TY - CONF A1 - Müller, Urs T1 - Lime mortar for the conservation of the Timur Shah Mausoleum T2 - Standort H23/R012, BAM CY - Berlin, Germany DA - 02.05.2006 PY - 2006 AN - OPUS4-12486 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Maultzsch, Matthias A1 - Kühne, Hans-Carsten A1 - Meinhold, Uwe A1 - Haamkens, Frank T1 - Entwicklung von Betonen mit geringer Festigkeit für die Beurteilung von Instandsetzungssystemen im Wasserbau T2 - Wissenschaftsrat N2 - Die Regelwerke (RL SIB, ZTV-ING) setzen für die Instandsetzung mit Betoninstandsetzungssystemen vergleichsweise hochwertige Betonuntergründe voraus. Speziell bei älterenWasserbauwerken sind oftmals nur geringerfeste Betonuntergründe vorhanden für die es bis jetzt keine geeigneten und geprüften Instandsetzungssysteme gab. Grundlage für die Entwicklung solcher Systeme sind entsprechende Referenzbetone als Untergrundbeton für die Verbundkörperprüfung. T2 - Wissenschaftsrat CY - Berlin, Germany DA - 17.01.2006 PY - 2006 AN - OPUS4-12028 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kühne, Hans-Carsten A1 - Mellmann, Günter T1 - Abschätzung der Druckfestigkeit von hochfestem Beton mit dem Rückprallhammer T2 - Wissenschaftsrat N2 - Ziel der Untersuchungen war es, herauszufinden ob die Druckfestigkeit hochfester Betone zerstörungsfrei mit dem Rückprallhammer PROCEQEQUOSCHMIDT durch Ermittlung des klassischen Rückprallwerts R in Kombination, mit einem aus der Untersuchung von Metallen bekannten neuen Messwert L mit ausreichender Sicherheit beschrieben werden kann. T2 - Wissenschaftsrat CY - Berlin, Germany DA - 17.02.2006 PY - 2006 AN - OPUS4-12029 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Jakubcová, Petra A1 - Rübner, Katrin A1 - Schnell, A. T1 - Leichtgranulate aus heterogenem Bauschutt zur Herstellung von Beton T2 - r2- Statusseminar 2011, "Innovative Technologien für Ressourceneffizienz - rohstoffintensive Produktionsprozesse, Fraunhofer-Institut N2 - Untersucht wird die Entwicklung einer Technologie zur Herstellung hochwertiger Leichtgranulate (Blähgranulate) mit definierten Produkteigenschaften aus heterogenen Bau- und Abbruchabfällen, Anwendung der Granulate als leichte Gesteinskörnung im Beton und die Möglichkeit des rohstofflichen Recyclings mineralischer Bauabfälle T2 - r2- Statusseminar 2011, "Innovative Technologien für Ressourceneffizienz - rohstoffintensive Produktionsprozesse, Fraunhofer-Institut CY - Berlin, Germany DA - 26.10.2011 PY - 2011 AN - OPUS4-24717 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Osterhus, Lennart A1 - Rübner, Katrin T1 - Kieselsäurehaltiger Filterrückstand aus industrieller Abwasserbehandlung für den Einsatz als hydraulisches Bindemittel T2 - GDCh-Tagung Bauchemie N2 - - 5.000 bis 10.000 t wasserhaltiger Filterrückstand (FR) entstehen jährlich pro Produzent bei der Neutralisation der Abwässer aus der Silicon- oder Kieselsäureherstellung - Anfall als fester, feuchter, schollenartiger Filterkuchen - Verwertung heute: Deponierung, Tagebauverfüllung -> ungenutzte Sekundärrohstoffquelle - Untersuchung der Einsatzmöglichkeiten der aufbereiteten Filterrückstände zur Eigenschaftsverbesserung zementgebundener Baustoffe analog der wohlbekannten Anwendung von hochdisperser Kieselsäure und Silicastaub T2 - GDCh-Tagung Bauchemie CY - Hamburg, Germany DA - 06.10.2011 PY - 2011 AN - OPUS4-24819 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Herbst, Tristan A1 - Rübner, Katrin A1 - Meng, Birgit T1 - Integrated and holistic suitability assessment of recycling options for masonry rubble T2 - European Geosciences Union (EGU) General Assembly 2012 N2 - Behandelt den Bausektor und die Verarbeitsungsqualität T2 - European Geosciences Union (EGU) General Assembly 2012 CY - Vienna, Austria DA - 22.04.2012 PY - 2012 AN - OPUS4-25868 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Reinsch, Stefan A1 - Dreßler, Martin A1 - Nofz, Marianne A1 - Pauli, Jutta A1 - Jäger, Christian A1 - Scholz, G. T1 - Phasentransformationen von anorganisch modifizierten Alumo-Xerogelen T2 - Jahrestagung der Gesellschaft für Thermische Analyse e.V. (GEFTA 2003) T2 - Jahrestagung der Gesellschaft für Thermische Analyse e.V. (GEFTA 2003) CY - Augsburg, Germany DA - 15.09.2003 PY - 2003 AN - OPUS4-4746 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rübner, Katrin A1 - Mellmann, Günter T1 - Porenstruktur von Beton mit Recyclingzuschlägen T2 - Tag der offenen Tür der BAM N2 - Recyclingzuschläge (rezyklierte Gesteinskörnungen, Betonsplitt) werden großtechnisch aus dem Material, das beim Abbruch von Betonbauwerken anfällt, hergestellt. Sie bestehen zu mehr als 90% aus Altbeton. Die Wiederverwendung dieser Materialien zur Herstellung von neuen hochwertigen Beton erfordert umfangreiche Kenntnisse über ihre betontechnologischen und chemisch-physikalischen Eigenschaften. Zwei unterschiedliche Recyclingzuschläge und die damit hergestellten Betone wurden im Vergleich zu einem Referenzbeton mit natürlichen Zuschlägen gleicher Sieblinie untersucht. T2 - Tag der offenen Tür der BAM CY - Berlin, Germany DA - 19.06.2004 PY - 2004 AN - OPUS4-11432 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rübner, Katrin A1 - Knölle, G. A1 - Voigtberger, K. T1 - Untersuchungen zur Nutzung eines kieselsäurehaltigen Filterschlamms als Zusatzstoff für Mörtel und Beton T2 - XII. Workshop der Porotec GmbH über die Charakterisierung von feinteiligen und porösen Festkörpern N2 - Der Filterschlamm (FS) fällt als Reststoff bei der Abwasserbehandlung des Chemiewerkes an. Er liegt als feinteiliges Granulat vor und enthält als Hauptbestandteil amorphe Kieselsäure. Damit eröffnet sich die Möglichkeit, ihn wie einen mineralischen Zusatzstoff bei der Beton- und Mörtelherstellung zu verwenden. Als Betonzusatzstoff werden fein aufgeteilte Zusätze zum Beton bezeichnet, die durch chemische und/oder physikalische Wirkung die Betoneigenschaften beeinflussen, und die als Stoffraumkomponente zu berücksichtigen sind. T2 - XII. Workshop der Porotec GmbH über die Charakterisierung von feinteiligen und porösen Festkörpern CY - Bad Soden, Germany DA - 16.11.2004 PY - 2004 AN - OPUS4-11433 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rübner, Katrin T1 - Mikrostruktur von hochfestem Beton T2 - Tag der offenen Tür der BAM N2 - Hochfeste Betone werden durch die Zugabe puzzolanischer Zusatzstoffe (Microsilica, Flugasche) und die Reduzierung des Wasser-Zement-Wertes bei gleichzeitiger Verwendung eines Fließmittels hergestellt. Diese Modifizierungen des Betons beeinflußen die Zusammensetzung und die Mikrostruktur seiner Mörtelmatrix. T2 - Tag der offenen Tür der BAM CY - Berlin, Germany DA - 19.06.2004 PY - 2004 AN - OPUS4-11431 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kalinka, Gerhard T1 - Bestimmung der Interface-Festigkeit in carbonfaserverstärkten Werkstoffen T2 - Verbundwerkstoffe und Werkstoffverbunde T2 - Verbundwerkstoffe und Werkstoffverbunde CY - Kassel, Germany DA - 06.04.2005 PY - 2005 AN - OPUS4-6085 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Beck, Matthias A1 - Rübner, Katrin A1 - Burkert, Andreas T1 - Einsatz der Quecksilberporosimetrie zur Charakterisierung von Feinkornbetonen für elektrochemische Untersuchungen T2 - XIII. Workshop über die Charakterisierung von feinteiligen und porösen Festkörpern N2 - Im Rahmen eines DFG-Forschungsvorhabens (FOR 537) wird ein Teilprojekt an der BAM bearbeitet. Ziel dieser Arbeit ist die quantitative Beschreibung und Bewertung des Korrosionsfortschrittes an Stahlproben mit kleinen Kathodenflächen (Eigenkorrosion) mittels elektrochemischer Messungen. Für die Untersuchungen wurden Betonproben mit eingebetteten Stahlelektroden hergestellt. Dabei wurden gezielt betontechnologische Parameter variiert. Dabei ist der Beton als Elektrolyt zu betrachten. Nach bestimmten Zeitintervallen werden die Betonproben aufgebrochen und die eingebetteten Stahlelektroden durch visuelle Inspektion und anschließende Bestimmung des Masseverlustes bewertet. Zur Charakterisierung des Betons (Elektrolyt) dient das Verfahren der Quecksilberporosimetrie. Mit dem Verfahren lassen sich die Zusammenhänge zwischen den betontechnologischen Parametern und der Porenstruktur aufzeigen und mittels der umfangreichen Variation der Betonparameter die Auswirkung auf den Korrosionsfortschritt nachweisen. T2 - XIII. Workshop über die Charakterisierung von feinteiligen und porösen Festkörpern CY - Bad Soden, Germany DA - 14.11.2006 PY - 2006 AN - OPUS4-14294 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rübner, Katrin A1 - Goering, Harald A1 - Klobes, Peter A1 - Tschritter, H. T1 - Investigation on the structure of silica/polyurethane nanocomposites T2 - 8th International Symposium on the Characterisation of Porous Solids N2 - Inorganic-organic nanocomposites are synthesised from polyethylene glycol with an average molar mass of 600 g/mol containing colloidal silica (silicic acid) and diphenyl methane diisocyanate as compact and foamed materials according to the European patent EP1414880. Beside the macroscopic properties, the pore structure and the structure of the polymer matrix of the silica/polyurethane nanocomposites with varying silica contents were studied. T2 - 8th International Symposium on the Characterisation of Porous Solids CY - Edinburgh, Scotland DA - 11.06.2008 PY - 2008 AN - OPUS4-16445 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Klobes, Peter A1 - Rübner, Katrin A1 - Prinz, Carsten A1 - Hempel, S. T1 - Investigation on the microstructure of ultra high performance concrete T2 - 8th International Symposium on the characterisation of Porous Solids N2 - Ultra-high performance concrete (UHPC) is characterised by compressive strengths above 150 MPa and an outstanding durability. These properties are achieved by optimisation of the mixture composition, the mixing procedure as well as the curing conditions of the concrete. Heat curing as well as the use of vacuum mixers may contribute to the high strength. The very high brittleness of UHPC can be compensated by the addition of steel or polymer fibres. UHPC is produced using a very low water/cement ratio of 0.25 or smaller in combination with adding of polycarboxylate ether based superplasticisers. Furthermore, finest cements with contents of 500 kg/m³, defined selections of coarse and fine aggregates with a maximum grain size between 0.5 and 8 mm and fine pozzolanic (silica fume, fly ash) and inert additives (quartz filler) are used. In doing so, the aim is to obtain a very high packing density of the cement paste matrix and the aggregate/paste interface while a very homogeneous microstructure with a high calcium silicate hydrate (CSH) portion is formed. In the case of optimal mixing and curing conditions, UHPC contains almost no pores and microcracks. Therefore, studies of porosity and pore structure are very important to characterise UHPC materials in connection with the mixture optimisation. Here, the experimental results for UHPC are presented in comparison with those of high-strength concrete (100 MPa) and normal-strength concrete (35 MPa), respectively. T2 - 8th International Symposium on the characterisation of Porous Solids CY - Edinburgh, Scotland DA - 11.06.2008 PY - 2008 AN - OPUS4-16396 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rübner, Katrin A1 - Kühne, Hans-Carsten T1 - Pore structure of concrete with recycling aggregates T2 - 33th International Geological Congress (IGC) Symposium on Mineral Resources - Constructions Materials (MRC) N2 - Processed building rubble containing about 90 % of crushed concrete can be used as recycling aggregates. The reuse for the production of new high-grade concrete requires a knowledge of the engineering properties as well as the pore structure of These materials. Two recycling aggregates and the concretes made with them were studied. T2 - 33th International Geological Congress (IGC) Symposium on Mineral Resources - Constructions Materials (MRC) CY - Oslo, Norway DA - 06.08.2008 PY - 2008 AN - OPUS4-16778 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rübner, Katrin T1 - Charakterisierung der Porenstruktur von ultrahochfestem Beton T2 - XIII. Workshop über die Charakterisierung von feinteiligen und porösen Festkörpern N2 - Ultrahochfeste Betone (UHPC) sind durch Druckfestigkeiten > 150 MPa und eine besonders hohe Dauerhaftigkeit gekennzeichnet. Ihre Herstellung gelingt durch die Optimierung der Mischungszusammensetzung, des Mischprozesses und der Nachbehandlung. Maßnahmen dazu bestehen in der Verwendung feinstgemahlener Zemente, puzzolanischer und inerter Feinststoffe, dem Einsatz gezielt ausgewählter grober und feiner Gesteinskörnungen, der Reduktion des Wasser/Bindemittel-Wertes bei Zugabe von Fließmitteln auf Polycarboxylat-Basis sowie einer Wärmebehandlung der Betone. Das Ziel dabei ist es, eine möglichst hohe Packungsdichte in der Bindemittelmatrix bei Ausbildung einer sehr gleichmäßigen und extrem dichten Gefügestruktur mit einem hohen Anteil an Calciumsilicathydrat-Phasen zu erreichen. Deshalb sind Untersuchungen zur Porosität und Porenstruktur ein wichtiger Bestandteil zur Materialcharakterisierung im Rahmen der Mischungsoptimierung. Die Ergebnisse der Mikrostrukturuntersuchungen werden im Vergleich zu denen an einem hochfesten Beton und einem Normalbeton betrachtet. T2 - XIII. Workshop über die Charakterisierung von feinteiligen und porösen Festkörpern CY - Bad Soden, Germany DA - 14.11.2006 PY - 2006 AN - OPUS4-14010 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Herbst, Tristan A1 - Rübner, Katrin A1 - Meng, Birgit A1 - Hauer, B. T1 - Nachhaltiges Bauen mit Beton - Einsatz sekundärer Gesteinskörnungen T2 - 17. IBAUSIL N2 - Im Hinblick auf eine nachhaltige Entwicklung sollen nach dem KrW/AbfG der Rohstoffeintrag und der Abfallaustrag in den Lebensphasen eines Bauwerks durch weitgehende Verwertung von Sekundärrohstoffen (Reststoffen) möglichst gering gehalten werden. Ein Einsatz von Reststoffen wie Hausmüllverbrennungsaschen (MV-Aschen) im Betonbau kann potenziell einen wesentlichen Beitrag zur nachhaltigen Entwicklung leisten. T2 - 17. IBAUSIL CY - Weimar, Germany DA - 23.09.2009 PY - 2009 AN - OPUS4-19731 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Gründer, Klaus-Peter A1 - Kadoke, Daniel T1 - Bewegungs- und Verformungsanalyse unter Fallbeanspruchungen T2 - Tag der offenen Tür der BAM im Rahmen der Initiative "Deutschland, Land der Ideen" N2 - Diese Untersuchung enthält die Qualifizierung eines Laservibrometers, die Kinematik in Fallbeanspruchung und das Messverfahren, den Prüfstand und Proben. T2 - Tag der offenen Tür der BAM im Rahmen der Initiative "Deutschland, Land der Ideen" CY - Horstwalde, Germany DA - 09.09.2009 PY - 2009 AN - OPUS4-20191 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ried, Peter A1 - Gaber, Martin A1 - Kluge, Martin A1 - Müller, Ralf A1 - Holtappels, Kai A1 - Eliezer, Dan T1 - H2-permeability and burst pressure of glass capillaries T2 - Intern. Con. on Glass ICG 2010 N2 - This publication deals with the topics: pressure loading, permeability and burst pressure T2 - Intern. Con. on Glass ICG 2010 CY - Bahia, Brazil DA - 20.09.2010 KW - Pressure loading KW - Permeability KW - Burst pressure PY - 2010 N1 - Geburtsname von Kluge, Martin: Beckmann-Kluge, M. - Birth name of Kluge, Martin: Beckmann-Kluge, M. AN - OPUS4-22296 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Herbst, Tristan A1 - Rübner, Katrin A1 - Müller, A. A1 - Seidemann, M. T1 - Verwertung kieselsäurehaltiger Filterrückstände in mineralischen Baustoffen T2 - GDCh Tagung Bauchemie N2 - - jährlicher Anfall von 5.000 bzw. 10.000 Tonnen wasserhaltiger Filterrückstände (FR) pro Produzent bei der Abwasser-Neutralisation aus der Kieselsäure- bzw. Chlorsilanherstellung (FR1, FR2) - heute: Deponierung, Tagebauverfüllung - ungenutzte Sekundärrohstoffquelle - Untersuchung möglicher Anwendungsbereiche für FR T2 - GDCh Tagung Bauchemie CY - Dübendorf, Switzerland DA - 11.10.2012 PY - 2012 AN - OPUS4-26673 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rübner, Katrin A1 - Meinel, Dietmar A1 - Prinz, Carsten A1 - Zimathies, Annett A1 - Klobes, Peter A1 - Schnell, A. A1 - Hempel, S. T1 - Porenstruktur leichter Gesteinskörnungen aus Mauerwerkbruch T2 - XVI. Porotec-Workshop über die Charakterisierung von feinteiligen und porösen Festkörpern N2 - Leichte Gesteinskörnungen mit Kornrohdichten < 2 g/cm³ werden industriell aus natürlichen Rohstoffen, wie Ton und Schiefer, hergestellt. Dabei fallen hohe Energiekosten an, während außerdem fortwährend die Verfügbarkeit geeigneter Rohstoffe sinkt. Eine Alternative stellen Leichtgranulate, die aus mineralischen Bau- und Abbruchabfällen hergestellt werden, dar. Im Forschungsprojekt „Aufbaukörnungen“ wurde eine Technologie zur Herstellung hochwertiger leichter Gesteinskörnungen aus Mauerwerkbruch entwickelt. Ziegelhaltige Bau- und Abbruchabfälle fallen in Deutschland mit bis zu 26 Mio. t pro Jahr an und weisen größere Verwertungsdefizite als Betonbruch auf. Der neuen Verwertungsstrategie liegt die Idee des rohstofflichen Recyclings zu Grunde. Die leichten Gesteinskörnungen werden am Ende eines mehrstufigen Herstellungsprozesses durch thermische oder hydrothermale Erhärtung im Labor- und halbtechnischen Maßstab produziert. Für Herstellungstechnologie und Eigenschaften der Leichtbetone sind neben Kornfestigkeit und Rohdichte die Porosität und Wasseraufnahme der leichten Gesteinskörnungen entscheidende Größen, die wiederum von Kornform, Oberflächenrauigkeit, Sinterschale und Porenstruktur der Körnungen beeinflusst werden. T2 - XVI. Porotec-Workshop über die Charakterisierung von feinteiligen und porösen Festkörpern CY - Bad Soden, Germany DA - 13.11.2012 PY - 2012 AN - OPUS4-27160 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Daum, Werner A1 - Tkachenko, Viktoriya A1 - Habel, Wolfgang T1 - Sensitive pultrudierte Tragwerke T2 - 2. TSB-TransferTreff "Materialeffizienz und Gestaltung" N2 - - Innovative Konstruktionskonzepte für den Leichtbau verwenden neue Material-Kombinationen - Erweiterte Anwendung der Sensortechnik bei der Entwicklung neuer Materialen - Integration von Sensoren in die Struktur, um synergetische Effekte effizienter auszunutzen und Eigenschaften zu steuern T2 - 2. TSB-TransferTreff "Materialeffizienz und Gestaltung" CY - Berlin, Germany DA - 11.06.2012 PY - 2012 AN - OPUS4-26464 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Karafiludis, Stephanos A1 - Stawski, Tomasz T1 - Trash to treasure: recovery of transition metal phosphates for (electro-)catalytical applications N2 - Wastewaters containing high concentrations of NH4+, PO43- and transition metals are environmentally harmful and toxic pollutants. At the same time phosphorous and transition metals constitute valuable resources. Here, we report the synthesis routes for Co- and Ni-struvites (NH4MPO4∙6H2O, M = Ni2+, Co2+) out of aqueous solutions resembling synthetic/industrial waste water compositions, and allowing for P, ammonia and metal co-precipitation. Furthermore, the as-obtained struvites were further up-cycled. When heated, these transition metal phosphates (TMPs) demonstrate significant changes in the degree of crystallinity/coordination environment involving a high amount of amorphous phases and importantly develop mesoporosity (Figure 1). In this regard, amorphous and mesoporous TMPs are known to be highly promising (electro-)catalysts. Amorphous phases do not represent a simple “disordered” crystal but more a complex system with a broad range of compositions and physicochemical properties, which remain mostly unknown. Consequently, we investigated the recrystallization and amorphization process during thermal treatment and a resolved the complex amorphous/crystalline structures (Figure 2). As a proof-of-principle for their applicational use, the as-obtained TMPs demonstrate significant proton conductivity properties similar to apatite-like structures from room to high temperatures (>800°C). Hence, we have developed a promising recycling route in which environmental harmful contaminants like PO43-, NH4+ and 3d metals would be extracted out of waste waters in the form of precursor raw materials. These raw materials can be then further up-cycled through a simple thermal treatment for their specific application in electrocatalysis. T2 - Goldschmidt Conference 2022 CY - Hawai'i, USA DA - 10.07.2022 KW - Mesoporosity KW - Amorphous phases KW - Transition metals KW - Struvite KW - Phosphates PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-552852 UR - https://conf.goldschmidt.info/goldschmidt/2022/meetingapp.cgi/Paper/9501 AN - OPUS4-55285 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mishurova, Tatiana A1 - Evsevleev, Sergei A1 - Mehta, Bharat A1 - Nyborg, L. A1 - Virtanen, E. A1 - Markötter, Henning A1 - Hryda, E. A1 - Bruno, Giovanni T1 - Failure Mechanisms Investigation by Means of in-situ Synchrotron Computed Tomography in Aluminum MMC-based Alloy Tailored for Additive Manufacturing (AM) N2 - Most of the Al alloys used in additive manufacturing (AM), in particular Laser Powder Bed Fusion (LPBF), do not exceed a strength of 200 MPa, whereas conventionally high-performance alloys exhibit strengths exceeding 400 MPa. The availability of such Al alloys in AM is limited due to difficulties in printability, requiring synergetic material and AM process development to satisfy harsh processing conditions during LPBF [1]. One approach is the addition of reinforcement to the based powder, allowing tailoring composition and properties of a Metal Matrix Composite (MMC) by AM. Still, the effect of the reinforcement on the resulting mechanical properties must be studied to understand the performance and limits of the newly developed material. The goal of this work was to investigate the failure mechanism of LPBF Al-based MMC material using in-situ Synchrotron X-ray Computed Tomography (SXCT) during mechanical testing. T2 - International conference on tomography of material and structures CY - Grenoble, France DA - 27.06.2022 KW - Additive manufacturing KW - Laser powder bed fusion KW - Al alloy KW - MMC PY - 2022 AN - OPUS4-55228 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bruno, Giovanni A1 - Mishurova, Tatiana A1 - Evlevleev, Sergei A1 - Khrapov, D. A1 - Meinel, Dietmar A1 - Surmenev, R. A1 - Surmeneva, M. A1 - Koptyug, A. T1 - Procedures to Quantitatively Characterize Morphological Features of Triply Periodic Minimal Surface Structures N2 - Additively manufactured (AM) metallic sheet-based Triply Periodic Minimal Surface Structures (TPMSS) meet several requirements in both bio-medical and engineering fields: Tunable mechanical properties, low sensitivity to manufacturing defects, mechanical stability, and high energy absorption. However, they also present some challenges related to quality control. In fact, the optimization of both the AM process and the properties of TPMSS is impossible without considering structural characteristics as manufacturing accuracy, internal defects, and as well as surface topography and roughness. In this study, the quantitative non-destructive analysis of TPMSS manufactured from Ti-6Al-4V alloy by electron beam melting was performed by means of laboratory X-ray computed tomography (XCT). T2 - International conference on tomography of material and structures 2022 CY - Grenoble, France DA - 27.06.2022 KW - Additive manufacturing KW - Scaffold KW - Lightweight structures KW - Computed tomography PY - 2022 AN - OPUS4-55229 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tavernaro, Isabella A1 - Chaudhary, A. A1 - Resch-Genger, Ute T1 - Development of amorphous silica particle based reference materials for surface functional group quantification N2 - Functionalized nanomaterials (NM) with their unique size-dependent properties are of increasing relevance for current and future developments in various fields such as medical and pharmaceutical industry, computing, electronics or food and consumer products. The performance and safety of NM are determined by the sum of their intrinsic physicochemical properties.1 Besides other key parameters, the particle surface chemistry, which is largely controlled by the chemical nature and density of functional groups and ligands, must be considered for a better performance, stability, and processibility of NM, as well as their interaction with the environment. Thus, particle standards with well-designed surfaces and methods for functional group quantification can foster the sustainable development of functional and safe(r) NM.2 Here we provide a brief overview of the ongoing research in division Biophotonics to design tailored amorphous silica reference particles with bioanalytically relevant functional groups and ligands, for the development of standardized and validated surface functional group quantification methods. T2 - Workshop NanoRiskSD project CY - Berlin, Germany DA - 09.06.2022 KW - Nanoparticle KW - Surface analysis KW - Silica KW - Fluorescence KW - Assay PY - 2022 AN - OPUS4-55004 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mishurova, Tatiana A1 - Serrano Munoz, Itziar A1 - Markötter, Henning A1 - Mehta, Bharat A1 - Hryha, Eduard A1 - Bruno, Giovanni T1 - In-situ imaging of additively manufactured alloys at the BAMline N2 - In this work, we present the recent in-situ imaging developments at the BAMline (of synchrotron BESSY II, HZB), focused on the in-situ characterization and understanding of microstructural evolution of additively manufactured materials subjected to different environments. Two show cases are presented. In the first, X-ray refraction radiography (SXRR) was combined with in-situ heat treatment to monitor the microstructural evolution as a function of temperature in a laser powder bed fusion (LPBF) manufactured AlSi10Mg alloy. We show that SXRR allows detecting the changes in the Si-phase morphology upon heating using statistically relevant volumes. SXRR also allows observing the growth of pores (i.e., thermally induced porosity), usually studied via X-ray computed tomography (XCT), but using much smaller fields-of-view. In the second case study, XCT was combined with in-situ tensile test to investigate the damage mechanism in a LPBF Aluminum Metal Matrix Composite (MMC). In-situ SXCT test disclosed the critical role of the defects in the failure mechanism along with pre-cracks in the reinforcement phase of MMC. We found that cracks were initiated from lack-of-fusion defects and propagated through coalescence with other defects. T2 - New Frontiers in Materials Design for Laser Additive Manufacturing CY - Montabaur, Germany DA - 22.05.22 KW - Additive manufacturing KW - Laser powder bed fusion KW - Synchrotron X-ray computed tomography KW - Synchrotron X-ray Refraction PY - 2022 AN - OPUS4-54900 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Linberg, Kevin A1 - Röder, Bettina A1 - Al-Sabbagh, Dominik A1 - Emmerling, Franziska A1 - Michalchuk, Adam T1 - Polymorphism in molecular cocrystals controlled by variable temperature ball milling N2 - Mechanochemistry offers a unique opportunity to modify or synthesize new crystal forms. Although the method is very promising, little is known about the mechanochemical means to control the synthesis of a solid form. Using an polymorphic organic cocrystal system, we show here that mechanochemistry can be used to obtain a polymorph transformation under the apparently conventional (thermal) transition point. T2 - Bessy User Meeting 2022 CY - Online meeting DA - 08.12.2022 KW - Mechanochemistry KW - Polymorphism KW - TRIS PY - 2022 AN - OPUS4-56473 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tielemann, Christopher A1 - Reinsch, Stefan A1 - Müller, Ralf T1 - Oriented Surface Crystallization N2 - Up to now, oriented surface crystallization phenomena are discussed controversially, and related studies are restricted to few glasses. For silicate glasses we found a good correlation between the calculated surface energy of crystal faces and oriented surface nucleation. Surface energies were estimated assuming that crystal surfaces resemble minimum energy crack paths along the given crystal plane. This concept was successfully applied by Rouxel in calculating fracture surface energies of glasses. Several oriented nucleation phenomena can be herby explained assuming that high energy crystal surfaces tend to be wetted by the melt. This would minimize the total interfacial energy of the nucleus. Furthermore, we will discuss the evolution of the microstructure and its effect on the preferred crystal orientation. T2 - 26th International Congress on Glass CY - Berlin, Germany DA - 03.07.2022 KW - Glass KW - Surface energy KW - Crystal orientation PY - 2022 AN - OPUS4-56074 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - del Giorgio, Elena A1 - Kumari, P. A1 - Lymer, K. A1 - Connell, S. A1 - Zhang, S. A1 - Hodoroaba, Vasile-Dan A1 - Pikramenou, Z. T1 - Visible and NIR emissive lanthanide(III) surfaces for new luminescent materials N2 - Luminescent lanthanides(III) offer exceptional optical properties that can overcome issues often encountered with other fluorophores (e.g. organic dyes). Their long lifetimes up to milliseconds, low photobleaching and sharp and characteristic emission peaks make the lanthanides extremely valuable for the development of advanced luminescent materials. Previous work on Ru(II) and Ir(III) gold surfaces further highlights the potential of employing the luminescence of metal complexes for the fabrication of sensing platforms and devices. Here, we incorporate visible and NIR-emitting lanthanide(III) complexes Ln2L3 (Ln = Eu(III), Nd(III), Yb(III)) to gold and plasmonic surfaces, translating the unique optical properties of the lanthanides(III) to practical devices. The Ln2L3 complexes are deposited on the surfaces with different methods, ranging from polymer aided physisorption to the covalent attachment on the gold surface. Furthermore, we exploit the high sensitivity to the coordination environment of lanthanides(III) to design and prepare a sensing platform. T2 - 17th Conference on Methods and Applications in Fluorescence (MAF 2022) CY - Göteborg, Sweden DA - 11.09.2022 KW - Luminescent materials KW - Lanthanide(III) KW - Surface morphology KW - AFM KW - SEM/EDS PY - 2022 UR - https://maf2022.com/ AN - OPUS4-56126 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Konert, Florian A1 - Nietzke, Jonathan A1 - Sobol, Oded A1 - Schütz, S. A1 - Böllinghaus, Thomas T1 - Application of an in-situ H2Test Method N2 - The degradation effect of hydrogen on the mechanical properties of steels is well known, but still not sufficiently understood. The fast and safe market ramp up of hydrogen technologies makes it evident to evaluate a wider understanding of this topic. In general it is often described as hydrogen embrittlement. Therefore it is desirable to achieve a test method which is able to provide material properties under hydrogen atmosphere in an easy way. Currently mechanical tests under hydrogen atmosphere are executed in autoclaves. For this technique complex hardware is needed, therefore tests are expensive and test capacities are only available in a small scale. The shown test method promises a trendsetting approach for reducing costs and machine time by using hollow specimen. T2 - 4th International Conference on Metals and Hydrogen - Steely & Hydrogen 2022 CY - Ghent, Belgium DA - 11.10.2022 KW - Hydrogen KW - Hollow specimen KW - In-situ KW - Test procedure PY - 2022 AN - OPUS4-56032 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mishurova, Tatiana A1 - Evsevleev, Sergei A1 - Mehta, B. A1 - Nyborg, L. A1 - Virtanen, E. A1 - Markötter, Henning A1 - Hryha, E. A1 - Bruno, Giovanni T1 - Failure Mechanisms Investigation by Means of in-situ Synchrotron Computed Tomography in Aluminum MMC-based Alloy Tailored for Additive Manufacturing (AM) N2 - The availability of high-performance Al alloys in AM is limited due to difficulties in printability, requiring both the development of synergetic material and AM process to mitigate problems such as solidification cracking during laser powder bed fusion (LPBF). The goal of this work was to investigate the failure mechanism in a LPBF 7017 Aluminium alloy + 3 wt% Zr + 0.5 wt% TiC. The processing leads to different categories of Zr-rich inclusions, precipitates and defects. T2 - Alloys for Additive Manufacturing Symposium 2022 (AAMS22) CY - Munich, Germany DA - 11.09.2022 KW - Additive manufacturing KW - Laser powder bed fusion KW - Synchrotron X-ray computed tomography KW - MMC PY - 2022 AN - OPUS4-56110 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Naik, Aakash Ashok A1 - George, Janine T1 - New descriptors for materials properties based on bonding indicators N2 - Includes a summary of the Ph.D. project that deals with generating a database populated with materials bonding properties and how we intend to gain deeper insights into material properties through this research. T2 - SALSA 2022 CY - Berlin, Germany DA - 15.09.2022 KW - Bonding analysis KW - Automation KW - Materials Informatics KW - Computational Chemistry PY - 2022 AN - OPUS4-56142 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - von Rüden, H. A1 - Meinel, Dietmar A1 - Fritsch, Tobias T1 - Röntgen-Computertomographie (CT) für die Kulturguterhaltung N2 - Als bildgebendes und zerstörungsfreies Verfahren eignet sich die Röntgen-Computertomographie (CT) insbesondere bei der Untersuchung von Kunst- und Kulturgütern. Die für Werkstoffprüfung und Materialanalyse konzipierten CT-Anlagen bieten dank hoher Röntgenleistung die Möglichkeit zusätzlich zu Holz, Keramiken und Kunststoffen auch stark schwächende Materialien, wie bspw. Metalle, zu durchdringen. Für eine hohe räumliche Auflösung im unteren Mikrometerbereich (2-200µm) sorgen entsprechend ausgelegte CT-Anlagen. In der Bundesanstalt für Materialforschung und -prüfung (BAM) stehen mehrere solcher CT-Anlagen für unterschiedliche Fragestellungen sowie Probengrößen und - materialien zur Verfügung. Einige Beispiele aus den vergangenen Arbeiten der BAM veranschaulichen das große Potential dieser Untersuchungsmethode. Da bei einer CT-Messung in der Regel das gesamte Untersuchungsobjekt erfasst und in ein digitales Volumenmodell überführt wird, eröffnet sich für Archäologen und Restoratoren die Möglichkeit Untersuchungen hinsichtlich Materialzusammensetzung, Erhaltungszustand und Herstellungstechnik am virtuellen Objekt vorzunehmen, ohne die Originalsubstanz zu beeinträchtigen. Gegenüber der klassischen Radiografie, bei der nur eine zweidimensionale Abbildung erreicht wird, bietet die CT-Untersuchung die Möglichkeit innenliegende Strukturen dreidimensional zu erfassen. Die notwendige Bestimmung der Objektoberfläche erlaubt zudem die Erstellung eines Oberflächenmodells des untersuchten Gegenstandes. Damit lassen sich unter anderem mechanische Simulationen (Belastung, Durchbiegung, Durchströmung) durchführen. Der erzeugte Datensatz kann somit auch zur Herstellung eines Replikats im 3D-Druckverfahren genutzt werden. Anhand der Untersuchung der Mandoline von Smorsone wird gezeigt, wie eine CT-Messung durchgeführt wird und wie in dem anschließend rekonstruierten 3D-Datensatz mittels Koordinatenmesstechnik Maße (Abstände, Wandstärken, Winkel) exakt ermittelt werden können. T2 - Jahrestagung der Gesellschaft für Musikforschung CY - Berlin, Germany DA - 28.09.2022 KW - Mikro-CT KW - Bildverarbeitung KW - Holz KW - Bronze KW - ZfP PY - 2022 AN - OPUS4-56412 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Karafiludis, Stephanos A1 - Kochovski, Z. A1 - Retzmann, Anika A1 - Scoppola, E. A1 - Emmerling, Franziska A1 - Stawski, Tomasz T1 - How do transition metal phosphates crystallise? N2 - Industrial and agricultural waste streams (waste waters, sludges, tailings etc.), which contain high concentrations of NH4+, PO43- and transition metals, are environmentally harmful due to their toxic pollutants. At the same time, phosphorus and selective transition metals such as Cobalt could be potentially depleted as a critical raw material due to the high demand and rapidly declining natural ore deposits. Therefore, due to simultaneous scarcity and abundance, the phosphorus and 3d metal recovery from agricultural, industrial, mining, or urban wastewaters have been an important factor in sustaining our global consumption and preservation of the natural environment. Typically, separate pathways have been considered to extract hazardous substances such as transition metals or phosphate, independently from each other. Here, we investigate the crystallization of transition metal phosphate (TMP) compounds (NH4MPO4∙6H2O, M3(PO4)2∙8H2O with M = Ni2+, Co2+, NixCo1-x2+ M-struvite and M-phosphate octahydrate) out of aqueous solutions, which allow for P, ammonia and metal co-precipitation. The precipitation of these compounds from industrial and agricultural waste waters has high potential as a P- and 3d metal recovery route. For this purpose, a detailed understanding of the crystallization process beginning from combination of solved ions and ending in a final crystalline product is required. Through adjusting the reaction conditions, the stability, crystallite size and morphology of the as-obtained TMPs could be controlled. Detailed investigations of the precipitation process in time using ex- and in-situ techniques provided new insights into their non-classical crystallization mechanism/crystal engineering of these materials. These TMPs involve transitional colloidal nanophases during the crystallization process. Over time, their complex amorphous framework changes significantly resulting simultaneously in an agglomeration and densification of the compound. After extended reaction times these colloidal nanophases condensed to a final crystal. However, the reaction kinetics of the formation of a final crystalline product and the lifetime of these intermediate phases vary significantly depending on the metal cation involved in the precipitation process. Ni-struvite is stable in a wide reactant concentration range and at different metal/phosphorus (M/P)-ratios, whereas Co tends to form Co-struvite and/or Co-phosphate octahydrate depending on the (M/P)-ratio. The mixed NixCo1-x system shows a significantly different crystallization behavior and reaction kinetics of the precipitation compared to the pure endmembers. The observed various degree of stability could be linked to the octahedral metal coordination environment in these compounds. The achieved level of control over the precipitates, is highly desirable for 3d- and P-recovery methods. Under this paradigm, the crystals can be potentially upcycled as precursor materials for (electro)catalytical applications. T2 - Granada Münster Discussion Meeting (GMDM) CY - Granada, Spain DA - 30.11.2022 KW - Struvite KW - Transition metal KW - Phosphates KW - Amorphous phases KW - Non-classical crystallization PY - 2022 AN - OPUS4-56478 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Karafiludis, Stephanos A1 - Kochovski, Z. A1 - Scoppola, E. A1 - Emmerling, Franziska A1 - Stawski, Tomasz T1 - Crystallization study of transition metal phosphates: a new example for non-classical crystallization theory N2 - Industrial and agricultural waste streams (waste waters, sludges, tailings etc.), which contain high concentrations of NH4+, PO43- and transition metals, are environmentally harmful due to their toxic pollutants. At the same time, phosphorus and selective transition metals such as Cobalt could be potentially depleted as a critical raw material due to the high demand and rapidly declining natural ore deposits. Therefore, due to simultaneous scarcity and abundance, the phosphorus and 3d metal recovery from agricultural, industrial, mining, or urban wastewaters have been an important factor in sustaining our global consumption and preservation of the natural environment. Typically, separate pathways have been considered to extract hazardous substances such as transition metals or phosphate, independently from each other. Here, we report the synthesis routes for transition metal phosphate (TMP) compounds (M3(PO4)2∙8H2O, NH4MPO4∙6H2O, M = Ni2+, Co2+, NixCo1-x2+ M-struvite and M-phosphate octahydrate), which allow for P, ammonia and metal co-precipitation. The precipitation of these compounds from industrial and agricultural waste waters could be a promising P-recovery route. Through adjusting the reaction conditions, the stability, crystallite size and morphology of the as-obtained TMP could be controlled. Detailed investigations of the precipitation process using ex- and in-situ techniques provided new insights into their non-classical crystallization mechanism/crystal engineering of these materials. These TMPs involve transitional colloidal nanophases which subsequently aggregate and condense to final crystals after extended reaction times. However, the reaction kinetics of the formation of a final crystalline product vary significantly depending on the metal cation involved in the precipitation process. Ni-struvite is stable in a wide reactant concentration range and at different metal/phosphorus (M/P)-ratios, whereas Co tends to form Co-struvite and/or Co-phosphate octahydrate depending on the (M/P)-ratio. The mixed NixCo1-x system shows a significantly different crystallization behavior and reaction kinetics of the precipitation compared to the pure endmembers. The observed various degree of stability could be linked to the octahedral metal coordination environment in these compounds. The achieved level of control over the precipitates, is highly desirable for 3d- and P-recovery methods. Under this paradigm, the crystals can be potentially upcycled as precursor materials for (electro)catalytical applications. T2 - Adlershofer Forschungsforum 2022 CY - Berlin, Gemany DA - 11.11.2022 KW - Transition metal KW - Phosphates KW - Non-classical crystallization KW - In-situ SAXS/WAXS KW - Cryo-TEM PY - 2022 AN - OPUS4-56479 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Waurischk, Tina A1 - Reinsch, Stefan A1 - Müller, Ralf A1 - Meyer, Christian A1 - Diegeler, A. A1 - Sorg, J. A1 - Schottner, G. A1 - Wondraczek, L. A1 - Sierka, M. A1 - Deubener, J. T1 - Data-driven Workflow for Accelerated Glass Development (GlasDigital) N2 - As part of a joint project involving the Fraunhofer Institute for Silicate Research (ISC), the Friedrich Schiller University of Jena, the Clausthal University of Technology and the Federal Institute for Materials Research and Testing (BAM), digital tools are to be created for the development of new types of glass materials. Current processes for the production of glasses with improved properties are usually very cost- and energy-intensive due to the low degree of automation and are subject to long development cycles. The use of robotic synthesis processes in combination with self-learning machines is intended to overcome these problems in the long term. The development of new types of glass can then not only be accelerated considerably, but also be achieved with much less effort. In this talk, data generation via a robotic high-throughput glass melting system is presented, which should be the experimental basis for the ontology developed within the project GlasDigital. T2 - Materials Science and Engineering Congress (MSE 2022) CY - Darmstadt, Germany DA - 27.09.2022 KW - Oxidglas KW - Robotische Glasschmelzanlage PY - 2022 AN - OPUS4-56489 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Waurischk, Tina A1 - Reinsch, Stefan A1 - Müller, Ralf A1 - Chen, Y.-F. A1 - Contreras Jaimes, A. T1 - Datengetriebener Workflow für die beschleunigte Entwicklung von Glas (GlasDigital) N2 - Das Projekt GlasDigital wurde im allgemeinen vorgestellt, sowie die einzelnen Zwischenstände der verschiedenen Arbeitspakete aller Projektpartner präsentiert. Die allgemeine Porjektvorstellung ist auf deutsch. Die Zwischenstände der Arbeitsinhalte sind auf englisch. T2 - PMD Vollversammlung CY - Berlin, Germany DA - 03.11.2022 KW - Oxidglas KW - Robotische Glasschmelzanlage KW - ML KW - Ontologie KW - Digitaler Zwilling KW - Bildanalyse PY - 2022 AN - OPUS4-56491 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schneider, M. A1 - Schlingmann, T. A1 - Schmidt, J. A1 - Bettge, Dirk A1 - Hilgenberg, Kai A1 - Binder, M. A1 - Klöden, B. T1 - A Round Robin Test To Investigate The Printing Quality Of PBF LB/M Processed AlSi10Mg N2 - When it comes to higher accuracies, new technologies and real applications in additive manufacturing, there is one topic which cannot be avoided: The material response on the chosen processing parameters and its agreement and correspondence with literature data of the wrought material grade counterpart. In industrial Additive Manufacturing (AM) standards in terms of printing parameters, protection gas atmospheres or powder handling instructions are not obligatory. Therefore, the question must be answered whether the AM process is reproducible and reliable over different printing companies. This was the motivation to realize a round robin test between 8 European printing companies and academic partners. The consortium had printed and tested fatigue and tensile testing bars under plant-specific conditions. A commonly used cast aluminum alloy, AlSi10Mg, was chosen as test material for the PBF-LB/M process. Differences of the results between the partners and the scatter itself were discussed in detail. T2 - World PM2022 CY - Lyon, France DA - 09.10.2022 KW - Additive manufacturing KW - AlSi10Mg KW - Laser powder bed fusion KW - Round robin KW - Reproducibility PY - 2022 AN - OPUS4-56303 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Epperlein, Martin A1 - Poka, Konstantin A1 - Hilgenberg, Kai T1 - QI-Digital - Qualitätssicherung für die Additive Fertigung N2 - Für die konventionelle Fertigung hat sich das bestehende System der Qualitätsinfrastruktur (QI) bewährt. Die additive Fertigung vergrößert den gestalterischen Spielraum von möglichen Bauteilgeometrien und Prozessfehlern jedoch erheblich. Hier gerät die QI an ihre Grenzen, sodass die Fertigung und Zulassung sicherheits-relevanter Bauteile sehr zeit- und kostenintensive Versuche erfordern. Eine moderne digitale QI erlaubt eine effizientere Qualitätssicherung für additiv gefertigte Bauteile. Dies erfordert eine durchgängig digitale Abbildung des physischen Materialflusses. T2 - QI-Forum CY - Berlin, Germany DA - 11.10.2022 KW - Additive Fertigung KW - Qualitätssicherung KW - Digitalisierung PY - 2022 AN - OPUS4-56382 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Merz, Benjamin A1 - Mohr, Gunther A1 - Hilgenberg, Kai T1 - Position Detection for Hybrid Repair of gas turbine blades using PBF-LB/M N2 - This poster presents a workflow for camera-based position detection of components within PBF-LB/M machines. This enables a hybrid repair process of highly stressed components such as gas turbine blades using PBF-LB/M. T2 - Kuratoriumsführung CY - Berlin, Germany DA - 21.06.2022 KW - Additive Manufacturing KW - PBF-LB/M KW - Position detection KW - Camera KW - Image processing PY - 2022 AN - OPUS4-56587 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Shakeel, Y. A1 - Soysal, M. A1 - Vitali, E. A1 - Ost, P. A1 - Aversa, R. A1 - Ávila Calderón, Luis Alexander A1 - Engstler, M. A1 - Fell, J. A1 - Fritzen, F. A1 - Hermmann, H.-G. A1 - Laadhar, A. A1 - Olbricht, Jürgen A1 - Pauly, C. A1 - Roland, M. A1 - Skrotzki, Birgit T1 - NFDI-MatWerk - Reference Datasets N2 - Within NFDI-MatWerk (“National Research Data Infrastructure for Material Sciences”/ “Nationale Forschungsdateninfrastruktur für Materialwissenschaften und Werkstofftechnik“), the Task Area Materials Data Infrastructure (TA-MDI) will provide tools and services to easily store, share, search, and analyze data and metadata. Such a digital materials environment will ensure data integrity, provenance, and authorship. The MatWerk consortium aims to develop specific solutions jointly with Participant Projects (PPs), which are scientific groups or institutes covering different domains, from theory and simulations to experiments. The Data Exploitation Methods group of the Karlsruhe Institute of Technology-Steinbuch Centre of Computing, as part of TA-MDI, is developing specific solutions in close collaboration with three PPs. PP07, together with the University of Stuttgart, aims at the image-based prediction of the material properties of stochastic microstructures using large-scale supercomputers. PP13, in cooperation with the University of Saarland, focuses on tomographic methods at various scales in materials research. PP18, together with the Federal Institute for Materials Research and Testing (“Bundesanstalt für Materialforschung und -prüfung”), aspires to define the criteria for materials reference datasets and usage analytics. The requirements and goals are comparable for each PP: their research outputs, which are scientific datasets, should conform to the FAIR (Findable, Accessible, Interoperable, Reusable) principles. We aim to shape them from a data management perspective making use of the FAIR Digital Object concept, including structured metadata and storage solutions. The results will be a blueprint which will act as a reference for future datasets. Even though the collaboration is in an early stage, the initial steps already show the added value of this approach. This research has been supported by the Federal Ministry of Education and Research (BMBF) – funding code M532701 / the Deutsche Forschungsgemeinschaft (DFG, German Research Foundation) - project number NFDI 38/1, project no. 460247524. T2 - HMC Conference 2022 CY - Online meeting DA - 05.10.2022 KW - NFDI KW - NFDI-MatWerk KW - Reference Data KW - FAIR KW - Creep PY - 2022 AN - OPUS4-56611 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Feiler, Torvid A1 - Bhattacharya, Biswajit A1 - Michalchuk, Adam A1 - Rhim, S.-Y. A1 - Schröder, V. A1 - List-Kratochvil, E. A1 - Emmerling, Franziska T1 - Mechanically plastic molecular crystals for shapeable optic waveguides N2 - Molecular crystalline materials are usually brittle and are prone to breaking when mechanically stressed. This fragility greatly limits they application in next the generation of adaptable, functional materials. The recent discovery of mechanical compliancy in molecular crystals has solved this problem.1 Based on the nature of the deformation, molecular crystals can be divided into being plastically (irreversibly) or elastically (reversibly) bendable. The plastic deformation is generally associated with anisotropic molecular arrangements and the existence of low energy slip planes which allow a permanent motion within the lattice. Here we report 4-bromo-6-[(6-chloropyridin-2-ylimino)methyl]phenol (CPMBP) as a promising candidate for future waveguide technologies.2 CPMBP has been found to have two different polymorphs with distinct optical and mechanical properties. The brittle crystals of Form I exhibits very weak emission at 605 nm (λex = 425 nm; photoluminescence quantum yield Φ = 0.4 %). In contrast, Form II has a large plastic regime together with a bright emission at 585 nm (λex = 425 nm; Φ = 8.7 %). Taking advantage of the favorable mechanical flexibility and optical properties, Form II was used as a shapeable optical waveguide. By changing the wavelength of the light source, active or passive waveguiding can be realized. CPMBP could thus be used as a flexible wavelength filter. T2 - 30. Jahrestagung der Deutschen Gesellschaft für Kristallographie CY - Online meeting DA - 14.3.2022 KW - Flexible crystals KW - Polymorphism KW - Waveguide PY - 2022 AN - OPUS4-54514 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Yu, C.-H. A1 - Sprengel, Maximilian A1 - Schröder, Jakob A1 - Serrano Munoz, Itziar A1 - Mohr, Gunther A1 - Evans, Alexander A1 - Kromm, Arne A1 - Peng, R. L. A1 - Kannengießer, Thomas A1 - Bruno, Giovanni A1 - Moverare, J. T1 - Distribution of subsurface residual stress as a function of wall thickness in stainless steel 316L LPBF structures N2 - The subsurface residual stress in laser powder bed fused 316L structures was analyzed using X-ray diffraction (XRD) and layer removal. The influence of varying structure thicknesses was investigated. In this study the importance of combining surface roughness measurements with XRD was shown. Moreover, a clear relation between the structure thickness and the subsurface residual stress profiles was observed. T2 - The 11th International Conference on Residual Stress CY - Nancy, Frankreich DA - 28.03.2022 KW - AGIL KW - Residual Stress KW - X-ray Diffraction KW - Additive Manufacturing PY - 2022 AN - OPUS4-54581 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lohrer, Christian T1 - Fachbereich 2.5 Konformitätsbewertung Explosivstoffe/Pyrotechnik N2 - Vorstellung der aktuellen Aufgaben und Tätigkeiten des FB 2.5 Konformitätsbewertung Explosivstoffe/Pyrotechnik T2 - 43. Informationstagung Sprengtechnik CY - Siegen, Germany DA - 22.04.2022 KW - Benannte Stelle KW - Konformitätsbewertung KW - Normung KW - FE KW - Beratung Behörden/Ministerien PY - 2022 AN - OPUS4-54688 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lohrer, Christian T1 - Forschungsschwerpunkte im Fachbereich 2.5 Konformitätsbewertung Explosivstoffe/Pyrotechnik N2 - Vorstellung der aktuellen Forschungsthemen mit Bezug zu Explosivstoffen und pyrotechnischen Gegenstände T2 - 43. Informationstagung Sprengtechnik CY - Siegen, Germany DA - 22.04.2022 KW - Alterung von Pyrotechnik KW - Sprengplattieren KW - Fallhammer KW - Zünder PY - 2022 AN - OPUS4-54689 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lohrer, Christian T1 - Fachbereich 2.5 Konformitätsbewertung Explosivstoffe/Pyrotechnik N2 - Vorstellung der Kernaufgaben Konformitätsbewertung Explosivstoffe und pyrotechnische Gegenstände und Hauptaktiviäten in diesem Sektor T2 - 42. Informationstagung Sprengtechnik CY - Siegen, Germany DA - 15.10.2021 KW - Explosivstoffe KW - Pyrotechnik KW - Normung KW - Konformitötsbewertung KW - Politikberatung PY - 2021 AN - OPUS4-54396 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Stargardt, Patrick A1 - Junge, P. A1 - Greinacher, M. A1 - Kober, D. A1 - Mieller, Björn T1 - Bulk vs thermal sprayed alumina for insulation applications: A comparison of electrical and dielectrical properties N2 - Additive manufacturing (AM) processes are opening new design possibilities for large scale electrical devices such as power generators. Conventional manufacturing methods use copper rods which are wrapped, vacuum impregnated, bend and welded. These processes are labor-intensive and time-consuming. The introduction of AM methods for manufacturing the copper conductor and electrical insulation can reduce the size of the generator head, the most complex part of the generator. In this study, the electrical and dielectrical properties of additively deposited ceramic layers are investigated and compared with the properties of conventionally fabricated bulk ceramics. The ceramic layers are thermally deposited by atmospheric plasma spraying of a commercially available alumina powder. Bulk ceramics are fabricated by dry pressing and sintering of the same powder. Microstructure and porosity were analyzed by scanning electron microscopy (SEM). Electrical and dielectrical properties such as DC resistance, dielectric strength, dielectric loss, and relative permittivity were determined according to the standards. The microstructures of sprayed and sintered alumina show significant differences with respect to grain form and porosity. The density of the bulk ceramic is lower than the density of the sprayed layer due to the coarse particle size (d50 = 33 μm). Therefore, data from dense samples of the same chemical composition but lower particle size alumina powder were used for comparison. T2 - Keramik 2022 CY - Online meeting DA - 07.03.2022 KW - High Voltage Insulation KW - Thermal Spray KW - Dielectric Spectroscopy KW - Atmospheric Plasma Spraying PY - 2022 AN - OPUS4-54446 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kang, M. A1 - Czasny, M. A1 - Kober, D. A1 - Reschetnikow, A. A1 - Stargardt, Patrick A1 - Mieller, Björn A1 - Gurlo, A. T1 - Influence of mica particle content in composites for high voltage applications produced by additive manufacturing and mold casting N2 - The insulation system of high voltage electrical devices like generators and electrical motors has to withstand thermal, electrical, ambient and mechanical influences (TEAM) during operation. Especially the dielectric properties have to satisfy the requirements also under elevated temperatures and extreme environments. To provide this high quality, the conventional fabrication process uses partly manually applied insulation tapes combined with a cost-intensive and under safety concerns at least problematic vacuum pressure impregnation step (VPI). In order to reduce process costs by increasing the degree of automation and avoiding the VPI process, additively manufactured (AM) insulations were studied. This study focuses on the fabrication of ceramic/polymer compounds via AM technique. The AM technology used a rotating screw extrusion print head with air pressure to supply the paste. Plate-like samples with dimensions of 55 mm x 55 mm x1mm thickness were produced. This work focuses on the homogeneously high viscous paste with 12.5 to 50 volume % ratio of filler particles. Three types of mica powders as ceramic filler materials with different particle sizes from micro to mm scale were evaluated. The controlled volume % ratio of particles affects the paste viscosity which enables stacking of paste layers with a viscosity close to clay pastes. The mixed pastes were cured by heating and UV light to increase mechanical properties. A TG/DTA was performed, and electrical properties were investigated. First experiments with respect to the dielectric properties such as volume resistance, permittivity and dielectric strength revealed promising results and the possibility to use AM techniques for the fabrication of high voltage insulations for electrical machines. T2 - MaterialsWeek 2021 CY - Online meeting DA - 07.09.2021 KW - HV-Insulation KW - Polymer-Ceramic-Composite KW - Additive manufacturing PY - 2021 AN - OPUS4-54368 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Carstensen, Niels A1 - Schirdewahn, S. A1 - Merklein, M. A1 - Hilgenberg, Kai T1 - Generation of Tribosystems by Additive Surface Treatment on Tool Steel Substrate N2 - Laser implantation aims at reducing friction and wear on highly stressed surfaces in forming processes. Especially the hot stamping process that is used as a resource efficient process for manufacturing geometrical complex and high-strength structures, exhibits severe wear and high friction during the forming operation. The laser implantation process addresses this problem by combining two different approaches (surface modification and surface structuring) in surface technology by creating elevated, highly wear-resistant micro-features to influence the tribological performance. Pure TiB2 implants have shown to reduce tool-sided wear significally and improve the part formability by reducing local necking in deep drawing tests. Within the scope of this work, TiB2-TiC and TiB2-TaC hard material mixtures are implanted on X38CrMoV5-3 hot work tool steel. The aim is to investigate how the implant material properties can be influenced by the application of different mixing ratios of hard material mixtures under the specific variation of the process parameters. Distinct implant formations are tested on a novel test apparatus to examine the influence on the tribological properties. From the analyses of the implant properties by hardness measurements, light microscopic images, EDX and XRD analyses process parameter ranges are identified to produce defect-free dome- and ring-shaped implants. The specific process parameters (pulse power, pulse duration, mixing ratio and coating thickness) can be used for the determination of the implant geometry (height, width and depth). The tribological tests exhibit improved friction and wear properties. Based on these results, a tribosystem manufactured by this additive surface treatment technology shows great potential to enhance the effectiveness of the hot stamping process. T2 - Friction 2021 CY - Sankt Augustin, Germany DA - 18.11.2021 KW - Laser implantation KW - Surface modification KW - Additive surface treatment KW - Hot stamping KW - Tool steel PY - 2021 AN - OPUS4-53809 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -