TY - CONF A1 - Mishurova, Tatiana T1 - 3D Imaging and residual stress analysis of additively manufactured materials N2 - The focus of the presentation focus will be on 3D imaging by means of X-ray Computed Tomography (XCT) at the lab and at synchrotron, and the non-destructive residual stress (RS) characterization by diffraction of additively manufactured (AM) materials in BAM (Berlin, Germany). The manufacturing defects and high RS are inherent of AM techniques and affect structural integrity of the components. Using XCT the defects size and shape distribution as well as geometrical deviations can be characterized, allowing the further optimization of the manufacturing process. Diffraction-based RS analysis methods using neutron and synchrotron X-rays at large scale facilities offer the possibility to non-destructively spatially resolve both surface and bulk RS in complex components and track their changes following applied thermal or mechanical loads. T2 - The International Symposium on Nondestructive Characterization of Materials 2023 CY - Zurich, Switzerland DA - 15.08.2023 KW - Additive manufacturing KW - Residual stress KW - X-ray computed tomography PY - 2023 AN - OPUS4-58113 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Khrapov, D. A1 - Kozadayeva, M. A1 - Koptyug, A. A1 - Mishurova, Tatiana A1 - Meinel, Dietmar A1 - Surmenev, R. A1 - Surmeneva, M. T1 - Geometrical features and mechanical properties of the sheet-based gyroid scaffolds with functionally graded porosity manufactured by electron beam melting N2 - Functionally graded porous scaffolds (FGPS) constructed with pores of different size arranged as spatially continuous structure based on sheet-based gyroid with three different scaling factors of 0.05, 0.1 and 0.2 were produced by electron beam powder bed fusion. The pore dimensions of the obtained scaffolds satisfy the values required for optimal bone tissue ingrowth. Agglomerates of residual powder were found inside all structures, which required post-manufacturing treatment. Using X-ray Computed Tomography powder agglomerations were visualized and average wall thickness, wall-to-wall distances, micro- and macro-porosities were evaluated. The initial cleaning by powder recovery system (PRS) was insufficient for complete powder removal. Additional treatment by dry ultrasonic vibration (USV) was applied and was found successful for gyroids with the scaling factors of 0.05 and 0.1. Mechanical properties of the samples, including quasi-elastic gradients and first maximum compressive strengths of the structures before and after USV were evaluated to prove that additional treatment does not produce structural damage. The estimated quasi-elastic gradients for gyroids with different scaling factors lie in a range between 2.5 and 2.9 GPa, while the first maximum compressive strength vary from 52.5 for to 59.8 MPa, compressive offset stress vary from 46.2 for to 53.2 MPa. KW - Additive manufacturing KW - Electron beam KW - Powder bed fusion KW - Triply periodic minimal surfaces KW - Functionally graded porous scaffolds KW - X-ray computed tomography PY - 2023 DO - https://doi.org/10.1016/j.mtcomm.2023.106410 SN - 2352-4928 VL - 35 SP - 1 EP - 9 PB - Elsevier Ltd. AN - OPUS4-57682 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Obaton, A.-F. A1 - Fain, J. A1 - Meinel, Dietmar A1 - Tsamos, Athanasios A1 - Léonard, F. A1 - Lécuelle, B. A1 - Djemaï, M. T1 - In Vivo Bone Progression in and around Lattice Implants Additively Manufactured with a New Titanium Alloy N2 - The osseointegration in/around additively manufactured (AM) lattice structures of a new titanium alloy, Ti–19Nb–14Zr, was evaluated. Different lattices with increasingly high sidewalls gradually closing them were manufactured and implanted in sheep. After removal, the bone–interface implant (BII) and bone–implant contact (BIC) were studied from 3D X-ray computed tomography images. Measured BII of less than 10 µm and BIC of 95% are evidence of excellent osseointegration. Since AMnaturally leads to a high-roughness surface finish, the wettability of the implant is increased. The new alloy possesses an increased affinity to the bone. The lattice provides crevices in which the biological tissue can jump in and cling. The combination of these factors is pushing ossification beyond its natural limits. Therefore, the quality and speed of the ossification and osseointegration in/around these Ti–19Nb–14Zr laterally closed lattice implants open the possibility of bone spline key of prostheses. This enables the stabilization of the implant into the bone while keeping the possibility of punctual hooks allowing the implant to be removed more easily if required. Thus, this new titanium alloy and such laterally closed lattice structures are appropriate candidates to be implemented in a new generation of implants. KW - Osseointegration KW - X-ray computed tomography KW - Additive manufacturing KW - Machine learning segmentation PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-577066 DO - https://doi.org/10.3390/app13127282 VL - 13 IS - 12 SP - 1 EP - 18 PB - MDPI CY - Basel, Switzerland AN - OPUS4-57706 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Srinivasan, Krishnanand A1 - Gumenyuk, Andrey A1 - Rethmeier, Michael T1 - Laser Metal Deposition of Rene 80 – Microstructure and Solidification Behaviour Modelling N2 - New developments in nickel-based superalloys and production methods, such as the use of additive manufacturing (AM), can result in innovative designs for turbines. It is crucial to understand how the material behaves during the AM process to advance industrial use of these techniques. An analytical model based on reaction-diffusion formalism is developed to better explain the solidification behavior of the material during laser metal deposition (LMD). The well-known Scheil-Gulliver theory has some drawbacks, such as the assumption of equilibrium at the solid-liquid interface, which is addressed by this method. The solidified fractions under the Scheil model and the pure equilibrium model are calculated using CALPHAD simulations. Differential scanning calorimeter is used to measure the heat flow during the solid-liquid phase transformation, the result of which is further converted to solidified fractions. The analytical model is compared with all the other models for validation. T2 - Lasers in Manufacturing Conference 2023 CY - Munich, Germany DA - 26.06.2023 KW - Additive manufacturing KW - Laser metal deposition KW - Solidification behaviour KW - Analytical model KW - Nickel-based superalloy PY - 2023 SP - 1 EP - 10 AN - OPUS4-58612 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mishurova, Tatiana T1 - In-situ hot isostatic pressing combined with x-ray imaging and diffraction of laser powder bed fusion ti-6al-4v N2 - Hot Isostatic Pressing (HIP) is often introduced to tackle the porosity issue in additively manufactured (AM) materials. For instance, HIP post-processing is recommended to improve fatigue resistance of Laser powder bed fusion (PBF-LB) manufactured parts [1, 2]. Even though HIP cannot completely remove porosity, it significantly decreases the defect population and its average size below the critical threshold value leading to early crack initiation. In the present study, in-situ investigation of HIP procedure of PBF-LB Ti-6Al-4V parts was carried out to gain further insights into the densification mechanism occurring during HIP. The in-situ observations at high pressure and high temperature are uniquely possible at the PSICHE beamline of the Soleil synchrotron (France), thanks to the Ultrafast Tomography on a Paris-Edinburgh Cell (UToPEC) and the combination of the fast phase-contrast tomography and energy-dispersive diffraction [3, 4]. A detailed methodology was developed to ensure that the correct pressure and temperature were maintained during the experiments. The results allowed an estimation of the global dentification rate during HIP of PBF-LB Ti-Al-4V material, as well as a detailed quantitative characterization of the influence of pore size and shape on the densification process, thereby understanding the effectiveness of HIP process on different pore categories. After 20 mins, 75% of porosity can be considered as closed or has size below the resolution of the XCT reconstruction. We also observed that the smallest defects showed higher densification rate, while the defect shape did not have significant effect on such rate. The current development of in-situ HIP experiment allows experimental quantification and validation of the simulation work. Ultimately it paves the road to tailoring the HIP procedure for different materials depending on the porosity and microstructure. T2 - AAMS 2023 CY - Madrid, Spain DA - 26.09.23 KW - Additive manufacturing KW - HIP KW - X-ray computed tomography PY - 2023 AN - OPUS4-58482 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mishurova, Tatiana T1 - 3D imaging and residual stress analysis for AM Materials N2 - The overview of the activity of Federal Institute for Material Research and Testing (BAM, Belin, Germany) in the field of additively manufacturing material characterization will be presented. The research of our group is focused on the 3D imaging of AM materials by means of X-ray Computed Tomography at the lab and at synchrotron, and the residual stress characterization by diffraction (nondestructive technique). T2 - Seminar at Integrated Additive Manufacturing center, Politecnico Torino CY - Turin, Italy DA - 14.02.2023 KW - Additive manufacturing KW - Laser powder bed fusion KW - Residual stress KW - Computed tomography KW - Synchrotron X-ray diffraction PY - 2023 AN - OPUS4-57047 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Merz, Benjamin A1 - Nilsson, R. A1 - Garske, C. A1 - Hilgenberg, Kai T1 - Camera-based high precision position detection for hybrid additive manufacturing with laser powder bed fusion N2 - Additive manufacturing (AM) in general and laser powder bed fusion (PBF-LB/M) in particular are becoming increasingly important in the field of production technologies. Especially the high achievable accuracies and the great freedom in design make PBF-LB/M interesting for the manufacturing and repair of gas turbine blades. Part repair involves building AM-geometries onto an existing component. To minimise the offset between component and AM-geometry, a precise knowledge of the position of the component in the PBF-LB/M machine is mandatory. However, components cannot be inserted into the PBF-LB/M machine with repeatable accuracy, so the actual position will differ for each part. For an offset-free build-up, the actual position of the component in the PBF-LB/M machine has to be determined. In this paper, a camera-based position detection system is developed considering PBF-LB/M constraints and system requirements. This includes finding an optimal camera position considering the spatial limitations of the PBF-LB/M machine and analysing the resulting process coordinate systems. In addition, a workflow is developed to align different coordinate systems and simultaneously correct the perspective distortion in the acquired camera images. Thus, position characteristics can be determined from images by image moments. For this purpose, different image segmentation algorithms are compared. The precision of the system developed is evaluated in tests with 2D objects. A precision of up to 30μm in translational direction and an angular precision of 0.021∘ is achieved. Finally, a 3D demonstrator was built using this proposed hybrid strategy. The offset between base component and AM-geometry is determined by 3D scanning and is 69μm. KW - Laser powder bed fusion KW - Additive manufacturing KW - Hybrid repair KW - Machine vision KW - Image processing KW - Position detection PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-568583 DO - https://doi.org/10.1007/s00170-022-10691-5 SP - 1 EP - 16 PB - Springer AN - OPUS4-56858 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schröpfer, Dirk T1 - Residual stress formation in DED-arc manufactured high strength steel components N2 - Additive manufacturing (AM) processes enable the efficient production of advanced constructions. New developments in topology optimization are leading to weight-optimized designs of increasing complexity. Direct energy deposition processes (DED) such as wire and arc-based additive manufacturing are an important method of additive manufacturing. The wire filler metals enable a wide range of materials, while the arc process provides a high deposition rate compared to laser and powder-based processes. Combined with the use of high-strength steels, the thickness of walls or components can be significantly reduced in the context of lightweight construction, which results in significant savings in energy, costs, time and resources. Suitable high-strength steel filler metals are commercially available for DED-arc AM processes. However, guidelines and quantitative knowledge about welding stresses and cold cracking issues during component production and service are lacking. This limits the industrial application considerably. In a joint project of BAM and Chemnitz University of Technology, the main influences and complex interactions of material, production process, design and processing steps on the residual stress level are investigated. The aim is to develop processing recommendations and a cold cracking test for economical processing and stress-related design of high-strength steels with DED-arc. This study focuses on residual stress analysis by neutron diffraction (ND) and X-ray diffraction (XRD) on defined test specimens. The ND analysis were performed at the Paul Scherrer Institute- Villigen, Switzerland (PSI) and the XRD analysis at BAM. The study shows a quantitative and qualitative comparison of the residual stress magnitudes and distribution between the component bulk (ND) and surface (XRD) analyses. The ND analysis reveals that in DED-arc AM walls the residual stresses dominate in the direction of welding and are negligibly small in each case transverse to the direction of welding. The topology of the analyzed residual stresses shows almost identical residual stress maps compared to XRD. In addition, the residual stresses are significantly influenced by the solid phase transformation of the material due to low cooling times and less post heat treatment cycles of following AM layers in the area of the top layer. T2 - IIW Intermediate Meeting C-II/CIX CY - Munich, Germany DA - 06.03.2023 KW - Additive manufacturing KW - High strength steel KW - Residual stress PY - 2023 AN - OPUS4-59307 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Engelking, Lorenz A1 - Eissel, A. A1 - Schröpfer, Dirk A1 - Treutler, K. A1 - Kannengießer, Thomas A1 - Wesling, V. T1 - Optimisation of surface residual stresses using ultrasonic‑assisted milling for wire‑arc additive manufactured Ni alloy components N2 - Nickel alloys are cost intensive materials and generally classified as difficult-to-cut material. However, machining of these materials is needed especially in case of alloy 36 (1.3912), which is commonly used in mould construction for the production of fibre-reinforced composites. With regard to repair, modification and manufacturing of such components, additive manufacturing offers significant economic advantages. Nevertheless, subsequent machining steps are needed to achieve the final component contour and defined surface conditions. Dependent on the material and machining process conditions, detrimental tensile residual stresses may be the result on the machined surface, having negative impact on the component performance and safety. In this investigation, machining experiments were carried out on wire arc additive manufactured components made of alloy 36, varying the cutting speed and the feed rate. In addition, the conventional milling process (CM) was compared with a modern, hybrid machining process, the ultrasonic-assisted milling (US). The cutting forces and the surface-near residual stresses were analysed using X-ray diffraction. A significant improvement of the machinability as well as the surface integrity by using the ultrasonic assistance was observed, especially at low cutting speeds. The CM induced mainly tensile residual stresses, the US mainly compressive residual stresses. KW - Surface integrity KW - Ultrasonic-assisted milling KW - Additive manufacturing KW - Ni alloy KW - Alloy 36 PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-575246 DO - https://doi.org/10.1007/s00170-023-11326-z SN - 1433-3015 VL - 126 IS - 9 SP - 4191 EP - 4198 PB - Springer Nature AN - OPUS4-57524 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wandtke, Karsten A1 - Schröpfer, Dirk A1 - Scharf-Wildenhain, R. A1 - Hälsig, A. A1 - Kannengießer, Thomas A1 - Kromm, Arne A1 - Hensel, J. T1 - Influence of the WAAM process and design aspects on residual stresses in high-strength structural steels N2 - Wire arc additive manufacturing (WAAM) enables the efficient production of weight-optimized modern engineering structures. Further increases in efficiency can be achieved by using high-strength structural steels. Commercial welding consumables for WAAM are already available on the market. Lack of knowledge and guidelines regarding welding residual stress and component safety during production and operation leads to severely limited use for industry applications. The sensitive microstructure of high-strength steels carries a high risk of cold cracking; therefore, residual stresses play a crucial role. For this reason, the influences of the material, the WAAM process, and the design on the formation of residual stresses and the risk of cold cracking are being investigated. The material used has a yield strength of over 800 MPa. This strength is adjusted via solid solution strengthening and a martensitic phase transformation. The volume expansion associated with martensite formation has a significant influence on the residual stresses. The focus of the present investigation is on the additive welding parameters and component design on their influence on hardness and residual stresses, which are analyzed by means of X-ray diffraction (XRD). Reference specimens (hollow cuboids) are welded fully automated with a systematic variation of heat control and design. Welding parameters and AM geometry are correlated with the resulting microstructure, hardness, and residual stress state. Increased heat input leads to lower tensile residual stresses which causes unfavorable microstructure and mechanical properties. The component design affects heat dissipation conditions and the intensity of restraint during welding and has a significant influence on the residual stress. KW - DED-arc KW - Additive manufacturing KW - High-strength steel filler metal KW - Residual stress PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-572698 DO - https://doi.org/10.1007/s40194-023-01503-9 SN - 1878-6669 VL - 67 IS - 4 SP - 987 EP - 996 PB - Springer CY - Berlin AN - OPUS4-57269 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -