TY - CONF A1 - Woydt, Mathias T1 - Tailoring the functional properties of niobium carbide N2 - Several phases, like Nb₄C₃, Nb₆C₅ and other short and long range ordered phases occur in the region of homogeneity of NbCₓ (0,75≤ x ≤1.0) in the binary phase diagram. Properties, like micro-hardness, hot hardness, sliding wear resistance, elastic modulus and toughness can be tailored by the C/Nb ratio, the addition of secondary carbides and the type of binder. Supporting results from different grades with varying C/Nb ratio or binder types were illuminated. Thus, the NbC system offers to producers a wider process window, than WC. The impact of These tailored properties on sliding wear and cutting performance was illuminated by tribological and machining results. Niobium is today largely available. NbC can be synthesized by carbothermal conversion of Nb₂O₅ or be metallurgically grown and leached out, provides comparably low friction in many relevant tribo-contacts and displays low wear. NbC and Nb₂O₅ have so far no REACH classification related to human toxicology and are not listed as substances of very high concern contrary to WO₃ and Co₃O₄. T2 - 40th International Conference and Exposition on Advanced Ceramics and Composites CY - Daytona Beach, FL, USA DA - 24.01.2016 KW - Niobium carbide KW - Hard metal KW - Wear KW - Friction KW - Machining KW - Cutting KW - Metal matrix composite PY - 2016 SP - Paper: 2347292, 1 EP - 13 AN - OPUS4-35640 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bonse, Jörn T1 - Tribological properties of femtosecond laserinduced periodic surface structures on metals N2 - Laser-induced periodic surface structures (LIPSS, ripples) were generated on steel and titanium surfaces upon irradiation with multiple linear polarized femtosecond laser pulses (pulse duration 30 fs, central wavelength 790 nm). The experimental conditions (laser fluence, spatial spot overlap) were optimized in a sample-scanning geometry for the processing of large surface areas covered homogeneously by the nanostructures. The irradiated surface regions were subjected to optical microscopy (OM), white light interference microscopy (WLIM) and scanning electron microscopy (SEM) revealing sub-wavelength spatial periods. The nanostructured surfaces were tribologically tested under reciprocal sliding conditions against a sphere of hardened 100Cr6 steel at 1 Hz using paraffin oil and engine oil as lubricants. After 1000 sliding cycles at a load of 1.0 N, the corresponding wear tracks were characterized by OM and SEM. For specific conditions the laser-generated nanostructures endured the tribological treatment. Simultaneously, a significant reduction of the friction coefficient was observed in the laser-irradiated (LIPSS-covered) areas when compared to the non-irradiated surface, indicating the potential benefit of laser surface structuring for tribological applications. T2 - SPIE Photonics West Conference, Symposium "Laser Applications in Microelectronic and Optoelectronic Manufacturing" (LAMOM) XXI CY - San Francisco, CA, USA DA - 13.02.2016 KW - Femtosecond laser ablation KW - Laser-induced periodic surface structures (LIPSS) KW - Tribology KW - Friction KW - Wear PY - 2016 AN - OPUS4-36041 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kirner, Sabrina T1 - Femtosecond laser-induced periodic surface structures on titanium nitride coatings for tribological applications N2 - Laser-induced periodic surface structures (LIPSS) were generated on titanium nitride (TiN) hardcoating surfaces (deposited on metallic substrates) upon irradiation with multiple linearly polarized femtosecond laser pulses in air (30 fs duration, 790 nm wavelength, 1 kHz pulse repetition rate). The conditions were optimized in a sample-scanning geometry for the processing of large surface areas (5 mm x 5 mm) covered homogeneously by nanostructures with sub-wavelength periods ranging between ~200 nm and 700 nm. For these nanostructures the coefficient of friction was characterized under reciprocating sliding condition against a ball of hardened steel at 1 Hz using different lubricants (regime of mixed friction). After 1000 cycles, the corresponding wear tracks were characterized by optical and scanning electron microscopy. High-resolution energy dispersive X-ray analyzes (EDX) allowed the visualization of chemical alterations within the wear tracks. For specific conditions, the nanostructures endured the tribological treatment. Our experiments provide a qualification of the tribological performance of the fs-LIPSS on TiN surfaces. T2 - E-MRS 2016 Spring Meeting, Symposium C: "Laser-material interactions for tailoring future applications" CY - Lille, France DA - 02.05.2016 KW - Femtosecond laser ablation KW - Laser-induced periodic surface structures (LIPSS) KW - Tribology KW - Friction KW - Wear KW - Titanium nitride PY - 2016 AN - OPUS4-36042 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Woydt, Mathias T1 - Substituting tungsten carbide (WC) as cutting tools and for wear protection by niobium carbide (NbC) N2 - As a refractory carbide, niobium carbide (NbC) is today still a forgotten carbide with hidden properties, such as wear resistance, thus qualifying NbC for the group of tribological materials with enhanced wear resistance. Several phases, like Nb₄C₃, Nb₆C₅ and other short and long range ordered phases occur In the region of homogeneity of NbCx (0,75≤ x ≤1.0) in the binary phase diagram, which enable the tailoring of properties and offers a much wider process window than known from WC. The type binder (Co, Ni, NiMo) and its concentration as well as the sintering process (SPS, liquid phase sintering) determine the box “hardness-toughness”, which will be illuminated based on more than 100 grades. The impact of these tailored properties on sliding wear (T= 22/400°C; v= 0,1-10 m/s) and cutting performance will be illuminated by tribological and machining results. Cutting test results under emulsion and coolant-free operation of cobalt and Fe3Al bonded, straight NbC versus WC based inserts against different alloys (C60, 100Cr6, 42CrMo4, X90CrMoV18, 300WA, GG35) will be highlighted. T2 - STLE 2016 Annual Meeting and Exhibition CY - Las Vegas, NV, USA DA - 15.05.2016 KW - Niobium Carbide (NbC) KW - Friction KW - Wear PY - 2016 AN - OPUS4-36152 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Bonse, Jörn A1 - Höhm, S. A1 - Koter, Robert A1 - Hartelt, Manfred A1 - Spaltmann, Dirk A1 - Pentzien, Simone A1 - Rosenfeld, A. A1 - Krüger, Jörg T1 - Tribological performance of sub-100-nm femtosecond laser-induced periodic surface structures on titanium N2 - Sub-100-nm laser-induced periodic surface structures (LIPSS) were processed on bulk titanium (Ti) surfaces by femtosecond laser pulse irradiation in air (30 fs pulse duration, 790 nm wavelength). The laser peak fluence, the spatial spot overlap, and the number of overscans were optimized in a sample-scanning geometry in order to obtain large surface areas (5 mm × 5 mm) covered homogeneously by the LIPSS. The laser-processed regions were characterized by optical microscopy (OM), white light interference microscopy (WLIM) and scanning electron microscopy (SEM). The friction coefficient of the nanostructured surfaces was tested during 1000 cycles under reciprocal sliding conditions (1 Hz, 1.0 N normal load) against a 10-mm diameter ball of hardened 100Cr6 steel, both in paraffin oil and in engine oil used as lubricants. Subsequently, the corresponding wear tracks were qualified by OM, SEM, and energy dispersive X-ray analyses (EDX). The results of the tribological tests are discussed and compared to that obtained for near wavelength-sized fs-LIPSS, processed under somewhat different irradiation conditions. Some constraints for a beneficial effect of LIPSS on the tribological performance are provided. KW - Femtosecond laser ablation KW - Laser-induced periodic surface structures, LIPSS KW - Friction KW - Wear KW - Nanostructures KW - Surface functionalization PY - 2016 UR - http://www.sciencedirect.com/science/article/pii/S0169433215026987 DO - https://doi.org/10.1016/j.apsusc.2015.11.019 SN - 0169-4332 SN - 1873-5584 VL - 374 SP - 190 EP - 196 PB - Elsevier B.V. CY - Amsterdam, Netherlands AN - OPUS4-35937 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - THES A1 - Burbank, John T1 - Reactive Boundary Layers in Metallic Rolling Contacts N2 - In order to meet the goal of reducing CO2 emissions, automotive industry places significant importance on downsizing components to achieve greater efficiency through lower weight and reduced friction. As friction reductions are associated with energy efficiency and wear protection with resource conservation, ever greater attention has been given to adamantine carbon- based coatings and high-alloyed steels. Such applications are, however, associated with high production costs and energy expenditures, as well as many technical difficulties. Therefore a key issue in meeting the goals of friction reduction, wear protection and development of comprehensive lightweight strategies is whether or not the functional profiles of state-of-the art alloys can be enhanced by affordable solutions. The running-in phase of mechanical systems is inevitable and, from a tribological standpoint, critical for the lifetime of such systems, though receives little attention and is poorly understood. The growth of micro-cracks accelerates premature material failure and wear during this phase of heightened friction. With this in mind, the ultimate goal of this current work is to transfer the running-in phase into the final step of the mechanical finishing process through the targeted pre-conditioning of novel, high toughness steel bearings without thermo-chemical treatments and compare these to conventional, case-hardened steels. Two mechanisms were investigated: a. Cold work hardening and b. Chemical tribofilm formation. Steels that showed a tendency toward work hardening and tribofilm formation in previous testing were chosen for this investigation. Thorough characterization of the chosen Steels was carried out before any pre-conditioning techniques were applied. The widely used 20MnCr5, seen as a reference gear steel, underwent case-hardening and subsequent deep freezing treatments in an attempt to yield discrete sample groups with respect to residual austenite. This allowed for a more thorough investigation into the effects of residual austenite on the properties of this material. The high-performance alternative steels, 36NiCrMoV1-5-7 (hot working steel) and 45SiCrMo6 (spring steel), were heat treated as recommended by their respective manufacturers, and were not case-hardened. The selection of materials with and materials without case-hardening allows for an investigation into whether or not case-hardening is even necessary to deliver acceptable friction behaviour and wear performance. Elemental analyses were conducted by multiple methods to ensure accurate results. Residual Austenite contents of the steels and the depth profiles of residual stresses were determined by X-Ray diffraction (XRD), for 20MnCr5 ranging from approximately 6 – 14 vol.%, and under 2 vol.% for the alternative alloys. Hardness profiles were taken from the testing surfaces into the material core. The carburization of 20MnCr5 led to higher hardness and the greater concentration of carbon in the carburization zone more representative of a hardened SAE E52100, or 100Cr6/102Cr6, than of a non-case-hardened 20MnCr5. Residual stresses from machining and case-hardening were measured directly at the sample surface. The high-performance Steels fulfilled manufacturer expectations in terms of elemental content, with hardness values between 50 – 55 HRC and strongly martensitic microstructure character. With characterization of the chosen materials complete, the materials could then be subjected to pre-conditioning. The first pre-conditioning method involved targeted generation of cold work hardening as induced boundary layers to protect the contact zone against wear. Work hardening was identified both by variations in residual stress profiles, i.e. the introduction of beneficial compressive residual stresses, and hardness increases in the contact zone, providing enhanced wear resistance. Parameters for work hardening were further optimized to reduce damage to the surface substrates of the treated materials. The second pre-conditioning method involved the targeted generation of chemically reactive tribolayers (tribofilms) on twin disk testing rigs. The lubrication strategies were based on: a. CaCO3, which is predominant in engine oils, and b. MoDTC, which is commonly used in engine and gear oils. The films generated in pre-conditioning were analyzed by SEM-EDX with Element-Mapping, Raman spectroscopy, and XPS to elucidate their molecular composition and concentration on the sample surfaces. The combination of these methods of analysis gave a clear indication that 104 cycles were sufficient to generate stable and lasting tribofilms. CaO and CaCO3 were the main components of the tribofilm from the first lubricant package, while MoS2, MoO2 and MoO3 were the main components from the second lubricant package. Finally, slip-rolling endurance testing (T = +120 °C, 107 cycles, approximately 19 days in a factory fill engine oil) was carried out on all materials. It was shown that both pre-conditioning methods could achieve significant reductions in friction and wear during testing at up to and including P0Mean =1.94 GPa (P0Max = 2.91 GPa, FN = 2,000 N). Ultimately, this research showed that: 1. non-case-hardened high-performance steels offer competitive wear performance and better friction behaviour than the case-hardened 20MnCr5. 2. pre-conditioning led to COF reductions to under 7/10 and wear coefficient reductions to an astonishing 1/10 of the original values for the untreated steels under mixed/boundary lubrication. 3. the observed improvements to friction behaviour and wear performance are indicative of a technically simple, cost- and energy-efficient pre-conditioning strategy that may prove N2 - Die Automobilindustrie legt im Hinblick auf das Ziel der CO2-Emissionsreduktionen viel Wert auf die Erhöhung des Wirkungsgrades von mechanischen Komponenten durch Leichtbau. Eine Reduzierung der Reibung wirkt sich direkt auf die Energieeffizienz aus, währenddessen eine Verschleißminderung zu Materialeinsparungen führt. Aus diesen Gründen genießen diamantartige, kohlenstoffbasierte Beschichtungen und hochlegierten Stähle derzeit große Aufmerksamkeit. Deren Herstellung ist allerdings sowohl mit einem hohen Energie- und Kostenaufwand verbunden, als auch technisch sehr anspruchsvoll. Zur Erreichung der Ziele der Reibungsminderung, des Verschleißschutzes und der Entwicklung umfassender Leichtbaustrategien ist es daher von großer Bedeutung, ob sich das Leistungsprofil neuartiger Legierungen durch kostengünstigere Lösungen verbessern lässt. Obwohl der mechanische Einlauf aus tribologischer Sicht entscheidend für die Lebensdauer mechanischer Systeme ist, genießt er wenig Aufmerksamkeit und ist bis heute nur begrenzt verstanden. So kann die Ausbreitung von Mikrorissen während dieser Phase der erhöhten Reibung zum vorzeitigen Materialversagen führen. In diesem Sinne war es das oberste Ziel dieser Forschungsarbeit, den Einlauf in die mechanische Endbearbeitung vorzuverlegen. Neuartige Stähle wurden dabei ohne kostenintensive, thermochemische Behandlungen gezielt vorkonditioniert und ihre so verbesserten Eigenschaften mit denen von gängigen Einsatzstählen verglichen. Zu den untersuchten Vorkonditionierungsmechanismen gehören die Erzeugung von: a. Kaltverfestigungen und b. chemischen Tribofilmen. Stähle, die in Vorversuchen eine Zuneigung zur Kaltverfestigung und Tribofilmentstehung, wurden für diese Forschungsarbeit ausgewählt. Die ausgewählten Stähle urden vor jeglicher Vorkonditionierung einer gründlichen, metallurgischen Charakterisierung unterzogen. Der Referenzgetriebestahl 20MnCr5 wurde einsatzgehärtet und in getrennten Gruppen bei verschiedenen Temperaturen tiefgekühlt, um Proben in verschiedenen Nuancen des Restaustenitgehaltes zu erhalten. Damit ließ sich der Einfluss des Restaustenits auf die Materialeigenschaften genauer untersuchen. Die Hochleistungsstähle, 36NiCrMoV1-5-7 (Warmarbeitsstahl) und 45SiCrMo6 (Federstahl), wurden nach den Vorschriften der jeweiligen Hersteller wärmebehandelt, und wurden nicht einsatzgehärtet. Die Auswahl an Stählen, mit und ohne Einsatzhärtung, lässt eine Untersuchung darüber zu, ob eine Einsatzhärtung überhaupt notwendig ist, um gutes Reibungs- und Verschleißverhalten zu erzielen. Elementanalysen wurden mittels mehrerer Methoden zur Gewährleistung der bestmöglichen Genauigkeit der Ergebnisse durchgeführt. Die Restaustenitgehalte der Stähle und Eigenspannungstiefenprofile wurden an einem Röntgendiffraktometer ermittelt. Die Restaustenitgehalte des 20MnCr5 lagen zwischen 6 – 14 Vol.-% und die Restaustenitgehalte der Alternativstähle lagen unter 2 Vol.-%. Härtetiefenprofile wurden auch ermittelt. Die Aufkohlung des 20MnCr5 führte zu einer Steigerung der Härte und der Kohlenstoffkonzentration im Randbereich, sodass dieser Bereich des Stahls eher einem gehärteten SAE 52100, oder 100Cr6/102Cr6, als einem nicht einsatzgehärtetem 20MnCr5 entsprach. Eigenspannungen, die durch die mechanische Endbearbeitung entstanden, wurden direkt unter der Oberfläche detektiert. Die Hochleistungsstähle erfüllten mit Härtewerten zwischen 50 – 55 HRC und ihrem ausgeprägt martensitischen Charakter die Herstellervorgaben. Nach dem Abschluss der metallurgischen Charakterisierung wurden die Stähle vorkonditioniert. Zur ersten Vorkonditionierungsmethode gehörte die Erzeugung gezielter Kaltverfestigungen an Zweischeibenprüfständen in der Form von induzierten Grenzschichten, die die Randschicht gegen Verschleiß schützen. Die Wirksamkeit dieser Vorkonditionierung wurde anhand der Zunahme der vorteilhaften Druckeigenspannungen und der Steigerung der Oberflächenhärte nachgewiesen. Beide Eigenschaften verleihen den Stählen eine erhöhte Verschleißbeständigkeit. In einem weiteren Schritt wurden die Vorkonditionierungsparameter zur Erzeugung von Kaltverfestigung optimiert, um die evtl. Deformierung der Substratoberflächen abzumildern. In einer alternativen, zweiten Vorkonditionierung wurden zwei verschiedene Schmierstoffkonzepte implementiert, um an den Zweischeibenprüfständen chemisch reaktive Triboschichten (Tribofilme) zu generieren. Die Schmierstoffkonzepte basierten auf: a. CaCO3, was überwiegend in Motorenölen eingesetzt wird und b. MoDTC, was häufig in Motoren- und Getriebeölen eingesetzt wird. Die durch die Vorkonditionierung erzeugten Tribofilme wurden mittels REM-EDX mit Element- Mapping, Raman-Spektroskopie und XPS analysiert, um ihre molekulare Zusammensetzung und Oberflächenkonzentration zu ermitteln. Der Tribofilm aus dem ersten Schmiermittel bestand hauptsächlich aus CaO und CaCO3 und der Tribofilm aus dem zweiten Schmiermittel bestand hauptsächlich aus MoS2, MoO2 und MoO3. Aus diesen Analysen wurde ersichtlich, dass 104 Laufzyklen zur Generierung stabiler und beständiger Tribofilme vollkommen ausreichend sind. Anschließend wurden alle Stähle in Dauerwälzversuchen (T = +120 °C, 107 Zyklen, etwa 19 Tage in einem Erstbefüllungsmotorenöl) in ihrem Reibungs- und Verschleißverhalten untersucht. Es wurde gezeigt, dass durch vorkonditionierte Kaltverfestigungen oder durch vorkonditionierte Tribofilme die Reibung und der Verschleiß in Wälzkontakten bei Dauerwälzen bis P0Mean =1,94 GPa (P0Max = 2,91 GPa, FN = 2.000 N) signifikant erniedrigt werden können. Im Endeffekt wurde in dieser Arbeit gezeigt, dass: 1. nicht einsatzgehärtete Hochleistungsstähle konkurrenzfähig zu dem einsatzgehärteten 20MnCr5 sind. 2. die Vorkonditionierungen zu einer Senkung des Reibungskoeffizienten bis auf 7/10 und zu einer Senkung des Verschleißkoeffizienten bis auf 1/10 der Koeffizienten der nicht vorkonditionierten Stähle unter Misch-/Grenzreibungsbedingungen führten. 3. die Verbesserungen des Reibungs- und Verschleißverhaltens auf eine technisch einfache, energie- und kosteneffiziente Vorkonditionierungsstrategie weisen, die noch bestehende thermochemische Behandlungen ersetzen könnte. T3 - BAM Dissertationsreihe - 143 KW - Work hardening KW - Steel KW - Friction KW - Wear KW - Tribofilm PY - 2016 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-354507 SN - 978-3-9817502-5-6 SN - 1613-4249 VL - 143 SP - 1 EP - 133 PB - Bundesanstalt für Materialforschung und -prüfung (BAM) CY - Berlin AN - OPUS4-35450 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Woydt, Mathias T1 - Adjusting the functional properties of niobium carbide N2 - The process window and range of functional properties of NbC is wide, because micro-hardness, hot hardness, sliding wear resistance, elastic modulus and toughness can be tailored by the C/Nb ratio, because Nb4C3, Nb6C5 and other short and long range ordered phases occur in the region of homogeneity of NbCx (0,75≤ x ≤1.0) in the binary Phase diagram, and by the type of binder. Further improvements enable the addition of secondary carbides. Supporting results from literature and different grades with varying C/Nb ratio or binder types were illuminated. Thus, the NbC system offers to producers a wider process window, than WC. The impact of these tailored properties on sliding wear and cutting performance was illuminated by tribological and machining results. NbC can be synthesized by carbothermal conversion of Nb2O5 or be metallurgically grown in melts and leached out as coarse NbC cubes. NbC provides comparably lower friction in many relevant tribo-contacts and displays low wear. NbC and Nb2O5 have so far no REACH classification related to human toxicology and are not listed as substances of very high concern contrary to WO3 and Co3O4. T2 - 2016 International Conference on Powder Metallurgy & Particulate Materials CY - Boston, MA, USA DA - 05.06.2016 KW - Niobium carbide KW - NbC KW - Wear KW - Friction PY - 2016 AN - OPUS4-36497 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Woydt, Mathias A1 - Scholz, C. A1 - Burbank, J. A1 - Spaltmann, Dirk T1 - Slip-rolling resistant steel alloys up to P0max of 3,920 MPa N2 - Downsizing (power-to-weight ratio) and higher speeds lead to a rise in Hertzian contact pressures in combination with an increase in surface or oil temperatures. Under such conditions, commonly used bearing steels, such as 100Cr6, reach their limits, creating a demand for alternative slip-rolling resistant steel alloys. The present work therefore compares the slip-rolling performance of various steel types with Maraging- and PM-type steel alloys such as e.g. CSS-42L™, ASP2012, BIMAX42+, in the Hertzian contact pressure range up to P0max of 4 GPa. Through-hardened 100Cr6H (AISI 52100), case-hardened 20MnCr5 (AISI 5120H) and nitrogen alloyed Croni-dur30 (AMS 5898) still compete in terms of slip-rolling and wear resistance and load carrying capacity, whereas Maraging- and PM-type steel alloys offer superior strength and toughness properties. KW - Steel KW - Alloy KW - Slip-rolling KW - Friction KW - Wear rate KW - Contact pressure KW - 100Cr6 KW - BIMAX42 KW - CSS-42L KW - ASP20212 PY - 2012 DO - https://doi.org/10.1016/j.wear.2021.203707 VL - 474-475 SP - 203707 PB - Elsevier B.V. AN - OPUS4-52549 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schirdewahn, S. A1 - Spranger, Felix A1 - Hilgenberg, Kai A1 - Merklein, M. T1 - Investigation of the thermal and tribological performance of localized laser dispersed tool surfaces under hot stamping conditions N2 - In the automotive industry, hot stamping has been established as a key technology for manufacturing safety-relevant car body components with high strength-to-weight ratio. However, hot stamping tools are stressed by cyclic thermo-mechanical loads, which leads to severe wear and high friction during the forming operation. Consequently, the quality of the parts, the durability of the tools and the efficiency of the process are negatively affected. Within the scope of this work, a promising approach named laser implantation process has been investigated for improving the tribological behavior of hot stamping tools. This technique enables the fabrication of highly wear resistant, separated and elevated micro-features by embedding hard ceramic particles into the tool via pulsed laser radiation. Hence, highly stressed tool areas can be modified, which influences the thermal and tribological interactions at the blank-die interface. To clarify these cause-effect relations, numerical simulations, quenching tests as well as tribological investigations have been conducted. In this context, laser-implanted tools reveal a significantly improved tribological performance while offering the possibility to adjust the thermal properties within hot stamping. Based on these results, a tailored tool modification can be pursued in future research work, in order to enhance the effectiveness of hot stamping tooling systems. KW - Hot stamping KW - Laser Implantation KW - Surface structuring KW - Wear KW - Friction PY - 2021 DO - https://doi.org/10.1016/j.wear.2021.203694 VL - 476 SP - 1 EP - 11 PB - Elsevier B.V. AN - OPUS4-52988 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Spaltmann, Dirk T1 - Tribological performance of FS-laser-induced periodic surface structures on titanium alloy against different counter-body materials using a ZDDP lubricant additive N2 - In this study the so-called laser-induced periodic surface structures (LIPSS, ripples) were produced on titanium alloy (Ti6Al4V) surfaces upon scan processing in air by a Ti:sapphire femtosecond (fs) laser. The tribological performance of the resulting surfaces was qualified in linear reciprocating sliding tribological tests (RSTT) against balls made of different materials (100Cr6 steel/Al2O3/Si3N4) using different oil-based lubricants. The admixture of the additive 2-ethylhexylzinc-dithiophosphate (ZDDP) to a base oil containing only anti-oxidants and temperature stabilizers disclosed the synergy of the additive with the laser-oxidized nanostructures. This interplay between the laser-textured sample topography and the local chemistry in the tribological contact area reduces friction and wear. T2 - 7th World Tribology Congress - WTC 2022 CY - Lyon, France DA - 11.07.2022 KW - Lubricant additives KW - Laser-induced periodic surface structures (LIPSS) KW - Wear KW - Friction PY - 2022 AN - OPUS4-55318 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -