - 1 SP - 511 EP - 524 AN - OPUS4-54551 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kositz, M. A1 - Hünger, K.-J. A1 - Weise, Frank T1 - Regression analysis of ASR expansions and silica dissolution in the presence of NaCl N2 - The durability of concrete structures due to alkali-silica-reaction (ASR) is usually been assessed by ASR concrete prism tests (CPT). Therefore, the expansion of concrete specimens indicates an alkalisensitivity. In Germany these tests are performed at 40°C or accelerated 60°C. Nevertheless, ASR prism tests are expensive, power and time-consuming. For these reasons, an alternative chemical test (“mod. BTU-test”) was developed in the past. The “mod. BTU-test” was correlated with German standard CPT. In this test, the solubility of silica and alumina in the liquid phase is measured by ICP-OES. For special requirements in concrete road construction, stricter test procedures are necessary. The specimens are repeatedly subjected to cyclic alternating storage in NaCl. On the one hand, the presence of NaCl increases the ASR expansion, on the other hand NaCl also changes the dissolution behaviour of silica and alumina. For now is not possible to correlate the solubilities of “mod. BTU-test” and ASR expansions influenced by NaCl. Therefore, four aggregates with different ASR sensitivities were chosen and ASR concrete prism tests (in addition with NaCl) have been performed. According to the “mod. BTU-test” the solubilities of silica and alumina in presence of different NaCl concentrations were measured. This paper is about the regression analysis of silica and alumina dissolution and ASR expansion tests in presence of NaCl. The regression analysis shows the influence of a quasi-continuous and an interrupted cyclic alternating storage. Additionally the effects of temperature and NaCl concentration are investigated. In the end, a suitable NaCl concentration of the “mod. BTU-test” for dissolution experiments is recommended. The “mod. BTU-Test” with NaCl might be a serious and reliable test method for ASR classification for concrete road construction. T2 - 16th International Conference on Alkali-Aggregate Reaction in Concrete CY - Lisboa, Portugal DA - 31.05.2022 KW - Alkali silica reaction KW - Alkaline solution KW - Alumina & silica dissolution KW - NaCl KW - Regression analysis PY - 2021 SN - 978-972-49-2315-4 VL - 1 SP - 711 EP - 723 AN - OPUS4-54552 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Krütt, Enno A1 - Pirskawetz, Stephan A1 - Wallau, Wilma A1 - Meng, Birgit T1 - Development of an automated 60 °C Concrete Prism Test N2 - ln most of the ASR-test procedures, the expansion of concrete or mortar specimens is used as an indicator to assess the ASR-potential of an aggregate or a specific concrete mix. For these tests, the specimens are stored in an ASR-provoking environment, where the reaction is accelerated by elevated temperature and humidity. To measure the length change, the storage must be interrupted for at least a few minutes. Düring the 60 °C Concrete Prism Test (60 °C-CPT), the specimens are cooled down to 20 °C for 24 hours, to ensure the same hygrothermal conditions for every measurement. This limits the number of measurements during the test period and may lead to additional effects, that probably influence the expansion development. With a recently developed device, it is possible to continuously monitor the expansion ofprisms without interrupting the ASR-provoking storage. Due to the dense database of this automated test, the results can contribute to a better understanding of the ASR-process. This study compares results of the automated and conventional 60 °C-CPT. Tests of different aggregates showed, that the results of the automated and conventional test are consistent, but the expansions during the conventional test are generally higher. Preliminary results led to the conclusion, that the cooling for the measurements leads to additional expansions. Therefore, a modified threshold should be discussed for the automated 60 °C-CPT. T2 - 16th International Conference on Alkali-Aggregate Reaction in Concrete CY - Lisboa, Portugal DA - 31.05.2022 KW - 60 °C-CPT KW - ASR expansion monitoring KW - Automated testing PY - 2021 SN - 978-972-49-2315-4 VL - 1 SP - 789 EP - 799 AN - OPUS4-54553 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rütters, H. A1 - Fischer, S. A1 - Le, Quynh A1 - Bettge, Dirk A1 - Bäßler, Ralph A1 - Maßmann, J. A1 - Ostertag-Henning, C. A1 - Wolf, J. Lennard A1 - Pumpa, M. A1 - Lubenau, U. A1 - Knauer, S. A1 - Jaeger, P. A1 - Neumann, A. A1 - Svensson, K. A1 - Lempp, C. A1 - Menezes, F. A1 - Hagemann, B. T1 - Towards defining reasonable minimum composition thresholds – impacts of variable CO2 stream compositions on transport, injection and storage N2 - The collaborative project “Impacts of impurities in CO2 streams captured from different emitters in a regional cluster on transport, injection and storage (CLUSTER)” aimed to set up recommendations on how to define “reasonable minimum composition thresholds” that CO2 streams should meet when accessing CO2 transport pipeline networks. Within CLUSTER, we investigated potential impacts of CO2 streams with different and temporally variable compositions and mass flow rates along the whole CCS chain. Investigations included, amongst others, impacts on: Corrosion of pipeline steel, pipeline network design and related transport costs, alteration of well bore cements, pressure development and rock integrity, geochemical reactions, and petrophysical and geomechanical rock properties. All investigations are based on a generic CCS chain scenario. In this scenario, CO2 streams are captured from a spatial cluster of eleven emitters and collected in a regional pipeline network. Emitters comprise seven fossil fuel-fired power plants equipped with different capture technologies, two cement plants, one refinery and one integrated iron and steel plant. In total, 19.78 Mio t CO2 (including impurities) are captured in the emitter cluster annually. The combined CO2 stream is transported in a trunk line with a length of 400 km (100 km of these offshore) and is injected into five generic storage structures. The storage reservoirs are saline aquifers of the Buntsandstein. The investigations revealed beneficial and deteriorating impacts of different impurities and combinations thereof. Overall, no fundamental technical obstacles for transporting, injecting and storing CO2 streams of the modelled variable compositions and mass flow rates were observed. Based on the results, the CLUSTER project team recommends not to define “minimum composition thresholds” for CO2 streams as strict threshold values for each individual impurity in the stream. Instead, CO2 stream compositions and variabilities for specific CCS projects should be constrained with regard to a set of parameters including i) the overall CO2 content, ii) maximum contents of relevant impurities or elements, iii) acceptable variability of CO2 stream composition, and iv) impurity combinations to be avoided. T2 - 15th International Conference on Greenhouse Gas Control Technologies, GHGT-15 CY - Online meeting DA - 15.03.2021 KW - Corrosion KW - Impurities KW - CO2 quality KW - Pipeline network KW - Whole-chain CCS scenario KW - Recommendations PY - 2021 DO - https://doi.org/10.2139/ssrn.3816427 SP - 1 EP - 18 AN - OPUS4-52418 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rütters, H. A1 - Fischer, S. A1 - Le, Quynh Hoa A1 - Bettge, Dirk A1 - Bäßler, Ralph A1 - Maßmann, J. A1 - Ostertag-Henning, C. A1 - Lennard Wolf, J. A1 - Pumpa, M. A1 - Lubenau, U. A1 - Knauer, S. A1 - Jaeger, P. A1 - Neumann, A. A1 - Svensson, K. A1 - Pöllmann, H. A1 - Lempp, C. A1 - Menezes, F. A1 - Hagemann, B. T1 - Towards Defining Reasonable Minimum Composition Thresholds – Impacts of Variable CO2 Stream Compositions on Transport, Injection and Storage N2 - The collaborative project “Impacts of impurities in CO2 streams captured from different emitters in a regional cluster on transport, injection and storage (CLUSTER)” aimed to set up recommendations on how to define “reasonable minimum composition thresholds” that CO2 streams should meet when accessing CO2 transport pipeline networks. Within CLUSTER, we investigated potential impacts of CO2 streams with different and temporally variable compositions and mass flow rates along the whole CCS chain. Investigations included, amongst others, impacts on: • corrosion of pipeline steel, • pipeline network design and related transport costs, • alteration of well bore cements, • pressure development and rock integrity, • geochemical reactions, and • petrophysical and geomechanical rock properties. All investigations are based on a generic CCS chain scenario. In this scenario, CO2 streams are captured from a spatial cluster of eleven emitters and collected in a regional pipeline network. Emitters comprise seven fossil fuel-fired power plants equipped with different capture technologies, two cement plants, one refinery and one integrated iron and steel plant. In total, 19.78 Mio t CO2 (including impurities) are captured in the emitter cluster annually. The combined CO2 stream is transported in a trunk line with a length of 400 km (100 km of these offshore) and is injected into five generic storage structures. The storage reservoirs are saline aquifers of the Buntsandstein. The investigations revealed beneficial and deteriorating impacts of different impurities and combinations thereof. Overall, no fundamental technical obstacles for transporting, injecting and storing CO2 streams of the modelled variable compositions and mass flow rates were observed. Based on the results, the CLUSTER project team recommends not to define “minimum composition thresholds” for CO2 streams as strict threshold values for each individual impurity in the stream. Instead, CO2 stream compositions and variabilities for specific CCS projects should be constrained with regard to a set of parameters including i) the overall CO2 content, ii) maximum contents of relevant impurities or elements, iii) acceptable variability of CO2 stream composition, and iv) impurity combinations to be avoided. T2 - The 15th Greenhouse Gas Control Technologies Conference CY - Online meeting DA - 15.03.2021 KW - Corrosion KW - Impurities KW - CO2 quality KW - Pipeline network KW - Whole-chain CCS scenario KW - Recommendations PY - 2021 DO - https://doi.org/10.2139/ssrn.3816427 SP - 1 EP - 18 PB - Elservier AN - OPUS4-52940 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Pötzsch, Sina A1 - Weltschev, Margit A1 - Bäßler, Ralph T1 - Compatibility of polymers exposed to heating oil blends with 10 % and 20 % biodiesel (FAME) N2 - Biodiesel (FAME) from rapeseed is an environmentally friendly alternative to common fossil fuels. It is also suitable to serve as blending component to fuels like heating oil. If the fuel composition is changed, materials compatibility must be guaranteed. Adding polar biodiesel to nonpolar heating oil, changes the blend’s solvency and might cause swelling, extraction and solvation of polymers. The objective of this research was to investigate the compatibility of polymeric materials, which are commonly used for components in middle distillate facilities, along with blends of heating oil and 20 % biodiesel (B20). For this propose, ACM, HNBR, FKM, PE, PA 6, POM, PUR and PVC were exposed to heating oil and B20 for 42 and 84 days at 40 °C. In addition, the polymers HNBR, FKM, PA, POM and PVC were also exposed at 70 °C. Furthermore, the resistance of polymers in eight-year aged B10 at 40 °C was evaluated. Ageing of biodiesel increases acidity which might propagate polymer corrosion. The materials were evaluated as resistant, if the loss in tensile properties (tensile strength and elongation at break) and Shore hardness remained under 15 % compared to the initial unexposed material values. For investigations under compressed conditions, the compression set was determined for specimens of ACM, FKM and HNBR after exposure in heating oil B0 and B20 for 3,7,14, 28, 56 and 90 days at 40 °C according to ISO 815-1. It was found that the resistance in B20 at 40 °C was given for all tested polymers except PUR. In the 8 years aged B10, PUR and POM were not compatible and ACM just conditionally compatible. At 70 °C, FKM and PVC were resistant in B20, whereas HNBR and PA 6 were not compatible. Swelling occurred for the elastomers ACM, HNBR and PUR. T2 - AMPP Annual International Corrosion Conference 2021 CY - Online Meeting DA - 19.04.2021 KW - Biodiesel KW - FAME KW - RME KW - Polymer in fuels PY - 2021 SP - 16222-01 EP - 16222-12 CY - Houston AN - OPUS4-52499 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Aristia, Gabriela A1 - Nofz, Marianne A1 - Bäßler, Ralph A1 - Sojref, Regine A1 - Le, Quynh Hoa T1 - Preliminary Study on Al2O3 Sol-Gel Coating for Corrosion Protection of Martensitic Stainless Steel in Artificial Geothermal Water N2 - Al2O3 coatings are often used as protective layers on steels against electrochemical and high-temperature corrosion because they are chemically inert and stable at elevated temperatures. This study presents preliminary work on the possibilities of using Al2O3 sol-gel coatings for corrosion protection of martensitic stainless steels in geothermal environments. Al2O3 sol-gel coatings were applied on UNS S42000, which is known to be susceptible to uniform and localized corrosion. The coated steel specimens were then tested in two types of artificial geothermal water, which simulate the geothermal fluids found in Sibayak (SBY), Indonesia, and North German Basin (NGB), Germany, respectively. SBY has pH 4 and 1.5 g/L of chloride ions, whereas NGB has a pH of 6 and 166 g/L of chloride ions. All experiments were carried out in autoclaves at 150 °C and 1 MPa under the deaerated condition. Evaluations were performed by investigating the surface profiles of both uncoated and coated steels before and after the corrosion test using a Laser Scanning Microscope (LSM) and Scanning Electron Microscope (SEM). Finally, Electrochemical Impedance Spectroscopy (EIS) was performed to compare the corrosion resistance of Al2O3 coated steels in SBY and NGB solutions. It was observed from the corrosion test that Al2O3 coatings are more suitable for use in the geothermal water with a higher pH. T2 - AMPP Annual International Corrosion Conference 2021 CY - Online Meeting DA - 19.04.2021 KW - Protective coating KW - Sol-gel coating KW - Geothermal KW - Martensitic steel KW - Corrosion PY - 2021 SP - 16777-01 EP - 16777-12 CY - Houston AN - OPUS4-52501 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bäßler, Ralph A1 - Stoljarova, A. A1 - Regenspurg, S. T1 - Influence of Precipitating Brine Components on Materials Selection for Geothermal Applications N2 - Since geothermal wells are a feasible energy source to replace fossil fuel supply, many technologies have been developed to take advantage of geothermal energy. Nevertheless, service conditions in geothermal facilities are in many cases extreme in terms of corrosion due to the chemical composition of hydrothermal fluids and temperatures. Therefore, materials selection based on preliminary material qualification is essential to guarantee a secure and reliable operation of the facilities. During operation of a geothermal research facility in Groß Schönebeck copper and lead effects have been found downhole. Occurring mechanisms and measures to prevent precipitation or scaling needed to be investigated as well as potential influences of such precipitates on corrosion resistance of metallic materials used for equipment. This contribution deals with the evaluation of the corrosion behavior of carbon steel and corrosion resistant alloys in copper and/or lead containing artificial geothermal water, simulating the conditions in the Northern German Basin. The behavior of these materials in an artificial geothermal water obtained by electrochemical measurements and exposure tests are presented. While carbon steel exhibits precipitation and deposition, higher alloyed material shows different response to such species and a higher resistance in saline geothermal water. Basing on these results the suitability of the investigated corrosion resistant alloy is given for use in such conditions, whereas carbon steel creates difficulties due to its susceptibility to Cu- and Pb-precipitation. T2 - World Geothermal Congress CY - Online meeting DA - 30.03.2021 KW - Copper KW - Lead KW - Corrosion KW - Steel KW - Geothermal energy PY - 2021 SP - 1 EP - 11 AN - OPUS4-52828 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Pirskawetz, Stephan A1 - Weise, Frank A1 - Rieffel, Y. A1 - Gorbushina, Anna T1 - Die Schlossbrücke Berlin - Schutz der Göttinnen N2 - Vielleicht nannten es die Berliner „Puppen putzen“, wenn in den 1880er Jahren die Marmorstatuen auf der Schlossbrücke vor dem Berliner Stadtschloss mit Bürste, Wasser und Seife von Staub, Ruß und Taubendreck befreit wurden. Soviel Pflege wurde diesen Göttinnen aus der griechischen Mythologie nicht immer zuteil. So haben Klima, Luftverschmutzung und der 2. Weltkrieg, wie bei anderen Kunstwerken auch, tiefe Spuren hinterlassen. Der Erhalt dieser zwischen 1847 und 1857 aufgestellten Skulpturen und vieler vergleichbarer Objekte im Stadtbild ist durch die auch heute weiter fortschreitende Schädigung des Marmors gefährdet. In den Jahren 2006 bis 2010 förderte die Deutsche Bundesstiftung Umwelt (DBU) ein Projekt zur „Entwicklung und Überprüfung von Einhausungssystemen zur Reduzierung umweltbedingter Schädigungen von außenexponierten Marmorobjekten mit dem Ziel des langfristigen Erhalts in situ an einem national bedeutenden Objektkomplex, den Schlossbrückenfiguren unter den Linden, Berlin“. Geleitet und restauratorisch betreut wurde das Projekt durch das Landesdenkmalamt (LDA) Berlin. Durch die Abteilung Strukturgeologie und Geodynamik (GZG) der Georg-August Universität Göttinnen wurden die Verwitterungsmechanismen des Marmors untersucht und auf dieser Basis Anforderungen an das Schutzsystem formuliert. Anhand von numerischen Simulationen des Instituts für Bauklimatik der Technischen Universität Dresden (TUD) wurde das bauphysikalische Konzept des Einhausungssystems optimiert. Die konstruktive Gestaltung eines Prototyps und des finalen Entwurfs erfolgte durch das Fachgebiet Konstruktives Entwerfen und Tragwerkslehre der Universität der Künste Berlin. Durch den Fachbereich Baustoffe der BAM erfolgten die Realisierung des Prototyps der Einhausung sowie ein umfangreiches Klimamonitoring an den Skulpturen. Anhand dieses interdisziplinären Projektes und ergänzt durch weitere Messungen wird gezeigt, mit welchen Methoden die für die Degradation von Marmor relevanten Mechanismen untersucht werden können. Die Erkenntnisse aus dem Projekt sind die Grundlage für die Entwicklung nachhaltiger Pflege- und Schutzkonzepte für die kulturhistorisch wertvollen Skulpturen. Nur mit solchen modernen konservatorischen Programmen können die Originalskulpturen im Berliner Stadtraum erlebbar bleiben. T2 - Workshop Kulturerhaltung - Vom Dampfkessel zu Nanomaterialien CY - Berlin, Germany DA - 17.11.2021 KW - Baustoffe KW - Marmor KW - Verwitterung KW - Kulturelles Erbe KW - Wintereinhausungen KW - Klima KW - Zerstörungsfreie Prüfung KW - Building materials KW - Marble KW - Degradation KW - Cultural heritage KW - Winter shelters KW - Climate KW - Nondestructive testing PY - 2021 SN - 2567-1251 VL - 3 SP - 87 EP - 96 PB - Druckerei G. Bohm CY - Berlin AN - OPUS4-54637 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Aristia, Gabriela A1 - Le, Quynh Hoa A1 - Bäßler, Ralph T1 - Study of Polyaniline/Silicon Dioxide based Coating on Carbon Steel in Artificial Geothermal Brine N2 - Geothermal brines are corrosive in nature because of their salt contents and high temperatures. Therefore, they pose a major challenge to geothermal power-plants, which are mostly built of low alloyed steels, e.g., carbon steel. Carbon steel is susceptible to uniform and localized corrosion when exposed to geothermal brines having acidic-saline properties. To overcome this limitation, geothermal power plants should be built by either high alloyed materials or by integrating protection systems on carbon steel, such as coatings and inhibitors. We studied a coating system containing polyaniline/silicon dioxide basing on locally available resources that provides protection against corrosion of carbon steel and enhance the thermal resistance in geothermal environments. Here, exposure and electrochemical tests of coated carbon steels were performed in an artificial geothermal brine. The solution had a pH of 4, with the composition of 1,500 mg/L of chlorides, which is based on the chemical analysis of geothermal brine found in Sibayak, Indonesia. All exposure tests were conducted using autoclaves at 150 °C with a total pressure of 1 MPa, which was performed for up to six months to evaluate the durability of the coating system. Post-experimental analyses were performed by assessing the surface of specimens using optical and electron microscopes. On the other hand, electrochemical tests were performed for seven days at 25 °C and 150 °C to investigate the kinetics of electrochemical reactions by measuring open circuit potential and electrochemical impedance spectra. Experimental results showed the corrosion resistance of PANI/SiO2 composite coatings, where polyaniline and SiO2 play their roles as stabilizers. T2 - World Geothermal Congress CY - Online meeting DA - 30.03.2021 KW - Coatings KW - Corrosion KW - Polyaniline KW - Sibayak KW - SiO2 PY - 2021 SP - 1 EP - 7 AN - OPUS4-52830 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Henning, Ricky A1 - Sturm, Patrick A1 - Kühne, Hans-Carsten A1 - Keßler, S. A1 - Gluth, Gregor T1 - Untersuchungen zur Wärmeentwicklung von hybriden Zementen N2 - Die Hauptfunktion von Verschlussbauwerken für End- und Zwischenlager von radioaktiven Abfällen besteht in der Erhaltung der geologischen Barriere. Vor allem soll ein potenzieller Stofftransport durch eine möglichst geringe Permeabilität des Bauwerks verhindert bzw. auf vernachlässigbare Werte herabgesetzt werden. Die in-situ-Permeabilität des Verschlussbauwerks steht dabei in direktem Zusammenhang mit dessen Poren- und Makrostruktur, welche bei Bauwerken auf Basis von Beton insbesondere durch Schwind-verformungen und durch thermisch induzierte Rissbildung infolge der Reaktionswärmeentwicklung des Bindemittels gestört werden kann. Die Betone müssen daher neben einer hohen chemischen Langzeitstabilität auch eine geringe bzw. langsame Wärmeentwicklung während der Erhärtungsreaktionen aufweisen. Als hybride Zemente werden Mischungen aus Portlandzement, Betonzusatzstoffen und einem alkalischen Aktivator bezeichnet. Dabei können u. a. Alkalisulfate, Alkalicarbonate, Alkalisilicate und Alkalihydroxide als Aktivatoren zum Einsatz kommen. Aufgrund ihrer hohen chemischen Stabilität im salinaren Milieu sind Betone aus solchen Zementen potenziell besonders gut als Verfüllmaterial für End- und Zwischenlager im Steinsalz geeignet. In der vorliegenden Studie wurden daher hybride Zemente hinsichtlich ihrer Wärmeentwicklung in einem isothermen Kalorimeter sowie hinsichtlich Phasenbestand und Festigkeiten untersucht. Hybride Zementleime wurden auf Basis von Portlandklinker, Hüttensandmehl, Flugasche und Natriumsulfat hergestellt und die Zusammensetzungen systematisch variiert, um den Einfluss der Komponenten auf Wärmeentwicklung, Phasenbestand und mechanische Eigenschaften der Leime zu untersuchen; zusätzlich wurden zu Vergleichszwecken ein Zementleim auf Basis der Betonrezeptur M2 sowie eine alkalisch aktivierte Flugasche untersucht. T2 - 2. Tage der Standortauswahl CY - Online meeting DA - 11.02.2021 KW - Hybride Zemente KW - Hydratationswärme KW - Kalorimetrie PY - 2021 SP - 137 EP - 139 AN - OPUS4-52216 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wachtendorf, Volker A1 - Schartel, Bernhard A1 - Lin, Xuebao A1 - Tan, Yi A1 - Schoch, R. A1 - Lang, M. A1 - Tröppner, O. A1 - Bosse, M. ED - Ziegahn, K.-F. T1 - Untersuchung der Witterungsbeständigkeit komplexer Funktionalitäten von Polymerwerkstoffen durch künstliche Bewitterung: Flammschutz N2 - In den letzten Jahrzehnten wurde die Degradation der polymeren Matrix von flammgeschützten Polymeren eingehend untersucht. Erst in den letzten Jahren jedoch hat sich die Frage der Lebensdauer der Funktionalität des Flammschutzes selbst als wichtige Fragestellung herauskristallisiert, z.B. bei Kabeln. Deshalb sollte diese Fragestellung durch systematisch-variierte künstliche Klima- und Bewitterungstests an flammgeschützten Polymerwerkstoffen untersucht werden. T2 - 50. Jahrestagung der Gesellschaft für Umweltsimulation (GUS) CY - Online meeting DA - 23.03.2022 KW - Flammschutz, Witterungsbeständigkeit, Langzeitbeständigkeit, UV, E&E PY - 2022 SN - 978-3-9818507-7-2 VL - 50 SP - 143 EP - 148 CY - Pfinztal (Berghausen) AN - OPUS4-54543 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Voigt, Marieke A1 - Gardei, Andre A1 - Meng, Birgit ED - di Prisco, M. ED - Meda, A. ED - Balazs, G.L. T1 - The adaption of the set-up for gas permeability measurements for ultra-high performance concrete N2 - In the framework of this project, a steam pressure vessel was to be developed from ultra-high perfor-mance concrete (UHPC) to withstand process temperatures of 200 °C and the respective steam pressure of 15,5 bar. To guarantee the long-term water vapour tightness of the system, the permeability of two UHPC mixtures were tested after long-term cyclic autoclaving. As UPHC shows a high density and therefore low permeability, measurements after the RILEM-Recommendation (TC 116-PCD) reached their detection limit. Therefore, the measurement set-up was adapted to measure the permeability of highly dense UHPC more reliably and quickly. This adaption includes measurements in a higher pres-sure range, the change of sample size thickness and the usage of Ar as a medium compared with the RILEM Recommendation. Additionally, the system was equipped with two pressure sensors and Ar-flowmeters to guarantee a continuous record of the experimental parameters. The new system was tested and evaluated by comparing measurements with the RILEM recommended system. Preliminary results show that the adapted system is capable to provide efficient and reliable results of concrete with low permeability. T2 - 14th fib PhD Symposium in Civil Engineering CY - Rom, Italy DA - 05.09.2022 KW - Durability KW - UHPC KW - gas permeability PY - 2022 SN - 978-2-940643-17-2 SN - 2617-4820 VL - 58 SP - 353 EP - 359 AN - OPUS4-56862 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Aristia, Gabriela A1 - Bäßler, Ralph T1 - A Coating System for Corrosion Protection of Carbon Steel as an Alternative for High Alloyed Materials N2 - Corrosive geothermal brines are a major challenge to geothermal power-plants. For cost reasons, plant designers favorize low alloyed steels, e.g., carbon steel, which are susceptible to uniform and localized corrosion when exposed to geothermal brines having acidic and saline properties. To solve such problem, coatings or inhibitors would be a protective solution as an alternative to the use of high alloyed materials. This study investigated a coating system consisting of polyaniline/silicon dioxide basing on locally available resources. Protection against corrosion of carbon steel is shown by long-term exposure and electrochemical tests of coated carbon steels, performed in an artificial acidic and saline geothermal brine, comparable to real conditions at a site in Indonesia. Therefore, an integrated coating system is presented for corrosion protection, combining the electro-chemical functionality of polyaniline and the physical advantages of silica. T2 - European Geothermal Congress CY - Berlin, Germany DA - 17.10.22 KW - Corrosion KW - Geothermal KW - Coatings KW - Polyaniniline KW - Silicate PY - 2022 SP - 1 EP - 7 CY - Berlin AN - OPUS4-56085 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Le, Quynh Hoa A1 - Bäßler, Ralph A1 - Bettge, Dirk T1 - Electrochemical behaviors of casing steel/mortar interface in CO2 saturated aquifer fluid N2 - To reveal the corrosion resistance of casing steel/mortar interface in CO2 injection condition, sandwich samples were prepared and exposed up to 20 weeks in aquifer fluid under 10 MPa and 60 °C. Cross section analysis revealed the crevice corrosion as main mechanism instead of pitting corrosion, which would be expected to happen in the extremely high Chloride concentration. Detailed analysis using EDS line scan shown the slow diffusion of Chloride, suggesting why pitting did not happen after 20 weeks. To mimic the passivated steel surface, the steel coupon was passivated in simulated pore solution having pH 13.5 for 42 days. The passivated coupon was further exposed to NGB solution for 28 days. Electrochemical characterization was performed along the exposure processes to reveal the change in impedance, indicating the corrosion resistance of steel casing/mortar interface. T2 - EUROCORR 2022 CY - Berlin, Germany DA - 28.08.2022 KW - Corrosion KW - CO2 quality KW - Pipeline network KW - CCS PY - 2022 SP - 859 EP - 865 PB - European Federation of Corrosion AN - OPUS4-55622 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zhang, K. A1 - Mezhov, Alexander A1 - Schmidt, Wolfram T1 - Thixotropic and chemical structural build-up of cement pastes with superplasticizer under different storage conditions N2 - Synopsis: The paper presents the results of a study on the influence of agitation on the structural build-up of fresh cement pastes using a penetration test. It first presents results about the influence of the penetrating shape’s geometry on the influence on the cement paste specimen. Then, results are shown for the load-deflection curves depending upon time and agitation before testing. Based on the observation of the force required to penetrate the sample, conclusions on the structural build-up can be made. The observations were made over the course of time with samples that were left at rest and partly agitated before testing at different time steps. The setup allows to identify the contribution of the chemical reaction to the structural build-up process. The presence of superplasticizer obviously reduces the load that cement paste can withstand, while the loss of thixotropy is found notably lower than that of neat cement pates T2 - 13th International Conference on Superplasticizers and Other Chemical Admixtures in Concrete CY - Milan, Italy DA - 10.07.2022 KW - Thixotropy KW - Superplasticizer KW - Structural build-up KW - Texture analyzer KW - Penetration test PY - 2022 DO - https://doi.org/10.14359/51736058 VL - 354 SP - 13 EP - 24 PB - ACI Special Publications AN - OPUS4-58324 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mezhov, Alexander A1 - Schmidt, Wolfram A1 - Zhang, H. A1 - Diesendruck, Ch. E. T1 - The effect of the charge density of a comb polyphosphate superplasticizer on the structural build-up of cement paste N2 - Synopsis: Lately, there has been rising attention to superplasticizers (SP) based on polyphosphate esters. However, the influence of the molecular structure of the polyphosphate polymers on time-dependent properties such as structural build-up has not been examined yet intensively. To investigate this effect, three comb polyphosphate superplasticizers with different charge densities were synthesised by free radical polymerisation. Our findings indicate that SP with the lowest and medium charge densities extend the induction period more strongly than the SP with the highest charge density. The reduction of the structural build-up rate is linearly dependent on the dosage and concentration of the functional group of polyphosphate SP in the cementitious system. This study proposes a mathematical equation expressing the relationship between the structural build-up rate during the induction period and the molecular structure of the polyphosphate SP. T2 - 13th International Conference on Superplasticizers and Other Chemical Admixtures in Concrete CY - Milan, Italien DA - 10.07.2022 KW - Admixture KW - Superplasticizer KW - Polyphosphate KW - Structural build-up PY - 2022 DO - https://doi.org/10.14359/51736079 VL - 354 SP - 255 EP - 262 PB - ACI Special Publications AN - OPUS4-58321 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mezhov, Alexander A1 - Robens-Radermacher, Annika ED - Mezhov, Alexander ED - Robens-Radermacher, Annika ED - Zhang, Kun ED - Kühne, Hans-Carsten ED - Unger, Jörg F. ED - Schmidt, Wolfram T1 - Temperature Impact on the Structural Build-Up of Cementitious Materials - Experimental and Modelling Study N2 - With increasing focus on industrialized processing, investigating, understanding, and modelling the structural build-up of cementitious materials becomes more important. The structural build-up governs the key property of fresh printable materials -- buildability -- and it influences the mechanical properties after the deposition. The structural build-up rate can be adjusted by optimization of the mixture composition and the use of concrete admixtures. Additionally, it is known, that the environmental conditions, i.e. humidity and temperature have a significant impact on the kinetic of cement hydration and the resulting hardened properties, such as shrinkage, cracking resistance etc. In this study, small amplitude oscillatory shear (SAOS) tests are applied to examine the structural build-up rate of cement paste subject to different temperatures under controlled humidity. The results indicate significant influences of the ambient temperature on the intensity of the re-flocculation (Rthix) rate, while the structuration rate (Athix) is almost not affected. A bi-linear thixotropy model extended by temperature dependent parameters coupled with a linear viscoelastic material model is proposed to simulate the mechanical behaviour considering the structural build-up during the SAOS test T2 - Third RILEM International Conference on Concrete and Digital Fabrication (Digital Concrete 2022) CY - Loughborough, UK DA - 27.06.2022 KW - Structural build-up KW - Rheological properties KW - Modelling PY - 2022 SN - 978-3-031-06116-5 DO - https://doi.org/10.1007/978-3-031-06116-5_49 VL - 37 SP - 330 EP - 336 PB - Springer International Publishing CY - Cham AN - OPUS4-55580 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Erning, Johann Wilhelm T1 - “Grabenkorrosion": How scientific debate leads to an solution. and modern failures due to neglection of well described facts N2 - In the late 1980s, a new type of corrosion appeared in drinking water installations where galvanized steel pipes failed forming a deep groove with no corrosion at the other surfaces. The reason was discussed quite fiercely between failure analysts and material suppliers. In the end the discussion lead to the solution: inductive welded pipes of a certain sulphur content were prone to selective corrosion. The history of the arguments is discussed using old communications between Wilhelm Schwenk and Wolfgang Stichel, who later published the results in a paper unfortunately only I german. Thus the knowledge got lost and new cases based on the same material problems are observed in application of so-called C-Steel piping systems. Failure cases are shown. T2 - MTech 2023 CY - Cavtat, Croatia DA - 02.10.2023 KW - Corrosion KW - Grabenkorrosion PY - 2023 SN - 2806-8769 SP - 1 EP - 6 PB - Croatian Society for Heat Treatment and Sufrace Engineering CY - Zagreb AN - OPUS4-58521 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hirsch, T. A1 - Voigt, Marieke A1 - Lehmann, Christian A1 - Meng, Birgit A1 - Lothenbach, B. T1 - Impact of autoclaving on the phase assemblage of Portland cement: Experiment and thermodynamic modelling N2 - Even after autoclaving for 2 weeks in the temperature range of 120 to 200 °C, CEM I paste with a water-to-cement ratio of 0.5 still contains some low-crystalline C-S-H. The conversion of low-crystalline C-S-H to crystalline is faster with increasing temperature. The observed low-crystalline and crystalline C-S-H phases (reinhardbraunsite, jaffeite) indicate that the sampleshave not reached equilibrium yet under these experimental conditions. However, there is a good agreement between experiment and thermodynamic modelling for the other solids indicating that the used datasets are suitable for this application. T2 - 16th International Congress on the Chemistry of cement 2023 - ICCC2023 CY - Bangkok, Thailand DA - 18.09.2023 KW - Zement KW - Thermodynamik KW - Phasenzusammensetzung KW - Mineralogie KW - Modellierung PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-589779 UR - https://iccc2023.org VL - 1 SP - 619 EP - 621 AN - OPUS4-58977 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Manninger, T. A1 - von Werder, Julia A1 - Rübner, Katrin T1 - Lehmstabilisierung mittels eines Biomasseasche basierten Alkali-Aktivators und kalziniertem Ton N2 - Lehm sowie Lehmziegel sind jahrtausendealte Baustoffe, die sich durch lokale Verfügbarkeit, Umweltverträglichkeit und geringe COa-Belastung auszeichnen. Diese Eigenschaften machen sie zu Baustoffen der Zukunft. Wasserbeständigkeit ist ein wichtiger Aspekt, der beim Einsatz beachtet werden muss. Es gibt verschiedene Ansätze zur Stabilisierung, Idealerwelse sollen dabei die positiven Aspekte des Lehms, wie beispielsweise die Luftfeuchteregullerung, bewahrt werden. Zement ist hierfür nur bedingt geeignet. Als Alternative zur Stabilisierung mit Zement wurden in einer Versuchsreihe Mischungen mit calclnierten Tonen untersucht. Diese bei 600 °C auf CO2 sparende Welse erzeugten, lokal verfügbaren Rohstoffe, können mittels Alkall-Aktivierung zu einem festen „Geopolymer" vernetzt werden. Zur Aktivierung wurde eine lokal verfügbare Biomasseasche aus Hackschnitzelholz, sowie Industriell hergestelltes KOH genutzt, da das in beiden enthaltene Kalium das umweltverträglichste Alkallion Ist. In einer Versuchsreihe wurde das Verhalten des reinen Lehms mit dem stabilisierten Material verglichen. Es wurden Festigkeitswerte, Wasserlagerungsbeständigkeit und Wasserdampfdiffusionswiderstand geprüft. T2 - Internationale Baustofftagung (ibausil) CY - Weimar, Germany DA - 13.09.2023 KW - Lehmstabilisierung KW - Alkali aktivierte Bindemittel KW - Wasserbeständigkeit KW - Putz KW - Erdbau KW - Kalzinierter Ton PY - 2023 UR - https://www.uni-weimar.de/de/bauingenieurwesen/institute/fib/ibausil/ VL - 2023 SP - 1 EP - 6 PB - Sonderausgabe des Online-Journals ce/papers von Wiley AN - OPUS4-58316 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Geburtig, Anja A1 - Wachtendorf, Volker A1 - Trubiroha, P. A1 - Giehl, A. A1 - Schönlein, A. A1 - Feil, F. T1 - Normenvorschlag zur Bewitterung transparenter oder transluzenter Kunststoffe N2 - Aufgrund des tieferen Eindringens der solaren Strahlung treten bei transparenten und bei transluzenten (durchscheinenden) Kunststoffen veränderte Bedingungen gegenüber opaken Proben auf. Dies kann zu speziellen Effekten und damit zu einem abweichenden Bewitterungsverhalten führen. Auch aus Mangel an geeigneten Normen werden diese Effekte häufig vernachlässigt. Deshalb initiiert der DIN-FNK auf ISO-Ebene ein entsprechendes Dokument. Die Norm ist in der Form eines Technical Reports geplant. In einem ersten Teil sollen die Besonderheiten transparenter oder transluzenter Kunststoffe erläutert werden, um den Nutzer für mögliche Probleme zu sensibilisieren. Im zweiten Teil werden Empfehlungen für Bestrahlung oder Bewitterung herausgearbeitet. In einem dritten Teil geht es dann um Besonderheiten bei der Messung von Eigenschaftsänderungen transparenter bzw. transluzenter Kunststoffe. In informativen Anhängen sollen verschiedene Beispiele die Thematik illustrieren. T2 - 51. Jahrestagung der GUS CY - Stutensee-Blankenloch, Germany DA - 29.03.2023 KW - Bewitterung KW - Polymer 3R KW - Bestrahlung KW - UV PY - 2023 SN - 978-3-9818507-8-9 SP - 39 EP - 46 PB - Gesellschaft für Umweltsimulation e.V. CY - Pfinztal (Berghausen) AN - OPUS4-57271 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Meng, Birgit A1 - Dehn, F. A1 - Unger, Jörg F. A1 - Shepherd, D. A. A1 - Tamsen, Erik A1 - Pirskawetz, Stephan T1 - Wissensbasierte Digitalisierung von betontechnologischen Materialdaten N2 - Die sprunghaft zunehmende Wichtigkeit von FAIR- und Open-Data für die Qualitätssicherung, aber auch für die Nachnutzbarkeit von Daten und den Erkenntnisfortschritt führt zu enormem Flandlungsbedarf in Forschung und Entwicklung. Damit verbunden laufen derzeit vielfältige, ambitionierte Aktionen, z. B. bezüglich der Erstellung von Ontologien und Wissensgraphen. Das Knowhow entwickelt sich rasant, die Ansätze zur Implementation entstehen in verschiedenen Fachwelten bzw. mit unterschiedlichen Zielsetzungen parallel, so dass recht heterogene Herangehensweisen resultieren. Diese Veröffentlichung fokussiert auf Arbeiten, die derzeit als möglichst ganzheitlicher Ansatz für Materialdaten im Rahmen der Digitalisierungsinitiative „Plattform MaterialDigital" vorangetrieben werden. Die Autoren bearbeiten baustoffbezogene Aspekte im Verbundprojekt „LeBeDigital - Lebenszyklus von Beton". Zielsetzung ist die digitale Beschreibung des Materialverhaltens von Beton über den kompletten Herstellungsprozess eines Fertigteils mit einer Integration von Daten und Modellen innerhalb eines Workflows zur probabilistischen Material- und Prozessoptimierung. Es wird über die Vorgehensweise und die dabei gewonnenen Erfahrungen berichtet, nicht ohne den Blick auf die oft unterschätzte Komplexität der Thematik zu lenken. T2 - Internationale Baustofftagung (ibausil) CY - Weimar, Germany DA - 13.09.2023 KW - Beton KW - Digitalisierung KW - Materialdaten KW - Datenmanagement KW - FAIR-Prinzip KW - Metadaten KW - Ontologie KW - Wissengraph PY - 2023 UR - https://www.uni-weimar.de/de/bauingenieurwesen/institute/fib/ibausil/ VL - 2023 SP - 1 EP - 11 PB - Sonderausgabe des Online-Journals ce/papers von Wiley AN - OPUS4-58315 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Fladt, Matthias A1 - Weise, Frank T1 - Bewertung der Innenhydrophobierung als neuartige AKR-Vermeidungsstrategie bei Betonfahrbahndecken N2 - Zur Vermeidung von AKR-Schäden an Betonfahrbahndecken im deutschen Autobahnnetz wurden mit dem ARS 04/2013 verbindliche Eignungsprüfungen zum Ausschluss alkaliempfindlicher Gesteinskörnungen bei Neubau- und Erhaltungsmaßnahmen eingeführt. Das hatte eine signifikante Reduzierung geeigneter Gesteinskörnungen zur Folge. Deshalb wird geprüft, ob durch die Zugabe eines Hydrophobierungsmittels während der Betonherstellung grenzwertig alkaliempfindliche Gesteinskörnungen nutzbar gemacht werden können. In diesem Beitrag wird der Einfluss der Dosierung eines Compounds mit Hydrophobierungsmittel (HM) auf die Frisch- und Festbetoneigenschaften eines Waschbetons mit einer reaktiven Grauwacke dargestellt. Es zeigt sich, dass aufgrund des Antagonismus die zunehmende Dosierung des HM-Compounds eine signifikante Erhöhung der Zugabe des Luftporenbildners auf Wurzelharzbasis erfordert. Der AKR-Schädigungsprozess wird ab einer Dosierung des HM-Compounds von 0,75 M.-%, bezogen auf den Zementgehalt, hinreichend vermindert. Die mechanischen Eigenschaften des hydrophobierten Waschbetons verschlechtern sich im betrachteten Dosierungsbereich des HMCompounds nur geringfügig. Auch der Frost-Tausalz-Widerstand vermindert sich, ohne den normativen Grenzwert für die Abwitterung zu überschreiten. T2 - Internationale Baustofftagung (ibausil) CY - Weimar, Germany DA - 13.09.2023 KW - Betonfahrbahndecke KW - Alkali-Kieselsäure-Reaktion KW - Massenhydrophobierung KW - AKRVermeidungsstrategie PY - 2023 UR - https://www.uni-weimar.de/de/bauingenieurwesen/institute/fib/ibausil/ VL - 2023 SP - 1 EP - 10 PB - Sonderausgabe des Online-Journals ce/papers von Wiley AN - OPUS4-58317 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Stohl, Leonie A1 - von Werder, Julia A1 - Manninger, T. T1 - Bioreceptive concrete: Greening facades on the microscale N2 - The accelerating climate crisis results in a rising demand for ecologically driven concepts. Regarding construction, this does not only include environmentally friendly materials but also the establishment of greenery in urban regions. This contribution presents the progress of two projects in which textured concrete slabs were designed to grow a stable biofilm of photosynthetic eukaryotic organisms. The greened panels represent an alternative to classic fa9ade greening with plants. Current literature suggests that the development of bioreceptive surface materials in the construction sector is difficult because there are no standardized methodological approaches for measuring said bioreceptivity. Therefore, the long-term. ahn is proposing a suitable measurement concept combining material Science and biology. Among other things, the intrinsic Substrate property pH value is expected to have a significant influence on biological colonization. In the current contribution the focus lies on the theoretical approach and design of experiment regarding this parameter. Available experimental data will be presented. T2 - 77th RILEM Annual Week and the 1st Interdisciplinary Symposium on Smart & Sustainable Infrastructures (ISSSI 2023) CY - Vancouver, Canada DA - 04.09.2023 KW - Bioreceptivity KW - Concrete KW - Surface pH measurement KW - Material characterization KW - Green Facade PY - 2023 UR - https://www.rilemweek2023.com/submissions/ SP - 1 EP - 6 AN - OPUS4-58304 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Andrés Arcones, Daniel A1 - Weiser, M. A1 - Koutsourelakis, F.-S. A1 - Unger, Jörg F. T1 - Evaluation of Model Bias Identification Approaches Based on Bayesian Inference and Applications to Digital Twins N2 - In recent years, the use of simulation-based digital twins for monitoring and assessment of complex mechanical systems has greatly expanded. Their potential to increase the information obtained from limited data makes them an invaluable tool for a broad range of real-world applications. Nonetheless, there usually exists a discrepancy between the predicted response and the measurements of the system once built. One of the main contributors to this difference in addition to miscalibrated model parameters is the model error. Quantifying this socalled model bias (as well as proper values for the model parameters) is critical for the reliable performance of digital twins. Model bias identification is ultimately an inverse problem where information from measurements is used to update the original model. Bayesian formulations can tackle this task. Including the model bias as a parameter to be inferred enables the use of a Bayesian framework to obtain a probability distribution that represents the uncertainty between the measurements and the model. Simultaneously, this procedure can be combined with a classic parameter updating scheme to account for the trainable parameters in the original model. This study evaluates the effectiveness of different model bias identification approaches based on Bayesian inference methods. This includes more classical approaches such as direct parameter estimation using MCMC in a Bayesian setup, as well as more recent proposals such as stat-FEM or orthogonal Gaussian Processes. Their potential use in digital twins, generalization capabilities, and computational cost is extensively analyzed. T2 - 5th ECCOMAS Thematic Conference on Uncertainty Quantificationin Computational Sciences and Engineering CY - Athen, Greece DA - 12.06.2023 KW - Model bias KW - Bayesian Uncertainty Quantification KW - Digital Twins KW - Gaussian Processes KW - Statistical Finite Element Method PY - 2023 UR - https://2023.uncecomp.org/ SP - 1 EP - 15 AN - OPUS4-58227 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bäßler, Ralph A1 - Stoljarova, A. A1 - Regenspurg, S. T1 - Influence Of Brine Precipitates On Materials Performance In Geothermal Applications N2 - Since geothermal wells are a feasible energy source to replace fossil fuel supply, many technologies have been developed to take advantage of geothermal energy. Nevertheless, service conditions in geothermal facilities are in many cases extreme in terms of corrosion due to the chemical composition of hydrothermal fluids and temperatures. Therefore, materials selection based on preliminary material qualification is essential to guarantee a secure and reliable operation of the facilities. During operation of a geothermal research facility in Groß Schönebeck copper and lead effects have been found downhole. Occurring mechanisms and measures to prevent precipitation or scaling needed to be investigated as well as potential influences of such precipitates on corrosion resistance of metallic materials used for equipment. This contribution deals with the evaluation of the corrosion behavior of carbon steel and corrosion resistant alloys in copper and/or lead containing artificial geothermal water, simulating the conditions in the Northern German Basin. The behavior of these materials in an artificial geothermal water obtained by electrochemical measurements and exposure tests are presented. While carbon steel exhibits precipitation and deposition, higher alloyed material shows different response to such species and a higher resistance in saline geothermal water. Basing on these results the suitability of the investigated corrosion resistant alloy is given for use in such conditions, whereas carbon steel creates difficulties due to its susceptibility to Cu- and Pb-precipitation. T2 - AMPP Annual 2023 Conference CY - Denver, CO, USA DA - 19.03.2023 KW - Geothermal KW - Electrochemistry KW - Copper KW - Lead KW - Corrosion PY - 2023 SP - 1 EP - 15 PB - AMPP CY - Houston TX USA AN - OPUS4-57233 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Robens-Radermacher, Annika A1 - Unger, Jörg F. A1 - Mezhov, Alexander A1 - Schmidt, Wolfram ED - Biondini, F. ED - Frangopo, D. M. T1 - Temperature dependent modelling approach for early age behavior of printable mortars N2 - Structural build-up describes the stability and early-age strength development of fresh mortar used in 3D printing. lt is influenced by several factors, i.e. the composition of the print­ able material, the printing regime, and the ambient conditions. The existing modelling approaches for structural build-up usually define the model parameters for a specific material composition with­ out considering the influence of the ambient conditions. The goal of this contribution is to explicitly include the temperature dependency in the modelling approach. Temperature changes have signifi­ cant impact on the structural build-up process: an increase of the temperature leads to a faster dissol­ ution of cement phases and accelerates hydration. The proposed extended model includes temperature dependency using the Arrhenius theory. The new model parameters are successfully calibrated based on Viskomat measurement data using Bayesian inference. Furthermore, a higher impact of the temperature in the re-flocculation as in the structuration stage is observed. T2 - The Eighth International Symposium on Life-Cycle Civil Engineering (IALCCE 2023) CY - Milano, Italien DA - 02.07.2023 KW - 3D concrete printing KW - Material characterization KW - Structural build-up KW - Thixotropy KW - Model calibration PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-582175 SN - 978-1-003-32302-0 DO - https://doi.org/10.1201/9781003323020-146 SN - 978-1-003-32302-0 VL - 1st Edition SP - 1193 EP - 1200 PB - CRC Press AN - OPUS4-58217 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Munsch, Sarah Mandy A1 - Telong, Melissa A1 - Grobla, Lili A1 - Schumacher, Katrin A1 - Völker, Christoph A1 - Yared, Kaleb A1 - Kruschwitz, Sabine ED - Ferrara, Liberato ED - Muciaccia, Giovanni ED - di Summa, Davide T1 - Study on the Predictability of Carbonation Resistance of Cementitous Materials Based on NMR Features and the Use of SLAMD N2 - This study explores the acceleration of material design in the concrete industry, focusing on improving carbonation resistance, a key factor in the durability of concrete structures. Traditional tests for carbonation resistance are lengthy, but with the construction industry aiming for sustainable production, finding a balance between carbonation resistance and CO2 footprint is crucial. Our research employs two innovative methods: 1. Applying the Sequential Learning App for Materials Discovery (SLAMD), an AI materials design framework, to an extensive dataset of real-world concrete compositions to selectively test materials that meet market demands: maximum durability, optimal eco-durability, and the best cost-durability trade-off. 2. Investigating 1H Nuclear Magnetic Resonance (NMR) relaxometry as a quick alternative for characterizing carbonation behavior, as it saves time compared to traditional tests and assesses the complete material’s pore space. Specific NMR features are then integrated into the material design model, with the model’s performance compared against traditional approaches. The results of our study are compelling, demonstrating that materials can be precisely tailored to meet specific requirements with minimal data points. This marks a significant stride in the concrete industry, indicating thatNMR-based, lowfidelity surrogate characterizations, combined with a focused, data-driven design approach, can substantially accelerate the development of durable, sustainable concrete mixtures. T2 - 4 RILEM Spring Convention and Conference on advanced construction materials and processes for a carbon neutral society 2024 CY - Milano, Italy DA - 07.04.2024 KW - Nuclear magnetic resonance KW - carbonation resistance KW - cement and concrete KW - SLAMD app KW - predictability PY - 2024 DO - https://doi.org/10.1007/978-3-031-70281-5_49 VL - 2 SP - 435 EP - 442 PB - Springer CY - Cham, Switzerland AN - OPUS4-61692 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wachtendorf, Volker A1 - Geburtig, Anja T1 - Digitale Umweltsimulation am Beispiel der Photooxidation von Polymeren N2 - Die Umweltwirkungen auf ein Material werden als Überlapp der Funktionskurven von Materialempfindlichkeit und einwirkenden Umweltparametern betrachtet. Wenn entweder die Empfindlichkeit oder die Beanspruchungen Null sind, ergibt sich auch keine Umweltwirkung und bei beidseitig Werten größer Null das jeweilige Produkt der beiden. Die Akkumulation der nicht-reversiblen Effekte über die Zeit und allen Eigenschaftsänderungen entspricht der Alterung des Materials für den jeweiligen Expositionszeitraum. Die digitale Umweltsimulation gliedert sich hier in drei Teilaspekte. Ein erster, rein materialwissenschaftlicher Teil hat die Aufgabe, alle relevanten Materialempfindlichkeiten experimentell zu quantifizieren. Ein zweiter – unter Umständen numerischer Teil – hat die Aufgabe, das Bauteil und seine Einbaulage zu digitalisieren und aus den makroskopischen Umgebungsbedingungen die relevanten mikroklimatischen Umweltparameter für alle Oberflächen- oder Volumenelemente zu bestimmen. In einem dritten Teil werden die Einwirkungen über den betrachteten Zeitraum berechnet und kumuliert. Dieses Konzept, das auf den so genannten Expositions-Reaktions-Funktionen (ERF) basiert, wird an Beispielen der Photoxidation erläutert. Dieses Vorgehen wurde schon beim ViPQuali-Projekt als Numerische Umweltsimulation umgesetzt. Überprüft werden muss das Modell unbedingt an einer realitätsnahen Validierungsbeanspruchung. Hier werden die ermittelten ERFs mit über den kompletten Beanspruchungszeitraum geloggten Umweltparametern gekoppelt, um die berechnete mit der experimentell erfahrenen Alterungswirkung zu vergleichen. Nur so kann sichergestellt sein, dass alle für die Anwendungsumgebung relevanten Materialempfindlichkeiten einbezogen wurden. T2 - 52. Jahrestagung der GUS CY - Stutensee-Blankenloch, Germany DA - 26.03.2024 KW - UV KW - Polymer 3R KW - Bewitterung KW - Bestrahlung PY - 2024 SN - 978-3-9826129-0-4 SP - 31 EP - 40 PB - Gesellschaft für Umweltsimulation e.V. CY - Pfinztal (Berghausen) AN - OPUS4-59830 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ratkovac, Mirjana A1 - Gerards-Wünsche, Paul A1 - Thiele, Marc A1 - Brackrock, Daniel A1 - Stamm, Michael T1 - Detection and monitoring of the fatigue crack growth on welds – Application-oriented use of NDT methods N2 - Early detection of fatigue cracks and accurate measurements of the crack growth play an important role in the maintenance and repair strategies of steel structures exposed to cyclic loads during their service life. Observation of welded connections is especially of high relevance due to their higher susceptibility to fatigue damage. The aim of this contribution was to monitor fatigue crack growth in thick welded specimens during fatigue tests as holistically as possible, by implementing multiple NDT methods simultaneously in order to record the crack initiation and propagation until the final fracture. In addition to well-known methods such as strain gauges, thermography, and ultrasound, the crack luminescence method developed at the Bundesanstalt für Materialforschung und -prüfung (BAM), which makes cracks on the surface particularly visible, was also used. For data acquisition, a first data fusion concept was developed and applied in order to synchronize the data of the different methods and to evaluate them to a large extent automatically. The resulting database can ultimately also be used to access, view, and analyze the experimental data for various NDT methods. During the conducted fatigue tests, the simultaneous measurements of the same cracking process enabled a comprehensive comparison of the methods, highlighting their individual strengths and limitations. More importantly, they showed how a synergetic combination of different NDT methods can be beneficial for implementation in large-scale fatigue testing but also in monitoring and inspection programs of in-service structures - such as the support structures of offshore wind turbines. T2 - Fatigue Design 2023 (FatDes 2023) CY - Senlis, France DA - 29.11.2023 KW - Fatigue KW - Welded KW - NDT KW - Crack growth PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-600238 DO - https://doi.org/10.1016/j.prostr.2024.03.062 VL - 57 SP - 560 EP - 568 PB - Elsevier B.V. AN - OPUS4-60023 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Geburtig, Anja A1 - Trubiroha, Peter A1 - Wachtendorf, Volker T1 - Significance of new data pairs for irradiance and (surface) temperature N2 - There is consent that UV irradiance and temperature at the place of photodegradation are the most important environmental parameters in weathering, along with humidity. This contribution shows how an improvement in the measurement data situation can improve the significance and comparability of outdoor exposures. Photooxidative ageing is calculated using sample polymers for which the corresponding modelling data (Exposure Response Functions, ERF) is available. The mean square deviations are estimated, which result from using different spectral irradiances and different spectral sensitivities, both of the sensors and the polymers. It will be shown here how the significance of the irradiance values increases with increasing approximation of the spectral sensitivities of the sensor and polymer. Also, the mean square deviations are estimated, which result from using different activation energies and surface temperatures. A selection of different variables to describe the weathering exposure is created. The potential of either individual values or data pairs is evaluated in terms of significance or correlation to the calculated photooxidative ageing. Recording hourly data also enables subsequent evaluations of individual test specimens, adapted to the respective colour or to determine activation energies. An accumulated value, calculated from PIT-radiometer irradiance and a suited surface temperature, can provide a comparison of different outdoor exposures over different locations or years. Thus, a characterisation of the weathering exposure would be related to a reference spectral sensitivity (much closer to a polymer than that of a common UV radiometer), one reference activation energy, and different surface temperature scenarios with, on the one hand, graded solar absorptions (white / grey / black) and, on the other hand, different thermal couplings (coated metal / thick plastic). This results in three values each for plastic samples and coated metals (light / grey / dark). It will never be possible to accurately predict the weathering tests for individual samples (with their specific sensitivities), but the proposed approaches can go a long way towards the comparability of outdoor weathering exposures. T2 - 10th European Weathering Symposium EWS CY - Graz, Austria DA - 11.09.2024 KW - Polymer 3R KW - Outdoor weathering PY - 2024 SN - 978-3-9826129-1-1 SP - 121 EP - 133 PB - Stober Medien GmbH CY - Eggenstein AN - OPUS4-61291 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Seifert, Lando A1 - Müller, Thoralf A1 - Ebell, Gino ED - Pillai, Radhakrishna G. T1 - Development of a new test method for assessing the susceptibility of prestressing steels to hydrogen-induced stress corrosion cracking N2 - For prestressing steel’s factory production control, approvals, and continuous surveillance in Germany, a susceptibility test against hydrogen-induced stress corrosion cracking is performed. The measured time to fracture results (in hours) must be reproducible and reliable in the test. ISO 15630-3 gives currently unpersuasive and diverging results using a free corrosion approach for hydrogen charging. A newly developed test method uses cathodic polarization for defined hydrogen charging instead of an uncontrolled and variable electron supply by metal dissolution during free corrosion. With this new test method, a reliable differentiation is possible between highly susceptible-known “old-type” quenched and tempered prestressing steel, i.e., Neptun, Hennigsdorfer, Sigma, and currently approved cold-drawn wires St 1470/1670 (CDS-1670) and St 1570/1770 (CDS-1770). The reproducibility of the new test method was evaluated in a round-robin test with eight attended testing institutes on a St 1470/1670 (CDS-1670) batch. T2 - Conference CONSEC24 CY - Chennai, India DA - 25.09.2024 KW - Hydrogen charging KW - ISO 15630-3 KW - Prestressing steels KW - Round-robin KW - Stress corrosion cracking PY - 2024 UR - https://consec24.com/# SP - 1 EP - 8 PB - Indian Institute of Technology (IIT) Madras, Centre of Excellence on Technologies for Low Carbon & Lean Construction CY - Chennai, India AN - OPUS4-61163 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Geburtig, Anja A1 - Wachtendorf, Volker A1 - Falkenhagen, Jana T1 - Combined impact of UV radiation and nitric acid (HNO3) on HDPE jerrycans – comparison of outdoor and lab test N2 - A damaging action of HNO3-55% only occurs in combination with its decomposition into nitrous gases, which can be caused by UV radiation. In a laboratory test, transparent HDPE jerrycans have been exposed to both UV radiation and 55 wt-% nitric acid solution at (41 ± 2)°C, for up to 20 days. For comparison, UV radiant exposure (21 days) and nitric acid exposure (up to 6 weeks) were performed separately, at nearly equal temperatures. The respective damages are compared with FTIR spectroscopy in ATR and HT-gel permeation chromatography (GPC) on a molecular level and with hydraulic internal pressure testing as a component test. For the used jerrycans, relevant oxidation can only be found after the combined exposure. The gradual increase in oxidative damage shows the good reproducibility of the lab exposure. The decomposition of nitric acid into nitrous gases by UV radiation – as well as the jerrycan oxidation – is also observed at lower HNO3 concentration (28 wt- %). Similar results are obtained after outdoor tests. Again, the damage occurs only after combined exposure, in contrast to the exposures to UV only and to HNO3 only, which were conducted in parallel. Outdoor exposures are most readily accepted as they represent possible end-use conditions. However, the reproducibility of these exposures is poor due to the large temporal variations in weather. There are also several safety risks, which is why the number of replicates remains limited. Since the outdoor and lab exposure tests show the same qualitative results, it is appropriate to conduct systematic studies in the laboratory. After 6 days of lab exposure, the oxidation damage is rated as critical, which corresponds to about 1/10 year in Central Europe, according to the UV radiant exposure. It should be noted that this amount can also occur in two sunny weeks. T2 - 24th iapri World Packaging Conference CY - Valencia, Spain DA - 17.06.2024 KW - Ppolyethylene KW - UV exposure KW - Nitric acid KW - Oxidation PY - 2024 VL - 2 SP - 30 EP - 37 PB - ITENE AN - OPUS4-60414 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bäßler, Ralph T1 - ISO 27913 - Example For Successful Standardization Activities In The Field Of CCUS N2 - Since 2016 ISO Technical Committee (TC) 265 is working on standardization the whole CCS-process chain. Around 30 countries are working together to provide international guidelines. As ISO 27913 was the first standard finished within these activities it is already in the stage of first revision. The objective of ISO 27913 is “to provide specific requirements and recommendations on certain aspects of safe and reliable design, construction and operation of pipelines intended for the large-scale transportation of CO2 that are not already covered in existing pipeline standards such as ISO 13623, ASME B31.8, EN 1594, AS 2885 or other standards. Existing pipeline standards cover many of the issues related to the design and construction of CO2 pipelines; however, there are some CO2 specific issues that are not adequately covered in these standards. The purpose of this document is to cover these issues consistently. Hence, this document is not a standalone standard, but is written to be a supplement to other existing pipeline standards for natural gas or liquids for both onshore and offshore pipelines.” This contribution shall provide information on the content, the current stage of the revision process, encourage to contribute to this standard and make listeners aware to consider the influence of ISO standard on documents currently in draft. T2 - AMPP's Annual Conference + Expo 2024 CY - New Orleans, LA, USA DA - 02.03.2024 KW - Corrosion resistant materials KW - Carbon dioxide KW - Corrosion prevention KW - Standardization KW - CCUS KW - CCS KW - CCU PY - 2024 SP - 1 EP - 6 PB - AMPP CY - Houston AN - OPUS4-59735 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -