TY - CONF A1 - Kempf, A. T1 - Correlation between quasistatic und fatigue properties of additively manufactured AlSi10Mg using Laser Powder Bed Fusion N2 - In order to find a resource efficient approach for the fatigue lifetime prediction of laser powder bed fusion (L-PBF) processed AlSi10Mg material, results of tensile and fatigue tests were compared. The specimens were manufactured with three different L-PBF machines and studied in different heat treatment conditions (as-built, annealed, T6 heat treated). The investigations showed that the high attainable tensile strength properties after the manufacturing process are not beneficial in the high cycle fatigue (HCF) regime. In contrast, the applied heat treatments, which lead typically to a decrease of ultimate tensile strength, improved dramatically the fatigue behavior. Additionally, a clear correlation between the elongation at fracture and HCF resistance has been found for individual heat treatment conditions. This empiric relationship provides an estimation of the fatigue resistance in the presence of material defects and can be implemented in part and process approvals. T2 - Fatigue Design 2021 CY - Online meeting DA - 17.11.2021 KW - Additive Manufacturing KW - Laser powder bed fusion KW - AlSi10Mg KW - Tensile properties KW - Fatigue properties PY - 2021 AN - OPUS4-53792 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Ponader, Marco A1 - Röder, Bettina A1 - Paul, Martin A1 - Weller, Michael G. T1 - Sintered glass monoliths as supports for affinity columns N2 - A novel stationary phase for affinity separations is presented. This material is based on sintered borosilicate glass readily available as semi-finished filter plates with defined porosity and surface area. The material shows fast binding kinetics and excellent long-term stability under real application conditions due to lacking macropores and high mechanical rigidity. The glass surface can be easily modified with standard organosilane chemistry to immobilize selective binders or other molecules used for biointeraction. In this paper, the manufacturing of the columns and their respective column holders by 3D printing is shown in detail. The model system protein A/IgG was chosen as an example to examine the properties of such monolithic columns under realistic application conditions. Several specifications, such as (dynamic) IgG capacity, pressure stability, long-term performance, productivity, non-specific binding, and peak shape, are presented. It could be shown that due to the very high separation speed, 250 mg antibody per hour and column can be collected, which surpasses the productivity of most standard columns of the same size. The total IgG capacity of the shown columns is around 4 mg (5.5 mg/mL), which is sufficient for most tasks in research laboratories. The cycle time of an IgG separation can be less than 1 min. Due to the glass material’s excellent pressure resistance, these columns are compatible with standard HPLC systems. This is usually not the case with standard affinity columns, limited to manual use or application in low-pressure systems. The use of a standard HPLC system also improves the ability for automation, which enables the purification of hundreds of cell supernatants in one day. The sharp peak shape of the elution leads to an enrichment effect, which might increase the concentration of IgG by a factor of 3. The final concentration of IgG can be around 7.5 mg/mL without the need for an additional nano-filtration step. The purity of the IgG was > 95% in one step and nearly 99% with a second polishing run. KW - Affinity Chromatography KW - Affinity Extraction KW - Affinity Separation KW - Protein Purification KW - Down Stream Processing KW - Antibody Purification KW - Diagnostic Antibodies KW - Therapeutic Antibodies KW - Automated Purification KW - HPLC KW - FPLC KW - IgG determination KW - Concentration step KW - Monoclonal Antibodies KW - Polyclonal Antibodies KW - Human Plasma KW - Glass Support KW - Borosilicate Glass KW - Monolith KW - Sintered Material KW - Additive Manufacturing KW - Column holder KW - Construction KW - Open Science KW - Citizen Science KW - Protein A KW - Regeneration KW - High-Speed Separations KW - Robustness PY - 2021 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-527581 DO - https://doi.org/10.3390/separations8050056 SN - 2297-8739 N1 - Geburtsname von Ponader, Marco: Wilke, M. - Birth name of Ponader, Marco: Wilke, M. VL - 8 IS - 5 SP - 1 EP - 16 PB - MDPI CY - Basel AN - OPUS4-52758 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Agea Blanco, Boris A1 - Walzel, S. A1 - Chi, J. A1 - Lüchtenborg, J. T1 - Making Binder Jetting Really Work for Technical Ceramics - Additive Manufacturing of Technical Ceramics N2 - As an alternative shaping method to the traditionally used processes, additive manufacturing (AM) can produce economical ceramic components in small lot sizes and/or with complex geometries. Powder-based additive manufacturing processes like binder jetting are popular in the field of metal AM. One reason is the increased productivity compared to other AM technologies. For ceramic materials, powder-based AM technologies result in porous ceramic parts, provided they are not infiltrated. CerAMing GmbH unites the advantages of powder-based processes with the production of dense ceramic by means of the Layerwise Slurry Deposition. By using a suspension, a high packing density of the powder bed is achieved which leads to high green body densities. Due to this advantage the approach overcomes the problems of other powder-based AM technologies. Furthermore, a very economical debinding time allows the production of parts with high wall thicknesses. KW - Additive Manufacturing KW - Binder Jetting KW - Layerwise Slurry Deposition KW - Lithography-based technologies KW - Technical Ceramics PY - 2021 SP - 49 EP - 52 PB - Göller Verlag CY - Baden-Baden AN - OPUS4-52948 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Werner, Tiago T1 - Comparison of the fatigue behavior of wrought and additively manufactured AISI 316L N2 - Additively Manufactured (AM) parts are still far from being used in safety-relevant applications, mainly due to a lack of understanding of the feedstock-process-propertiesperformance relationship. This work aims at providing a characterization of the fatigue behavior of the additively manufactured AISI 316L austenitic stainless steel and a direct comparison with the fatigue performance of the wrought steel. A set of specimens has been produced by laser powder bed fusion (L-PBF) and a second set of specimens has been machined out of hot-rolled plates. The L-PBF material shows a higher fatigue limit and better finite life performance compared to the wrought material, accompanied by an extensive amount of cyclic softening. T2 - Fatigue Design 2021 CY - Online meeting DA - 17.11.2021 KW - Additive Manufacturing KW - AM KW - 316L KW - Fatigue KW - High Cycle Fatigue KW - Low Cycle Fatigue PY - 2021 AN - OPUS4-53780 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kempf, Andreas A1 - Kruse, Julius A1 - Madia, Mauro A1 - Hilgenberg, Kai T1 - Correlation between quasistatic und fatigue properties of additively manufactured AlSi10Mg using Laser Powder Bed Fusion N2 - In order to find a resource efficient approach for the fatigue lifetime prediction of laser powder bed fusion (L-PBF) processed AlSi10Mg material, results of tensile and fatigue tests were compared. The specimens were manufactured with three different L-PBF machines and studied in different heat treatment conditions (as-built, annealed, T6 heat treated). The investigations showed that the high attainable tensile strength properties after the manufacturing process are not beneficial in the high cycle fatigue (HCF) regime. In contrast, the applied heat treatments, which lead typically to a decrease of ultimate tensile strength, improved dramatically the fatigue behavior. Additionally, a clear correlation between the elongation at fracture and HCF resistance has been found for individual heat treatment conditions. This empiric relationship provides an estimation of the fatigue resistance in the presence of material defects and can be implemented in part and process approvals. T2 - FATIGUE DESIGN 2021 CY - Online meeting DA - 17.11.2021 KW - Additive Manufacturing KW - Laser powder bed fusion KW - AlSi10Mg KW - Tensile properties KW - Fatigue properties PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-544921 DO - https://doi.org/10.1016/j.prostr.2022.03.009 SN - 2452-3216 VL - 38 SP - 77 EP - 83 PB - Elsevier B.V. AN - OPUS4-54492 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bettge, Dirk T1 - MGA Round Robin Test on Al-AM Fatigue Testing - Fractographic Results N2 - Presentation of results of an investigation of fracture mechanisms and crack start sites of an additive manufactured aluminium alloy after fatigue testing. Collaboration within the MGA initiative (Mobility Goes Additive). T2 - MGA Mid Term Meeting 2022 CY - Berlin, Germany DA - 05.07.2022 KW - Aluminium Alloy KW - Fractography KW - Additive Manufacturing PY - 2022 AN - OPUS4-55192 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Scheuschner, Nils T1 - In-situ Prozessüberwachung in der additiven Fertigung von Metallen (PBF-LB /M) mittels TT und ET N2 - Durch die additive Fertigung ergeben sich durch die nun mögliche wirtschaftliche Fertigung hochgradig individueller und komplexer metallischer Bauteile in kleinen Stückzahlen bis hinunter zum Einzelstück für viele Industriebereiche ganz neue Möglichkeiten. Gleichzeitig entstehen jedoch neue Herausforderungen im Bereich der Qualitätssicherung, da sich auf statistischen Methoden beruhende Ansätze nicht anwenden lassen, ohne wiederum die Vorteile der Fertigung massiv einzuschränken. Eine mögliche Lösung für dieses Problem liegt in der Anwendung verschiedener In-situ-Überwachungstechniken während des Bauprozesses. Jedoch sind nur wenige dieser Techniken kommerziell verfügbar und noch nicht so weit erforscht, dass die Einhaltung strenger Qualitäts- und Sicherheitsstandards gewährleistet werden kann. In diesem Beitrag stellen wir die Ergebnisse einer Studie über mittels L-PBF gefertigte Probekörper aus der Nickelbasis-Superlegierung Haynes 282 vor, bei denen die Bildung von Defekten durch lokale Variationen der Prozessparameter wie der Laserleistung provoziert wurde. Die Proben wurden in-situ mittels Thermographie, optischer Tomographie, Schmelzbadüberwachung und Wirbelstromprüfung sowie ex-situ mittels Computertomographie (CT) überwacht, mit dem Ziel, die Machbarkeit und die Aussichten der einzelnen Methoden für die zuverlässige Erkennung der Bildung relevanter Defekte zu bewerten. T2 - DGZfP Jahrestagung 2022 CY - Kassel, Germany DA - 23.05.2022 KW - Additive Manufacturing KW - Thermografie KW - Additive Fertigung KW - Thermography PY - 2022 AN - OPUS4-55851 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Scheuschner, Nils T1 - In-situ Monitoring of PBF-LB/M by thermography, optical tomography, melt-pool-monitoring and eddy current N2 - The formation of defects such as keyhole pores is a major challenge for the production of metal parts by Laser Powder Bed Fusion (LPBF). The LPBF process is characterized by a large number of influencing factors which can be hard to quantify. Machine Learning (ML) is a prominent tool to predict the outcome of complex processes on the basis of different sensor data. In this study, a ML model for defect prediction is created using thermographic image features as input data. As a reference, the porosity information calculated from an x-ray Micro Computed Tomography (µCT) scan of the produced specimen is used. Physical knowledge about the keyhole pore formation is incorporated into the model to increase the prediction accuracy. From the prediction result, the quality of the input data is evaluated and future demands on in-situ monitoring of LPBF processes are formulated. T2 - AM Bench 2022 CY - Bethesda, Washingthon DC, USA DA - 15.08.2022 KW - Additive Manufacturing KW - Thermography KW - Additive Fertigung KW - Thermografie PY - 2022 AN - OPUS4-55854 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Scheuschner, Nils T1 - In-situ monitoring of the laser powder bed fusion process by thermography, optical tomography and melt pool monitoring for defect detection N2 - For the wide acceptance of the use of additive manufacturing (AM), it is required to provide reliable testing methods to ensure the safety of the additively manufactured parts. A possible solution could be the deployment of in-situ monitoring during the build process. However, for laser powder bed fusion using metal powders (PBF-LB/M ) only a few in-situ monitoring techniques are commercially available (optical tomography, melt pool monitoring) but not researched to an extent that allows to guarantee the adherence to strict quality and safety standards. In this contribution, we present results of a study of PBF-LB/M printed parts made of the nickel-based superalloy Haynes 282. The formation of defects was provoked by local variations of the process parameters and monitored by thermography, optical tomography and melt pool monitoring. Afterwards, the defects were characterized by computed tomography (CT) to identify the detection limits of the used in-situ techniques. T2 - LiM Conference 2023 - Lasers in Manufacturing CY - Munich, Germany DA - 26.06.2023 KW - Thermography KW - High temperature alloys KW - Additive Manufacturing KW - PBF-LB/M PY - 2023 AN - OPUS4-57947 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Schumacher, David A1 - Waske, Anja T1 - XCT data of metallic feedstock powder with pore size analysis N2 - X-Ray computed tomography (XCT) scan of 11 individual metallic powder particles, made of (Mn,Fe)2(P,Si) alloy. The data set consists of 4 single XCT scans which have been stitched together [3] after reconstruction. The powder material is an (Mn,Fe)2(P,Si) alloy with an average density of 6.4 g/cm³. The particle size range is about 100 - 150 µm with equivalent pore diameters up to 75 µm. The powder and the metallic alloy are described in detail in [1, 2]. KW - Additive Manufacturing KW - Feedstock powder KW - Powder Characterization KW - X-Ray Computed Tomography PY - 2022 DO - https://doi.org/10.5281/zenodo.5796487 PB - Zenodo CY - Geneva AN - OPUS4-55556 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -