TY - CONF A1 - Erning, Johann Wilhelm T1 - Hygienic assessment of SLM-printed stainless steel N2 - Elektrochemische Messungen zur hygienischen Bewertung additiv gefertigter Bauteile werden diskutiert. Die Bewertung und Details des Werkstoffs werden beschrieben, Anwendungsbeispiele gezeigt. T2 - Kormat 2022 CY - Online meeting DA - 26.04.2022 KW - Korrosion KW - Trinkwasser KW - Hygienische Bewertung KW - Additive Fertigung PY - 2022 AN - OPUS4-54709 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Erning, Johann Wilhelm T1 - Hygienische Eigenschaften von additiv gefertigtem 1.4404 in Trinkwasser N2 - Elektrochemische Messungen zur hygienischen Bewertung additiv gefertigter Bauteile werden diskutiert. Die Bewertung und Details des Werkstoffs werden beschrieben, Anwendungsbeispiele gezeigt. T2 - 3. Fachtagung Werkstoffe und Additive Fertigung CY - Dresden, Germany DA - 11.05.2022 KW - Korrosion KW - Trinkwasser KW - Hygiene KW - Additive Fertigung PY - 2022 AN - OPUS4-54829 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Erning, Johann Wilhelm T1 - Hygienische Bewertung von SLM-gedrucktem rostfreiem Stahl N2 - Werkstoffe im Kontakt mit Trinkwasser müssen hygienisch bewertet werden. Hier wird ein bereits bewerteter Werkstoff wegen neuer Fertigungsmethoden (additive Fertigung) erneut geprüft und die Besonderheiten durch das Verfahren dargestellt. Der Werkstoff ist auch mit additiver Produktionsmethode geeignet. T2 - GfKORR - Jahrestagung CY - Frankfurt am Main, Germany DA - 05.11.2024 KW - Additive Fertigung KW - Trinkwasser KW - Korrosion KW - Nichtrostender Stahl PY - 2024 AN - OPUS4-61845 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Strobl, Domninic T1 - PGD in thermal transient problems with a moving heat source – a sensitivity study on factors affecting accuracy and efficiency N2 - Thermal transient problems, essential in applications like welding and additive metal manufacturing, are characterized by a dynamic evolution of temperature. Accurately simulating these phenomena is often computationally expensive, thus limiting the application, e. g. for model parameter estimation or online process control. Model order reduction, a solution to preserve accuracy while reducing complexity, is explored. This paper addresses challenges in developing a reduced model using the Proper Generalized Decomposition (PGD) for transient thermal problems with a specific treatment of the moving heat source within the reduced model. Factors affecting accuracy, convergence, and computational cost, such as discretization methods (finite element and finite difference), a dimensionless formulation, the size of the heat source, and the inclusion of material parameters as additional PGD variables are examined across progressively complex examples. The results demonstrate the influence of these factors on the PGD model's performance and emphasize the importance of their consideration when implementing such models. For thermal examples it is demonstrated that a PGD model with a finite difference discretization in time, a dimensionless representation, a mapping for a moving heat source, and a spatial domain non-separation yields the best approximation to the full order model. KW - Additive manufacturing KW - Mapping for unseparable load KW - Model order reduction KW - Proper generalized decomposition KW - Sensitivity analysis KW - Thermal transient problem PY - 2024 DO - https://doi.org/10.5281/zenodo.10102489 PB - Zenodo CY - Geneva AN - OPUS4-62235 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tamsen, Erik T1 - Towards an automatic optimization framework for performance oriented precast concrete design N2 - Concrete has a long history in the construction industry and is currently one of the most widely used building materials. Especially precast concrete elements are frequently utilized in construction projects for standardized applications, increasing the quality of the composite material, as well as reducing the required building time. Despite the accumulated knowledge, continuous research and development in this field is essential due to the complexity of the composite combined with the ever-growing number of applications and requirements. Especially in view of global climate change, design aspects as CO2 emissions and resource efficiency require new mix designs and optimization strategies. A result of the material’s high complexity and heterogeneity on multiple scales is that utilizing the full potential with changing demands is highly challenging, even for the established industry. We propose a framework based on an ontology, which automatically combines experimental data with numerical simulations. This not only simplifies experimental knowledge transfer, but allows the model calibration and the resulting simulation predictions to be reproducible and interpretable. This research shows a way towards a more performance oriented material design. Within this talk we present our workflow for an automated simulation of a precast element, demonstrating the interaction of the ontology and the finite element simulation. We show the automatic calibration of our early-age concrete model [1, 2], to improve the prediction of the optimal time for the removal of the form work. T2 - The 8th European Congress on Computational Methods in Applied Sciences and Engineering (ECCOMAS) 2022 CY - Oslo, Norway DA - 05.06.2022 KW - Performance oriented concrete design KW - Early-age concrete KW - Precast concrete KW - Ontology KW - Optimization workflow PY - 2022 AN - OPUS4-55302 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Andrés Arcones, Daniel A1 - Diercks, Philipp A1 - Robens-Radermacher, Annika A1 - Rosenbusch, Sjard Mathis A1 - Tamsen, Erik A1 - Tyagi, Divyansh A1 - Unger, Jörg F. T1 - FenicsXConcrete N2 - FenicsXConcrete is a Python package for the simulation of mechanical problems. The general PDE solving software FEniCSx is extended with classes describing experimental setups, mechanical problems, thermo-mechanical problems, additive manufacturing and sensors. KW - FEM KW - Fenics KW - Concrete modelling PY - 2023 UR - https://github.com/BAMresearch/FenicsXConcrete DO - https://doi.org/10.5281/zenodo.7780757 PB - Zenodo CY - Geneva AN - OPUS4-59121 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Robens-Radermacher, Annika T1 - Efficient cooling time optimization in Wire Arc Additive Manufacturing using a multi-layer reduced order model N2 - Additive manufacturing (AM) has transformed the industry by enabling the production of complex geometries and parts with customized properties. Among various AM techniques, wire arc additive manufacturing (WAAM) stands out due to its high deposition rate and low equipment cost. However, WAAM’s complex thermal history poses challenges for real-time simulation, essential for online process control and optimization. Consequently, experimental optimization remains the state-of-the-art approach. A critical parameter to optimize is the cooling phase duration, which prevents structural overheating, controls the molten pool size, and influences the mechanical properties of the final product. For efficient cooling time optimization, a fast-to-evaluate model of the temperature field during multi-layer deposition is necessary. This study proposes a reduced order model (ROM) using the proper generalized decomposition (PGD) method as a powerful tool to minimize computational effort. Given the moving heat source in WAAM processes, a mapping approach is employed to achieve a fully separated representation of the temperature field. Building on the authors’ previous one-layer approach, this contribution extends the model to multiple layers through enhanced mapping and compression techniques. The compression reduces the total number of PGD modes as the number of layers increases. The extended mapping allows computations with a fixed mesh over the simulation time, in contrast to standard methods such as the element birth technique. For cooling time optimization, the cooling duration of each layer is incorporated as PGD variables, enabling time-efficient computation of the temperature field for varying cooling times. The developed ROM is applied to optimize the cooling time of a multiple layer example. Therefore a 5-10 layer wall structure is investigated using the austenitic stainless steel 1.4404 (AISI 316 L). The resulting cooling times and the efficiency of the approach are discussed. T2 - 12th European solid mechanics conference (ESMC) CY - Lyon, France DA - 07.07.2025 KW - Model order reduction KW - Proper generalized decomposition KW - Welding KW - Additive manufacturing KW - Optimzation PY - 2025 UR - https://esmc2025.sciencesconf.org/ AN - OPUS4-63855 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Meinel, Dietmar T1 - Classic Materials Testing in the Light of CT N2 - Currently, mandatory requirements and recommendations for the detection of irregularities in laser beam welded joints are based on classic micrographs as set out in the standard ISO 13919-1:2019. Compared to classic micrographs, computed tomography enables a non-destructive, three-dimensional and material-independent mode of operation, which delivers much more profound results. Even in building material testing, methods with limited informative value can be checked and supplemented by CT examinations. T2 - 13th International Conference on Industrial Computed Tomography (iCT2024) CY - Wels, Austria DA - 06.02.2024 KW - Computed Tomography KW - Additive Manufacturing KW - Machine-Learning Segmentation KW - Air Void System PY - 2024 AN - OPUS4-59568 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Strobl, Dominic A1 - Unger, Jörg F. A1 - Chady, G. A1 - Klawoon, Alexander A1 - Pittner, Andreas A1 - Rethmeier, Michael A1 - Robens-Radermacher, Annika T1 - Efficient bead-on-plate weld model for parameter estimation towards effective wire arc additive manufacturing simulation N2 - Despite the advances in hardware and software techniques, standard numerical methods fail in providing real-time simulations, especially for complex processes such as additive manufacturing applications. A real-time simulation enables process control through the combination of process monitoring and automated feedback, which increases the flexibil- ity and quality of a process. Typically, before producing a whole additive manufacturing structure, a simplified experiment in form of a bead-on- plate experiment is performed to get a first insight into the process and to set parameters suitably. In this work, a reduced order model for the transient thermal problem of the bead-on-plate weld simulation is devel- oped, allowing an efficient model calibration and control of the process. The proposed approach applies the proper generalized decomposition (PGD) method, a popular model order reduction technique, to decrease the computational effort of each model evaluation required multiple times in parameter estimation, control and optimization. The welding torch is modeled by a moving heat source, which leads to difficulties separating space and time, a key ingredient in PGD simulations. A novel approach for separating space and time is applied and extended to 3D problems allowing the derivation of an efficient separated representation of the tem- perature. The results are verified against a standard finite element model showing excellent agreement. The reduced order model is also leveraged in a Bayesian model parameter estimation setup, speeding up calibrations and ultimately leading to an optimized real-time simulation approach for welding experiment using synthetic as well as real measurement data. KW - Ermüdung PY - 2023 DO - https://doi.org/10.5281/zenodo.7456813 PB - Zenodo CY - Geneva AN - OPUS4-59651 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Strobl, Dominic T1 - Real-time Bead-on-Plate weld Simulation for Wire Arc Additive Manufacturing using Reduced Order modelling coupled with stochastic model Calibration N2 - Numerical simulations are essential in predicting the behavior of systems in many engineering fields and industrial sectors. The development of accurate virtual representations of actual physical products or processes (also known as digital twins) allows huge savings in cost and resources. In fact, digital twins would allow reducing the number of real, physical prototypes, tests, and experiments, thus also increasing the sustainability of production processes and products’ lifetime. Standard numerical methods fail in providing real time simulations, especially for complex processes such as additive manufacturing applications. This work aims to use a reduced order model for efficient wire arc additive manufacturing simulations, calibrations and real-time process control. Model reduction, e.g. the proper generalized decomposition [1,2] method, is a popular concept to decrease the computational effort. A new mapping approach [3] was applied to simulate a moving heat source with the proper generalized decomposition. Using this procedure even complex models can be simulated in real-time. The physical model is later on calibrated with the use of a stochastic model updating process and the reduced order model, leading to an optimized real-time simulation. In this contribution, a proper generalized decomposition model for a bead-on-plate wire arc additive manufacturing is presented. It is also coupled with a stochastic model updating process identifying the heat source characteristics as well as the boundary conditions of the transient thermal problem, whereas the heat source shape is simulated using a Goldak heat source T2 - 15th World Congress on Computational Mechanics (WCCM-XV) CY - Yokohama, Japan DA - 31.07.2022 KW - Wire arc additive manufacturing KW - Reduced order modelling KW - Model calibration PY - 2022 AN - OPUS4-55576 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Strobl, Domninic T1 - Reduced order model for temperature field simulation of wire arc additive manufacturing N2 - Additive manufacturing (AM) has revolutionized the manufacturing industry, offering a new paradigm to produce complex geometries and parts with customized properties. Among the different AM techniques, the wire arc additive manufacturing (WAAM) process has gained significant attention due to its high deposition rate and low equipment cost. However, the process is characterized by a complex thermal history making it challenging to simulate it in real-time for online process control and optimization. In this context, a reduced order model (ROM) using the proper generalized decomposition (PGD) method [1] is proposed as a powerful tool to overcome the limitations of conventional numerical methods and enable the real-time simulation of the temperature field of WAAM processes. These simulations use a moving heat source leading to a hardly separable parametric problem, which is handled by applying a novel mapping approach [2]. This procedure makes it possible to create a separated representation of the model, which is required to apply the PGD method, allowing a simulation of multiple layers. In this contribution, a PGD model is derived for the temperature field simulation of the WAAM process. A layer-by-layer simulation in combination with a compression of the PGD modes, without influencing the approximation error, is shown. The compression is an essential step since the modes sum up quickly over the layers and thus a reduction of the number of modes is needed. Furthermore, using an element birth technique leads usually to an update of the mesh or a new mesh in each time step. Though, this is not the case applying the mapping approach, where only a single nonchanging mesh is required to simulate the deposition of a whole layer. T2 - ECCOMAS Congress 2024 CY - Lisbon, Portugal DA - 03.06.2024 KW - Reduced Order Model KW - Proper Generalized Decomposition KW - Thermal transient problem KW - Additive manufacturing PY - 2024 AN - OPUS4-62231 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wilbig, Janka A1 - Borges de Oliveira, F. A1 - Obaton, A.-F. A1 - Schwentenwein, M. A1 - Rübner, Katrin A1 - Günster, Jens T1 - Defect detection in additively manufactured lattices N2 - This paper investigates fast and inexpensive measurement methods for defect detection in parts produced by Additive Manufacturing (AM) with special focus on lattice parts made of ceramics. By Lithography-based Ceramic Manufacturing, parts were built both without defects and with typical defects intentionally introduced. These defects were investigated and confirmed by industrial X-ray Computed Tomography. Alternative inexpensive methods were applied afterwards on the parts such as weighing, volume determination by Archimedes method and gas permeability measurement. The results showed, that defects resulting in around 20% of change in volume and mass could be separated from parts free of defects by determination of mass or volume. Minor defects were not detectable as they were in the range of process-related fluctuations. Permeability measurement did not allow to safely identify parts with defects. The measurement methods investigated can be easily integrated in AM process chains to support quality control. KW - Additive manufacturing KW - Quality assurance KW - Defect detection KW - Lattices KW - Ceramics PY - 2020 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-513547 DO - https://doi.org/10.1016/j.oceram.2020.100020 VL - 3 SP - 100020 PB - Elsevier Ltd. AN - OPUS4-51354 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Bäßler, Ralph T1 - Review: Science, Technology and Applications of Metals in Additive Manufacturing N2 - Often 3D‐printing and additive manufacturing are mentioned as the 3rd industrial revolution. In this conjunction this book provides a brief overview on additively manufactured metal pieces. This book fulfills its intension to serve as an educational guide, providing a holistic picture encompassing science, technology and applications for the real‐life use of Metal Additive Manufacturing. KW - Additive manufacturing KW - Corrosion KW - Material properties PY - 2020 DO - https://doi.org/10.1002/maco.202070114 SN - 1521-4176 SN - 0947-5117 VL - 71 IS - 11 SP - 1929 EP - 1930 PB - WILEY‐VCH Verlag GmbH & Co. KGaA CY - Weinheim AN - OPUS4-51514 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Ginés-Palomares, J.-C. A1 - Fateri, M. A1 - Schubert, T. A1 - de Peindray d’Ambelle, L. A1 - Simon, Sebastian A1 - Gluth, Gregor A1 - Günster, Jens A1 - Zocca, Andrea T1 - Material aspects of sintering of EAC-1A lunar regolith simulant N2 - Future lunar exploration will be based on in-situ resource utilization (ISRU) techniques. The most abundant raw material on the Moon is lunar regolith, which, however, is very scarce on Earth, making the study of simulants a necessity. The objective of this study is to characterize and investigate the sintering behavior of EAC-1A lunar regolith simulant. The characterization of the simulant included the determination of the phase assemblage, characteristic temperatures determination and water content analysis. The results are discussed in the context of sintering experiments of EAC-1A simulant, which showed that the material can be sintered to a relative density close to 90%, but only within a very narrow range of temperatures (20–30 °C). Sintering experiments were performed for sieved and unsieved, as well as for dried and non-dried specimens of EAC-1A. In addition, an analysis of the densification and mechanical properties of the sintered specimens was done. The sintering experiments at different temperatures showed that the finest fraction of sieved simulant can reach a higher maximum sintering temperature, and consequently a higher densification and biaxial strength. The non-dried powder exhibited higher densification and biaxial strength after sintering compared to the dried specimen. This difference was explained with a higher green density of the non-dried powder during pressing, rather than due to an actual influence on the sintering mechanism. Nevertheless, drying the powder prior to sintering is important to avoid the overestimation of the strength of specimens to be fabricated on the Moon. KW - Lunar regolith KW - Ceramics KW - Microstructure KW - Sintering KW - Softening temperature PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-592668 DO - https://doi.org/10.1038/s41598-023-50391-y SN - 2045-2322 VL - 13 SP - 1 EP - 14 PB - Springer Nature AN - OPUS4-59266 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Silvestro, L. A1 - Ruviaro, A. S. A1 - Lima, G. A1 - Durlo Tambara, Luís Urbano A1 - Feys, D. A1 - Kirchheim, A. P. T1 - Rotational rheometry test of Portland cement-based materials - A systematic literature review N2 - This study systematically reviews 62 papers on the use of rotational rheometry to assess the fresh state behavior of Portland cement-based materials. The research highlights the wide variation in test methods and aims to provide a comprehensive overview. Findings reveal that 50.0% of studies employed vane geometry, despite its limitations in providing transformation equations. Regarding dynamic shearing tests, 67.0% followed a consensus using a pre-shearing step and a step-wise routine with stabilization times ≥ 10 s. While the Bingham model is commonly used, the study emphasizes the importance of considering shear-thinning behavior in cementitious materials. Models like Herschel-Bulkley and modified Bingham may be more appropriate. This review offers insights into testing conditions for rotational rheometry of cementitious materials, serving as a foundation for future research in the field. KW - Review KW - Rheology KW - Rheometry KW - Rotational KW - Cement PY - 2024 DO - https://doi.org/10.1016/j.conbuildmat.2024.136667 SN - 0950-0618 VL - 432 SP - 1 EP - 14 PB - Elsevier Ltd. CY - Amsterdam AN - OPUS4-60075 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Tidblad, Johan A1 - Moya Núñez, Alice A1 - de la Fuente, Daniel A1 - Ebell, Gino A1 - Flatlandsmo Berglen, Tore A1 - Grøntoft, Terje A1 - Hans, Ulrik A1 - Christodoulakis, Ioannis A1 - Kajánek, Daniel A1 - Kreislová, Kateřina A1 - Kwiatkowski, Lech A1 - La Torreta, Teresa A1 - Lutze, Rafał A1 - Pinar Larrubia, Guadalupe A1 - Pintus, Valentina A1 - Prange, Michael A1 - Spezzano, Pasquale A1 - Varotsos, Costas A1 - Verney-Carron, Aurélie A1 - Vuorio, Tiina A1 - Yates, Tim T1 - Corrosion and Soiling in the 21st Century: Insights from ICP Materials and Impact on Cultural Heritage N2 - This paper reviews results published by the International Co-operative Programme on Effects on Materials including Historic and Cultural Monuments (ICP Materials) with emphasis on those obtained after the turn of the century. Data from ICP Materials come from two main sources. The first is through exposures of materials and collection of environmental data in a network of atmospheric exposure test sites mainly distributed across Europe. Corrosion of carbon steel has continued to decrease during the period 2000–2020 but corrosion of zinc only up until 2014, and the trend in zinc corrosion is only visible when examining four-year data. Surface recession of limestone as well as soiling of modern glass show no decreasing trend during 2000–2020. The second is through case studies performed at heritage sites across Europe. Risk analysis of corrosion and soiling for twenty-six sites indicate that currently soiling is a more significant maintenance trigger than corrosion. Costs for maintaining heritage sites are substantial and costs attributable to air pollution is estimated from 40% to as much as 80% of the total cost. Future directions of the program are work on effects of particulate matter, improving the scientific basis for the work, and making the monitoring data publicly available. KW - Corrosion KW - Atmospheric corrosion KW - Soiling PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-644651 DO - https://doi.org/10.3390/cmd6040054 SN - 2624-5558 VL - 6 IS - 4 SP - 1 EP - 25 PB - MDPI AG AN - OPUS4-64465 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Simon, Sebastian A1 - Bertmer, M. A1 - Gluth, Gregor T1 - Sol–gel synthesis and characterization of lithium aluminate (L–A–H) and lithium aluminosilicate (L–A–S–H) gels N2 - Hydrous lithium aluminosilicate (L–A–S–H) and lithium aluminate (L–A–H) gels are candidate precursors for glass-ceramics and ceramics with potential advantages over conventional processing routes. However, their structure before calcination remained largely unknown, despite the importance of precursor structure on the properties of the resulting materials. In the present study, it is demonstrated that L–A–S–H and L–A–H gels with Li/Al ≤ 1 can be produced via an organic steric entrapment route, while higher Li/Al ratios lead to crystallization of gibbsite or nordstrandite. The composition and the structure of the gels was studied by thermogravimetric analysis, X-ray diffraction, 27Al and 29Si magic-angle spinning nuclear magnetic resonance, and Raman spectroscopy. Aluminium was found to be almost exclusively in six-fold coordination in both the L–A–H and the L–A–S–H gels. Silicon in the L–A–S–H gels was mainly in Q4 sites and to a lesser extent in Q3 sites (four-fold coordination with no Si–O–Al bonds). The results thus indicate that silica-rich and aluminium-rich domains formed in these gels. KW - Lithium aluminosilicates KW - Raman spectroscopy KW - Sol-gel PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-558756 DO - https://doi.org/10.1111/ijac.14187 SN - 1546-542X VL - 19 IS - 6 SP - 3179 EP - 3190 PB - Wiley AN - OPUS4-55875 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Simon, Sebastian A1 - Gluth, Gregor ED - Rossignol, S. ED - Gluth, Gregor T1 - Unraveling the hardening mechanism during laser-induced slip casting of lithium aluminate-microsilica slurry N2 - Additive manufacturing (AM) of alkali-activated materials is a promising method for producing ceramic precursors, construction elements and other parts. A recently introduced AM process is laser-induced slip casting of lithium aluminate/microsilica slurries, which yields parts with excellent mechanical strengths. To clarify the underlying mechanisms, μ-Raman spectroscopy was applied to parts produced by the process, and the dissolution and hydration of lithium aluminate was studied inter alia using conventional and in-situ X-ray diffraction. The results show that significant dissolution of lithium aluminate occurs, particularly at increased temperatures during laser interaction, which leads to an increase of pH and precipitation of an akopovaite-like Li-Al-CO3 layered double hydroxide. The increase of the pH is likely to induce dissolution of the microsilica and possibly formation of a hydrous lithium aluminosilicate gel. These observations explain the strength evolution of the studied parts and can also aid the development and improvement of related AM methods. KW - Alkali-activated materials KW - Additive manufacturing KW - Laser-induced slip casting KW - Lithium KW - Layered double hydroxide PY - 2021 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-520557 DO - https://doi.org/10.1016/j.oceram.2021.100060 SN - 2666-5395 VL - 5 IS - Special issue: Alkali-activated materials and geopolymers in ceramics and beyond SP - 1 EP - 7 PB - Elsevier CY - Amsterdam AN - OPUS4-52055 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -