TY - CONF A1 - Kromm, Arne A1 - Kannengießer, Thomas A1 - Dixneit, Jonny T1 - Observation of martensite formation by combined use of synchrotron diffraction and dilatometry N2 - Welding residual stress engineering by means of an adjusted martensite phase transformation would be highly attractive as detrimental tensile residual stresses may be prevented already during welding without time and cost intensive post processing. The present study shows a synchrotron diffraction analysis of a martensitic steel subjected to thermo-mechanical load cycles. Experiments were conducted regarding the microstructural strain response during the austenite to martensite transformation. The strains are a function of the temperature and the specific loads applied during cooling. The relation between the transformation plasticity of the material, the amount of martensite formed and the arising strains can thus be assessed. The lattice plane specific strains were compared to experimental findings from (macro) dilatation tests. It is shown that the microscopic material behavior differs remarkably from the one observed on the macroscopic scale, what leads to characteristic residual stresses in the material. T2 - Material Science & Technology (MS&T16) 3rd International Workshop of In-situ Studies with Photons, Neutrons and Electrons Scattering CY - Salt Lake City, UT, USA DA - 23.10.2016 KW - Residual stress KW - Martensite KW - Dilatometry KW - Synchrotron diffraction KW - Neutron diffraction PY - 2016 AN - OPUS4-37999 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne A1 - Kannengießer, Thomas T1 - Online-Observation of Martensite Formation by combined use of Synchrotron Diffraction and Dilatometry N2 - Welding residual stress engineering by means of an adjusted martensite phase transformation would be highly attractive as detrimental tensile residual stresses may be prevented already during welding without time and cost intensive post processing. The present study shows a synchrotron diffraction analysis of a martensitic steel subjected to thermo-mechanical load cycles. Experiments were conducted regarding the microstructural strain response during the austenite to martensite transformation. The strains are a function of the temperature and the specific loads applied during cooling. The relation between the transformation plasticity of the material, the amount of martensite formed and the arising strains can thus be assessed. The lattice plane specific strains were compared to experimental findings from (macro) dilatation tests. It is shown that the microscopic material behavior differs remarkably from the one observed on the macroscopic scale, what leads to characteristic residual stresses in the material. T2 - Visual-JW 2019 & WSE 2019 The 5th International Symposium on Visualization in Joining & Welding Science through Advanced Measurements and Simulation & The 8th International Conference of Welding Science and Engineering CY - Osaka, Japan DA - 21.11.2019 KW - Martensite KW - Synchrotron KW - Dilatometry KW - Residual stress KW - Phase transformation PY - 2019 AN - OPUS4-49768 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Falkenreck, Thora A1 - Kromm, Arne A1 - Böllinghaus, Thomas T1 - Investigation of Physically Simulated Weld HAZ and CCT-diagram of HSLA steel N2 - The phase transformation under various cooling rates and in different HAZ regions for high strength armour steel was analysed by dilatometry. To develop a Continuous Colling Transformation (CCT) diagram, the samples were heated up to a peak temperature of 1250 °C to achieve a coarse grained microstructure and then cooled down with a cooling time t8/5 varying from 3 s to 240 s. Analysis of dilatation curves revealed the austenite decomposition process, during which transformation temperatures were determined. The results showed martensitic transformations for all welding relevant cooling times. Furthermore, to analyse different heat affected subzones of the weld, the peak temperature was varied between 550 °C and 1250 °C at a constant cooling time t8/5 of 6 s. The simulated coarse grained heat affected zone (CGHAZ) and fine grained heat affected zone (FGHAZ) showed only martensitic transformations with transformation temperatures below 400 °C. The steel exhibited an inhomogeneous hardness with hardening in the CGHAZ and FGHAZ and softening in the intercritical and subcritical HAZ. The physically simulated microstructure was validated by a real hybrid laser-arc weld microstructure. T2 - IIW Intermediate meeting, IX-L CY - Trollhättan, Sweden DA - 06.03.2017 KW - Dilatometry KW - High strength stells KW - CCT diagrams KW - Heat affected zone PY - 2017 AN - OPUS4-39437 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -