TY - JOUR A1 - Schröder, Nina A1 - Rhode, Michael A1 - Kannengießer, Thomas T1 - Influence of microalloying on precipitation behavior and notch impact toughness of welded high‑strength structural steels N2 - Microalloying elements such as Nb and Ti are essential to increase the strength of quenched and tempered high-strength low alloy (HSLA) structural steels with nominal yield strength ≥ 690 MPa and their welded joints. Standards such as EN 10025–6 only specify limits or ranges for chemical composition, which leads to variations in specific compositions between steel manufacturers. These standards do not address the mechanical properties of the material, and even small variations in alloy content can significantly affect these properties. This makes it difficult to predict the weldability and integrity of welded joints, with potential problems such as softening or excessive hardening of the heat-affected zone (HAZ). To understand these metallurgical effects, previous studies have investigated different microalloying routes with varying Ti and Nb contents using test alloys. The high-strength quenched and tempered fine-grained structural steel S690QL is the basic grade regarding chemical composition and heat treatment. To evaluate weldability, three-layer welds were made using high-performance MAG welding. HAZ formation was investigated, and critical microstructural areas were identified, focusing on phase transformations during cooling and metallurgical precipitation behavior. Isothermal thermodynamic calculations for different precipitations were also carried out. Mechanical properties, especially Charpy notch impact toughness, were evaluated to understand the influence of different microalloys on the microstructure of the HAZ and mechanical properties. KW - High-strength structural steel KW - Gas metal arc welding KW - HAZ-softening KW - Notch impact toughness KW - Microalloying influences KW - Thermodynamic simulation PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-608548 DO - https://doi.org/10.1007/s40194-024-01827-0 SN - 0043-2288 SP - 1 EP - 13 PB - Springer AN - OPUS4-60854 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Quackatz, Lukas A1 - Westin, Elin Marianne A1 - Griesche, Axel A1 - Kromm, Arne A1 - Kannengießer, Thomas A1 - Treutler, Kai A1 - Wesling, Volker A1 - Wessman, Sten T1 - Assessing ferrite content in duplex stainless weld metal: WRC ‘92 predictions vs. practical measurements N2 - AbstractThe weldability of stainless steels is largely controlled by the chemical composition, and alloys with ferritic or ferritic-austenitic solidification show the highest resistance to hot cracking. As the resulting phase balance also affects the final properties, it may be beneficial to both foresee and measure the weld metal ferrite content. The WRC ‘92 constitution diagram is currently the most accurate prediction tool available, but it does not take the cooling rate into consideration and the precision may be less accurate for stainless steels with high ferrite numbers (FNs). This study aims to assess the reliability of the WRC ‘92 diagram for weld metals with FN  50. The chemical composition was altered through gas tungsten arc welding (GTAW) of UNS S32205 with ER347 filler wire that had been coated using physical vapor deposition (PVD) with either niobium (Nb), copper (Cu), nickel (Ni), manganese (Mn), carbon (C), or silicon (Si). The actual ferrite content was evaluated using image analysis, FeriteScope and X-ray diffraction (XRD). While predictions from the WRC ‘92 diagram were deemed acceptable for Ni, Si, and Mn, notable deviations were observed for Nb, Cu, and C. The FeriteScope exhibited a consistent trend with image analysis, albeit with slightly higher FN values, wider scatter, and the conversion factor from FN to vol% is open for discussion. The lowest accuracy and largest spread were obtained using non-contact XRD, rendering it unsuitable for ferrite measurements of welds. These findings underscore the need for improved prediction tools and appropriate measurement methods for assessing ferrite content in duplex weld metals. KW - Duplex stainless steel KW - Welding KW - Phase balance KW - Microscopy KW - Microstructure PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-618777 DO - https://doi.org/10.1007/s40194-024-01878-3 SN - 1878-6669 VL - 69 IS - 1 SP - 31 EP - 45 PB - Springer CY - Berlin AN - OPUS4-61877 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Quackatz, Lukas A1 - Westin, Elin Marianne A1 - Griesche, Axel A1 - Kromm, Arne A1 - Kannengießer, Thomas A1 - Treutler, Kai A1 - Wesling, Volker A1 - Wessman, Sten T1 - Assessing ferrite content in duplex stainless weld metal: WRC ‘92 predictions vs. practical measurements N2 - AbstractThe weldability of stainless steels is largely controlled by the chemical composition, and alloys with ferritic or ferritic-austenitic solidification show the highest resistance to hot cracking. As the resulting phase balance also affects the final properties, it may be beneficial to both foresee and measure the weld metal ferrite content. The WRC ‘92 constitution diagram is currently the most accurate prediction tool available, but it does not take the cooling rate into consideration and the precision may be less accurate for stainless steels with high ferrite numbers (FNs). This study aims to assess the reliability of the WRC ‘92 diagram for weld metals with FN  50. The chemical composition was altered through gas tungsten arc welding (GTAW) of UNS S32205 with ER347 filler wire that had been coated using physical vapor deposition (PVD) with either niobium (Nb), copper (Cu), nickel (Ni), manganese (Mn), carbon (C), or silicon (Si). The actual ferrite content was evaluated using image analysis, FeriteScope and X-ray diffraction (XRD). While predictions from the WRC ‘92 diagram were deemed acceptable for Ni, Si, and Mn, notable deviations were observed for Nb, Cu, and C. The FeriteScope exhibited a consistent trend with image analysis, albeit with slightly higher FN values, wider scatter, and the conversion factor from FN to vol% is open for discussion. The lowest accuracy and largest spread were obtained using non-contact XRD, rendering it unsuitable for ferrite measurements of welds. These findings underscore the need for improved prediction tools and appropriate measurement methods for assessing ferrite content in duplex weld metals. KW - Duplex stainless steel KW - Phase fraction prediction KW - WRC diagram PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-623682 DO - https://doi.org/10.1007/s40194-024-01878-3 VL - 69 SP - 31 EP - 45 PB - Springer Science and Business Media LLC AN - OPUS4-62368 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Giese, Marcel A1 - Gräbner, Maraike A1 - Schröpfer, Dirk A1 - Treutler, Kai A1 - Lorenz, Svenja A1 - Kannengießer, Thomas A1 - Wesling, Volker T1 - Alloy modification and ultrasonic-assisted milling of wear-resistant alloys with defined surfaces N2 - The reduction of CO2 emissions is closely linked to the development of highly efficient and economical steel components in plant and process engineering. To withstand the high combined corrosive, tribological, thermal, and mechanical stresses, wear-resistant coatings tailored to the application and steel grade are used. In addition to the increasing demand to substitute conventional cobalt alloys with nickel alloys, there is also a growing need for defined or functional surfaces of high integrity. Due to high tool wear, milling operations required to produce the complex geometries of the components are often not economically feasible for SMEs. By means of alloy modification of the filler metals for nickel-based plasma build-up welded wear-resistant coatings and by the use of innovative ultrasonic-assisted milling processes more favourable machinability shall be achieved without reducing the wear protection potential. In this paper, the influence of the microstructure and precipitation morphology adjusted by means of alloy modification on the machinability is investigated. This is done based on a wear protection alloy NiCrMoSiFeB (trade name: Colmonoy 56 PTA) typically used for screw machines, which substitutes conventional CoCr alloys (Stellite). Metallurgical investigations and in-situ measurements of occurring process forces and temperatures at the tool cutting edge during milling as well as subsequent investigations of tool wear and surface integrity allow a detailed analysis and correlation between microstructural properties and machinability. For the cast samples, a clear change in the microstructure and hardness can be seen through the addition of Al, Ti, or Nb. These differences lead to an improvement in the machining process for Nb. Al and Ti cause long-needled or star-shaped precipitations and hardness increases, which lead to higher cutting forces and increased tool wear. KW - Cladding KW - Wear resistant alloys KW - Alloy modification KW - Post-processing KW - Ultrasonic assisted milling KW - Renewable energy PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-622918 DO - https://doi.org/10.1007/s40194-024-01786-6 SN - 1878-6669 VL - 68 SP - 2567 EP - 2575 PB - Springer Science and Business Media LLC CY - Berlin ; Heidelberg AN - OPUS4-62291 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Roveda, Ilaria A1 - Serrano-Munoz, Itziar A1 - Haubrich, Jan A1 - Requena, Guillermo A1 - Madia, Mauro T1 - Investigation on the fatigue strength of AlSi10Mg fabricated by PBF-LB/M and subjected to low temperature heat treatments N2 - This work provides an investigation of the influence of low temperature heat treatments on the fatigue behavior of a PBF-LB AlSi10Mg alloy. Fatigue specimens are produced in form of round bars on a build platform preheated at 200 ◦C. The specimens have been tested in three different conditions: as-built, and after heat treatments at 265 ◦C for 1 h and 300 ◦C for 2 h. Prior to the fatigue testing, the defect distribution is analyzed by means of micro computed tomography. Subsequently, the peak over threshold method is successfully applied to provide a prediction of the size of killer defect. The defect population was of gas porosity type. No clear improvement of the fatigue performance is observed after the heat treatments. The fatigue strength predicted using fracture mechanics-based approaches is in good agreement with the experimental data. Among the studied approaches, short crack models provided the most conservative predictions. KW - PBF-LB/M AlSi10Mg KW - Fatigue strength KW - Defects KW - Kitagawa-Takahashi Diagram KW - Short Crack Models PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-607071 DO - https://doi.org/10.1016/j.matdes.2024.113170 SN - 0264-1275 VL - 244 SP - 1 EP - 12 PB - Elsevier Ltd. AN - OPUS4-60707 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Merz, Benjamin A1 - Schmidt, Jonathan A1 - Poka, Konstantin A1 - Mohr, Gunther A1 - Polte, Julian A1 - Hilgenberg, Kai T1 - Impact of illumination technique on the detectability of irregularities in high-resolution images of visual in-situ process monitoring in Laser Powder Bed Fusion N2 - The layerwise geometry build-up of additive manufacturing (AM) enables the possibility of in-situ process monitoring. The objective is the detection of irregularities during the build cycle, ensuring component quality and process stability. Focus of this work is the visual in-situ monitoring of the process of powder bed fusion with laser beam of metals (PBF-LB/M). Current state of the art visual monitoring systems for PBF-LB/M are limited by low resolution, allowing the detection of gross flaws. In this work a 65 Mpixel high-resolution monochrome camera is integrated into a commercial PBF-LB/M machine enabling a spatial resolution of approx. 17.2 µm/Pixel. The observed inhomogeneities are clustered into directly detectable irregularities, and indirectly detectable irregularities that can be inferred from the surface. In parallel, two different illumination techniques are realized in the process chamber and compared. The impact of the distinct illumination technique, direct light and dark field, on the identification of irregularities is evaluated. KW - Powder bed fusion with laser beam of metals KW - In-situ monitoring KW - High-resolution camera KW - Illumination technique PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-610929 DO - https://doi.org/10.1016/j.procir.2024.08.079 SN - 2212-8271 VL - 124 SP - 98 EP - 103 PB - Elsevier B.V. AN - OPUS4-61092 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Scheuschner, Nils A1 - Oster, Simon A1 - Mohr, Gunther A1 - Hilgenberg, Kai T1 - Comparison of NIR and SWIR thermography for defect detection in Laser Powder Bed Fusion N2 - Since laser powder bed fusion (PBF-LB/M) is prone to the formation of defects during the building process, a fundamental requirement for widespread application is to find ways to assure safety and reliability of the additively manufactured parts. A possible solution for this problem lies in the usage of in-situ thermographic monitoring for defect detection. In this contribution we investigate possibilities and limitations of the VIS/NIR wavelength range for defect detection. A VIS/NIR camera can be based on conventional silicon-based sensors which typically have much higher spatial and temporal resolution in the same price range but are more limited in the detectable temperature range than infrared sensors designed for longer wavelengths. To investigate the influence, we compared the thermographic signatures during the creation of artificially provoked defects by local parameter variations in test specimens made of a nickel alloy (UNS N07208) for two different wavelength ranges (~980 nm and ~1600 nm). KW - Laser powder bed fusion KW - PBF-LB/M KW - Thermography KW - Additive manufacturing KW - NDT PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-610380 DO - https://doi.org/10.1016/j.procir.2024.08.122 VL - 124 SP - 301 EP - 304 PB - Elsevier B.V. AN - OPUS4-61038 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Preuß, Bianca A1 - Lindner, Thomas A1 - Hanisch, Niclas A1 - Giese, Marcel A1 - Schröpfer, Dirk A1 - Richter, Tim A1 - Rhode, Michael A1 - Lampke, Thomas T1 - Surface Functionalization of Novel Work‐Hardening Multi‐Principal‐Element Alloys by Ultrasonic Assisted Milling N2 - The development of multi‐principal‐element alloys (MPEAs) with unique characteristics such as high work hardening capacity similar to well‐known alloy systems like Hadfield steel X120Mn12 (ASTM A128) is a promising approach. Hence, by exploiting the core effects of MPEAs, the application range of conventional alloy systems can be extended. In the present study, work‐hardening MPEAs based on the equimolar composition CoFeNi are developed. Mn and C are alloyed in the same ratio as for X120Mn12. The production route consists of cast manufacturing by an electric arc furnace and surface functionalization via mechanical finishing using ultrasonic‐assisted milling (USAM) to initiate work hardening. The microstructure evolution, the hardness as well as the resulting oscillating wear resistance are detected. A pronounced lattice strain and grain refinement due to the plastic deformation during the USAM is recorded for the MPEA CoFeNi‐Mn12C1.2. Consequently, hardness increases by ≈380 HV0.025 in combination with a higher oscillating wear resistance compared to the X120Mn12. This shows the promising approach for developing work‐hardening alloys based on novel alloy concepts such as MPEAs. KW - Electric arc furnace KW - Finish milling KW - High manganese steels KW - Multi-principal element alloy KW - Ultrasonic-assisted milling KW - Work hardening PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-608008 DO - https://doi.org/10.1002/adem.202400339 SN - 1438-1656 SP - 1 EP - 12 PB - Wiley VHC-Verlag AN - OPUS4-60800 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Rhode, Michael A1 - Nietzke, Jonathan A1 - Mente, Tobias T1 - Trapping and diffusion in high-pressure hydrogen charged CoCrFeMnNi high entropy alloy compared to austenitic steel 316L N2 - High entropy alloys (HEAs) have attracted considerable research attention as potential substitute materials for austenitic steels in high-pressure hydrogen environments. The corresponding hydrogen absorption, diffusion and trapping has received less scientific attention. Therefore, the CoCrFeMnNi-HEA was investigated and compared to an austenitic steel AISI 316L. Both were subjected to high-pressure hydrogen charging at 200 bar and 1000 bar. Thermal Desorption Analysis (TDA) was used to clarify the specific desorption behavior and hydrogen trapping. For this purpose, the underlying TDA spectra were analyzed in terms of a reasonable peak deconvolution into a defined number of peaks and the activation energies for the respective and predominant hydrogen trapping sites were then calculated. Both materials show comparable hydrogen diffusivity. However, there were significant differences in the absorbed hydrogen concentrations at both charging pressures. The calculated activation energies suggest strong hydrogen trapping in the CoCrFeMnNi-HEA. KW - High-entropy alloy KW - Hydrogen diffusion KW - Trapping KW - High-pressure charging KW - Thermal desorption analysis PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-611901 DO - https://doi.org/10.1016/j.ijhydene.2024.09.393 SN - 0360-3199 VL - 89 IS - 89 SP - 772 EP - 782 PB - Elsevier B.V. CY - Amsterdam, Netherlands AN - OPUS4-61190 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Theiler, Geraldine A1 - Cano Murillo, Natalia A1 - Halder, Karabi A1 - Balasooriya, Winoj A1 - Hausberger, Andreas A1 - Kaiser, Andreas T1 - Effect of high-pressure hydrogen environment on the physical and mechanical properties of elastomers N2 - This study presents the influence of high-pressure hydrogen environment on the physical and mechanical properties of two types of cross-linked hydrogenated acrylonitrile butadiene rubbers. Based on the CSA/ANSI standard, static exposures in hydrogen experiments were performed up to 100 MPa at 120 °C. Characterization before and after exposure was conducted by means of density and hardness measurements, dynamic mechanical analysis (DMA), tensile tests, compression set, FT-IR and AFM analyses to assess effects after decompression. While the effect of high-pressure exposure is significant immediately after exposure, most of the physical and mechanical properties recover after 48 hours. FT-IR, AFM, SEM and compression set results indicate, however, permanent effects. KW - Hydrogen KW - Mechanical properties KW - Elastomers KW - High-pressure hydrogen environment PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-597102 DO - https://doi.org/10.1016/j.ijhydene.2024.01.148 SN - 0360-3199 VL - 58 SP - 389 EP - 399 PB - Elsevier Ltd. AN - OPUS4-59710 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Theiler, Geraldine A1 - Cano Murillo, Natalia A1 - Hausberger, Andreas T1 - Effect of hydrogen pressure on the fretting behavior of rubber materials N2 - Safety and reliability are the major challenges to face for the development and acceptance of hydrogen technology. It is therefore crucial to deeply study material compatibility, in particular for tribological components that are directly in contact with hydrogen. Some of the most critical parts are sealing materials that need increased safety requirements. In this study, the fretting behavior of several elastomer materials were evaluated against 316L stainless steel in an air and hydrogen environment up to 10 MPa. Several grades of cross-linked hydrogenated acrylonitrile butadiene (HNBR), acrylonitrile butadiene (NBR) and ethylene propylene diene monomer rubbers (EPDM) were investigated. Furthermore, aging experiments were conducted for 7 days under static contions in 100 MPa of hydrogen followed by rapid gas decompression. Fretting tests revealed that the wear of these compounds is significantly affected by the hydrogen environment compared to air, especially with NBR grades. After the aging experiment, the friction response of the HBNR grades is characterized by increased adhesion due to elastic deformation, leading to partial slip. KW - Fretting wear KW - Rubbers KW - Hydrogen KW - High-pressure PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-608462 DO - https://doi.org/10.3390/lubricants12070233 VL - 12 IS - 7 SP - 1 EP - 17 PB - MDPI AN - OPUS4-60846 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Jentzsch, Stefan A1 - Stock, Daniel A1 - Häcker, Ralf A1 - Skrotzki, Birgit A1 - Darvishi Kamachali, Reza A1 - Klingbeil, Dietmar A1 - Kindrachuk, Vitaliy T1 - Shear Band Formation with Split Hopkinson Bar Experiments N2 - The essence of dynamic failure is closely linked to dramatic shear deformations which often lead to the formation of adiabatic shear bands (ASB). Under high loading velocities and the subsequent rapid temperature increase, the localization of shear strain is crucial in view of safety issues of systems in mechanical and aircraft engineering, especially with respect to fast rotating components and diverse crash scenarios. In this research, we perform high speed impact tests at the split Hopkinson pressure bar (SHPB) setup and use particular hat-shaped specimen geometries that resemble the stresses and failure conditions at the component level. In the first step, we specify a notched specimen geometry using finite element (FE) simulations to ensure pure shear. Further, quasi-static compressive tests and a series of impact tests at high strain rates of 10^3-10^4 s^-1 are conducted on specimens manufactured from a fine-grain structural steel with the properties of S355. Optical microscopy and electron backscatter diffraction (EBSD) of the sheared zones unveil significant localization to maximal shear strains of about 0.9 accompanied by grain refinement by factors 5 to 14. The displacements across the surface of the specimens are captured with subset-based local digital image correlation (DIC) during the impact time, and serve as an objective to validate a viscoplastic constitutive relationship. More precisely, the deformation distribution is accurately reproduced by the widely recognized Johnson-Cook (JC) model, which features an enhanced description of damage evolution. Thus, combining experimental and characterization techniques, continuum mechanics and reasonable optimization strategies for the identification of model parameters provides an efficient approach for comprehensive insights into the strain localization behaviour and its impact on the mechanical performance of S355 under extreme strain rates and deformations. KW - Adiabatic shear bands KW - Finite element analysis KW - Viscoplastic material modelling KW - Split Hopkinson pressure bar KW - Hat-shaped specimen KW - Johnson–Cook parameter identification PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-613339 DO - https://doi.org/10.1016/j.ijmecsci.2024.109749 VL - 284 SP - 1 EP - 14 PB - Elsevier BV AN - OPUS4-61333 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Bhadeliya, Ashok A1 - Rehmer, Birgit A1 - Fedelich, Bernard A1 - Jokisch, T. A1 - Skrotzki, Birgit A1 - Olbricht, Jürgen T1 - Fatigue and fracture in dual-material specimens of nickel-based alloys fabricated by hybrid additive manufacturing N2 - The integration of additive manufacturing with traditional processes, termed hybrid additive manufacturing, has expanded its application domain, particularly in the repair of gas turbine blade tips. However, process-related defects in additively manufactured materials, interface formation, and material property mismatches in dual-material structures can significantly impact the fatigue performance of components. This investigation examines the low cycle fatigue and fatigue crack growth behaviors in dual-material specimens of nickel-based alloys, specifically the additively manufactured STAL15 and the cast alloy 247DS, at elevated temperatures. Low cycle fatigue experiments were conducted at temperatures of 950 °C and 1000 °C under a range of strain levels (0.3%–0.8%) and fatigue crack growth tests were conducted at 950 °C with stress ratios of 0.1 and −1. Fractographic and microscopic analyses were performed to comprehend fatigue crack initiation and crack growth mechanisms in the dual-material structure. The results consistently indicated crack initiation and fatigue fracture in the additively manufactured STAL15 material. Notably, fatigue crack growth retardation was observed near the interface when the crack extended from the additively manufactured STAL15 material to the perpendicularly positioned interface. This study highlights the importance of considering yield strength mismatch, as well as the potential effects of residual stresses and grain structure differences, in the interpretation of fatigue crack growth behavior at the interface. KW - Hybrid additive manufacturing KW - Dual-material nickel-based alloys KW - High-temperature fatigue crack growth KW - Low cycle fatigue PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-609340 DO - https://doi.org/10.1016/j.jmrt.2024.08.211 SN - 2238-7854 VL - 32 SP - 3737 EP - 3749 PB - Elsevier B.V. AN - OPUS4-60934 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Sonntag, Nadja A1 - Piesker, Benjamin A1 - Ávila Calderón, Luis A1 - Mohr, Gunther A1 - Rehmer, Birgit A1 - Agudo Jácome, Leonardo A1 - Hilgenberg, Kai A1 - Evans, Alexander A1 - Skrotzki, Birgit T1 - Tensile and Low‐Cycle Fatigue Behavior of Laser Powder Bed Fused Inconel 718 at Room and High Temperature N2 - This study investigates the room‐ and high‐temperature (650 °C) tensile and low‐cycle‐fatigue behavior of Inconel 718 produced by laser powder bed fusion (PBF‐LB/M) with a four‐step heat treatment and compares the results to the conventional wrought material. The microstructure after heat treatment is characterized on different length scales. Compared to the wrought variant, the elastic and yield properties are comparable at both test temperatures while tensile strength, ductility, and strain hardening capacity are lower. The fatigue life of the PBF‐LB/M variant at room temperature is slightly lower than that of the wrought material, while at 650 °C, it is vice versa. The cyclic stress response for both material variants is characterized by cyclic softening, which is more pronounced at the higher test temperature. High strain amplitudes (≥0.7%) at room temperature and especially a high testing temperature result in the formation of multiple secondary cracks at the transitions of regions comprising predominantly elongated grain morphology and columns of stacked grains with ripple patterns in the PBF‐LB/M material. This observation and pronounced crack branching and deflection indicate that the cracks are controlled by sharp micromechanical gradients and local crystallite clusters. KW - Additive manufacturing KW - Fatigue damage KW - Heat treatment KW - Inconel 718 KW - Laser powder bed fusion KW - Low-cycle fatigue KW - Tensile strength PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-599316 DO - https://doi.org/10.1002/adem.202302122 SN - 1527-2648 SP - 1 EP - 17 PB - Wiley AN - OPUS4-59931 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Campari, Alessandro A1 - Konert, Florian A1 - Sobol, Oded A1 - Alvaro, Antonio T1 - A comparison of vintage and modern X65 pipeline steel using hollow specimen technique for in-situ hydrogen testing N2 - The transition toward a hydrogen-based economy requires a widespread transport and distribution network, and repurposed natural gas pipelines are a viable option. An assessment of the hydrogen-induced degradation of pipeline steels is needed to inject H2 gas into the existing infrastructure safely. The conservative and standardized method consists of in-situ tensile tests in an autoclave filled with high-pressure hydrogen gas. A proposed alternative method involves using a hollow specimen as containment volume and applying the gas pressure in the inner cavity. This technique has lower costs and shorter test preparation time but is not standardized yet. This study aims to evaluate and compare the tensile properties of API 5L X65 pipeline steel in two states: vintage and modern. The influence of the surface roughness is investigated through parallel tests with drilled and reamed specimens. Hydrogen tests are compared with reference tests in an inert environment. A significant hydrogen-induced decrease in tensile properties is observed, and no significant difference between vintage and modern X65 can be drawn. The reduction in tensile properties is more significant in specimens with higher inner surface roughness. The evaluation of surface conditions appears crucial when assessing the HE susceptibility of hydrogen transport and storage equipment. KW - Hydrogen embrittlement KW - Hollow specimen technique KW - Pipeline steel KW - SSRT PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-603013 DO - https://doi.org/10.1016/j.engfailanal.2024.108530 VL - 163 SP - 1 EP - 15 PB - Elsevier Ltd. AN - OPUS4-60301 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Grimault de Freitas, Tomás A1 - Konert, Florian A1 - Nietzke, Jonathan A1 - Krzysch, Zephanja A1 - Böllinghaus, Thomas A1 - Michler, Thorsten A1 - Wackermann, Ken A1 - Oesterlin, Heiner A1 - Tlili, Mohamed A1 - Ruchti, Peter A1 - Beitelschmidt, Denise A1 - Elsen-Humberg, Stephan A1 - Koenigs, Timo A1 - Systermans, Thomas A1 - Sobol, Oded T1 - Tensile testing in high-pressure gaseous hydrogen using the hollow specimen method N2 - Metallic materials, predominantly steels, are the most common structural materials in the various components along the hydrogen supply chain. Ensuring their sustainable and safe use in hydrogen technologies is a key factor in the ramp-up of the hydrogen economy. This requires extensive materials qualification, however, most of the accepted; and standardized test methods for determining the influence of gaseous hydrogen on metallic materials describe complex and costly procedures that are only available to a very limited extent worldwide. The hollow specimen technique is a simple, rapid, and economical method designed to overcome the limitations of the current methods for the qualification of metallic materials under high-pressure hydrogen gas. However, this technique is not yet standardized. The TransHyDE-H2Hohlzug project is presented in this article, along with the main steps required to optimize the hollow specimen technique. This includes closing knowledge gaps related to the specimen geometry, surface quality, and gas purity in dedicated working packages, thus contributing to a comprehensive standardization of the technique for tests in high-pressure hydrogen gas. KW - High-pressure Gaseous Hydrogen KW - Hydrogen Embrittlement KW - Tensile Testing KW - Hollow Specimen Technique PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-610557 DO - https://doi.org/10.1557/s43577-024-00776-9 VL - 49 SP - 1 EP - 9 PB - Springer Nature AN - OPUS4-61055 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Konert, Florian A1 - Campari, Alessandro A1 - Nietzke, Jonathan A1 - Sobol, Oded A1 - Paltrinieri, Nicola A1 - Alvaro, Antonio T1 - Evaluation of the tensile properties of X65 pipeline steel in compressed gaseous hydrogen using hollow specimens N2 - Hydrogen has great potential on the path towards decarbonization of the energy and transport sectors and can mitigate the urgent issue of global warming. It can be sustainably produced through water electrolysis with potentially zero emissions, and efficiently used (e.g., in fuel cell systems). Despite its environmental advantages, hydrogen-metal interactions could result in the degradation of the mechanical properties of several structural materials. In order to determine the magnitude of the material degradation in relation to hydrogen exposure, extensive material testing is required. The standardized procedure for in-situ testing for the quantification of the impact of compressed gaseous hydrogen (CGH2) relies on the utilization of an autoclave around the tested specimen. Such test set-up is complex, expensive, time-consuming and requires special equipment, trained personnel, and strict safety procedures. A relatively recent method to circumvent these issues and provide affordable results consists of using hollow specimens, thus applying the hydrogen pressure inside rather than outside the specimen. It allows to reduce the volume of hydrogen by several orders of magnitude and to perform the tests more efficiently and in a safer manner. This study focuses on evaluating the tensile properties of X65 vintage pipeline steel tested in a high-pressure hydrogen environment using hollow specimens. Tests are performed in 6 MPa H2 and Ar at the nominal strain rate of 10−6 s−1 to evaluate the reduced area at fracture and the elongation loss. The effect of surface finishing on crack initiation and propagation is investigated by comparing two different manufacturing techniques. In this way, this study provides insights into the applicability of a novel, reliable, and safe testing method which can be used to assess the hydrogen-assisted ductility loss in metallic materials. KW - Mechanical Engineering KW - Hydrogen Embrittlement KW - SSRT KW - Hollow specimen KW - Pipeline steel KW - In-situ tensile test PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-595887 DO - https://doi.org/10.1016/j.prostr.2024.01.074 SN - 2452-3216 VL - 54 SP - 1 EP - 8 PB - Elsevier B.V. AN - OPUS4-59588 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Konert, Florian A1 - Wieder, Frank A1 - Nietzke, Jonathan A1 - Meinel, Dietmar A1 - Böllinghaus, Thomas A1 - Sobol, Oded T1 - Evaluation of the impact of gaseous hydrogen on pipeline steels utilizing hollow specimen technique and μCT N2 - The high potential of hydrogen as a key factor on the pathway towards a climate neutral economy, leads to rising demand in technical applications, where gaseous hydrogen is used. For several metals, hydrogen-metal interactions could cause a degradation of the material properties. This is especially valid for low carbon and highstrength structural steels, as they are commonly used in natural gas pipelines and analyzed in this work. This work provides an insight to the impact of hydrogen on the mechanical properties of an API 5L X65 pipeline steel tested in 60 bar gaseous hydrogen atmosphere. The analyses were performed using the hollow specimen technique with slow strain rate testing (SSRT). The nature of the crack was visualized thereafter utilizing μCT imaging of the sample pressurized with gaseous hydrogen in comparison to one tested in an inert atmosphere. The combination of the results from non-conventional mechanical testing procedures and nondestructive imaging techniques has shown unambiguously how the exposure to hydrogen under realistic service pressure influences the mechanical properties of the material and the appearance of failure. KW - Energy Engineering and Power Technology KW - Condensed Matter Physics KW - Fuel Technology KW - Renewable Energy, Sustainability and the Environment KW - µCT KW - Hollow Specimen Technique KW - Hydrogen Embrittlement PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-595077 DO - https://doi.org/10.1016/j.ijhydene.2024.02.005 SN - 0360-3199 VL - 59 SP - 874 EP - 879 PB - Elsevier B.V. AN - OPUS4-59507 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Böllinghaus, Thomas A1 - Cross, Carl T1 - Obituary: Prof. Dr.-Ing. Hans Hoffmeister N2 - On November 3, 2023, our dear colleague, Prof. Dr.-Ing. Hans Hoffmeister, born in 1932 in Kassel, Germany, passed away in Ahrensburg, near Hamburg, Germany. KW - Metals and Alloys KW - Mechanical Engineering KW - Mechanics of Materials PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-594160 DO - https://doi.org/10.1007/s40194-023-01675-4 SP - 1 EP - 2 PB - Springer Science and Business Media LLC AN - OPUS4-59416 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Strauß, Lea A1 - Duarte, Larissa A1 - Kruse, Julius A1 - Madia, Mauro A1 - Löwisch, Günther T1 - An equivalent stress approach for predicting fatigue behavior of additively manufactured AlSi10Mg N2 - Laser-based powder bed fusion (PBF-LB) is an advanced additive manufacturing technique renowned for its precision and capability to fabricate complex metal components. However, the high thermal gradients and rapid cooling rates intrinsic to this process introduce significant process-induced effects, such as inhomogeneities, surface roughness, anisotropy, and residual stress, all of which critically influence the fatigue behavior of the produced parts. This study investigates the fatigue performance of AlSi10Mg samples produced by PBF-LB, examining the impact of varying surface conditions, geometries, and residual stress levels. Fatigue-life prediction models are formulated based on nominal stress amplitude, residual stress, form factor, crack-initiating inhomogeneity, and surface roughness, with smooth samples serving as a baseline reference. The study presents two empirical models for predicting fatigue life and fatigue strength using S–N curves and the Kitagawa–Takahashi diagram with the El Haddad approach, derived from comprehensive experimental data, including finite element modeling, fatigue-life measurements, surface roughness evaluations, and residual stress analysis. KW - AlSi10Mg KW - Kitagawa–Takahashi diagram KW - El Haddad KW - Equivalent stress KW - Fatigue-life prediction KW - PBF-LB/M PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-625176 DO - https://doi.org/10.1007/s40964-025-00974-0 SP - 1 EP - 16 PB - Springer Science and Business Media LLC AN - OPUS4-62517 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Poka, Konstantin A1 - Ali, Sozol A1 - Saeed, Waleed A1 - Merz, Benjamin A1 - Epperlein, Martin A1 - Hilgenberg, Kai T1 - Quality assurance via a cyber physical system of a PBF-LB/M machine N2 - Powder Bed Fusion with Laser Beam of Metals (PBF-LB/M) faces challenges in reproducibility and quality assurance, even for widely applied alloys like AlSi10Mg. This work introduces a digital provenance framework for PBF-LB/M, showcased through the EOS M 300–4 multi-laser machine. An Extract, Transform, Load (ETL) pipeline autonomously captures machine data, including scan vectors as well as process signals, and organizes them into a Digital Shadow (DS). The DS is further extended by external data sources, such as Melt Pool Monitoring (MPM), to enable comprehensive analysis and root cause identification. This approach ensures continuous data representation and facilitates the development of new quality metrics. Moreover, the framework enhances quality assurance and traceability, supports compliance with industry standards, and improves productivity. It also enables more precise cost calculations and predictive maintenance. By addressing these challenges, the framework is essential for advancing PBF-LB/M in industrial applications, achieving greater consistency and scalability in production. KW - PBF-LB/M KW - Data driven quality assurance KW - Data engineering KW - Digital shadow PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-625187 DO - https://doi.org/10.1007/s40964-025-00978-w SN - 2363-9520 VL - 10 IS - 3 SP - 1771 EP - 1783 PB - Springer Science and Business Media LLC AN - OPUS4-62518 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Zhu, Jiangchao A1 - Madia, Mauro A1 - Schurig, Michael A1 - Kruse, Julius A1 - Conrad, Fabian A1 - Schlums, Hartmut A1 - Kontermann, Christian A1 - Zerbst, Uwe T1 - On the use of representative specimens for the structural integrity assessment of safety-relevant rotating components N2 - Safety-relevant components, for which a failure in service could have catastrophic consequences, are usually designed for extremely low probability of failure and they are subjected to stringent part qualification procedures according to guidelines set by regulatory agencies. Manufacturers are often forced to perform tests on full scale or scaled components to ensure the structural integrity under defined loading conditions, which usually implies a huge experimental and financial effort. Therefore, companies try to develop new strategies such as digital twins, which allow to massively reduce costs, without compromising safety. This work presents a new quasi-static testing and assessment concept, the main idea of which is to replace, or at least reduce, the experimental testing on components by testing specimens representative of the component. Fracture mechanics specimens have been designed iteratively by numerical simulations to match the stress state at the crack-tip of the maximum permissible defect defined by regulatory agencies for the component. Potentially, the major benefit of the proposed approach is that the tests can be performed on conventional laboratory testing machines. The effectiveness of the methodology is demonstrated in case of the structural integrity assessment of a Ni-base superalloy aero-engine turbine disk at overspeed conditions. KW - Structural integrity KW - Turbine disk KW - Burst KW - Fracture mechanics KW - Representative specimens KW - Quasi-static testing PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-624208 DO - https://doi.org/10.1016/j.engfracmech.2024.110710 SN - 0013-7944 VL - 314 SP - 1 EP - 23 PB - Elsevier Ltd. AN - OPUS4-62420 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Erxleben, Kjell A1 - Kaiser, Sebastian A1 - Rhode, Michael A1 - Kannengiesser, Thomas A1 - Kromm, Arne T1 - In-service and repair welding of pressurized hydrogen pipelines–a review on current challenges and strategies N2 - Hydrogen is the energy carrier for a sustainable future without fossil fuels. As this requires a reliable transportation infrastructure, the conversion of existing natural gas (NG) grids is an essential part of the worldwide individual national hydrogen strategies, in addition to newly erected pipelines. In view of the known effect of hydrogen embrittlement, the compatibility of the materials already in use (typically low-alloy steels in a wide range of strengths and thicknesses) must be investigated. Initial comprehensive studies on the hydrogen compatibility of pipeline materials indicate that these materials can be used to a certain extent. Nevertheless, the material compatibility for hydrogen service is currently of great importance. However, pipelines require frequent maintenance and repair work. In some cases, it is necessary to carry out welding work on pipelines while they are under pressure, e.g., the well-known tapping of NG grids. This in-service welding brings additional challenges for hydrogen operations in terms of additional hydrogen absorption during welding and material compatibility. The challenge can be roughly divided into two parts: (1) the possible austenitization of the inner piping material exposed to hydrogen, which can lead to additional hydrogen absorption, and (2) the welding itself causes an increased temperature range. Both lead to a significantly increased hydrogen solubility in the respective materials compared to room temperature. In that connection, the knowledge on hot tapping on hydrogen pipelines is rare so far due to the missing service experiences. Fundamental experimental investigations are required to investigate the possible transferability of the state-of-the-art concepts from NG to hydrogen pipeline grids. This is necessary to ensure that no critical material degradation occurs due to the potentially increased hydrogen uptake. For this reason, the paper introduces the state of the art in pipeline hot tapping, encompassing current research projects and their individual solution strategies for the problems that may arise for future hydrogen service. Methods of material testing, their limitations, and possible solutions will be presented and discussed. KW - In-service KW - Welding KW - Hydrogen pipeline KW - Review PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-638847 DO - https://doi.org/10.1007/s40194-025-02127-x SN - 0043-2288 SP - 1 EP - 24 PB - Springer Science and Business Media LLC AN - OPUS4-63884 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Liepold, Philipp A1 - Kromm, Arne A1 - Kannengießer, Thomas T1 - A Force Based Determination of Hot Cracking Susceptibility N2 - Two high-strength, low-alloy Gas Metal Arc Welding (GMAW) wires were evaluated for their susceptibility to Solidification Cracking (SC) using a modified version of the Transverse Motion Weldability (TMW) test. In theoriginal TMW test, the Transverse Displacement Speed (TDS) is varied iteratively, and crack lengths are measured in each iteration. The modified version eliminates the need for multiple runs by continuously reducing the TDS over a single run. Rather than emphasizing crack lengths, this method assesses the reaction force to the TDS, thereby determining a Critical TDS (CTDS). This critical point directly correlates with the cessation of SC growth. CTDS values were measured under a range of welding parameters, thereby demonstrating the influence of Welding speed and arc energy (U × I/welding speed) on SC susceptibility for the tested filler metals. The CTDS data obtained from this testing method have the potential to provide valuable insights for practical applications in the field. KW - Force based KW - Neural Network KW - TRS PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-640140 DO - https://doi.org/10.5781/JWJ.2025.43.4.10 SN - 2466-2100 VL - 43 IS - 4 SP - 447 EP - 457 AN - OPUS4-64014 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Yang, Fan A1 - Meng, Xiangmeng A1 - Putra, Stephen Nugraha A1 - Bachmann, Marcel A1 - Rethmeier, Michael T1 - Numerical studies of process porosity suppression by magnetohydrodynamic technology during the laser beam welding of aluminum alloy N2 - Magnetohydrodynamic (MHD) technology is acknowledged as a promising method for mitigating the porosity defects in laser-welded joints of aluminum alloys. A transient 3D multi-physical numerical model of laser beam welding (LBW), coupled with the MHD and oscillating metal vapor plume model, is developed to study the suppression mechanisms of process porosity by an external magnetic field. The experimental results demonstrate that the porosity ratio is reduced by 93.5 % as the oscillating magnetic field is applied. This significant reduction confirms the effectiveness of the MHD technology in suppressing porosity defects. A downward time-averaged Lorentz force is induced in the weld pool, which affects the fluid flow pattern and the weld pool profile. The change of the flowing pattern in the weld pool by the magnetic field does not always have a positive effect on the porosity suppression. In addition, an analytical model shows that the bubble escape window is expanded by 62 % under the effect of the oscillating magnetic field. The additional upward velocity provided by the electromagnetic expulsive force on the bubbles and the change of weld pool profile are considered favorable factors in eliminating the porosity defects. The numerical and analytical model developed for analyzing the bubble escape window have been validated by experimental results. KW - Laser beam welding KW - Aluminum alloy KW - Process porosity defects KW - Magnetohydrodynamic technology KW - Bubble escape KW - Numerical simulation PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-637642 DO - https://doi.org/10.1016/j.ijheatmasstransfer.2025.127525 SN - 0017-9310 VL - 253 SP - 1 EP - 13 PB - Elsevier Ltd. AN - OPUS4-63764 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Yang, Keke A1 - Wang, Zhuoqun A1 - Haak, Viktor A1 - Olfert, Viktoria A1 - El-Sari, Bassel A1 - Hein, David A1 - Biegler, Max A1 - Rethmeier, Michael A1 - Meschut, Gerson T1 - A novel welding schedule for expanding the expulsion-free process window in resistance spot welding of dissimilar joints with ultra-high strength steel N2 - This study introduces a novel approach to expanding the maximum expulsion-free process window in resistance spot welding (RSW) of dissimilar joints between ultra-high strength steel (UHSS) and mild steel. Quantitative analysis revealed that expulsion is driven by the interaction between nugget growth rate and plastic shell thickness. Based on this finding, the welding schedule was optimized by applying a preheating current to form an initial plastic shell, followed by a ramp-up current profile during the main welding phase. Welding simulations indicated that the ramp-up current slowed nugget growth, improved plastic shell formation, and prevented nugget breakthrough, thereby reducing the risk of expulsion. Experimental validation showed a 19 % increase in maximum expulsion-free heat input, with the nugget diameter increasing by 7.6 % to 8.94 mm compared to the reference welding schedule. Furthermore, even when expulsion occurred beyond the process window, this optimization delayed its occurrence, minimizing its impact on spot weld quality. Finally, the optimized welding schedule also exhibited significant robustness. Despite a 2 mm initial gap disturbance, the maximum expulsionfree heat input increased by 57 %, while the nugget diameter grew by 30 % to 8.92 mm. These results confirm that the proposed approach effectively extends the process window by preventing expulsion and enhances process stability. KW - Expulsion KW - Resistance spot welding KW - Finite element modelling KW - Preheating KW - Ultra-high-strength steel PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-626877 DO - https://doi.org/10.1016/j.jmapro.2025.02.009 SN - 2212-4616 VL - 137 SP - 306 EP - 309 PB - Elsevier BV AN - OPUS4-62687 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Yalçınyüz, Aybike A1 - Raute, Julius A1 - Gonzalez-Gutierrez, Joamin A1 - Pei, Eujin A1 - Biegler, Max A1 - Rethmeier, Michael T1 - Electron Beam Bonding: A novel method for joining additively manufactured carbon fiber thermoplastic composites with aluminum to produce multi-material joints for lightweight applications N2 - In recent years, new solutions have been explored to reduce the weight of components for the automotive, railway, and aerospace industries. For this reason, Carbon Fiber Composites (CFCs) have increasingly replaced metals in products that need to be lightweight. However, due to their poor thermal conductivity, CFCs have limited use in applications requiring efficient heat dissipation. In such applications, conventionally manufactured metal alloys are typically utilized. To address these limitations, a novel approach using a combination of additively manufactured aluminum and CFCs is proposed to exploit the distinct advantages of both materials. These innovative hybrid structures aim to combine good structural and thermal management properties with reduced weight compared to conventionally produced metal products. In this study, additively manufactured aluminum alloy (AlSi10Mg) and short carbon fiber Polyamide 6 composite (sCF-PA6) are utilized to produce metal–polymer pairs using electron beam energy to bond the two materials. Direct irradiation of short CFCs with electron beam leads to polymer degradation. Thus, a novel method “Electron Beam Bonding” for joining CFCs with aluminum alloy in various joint configurations using electron beam technology is demonstrated. This innovative approach presents a promising solution for creating metal–polymer multi-materials for lightweight applications. KW - Electron beam bonding KW - Multi-material KW - Lightweight KW - Additive manufactured materials KW - Short carbon fiber composites KW - AlSi10Mg KW - Joining PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-641705 DO - https://doi.org/10.1007/s40964-025-01206-1 SN - 2363-9512 SP - 1 EP - 7 PB - Springer International Publishing CY - Cham AN - OPUS4-64170 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Meng, Xiangmeng A1 - Bachmann, Marcel A1 - Yang, Fan A1 - Rethmeier, Michael T1 - Toward prediction and insight of porosity formation in laser welding: A physics-informed deep learning framework N2 - The laser welding process is an important manufacturing technology for metallic materials. However, its application is often hindered by the occurrence of porosity defects. By far, an accurate prediction of the porosity defects and an insight into its formation mechanism are still challenging due to the highly nonlinear physics involved. In this paper, we propose a physics-informed deep learning (PIDL) framework by utilizing mechanistic modeling and experimental data to predict the porosity level during laser beam welding of aluminum alloys. With a proper selection of the physical variables (features) concerning the solidification, liquid metal flow, keyhole stability, and weld pool geometry, the PIDL model shows great superiority in predicting the porosity ratio, with a reduction of mean square error by 41 %, in comparison with the conventional DL model trained with welding parameters. Furthermore, the selected variables are fused into dimensionless features with explicit physical meanings to improve the interpretability and extendibility of the PIDL model. Based on a well-trained PIDL model, the hierarchical importance of the physical variables/procedures on the porosity formation is for the first time revealed with the help of the Shapley Additive Explanations analysis. The keyhole ratio is identified as the most influential factor in the porosity formation, followed by the downward flow-driven drag force, which offers a valuable guideline for process optimization and porosity minimization. KW - Laser beam welding KW - Physics-informed deep learning KW - Porosity prediction KW - Feature fusion KW - Hierarchical importance PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-624708 DO - https://doi.org/10.1016/j.actamat.2025.120740 VL - 286 SP - 1 EP - 13 PB - Elsevier B.V. AN - OPUS4-62470 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Akyel, Fatma A1 - Üstündag, Ömer A1 - Bakir, Nasim A1 - Brunner-Schwer, Christian A1 - Gumenyuk, Andrey A1 - Rethmeier, Michael T1 - Influence of heat input on cooling rates and mechanical properties of laser hybrid welded thick structural steels N2 - Laser hybrid welding presents several challenges when used to weld thick steels. A typical weld is divided into the arcdominated and laser-dominated zone. These zones lead to variations in the mechanical properties of the weld. The laserdominated zone is of particular importance regarding mechanical properties, notably Charpy impact toughness, due to the high cooling rates and the absence of filler wire. The low heat input of the laser can lead to martensitic microstructure causing hardening and deterioration of impact toughness. The high heat input of the arc can lead to grain coarsening and even loss of impact toughness. This study examines the influence of heat input on the cooling rates, microstructure and mechanical properties of single-pass laser hybrid welded steels of S355J2 and EH36 with thicknesses up to 30 mm. The experiments were performed with a 20-kW fibre laser and a contactless electromagnetic weld backing in the butt-joint configuration in 1G welding position. The cooling time was measured in three different locations near the fusion lines corresponding to different heights of the seam using a special configuration with pyrometers, collimators and optical fibres. The test specimens for the Charpy impact testing and tensile testing were extracted in three different depths. The experiments indicated that a heat input of 1.6 kJ/mm–2 kJ/mm, 2 kJ/mm–2.4 kJ/mm and 3.7 kJ/mm were recommended when single-pass laser hybrid welding of 20-, 25-, and 30-mm-thick structural steels regarding the minimum requirements of the mechanical properties, respectively. KW - Laser hybrid welding KW - Heat input KW - Mechanical properties KW - Charpy impact toughness KW - Cooling rate PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-625282 DO - https://doi.org/10.1007/s40194-025-01924-8 SN - 1878-6669 SP - 1 EP - 15 PB - Springer CY - United Kingdom AN - OPUS4-62528 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Willeke, Maraike A1 - Giese, Marcel A1 - Lorenz, Swenja A1 - Treutler, Kai A1 - Schröpfer, Dirk A1 - Wesling, Volker A1 - Kannengießer, Thomas T1 - Effect of alloy modification on the wear protection coatings made of Ni- and Co-based materials and surface machinability via ultrasonic milling process N2 - AbstractWear-resistant coatings are required for highly efficient and economical steel components in equipment, process, and power plant engineering to withstand high corrosive, tribological, thermal, and mechanical stresses. Co-alloys are used as wear-resistant coatings for steel components, tailored to the specific application. The substitutability of Co alloys with Ni-based wear protection systems, in addition to price and supply uncertainties, is facilitated by the combination of innovative welding and machining processes such as ultrasonic-assisted milling. The aim of the study is to improve the machinability of two different hard-facing alloys while maintaining the same wear protection potential. Therefore, the wear-resistant alloys NiMoCrSi (Colmonoy C56) and CoMnCrSi (Tribaloy T400) were modified by the alloying additions Nb, Hf, and Ti and then applied to a carbon-manganese steel S355 using the plasma transfer arc (PTA) welding process. The influence of the alloying additions on the microstructure as KW - Wear resistance KW - Co-based alloy KW - Ni-based alloy KW - PTA welding process KW - Ultrasonic assisted milling process PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-623931 DO - https://doi.org/10.1007/s00170-024-14955-0 SN - 0268-3768 SP - 1 EP - 17 PB - Springer Science and Business Media LLC AN - OPUS4-62393 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Liepold, Philipp A1 - Kromm, Arne A1 - Kannengießer, Thomas T1 - Transvarestraint testing of high-strength steel filler metal N2 - High-strength steel welds are typically not known to be susceptible to Solidification Cracking (SC). However, modern light-weight constructions may force welding in highly restrained conditions, which are known to increase the probability of Solidification Crack (SC) emergence. In this article, the Modified Varestraint-Transvarestraint (MVT) test was used to evaluate the hot cracking susceptibility of welds made from high-strength, low-alloyed filler material. The materials tested include solid wires and a metal-cored wire. All wires are typically used in the Gas Metal Arc Welding (GMAW) process. Susceptibility to SC was measured over a wide range of welding parameters and bending speeds. Results show little affinity of the tested materials to SC. However, crack length increases in most cases with arc energy ( U ∙ I∕welding speed ) and welding speed. The length of the longest crack in one test specimen follows a similar trend until high welding speeds, where stagnation of crack length with changing arc energy was observed. KW - MVT KW - Varestraint KW - Transvarestraint KW - Solidification cracking KW - High-strength steel PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-630084 DO - https://doi.org/10.1007/s40194-025-02042-1 SN - 1878-6669 VL - 2025 SP - 1 EP - 12 PB - Springer CY - Berlin ; Heidelberg AN - OPUS4-63008 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Reichel, Levin A1 - Kromm, Arne A1 - Michael, Thomas A1 - Schroepfer, Dirk A1 - Kannengiesser, Thomas T1 - Modern welding processes for optimizing repair welding on high-strength offshore steels N2 - The successful energy transition in Germany will require offshore wind turbines with outputs >10 MW in the future, for which high-strength steels with a yield strength of up to 500 MPa and wall thicknesses up to 150 mm are increasingly being used. The repair of weld seams when detecting defects during NDT requires localized gouging and rewelding. This involves high demands on welding manufacturing, especially for highstrength steels. Due to a lack of investigations, there are no repair concepts and information in standards and guidelines, particularly for high-strength thick plate joints made of high-strength offshore steels. However, these are urgently needed to enable processors, especially SMEs, to carry out safe and economical repairs. Therefore, BAM startedthe FOSTA project P1629 (IGF 01IF22746N) to investigate the stress-optimized repair(local gouging and welding) of high-strength thick plate joints made of offshore grades in the yield strength range off 355 to 460 MPa and similar weld metal with controlled high-performance GMAW processes and optimized narrower gouging grooves. The experimental analyses consider the complex interaction of material, process, and designrelated influences on the formation of weld-related stresses and the special microstructure of high-strength fine-grain structural steels. Welding-related material Degradation and crack-critical residual tensile stresses need to be avoided to ensure high component safety and performance. With component-related welding experiments on special testing equipment, adapted process and heat control concepts along with variable groove configurations will be developed and recommendations for guidelines elaborated. This is the prerequisite for fully utilizing the strength potential of high-strength steels and making a valuable contribution to the energy transition in Germany, especially for steelprocessing SMEs. T2 - 6. Symposium Materialtechnik CY - Clausthal-Zellerfeld, Germany DA - 20.02.2025 KW - Narrow groove KW - Optimized repair welding KW - Modern welding processes KW - High-strength steel PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-636520 DO - https://doi.org/10.21268/20250507-5 SP - 3 EP - 15 AN - OPUS4-63652 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Yang, Chunliang A1 - Yang, Fan A1 - Meng, Xiangmeng A1 - Putra, Stephen Nugraha A1 - Bachmann, Marcel A1 - Rethmeier, Michael T1 - Multi-refining effects of an AC electromagnetic field on the microstructure in AA5754 laser beam welding N2 - Fine-grain structure is beneficial to the mechanical properties of the joint. Different kinds of grain and sub-grain structures refined by magnetic field during laser beam welding of AA5754 aluminum alloy are analyzed in this manuscript, and the influences of different magnetic field parameters (magnetic flux density and frequency) in these refining effects are also studied. Using the scanning electron microscope (SEM), the sub-grain structure near the fusion line was obtained, and it was found that the branching promotion and branches refinement can be achieved by the magnetic field. The branches become finer with the magnetic flux density or frequency increases, and this effect is stronger in the dendritic region than in the equiaxed region. The results of electron backscatter diffraction (EBSD) in the equiaxed region show that a high-frequency magnetic field can greatly reduce the average grain size, while a low-frequency one has little effect. A phenomenological nucleation model based on dendrite fragmentation theory was established, and it was introduced into the phase field model to analyze the equiaxed grains evolution process. In addition, another refinement mechanism was also observed. The periodic solidification pattern caused by the unstable solidification in the molten pool can refine the grains, and the magnetic field promotes this kind of grain refinement by promoting the solidification period. KW - Laser beam welding KW - Magnetic field KW - Aluminum alloy KW - Crystal branch development KW - Periodic solidification pattern KW - Grain refinement PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-637222 DO - https://doi.org/10.1016/j.ijheatmasstransfer.2025.127509 SN - 0017-9310 VL - 252 SP - 1 EP - 16 PB - Elsevier Ltd. AN - OPUS4-63722 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Biegler, Max A1 - Yang, Keke A1 - Meschut, Gerson A1 - Rethmeier, Michael T1 - Occurrence and avoidance of liquid metal embrittlement in resistance spot welding of springback-afflicted deep-drawn components N2 - This study investigates the occurrence and mitigation of liquid metal embrittlement occurring during resistance spot welding in deep-drawn automotive components, specifically focusing on an S-Rail made from advanced high-strength steel. A simulation-based liquid metal embrittlement risk criterion based on local major component stresses was established and used to quantify and compare liquid metal embrittlement risks between different tests. Experimental and numerical analyses were conducted, revealing that springback significantly impacts liquid metal embrittlement formation. Adjustments in electrode geometry and hold time post-welding were found to mitigate liquid metal embrittlement risks. The effects of stack-up configuration and related parameter settings on liquid metal embrittlement occurrence were identified and liquid metal embrittlement was effectively prevented across both stack-up configurations. These findings advance the understanding of liquid metal embrittlement mechanisms and provide practical approaches to enhance the spot weld quality in AHSS-based body-in-whites. KW - Liquid metal embrittlement KW - Crack KW - Advanced high-strength steels KW - Resistance spot welding KW - Weld current KW - Heat input KW - Simulation KW - Springback KW - Deep drawing KW - S-Rail PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-636577 DO - https://doi.org/10.1177/13621718251340452 SN - 1362-1718 SP - 1 EP - 9 PB - SAGE Publications AN - OPUS4-63657 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Müller, Vinzenz A1 - Fasselt, Janek Maria A1 - Klötzer-Freese, Christian A1 - Kruse, Tobias A1 - Kleba-Ehrhardt, Rafael A1 - Biegler, Max A1 - Rethmeier, Michael T1 - Recycling nickel aluminium bronze grinding chips to feedstock for directed energy deposition via impact whirl milling: Investigation on processability, microstructure and mechanical properties N2 - During the production of ship propellers, considerable quantities of grinding chips from nickel aluminium bronze are produced. This paper examines the mechanical comminution of such chips via impact whirl milling and the utilization of two chip-powder batches as feedstock for a laser-based directed energy deposition process. The materials are characterized via digital image analysis, standardized flowability tests, scanning electron microscopy and energy dispersive X-ray spectroscopy and are compared to conventional, gas atomized powder. The specimens deposited via directed energy deposition are analyzed for density, hardness and microstructure and tensile properties for vertical and horizontal build up directions are compared. At elevated mill rotation speeds, the comminution with impact whirl milling produced rounded particles, favorable flow properties and particle size distribution, making them suitable to deposit additive specimens. The microstructure exhibited characteristic martensitic phases due to the high cooling rates of the additive manufacturing process. The presence of ceramic inclusions was observed in both the powder and on the tensile fracture surfaces, partly impairing the mechanical properties. However, specimens in the vertical build-up direction (Z) showed competitive tensile results, with 775 MPa in tensile strength, 455 MPa in yield strength and 12.6 % elongation at break. The findings of this study indicate that recycling of machining chips to additive manufacturing feedstock can be a viable option for reducing material costs and environmental impact. KW - Nickel aluminium bronze KW - Grinding chips KW - Recycling KW - Directed energy deposition KW - Material characterization PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-633442 DO - https://doi.org/10.1016/j.addma.2025.104804 SN - 2214-8604 VL - 105 SP - 1 EP - 9 PB - Elsevier BV AN - OPUS4-63344 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Marquardt, Raphael A1 - Biegler, Max A1 - Rethmeier, Michael T1 - Influence of laser power on the melt pool shape of handheld laser beam welding of 1.5 mm thick micro alloyed steel N2 - Manual welding of structures requires highly skilled welders due to the large heat-affected zone of arc-based processes, that can negatively impact microstructure and cause distortion. Handheld laser beam welding is a promising alternative with high welding velocity and a concentrated heat input. However, its current use in industry is limited to parts with aesthetic requirements, often made of high-alloyed steel. To extend the use of handheld laser beam welding to low-cost steels with good mechanical properties, this study investigates the influence of laser power on the melt pool shape for micro-alloyed steel with a thickness of 1.5 mm. Tested joint geometries are T-joints welded with filler wire as well as butt joints and overlap joints without filler wire, which are typically found in assemblies under mechanical load. Weld quality is assessed by weld porosity analysis. The results show that the handheld laser beam welding with filler wire produces T-joints with a very good external appearance, but with porosity between level C and D in the cross sections according to DIN EN ISO 13919-1. By increasing the laser power, a deep penetration of the T-joint zone can be achieved without increasing the actual throat thickness. For handheld laser beam welding of butt joints a full penetration weld of the highest quality class can be reached. Overlap joints can be welded with full or partial penetration depending on the laser power selected, with quality classes between B and C in terms of porosity. T2 - 20th Nordic Laser Materials Processing Conference CY - Kongens Lyngby, Denmark DA - 26.08.2025 KW - Hand held laser welding KW - Laser beam welding KW - Low alloyed steel KW - Process parameter PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-641671 DO - https://doi.org/10.1088/1757-899X/1332/1/012015 SN - 1757-899X VL - 1332 SP - 1 EP - 6 PB - Institute of Physics CY - London [u.a.] AN - OPUS4-64167 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Savitsky, Viktor A1 - Schmies, Lennart A1 - Gumenyuk, Andrey A1 - Rethmeier, Michael T1 - Comparative performance of DIC and optical flow algorithms for displacement and strain analysis in laser beam welding N2 - The measurement of strain and displacement in the context of the welding process represents a significant challenge. Optical methods, such as digital image correlation (DIC) or optical flow algorithms, have demonstrated their efficacy in robust and reliable data acquisition in harsh environments, including those encountered in welding processes. Concurrently, a trade-off between the accuracy of the measurement and the computational resources required for the associated calculations must be evaluated on a case-by-case basis. The application of filters to initial images represents a technique that serves to enhance the quality and accuracy of the strain and displacement prediction. In the present study, the estimated error of two algorithms, namely the Lucas-Kanade (LK) and the inverse compositional Gauss-Newton (IC-GN), is compared on the basis of both synthetic and real welding images. The displacement field is evaluated for different zones in the laser weld seam with varying contrast performance. Based on the aforementioned results, a strain calculation was conducted for both methods, which yielded comparable results for the LK and IC-GN algorithms. KW - Laser speckle KW - DIC KW - Optical flow KW - Error estimation KW - Strain measurement KW - Laser beam welding PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-625919 DO - https://doi.org/10.1016/j.optlaseng.2025.108870 SN - 1873-0302 VL - 187 SP - 1 EP - 15 PB - Elsevier Ltd. AN - OPUS4-62591 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Tobias, Charlie A1 - Gehrenkemper, Lennart A1 - Bernstein, Thomas A1 - Schlau, Sven A1 - Simon, Fabian A1 - Röllig, Mathias A1 - Meermann, Björn A1 - von der Au, Marcus T1 - Development of a fully automated slurry sampling introduction system for GF-AAS and its application for the determination of cadmium in different matrices N2 - element analysis, offering high sensitivity and precision. However, its effectiveness is limited by sample preparation challenges for solid samples like soils and microplastics. Traditional methods include sample preparation, such as digestion, which is time-consuming and involves reagents, like acids, contributing to measurement uncertainty and higher carbon footprints. Slurry sampling allows direct analysis of suspensions, offering a more efficient alternative. However, maintaining suspension stability is challenging, requiring robust autosampler systems to streamline the process and enhance analytical performance. Results: We present a novel autosampler extension for slurry sample introduction into GF-AAS. This system ensures suspension stability with a stirring device and closed vessels to prevent evaporation and contamination, incorporating a cooling unit to reduce solvent and analyte losses. It installs and removes in minutes without additional connections. Validation with cadmium analysis in BAM-U110 (Soil) and BAM-H010 (ABS) showed high reliability. For BAM-U110 (Soil), we achieved recovery rates of 94 % ± 13 % in water suspension. The recovery rate for BAM-H010 (ABS) was 104 % ±11 % in acetonitrile suspension. These results demonstrate the system’s robustness, versatility, and accuracy for different matrices. Significance: The autosampler extension helps solve key problems in trace element analysis of solid samples, making the process faster and more accurate. It works well with complex materials, making it useful for areas like microplastic or nanoparticle analysis. This improvement also helps meet regulations for monitoring environ mental and polymer samples, offering a reliable and flexible tool for high-throughput analysis with fewer errors. KW - Slurry AAS KW - Soil KW - Cd PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-618531 DO - https://doi.org/10.1016/j.aca.2024.343460 SN - 0003-2670 VL - 1335 SP - 1 EP - 7 PB - Elsevier BV AN - OPUS4-61853 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Erxleben, Kjell A1 - Kaiser, Sebastian A1 - Rhode, Michael A1 - Kannengiesser, Thomas A1 - Kromm, Arne T1 - In-service and repair welding of pressurized hydrogen pipelines–a review on current challenges and strategies N2 - Hydrogen is the energy carrier for a sustainable future without fossil fuels. As this requires a reliable transportation infrastructure, the conversion of existing natural gas (NG) grids is an essential part of the worldwide individual national hydrogen strategies, in addition to newly erected pipelines. In view of the known effect of hydrogen embrittlement, the compatibility of the materials already in use (typically low-alloy steels in a wide range of strengths and thicknesses) must be investigated. Initial comprehensive studies on the hydrogen compatibility of pipeline materials indicate that these materials can be used to a certain extent. Nevertheless, the material compatibility for hydrogen service is currently of great importance. However, pipelines require frequent maintenance and repair work. In some cases, it is necessary to carry out welding work on pipelines while they are under pressure, e.g., the well-known tapping of NG grids. This in-service welding brings additional challenges for hydrogen operations in terms of additional hydrogen absorption during welding and material compatibility. The challenge can be roughly divided into two parts: (1) the possible austenitization of the inner piping material exposed to hydrogen, which can lead to additional hydrogen absorption, and (2) the welding itself causes an increased temperature range. Both lead to a significantly increased hydrogen solubility in the respective materials compared to room temperature. In that connection, the knowledge on hot tapping on hydrogen pipelines is rare so far due to the missing service experiences. Fundamental experimental investigations are required to investigate the possible transferability of the state-of-the-art concepts from NG to hydrogen pipeline grids. This is necessary to ensure that no critical material degradation occurs due to the potentially increased hydrogen uptake. For this reason, the paper introduces the state of the art in pipeline hot tapping, encompassing current research projects and their individual solution strategies for the problems that may arise for future hydrogen service. Methods of material testing, their limitations, and possible solutions will be presented and discussed. KW - In-service KW - Hydrogen KW - Repair welding KW - Pipeline PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-638944 DO - https://doi.org/10.1007/s40194-025-02127-x SN - 0043-2288 SP - 1 EP - 24 PB - Springer Science and Business Media LLC AN - OPUS4-63894 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schmidt, Jonathan A1 - Merz, Benjamin A1 - Poka, Konstantin A1 - Mohr, Gunther A1 - Hilgenberg, Kai T1 - Surface structure analysis using visual high-resolution in situ process monitoring in laser powder bed fusion N2 - Parameter studies are a common step in selecting process parameters for laser powder bed fusion of metals (PBF-LB/M). Density cubes are commonly used for this purpose. Density cubes manufactured with varied process parameters can exhibit distinguishable surface structures visible to the human eye. The layer-wise process enables such surface structures to be detected during manufacturing. However, industrial visual in situ monitoring systems for PBF-LB/M currently have limited resolution and are incapable of reliably capturing small differences in the surface structures. In this work, a 65 MPixel high-resolution monochrome camera was integrated into an industrial PBF-LB/M machine together with a high-intensity LED (light-emitting diode) bar. Post-exposure images were taken to analyse differences in light reflection of fused areas. It is revealed that the grey-level co-occurrence matrix can be used to quantify the visual surface structure of nickel-based superalloy Inconel®939 density cubes per layer. The properties of the grey-level co-occurrence matrix correlate to the energy input and the resulting porosity of density cubes. Low-energy samples containing lack of fusion flaws show an increased contrast in the grey-level co-occurrence matrix compared to specimens with optimal energy input. The potential of high-resolution images for quality assurance via in situ process monitoring in PBF-LB/M is further discussed. KW - Additive manufacturing KW - Powder bed fusion KW - In situ monitoring KW - Image processing KW - High resolution camera PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-626685 DO - https://doi.org/10.1007/s40194-025-01955-1 SN - 1878-6669 SP - 1 EP - 15 PB - Springer Science and Business Media LLC AN - OPUS4-62668 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Rhode, Michael A1 - Czeskleba, Denis A1 - Fleißner-Rieger, H. A1 - Nietzke, Jonathan A1 - Kannengießer, Thomas T1 - Combined heating rate and restraint condition effect on stress relief cracking during PWHT of thick-walled Cr–Mo-V steel SAW joints N2 - Creep-resistant steels such as 13CrMoV9-10 are utilized in the manufacture of thick-walled pressure vessels and are typically joined by submerged arc welding (SAW). However, these materials are susceptible to stress relief cracking (SRC) if the required post weld heat treatment (PWHT) is not applied correctly. Existing PWHT guidelines, encompassing heating rate and dwell (or holding) time at a given temperature, are derived from a synthesis of empirical knowledge and typically free-shrinkage weld experiments to assess the susceptibility to SRC. Therefore, this study discusses the combined effect of the PWHT heating rate under free-shrinkage compared to restrained shrinkage. Welding experiments were conducted (using plates with a thickness of 25 mm) for both shrinkage conditions for a variety of heating rates and maximum temperatures. In-situ acoustic emission analysis was used to locate propagating SRCs during PWHT. Hardness measurements, mechanical property characterization (Charpy impact strength), and microstructure correlation were used to evaluate the SRC susceptibility. The results suggested that the influence of heating rate could not be directly related to SRC formation and that the initial weld microstructure prior to PWHT was more relevant in terms of very high hardness in the coarse grain heat affected zone, especially that of the last beads in the top layer of the welding sequence. This was seen in the form of random, unexpected SRC occurrence in only one specimen at a heating rate commonly used in welding practice (approximately 100 K/h). In this context, the additional effect of an external shrinkage restraint on SRC must be considered in the form of increasing mechanical loads during welding, which are typically not within the scope of welding practice. To mitigate the probability of SRC during PWHT, it is imperative to reduce the welding heat input and to restrict the structural shrinkage restraint of the weld joint. KW - Component test KW - Stress relief cracking KW - PWHT KW - Creep-resistant steel PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-631439 DO - https://doi.org/10.1007/s40194-025-02062-x SN - 1878-6669 SP - 1 EP - 17 PB - Springer Nature AN - OPUS4-63143 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Liepold, Philipp A1 - Kromm, Arne A1 - Kannengießer, Thomas T1 - Investigation of restraint intensity influence on solidification cracking of high-strength filler materials in fillet welds via CTS testing N2 - In addition to chemical composition, metallurgy, and welding parameters, the intensity of restraint is one of the key variables influencing solidification cracking (SC). Due to their high strength-to-density ratio, many modern lightweight steel constructions increasingly rely on high-strength steel. Given the theoretical framework of solidification cracking theory, tests tend to focus on the effects of strain rate. Externally restrained tests have provided valuable insights into solidification crack susceptibility. In practice, most welded structures are self-restrained; therefore, self-restraint tests more accurately reflect real-world applications. By varying the plate thickness in controlled thermal severity (CTS) tests conducted on S1100 QL, it was possible to adjust the intensity of restraint on fillet welds at a high level. Testing was performed using four different filler wires for gas metal arc welding (GMAW), including three solid wires and one metal-cored wire. Additionally, two sets of welding parameters were evaluated. High arc energy (U × I/welding speed) and increased welding speed were found to be more prone to solidification cracking compared to the parameter set with lower arc energy and welding speed. The results indicate a correlation between increasing restraint severity and a higher incidence of solidification cracking. KW - CTS KW - Controlled thermal severity KW - High-strength steel KW - GMAW KW - Restraint PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-631315 UR - 1878-6669 DO - https://doi.org/10.1007/s40194-025-02046-x SP - 1 EP - 13 PB - Springer AN - OPUS4-63131 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hübner, Martin A1 - Dittmann, Florian A1 - Kromm, Arne A1 - Varfolomeev, Igor A1 - Kannengießer, Thomas T1 - Residual stress reduction using a low transformation temperature welding consumable with focus on the weld geometry N2 - Low transformation temperature (LTT) welding consumables represent an innovative approach to realize compressive residual stress in the weld seam and HAZ. LTT welding consumables use the volume-expanding martensitic phase transformation near room temperature to generate compressive residual stress during cooling. This article focuses on the weld geometry and its influence on residual stress reduction using an LTT welding consumable. For this purpose, layers with an LTT welding consumable were additionally applied to the front sides of conventionally welded longitudinal stiffeners. Different weld geometries of the second weld seam could be realized by varying the welding parameters. These samples were analyzed for geometric parameters, chemical composition, and residual stress. While the chemical composition and martensite start temperature (MS) were only slightly influenced by parameter changes, a clear influence with regard to residual stress and weld geometry was observed. Depending on the shape of the second LTT weld seam, residual stress reductions of 200 to 500 MPa were achieved using the same LTT welding consumable. T2 - IIW Annual Assembly and International Conference CY - Rhodes Island, Dodecanisa, Greece DA - 07.07.2024 KW - Low transformation temperature (LTT) KW - Martensite start temperature KW - Dilution KW - Weld geometry KW - Residual stress PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-633707 DO - https://doi.org/10.1007/s40194-025-02094-3 SN - 1878-6669 SP - 1 EP - 11 PB - Springer Nature CY - Berlin ; Heidelberg AN - OPUS4-63370 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Engelking, Lorenz A1 - Scharf-Wildenhain, R. A1 - Schröpfer, Dirk A1 - Hälsig, A. A1 - Kannengießer, Thomas A1 - Hensel, J. T1 - Influence of heat input on properties and residual stresses in hybrid addi-tive manufacturing of high strength steels using MSG processes N2 - The application of steels with a higher yield strength allows reductions in wall thickness, component weight and production costs. Hybrid additive manufacturing based on Gas Metal Arc Welding (GMAW) processes (DED-Arc) can be used to realise highly effi-cient component modifications and repairs on semi-finished products and additively manufactured structures. There are still a number of key issues preventing widespread implementation, particularly for SMEs. In addition to the manufacturing design, detailed information about assembly strategy and geometric adaptation of the component for modifications or repairs are missing. These include the welding-related stresses associ-ated with the microstructural influences caused by the additive manufacturing steps, particularly in the transition area of the substrate and filler material interface. The pre-sent research focuses the effect of welding heat control during DED-Arc process on the residual stresses, especially in the transition area. Defined specimens were welded fully automatically with a high-strength solid wire (yield strength > 790 MPa) especially adapted for DED-Arc on S690QL substrate. The working temperature and heat input were systematically varied for a statistical effect analysis on the residual stress state of the hybrid manufactured components. Regarding heat control, t8/5 cooling times within the recommended processing range (approx. 5 s to 20 s) were complied. The investiga-tion revealed a significant influence of the working temperature Ti on the compressive residual stresses in the transition area and the tensile residual stresses at the base of the substrate. High working temperatures result in lower compressive residual stresses, heat input E does not significantly affect the tensile stresses. T2 - 6. Symposium Materialtechnik CY - Clausthal-Zellerfeld, Germany DA - 20.02.2025 KW - DED-Arc KW - Residual stress KW - Heat control PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-632188 DO - https://doi.org/10.21268/20250506-3 SP - 110 EP - 122 AN - OPUS4-63218 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kaiser, Sebastian A1 - Erxleben, Kjell A1 - Rhode, Michael A1 - Kannengießer, Thomas T1 - Schweißen im Betrieb an Wasserstoff-Ferngasleitungen N2 - Wasserstoff gilt als Energieträger für die Erreichung der Klimaziele und einer nachhaltigen zukünftigen Energieversorgung. Für den notwendigen Transport des Wasserstoffs in großem Maßstab und über weite Entfernungen ist eine zuverlässige Pipeline-Infrastruktur erforderlich. Umfassende weltweite Forschungsprojekte deuten auf die allgemeine Kompatibilität der verwendeten überwiegend ferritischen Stähle für die vorgesehenen Betriebsbedingungen von bis zu 60 °C bei 100 bar Wasserstoff hin. Dies ist jedoch nicht direkt übertragbar auf schweißtechnische Reparatur- und Wartungsarbeiten an im Betrieb befindlichen Pipelines. Ein im Erdgasnetz etabliertes Verfahren stellt das „Hot-Tapping“ dar, bei dem eine unter Druck stehende Pipeline im Betrieb angebohrt wird. Hierfür kommt ein an die Rohrleitung geschweißtes Formstück zum Einsatz, das die Montage der Bohr-/Lochschneidemaschine ermöglicht. In den Richtlinien EIGA 121/14 bzw. AIGA 033/14 wird darauf hingewiesen, dass das Anbohren von Wasserstoffleitungen kein Routineverfahren darstellt: “[…] a hydrogen hot-tap shall not be considered a routine procedure […]“. Dieser Aussage liegt unter anderem zugrunde, dass das Anschweißen des Formstücks an das Rohr und alle zu erwartenden Wärmebehandlungen vor und nach dem Schweißen eine lokale Temperaturerhöhung verursachen. Insbesondere auch an der Rohrinnenfläche, die dem Wasserstoff ausgesetzt ist. Diese erhöhten Temperaturen begünstigen die Absorption und Diffusion von Wasserstoff in das Material. Besonders zu beachten ist außerdem die lokal auftretende kurzzeitige Austenitisierung des Materials, die eine lokal stark erhöhte Wasserstoffkonzentration verursachen kann. Aus den genannten Gründen gibt diese Studie einen kurzen Überblick über die derzeit weltweit verfügbaren Forschungsprojekte zum Schweißen von Wasserstoff-Pipelines im Betrieb. Vorgestellt werden unter anderem erste Ergebnisse des Kooperationsforschungsprojektes H2SuD, das derzeit an der BAM bearbeitet wird. T2 - 6. Symposium Materialtechnik CY - Clausthal-Zellerfeld, Germany DA - 20.02.2025 KW - Materialdegradation KW - Pipeline KW - Schweißen KW - Wasserstoff PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-632731 SN - 978-3-8440-9961-4 SN - 978-3-8191-0041-3 DO - https://doi.org/10.21268/20250506-12 SN - 2364-0804 SN - 3052-3524 N1 - Serientitel: Fortschrittsberichte der Materialforschung und Werkstofftechnik – Series title: Bulletin of Materials Research and Engineering VL - 15 SP - 381 EP - 390 PB - Shaker Verlag CY - Düren AN - OPUS4-63273 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schröder, Nina A1 - Kromm, Arne A1 - Schröpfer, Dirk A1 - Kannengießer, Thomas T1 - Innovatives Instandsetzungsschweißen von Altstahl: Materialverhalten und Herausforderungen N2 - Aus Gründen der Nachhaltigkeit und Wirtschaftlichkeit gibt es in der stahlverarbeiten-den Industrie einen Trend zum Bauen im Bestand, um kostenintensive Sperrungen oder Rückbau zu vermeiden. Schweißen wird dabei als wirtschaftliches Fügeverfahren im Zusammenhang mit Altstählen kaum genutzt, obwohl Nieten- und Schraubenverbindungen oft unwirtschaftlich sind. Für die Instandsetzung ist häufig beschädigtes Bestands-material durch neue Stähle zu ersetzen bzw. Alt-Neu-Stahl-Mischverbindungen herzu-stellen. Aufgrund der verschiedenen Herstellungsprozesse von Altstählen ist nicht jeder Stahl aus dem 20. Jahrhundert schweißgeeignet. Daher ist zunächst eine Schweißeignungsprüfung erforderlich. In den vorliegenden Untersuchungen wurden verschiedene Altstähle hinsichtlich ihres Schweißverhaltens mittels Dilatometrie analysiert. Ziel war es, eine Datenbasis aus Schweiß-Zustands-Zeit-Diagrammen und Simulationen der Wärmeeinflusszone zu erstellen, um praxisrelevante Schweißuntersuchungen ableiten zu können. Diese geben wesentlichen Aufschluss hinsichtlich ihres schweißmetallurgischen Verhaltens und ihrer Schweißeignung. Solche Grundlagen sind zur Entwicklung innovativer schweißtechnischer Konzepte zur beanspruchungsgerechten Instandsetzung bestehender Altstahl-Infrastruktur in Deutschland notwendig. T2 - 6. Symposium Materialtechnik, 20. bis 21. Februar 2025 CY - Clausthal-Zellerfeld, Germany DA - 20.02.2025 KW - Altstahl KW - Schweiß-ZTU Diagramme KW - Instandsetzungsschweißen KW - Schweißeignungsprüfung KW - Dilatometrie PY - 2025 SN - 978-3-8440-9961-4 DO - https://doi.org/10.21268/20250505-1 VL - 15 SP - 370 EP - 380 PB - Shaker Verlag GmbH CY - Düren AN - OPUS4-63377 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Rhode, Michael A1 - Mente, Tobias A1 - Kannengießer, Thomas A1 - Czeskleba, Denis T1 - Simulation of hydrogen distribution in submerged arc welded heavy plates as tool for evaluating cold cracking sensitivity for offshore structures N2 - Foundation structures for offshore wind turbines are typically made of heavy plate struc-tural steels, such as S420ML, welded by submerged arc welding. Due to the welding process conditions, higher amounts of hydrogen can be introduced. In this context, large plate thicknesses result in long diffusion paths and a prolonged diffusion time for hydrogen at ambient temperature and possible delayed hydrogen-assisted cold cracking. As a result, hydrogen can accumulate in areas of high mechanical stress and strain. Due to the delayed diffusion, a minimum waiting time of up to 48 h must be observed before non-destructive testing can be performed. In addition, the assessment of possible cold crack locations is very complex. For this reason, a numerical model of a component-like weld test was developed to simulate the temperature field during welding and subsequent cooling. A hydrogen diffusion model based on the temporal-local temperature distribution was established. It was applied to simulate the change of hydrogen distribution as a function of temperature cycle during multi-layer welding and further for the entire waiting time interval ≤ 48 h. As a result, crack critical areas could be evaluated in terms of accu-mulated hydrogen. An advantage of the diffusion model is the simulation of a normalized concentration, i.e. between "0" (no hydrogen) and "1" (max. concentration), which can be scaled to experimentally determined hydrogen concentrations. Finally, selected results for increased real hydrogen ingress are presented, which confirm the relatively high crack resistance of the S420 submerged arc welded joint. KW - Hydrogen assisted cracking KW - Diffusion KW - Numerical simulation KW - Offshore steel PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-632416 DO - https://doi.org/10.21268/20250507-6 SP - 1 EP - 12 PB - Technische Universität Clausthal CY - Clausthal-Zellerfeld, Deutschland AN - OPUS4-63241 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Gupta, Kanhaiya A1 - Poka, Konstantin A1 - Ulbricht, Alexander A1 - Waske, Anja T1 - Identification and authentication of additively manufactured components using their microstructural fingerprint N2 - In the field of additive manufacturing, the ability to uniquely identify and authenticate parts is crucial for certification, logistics, and anti-counterfeiting efforts. This study introduces a novel methodology that leverages the intrinsic microstructural features of additively manufactured components for their identification, authentication, and traceability. Unlike traditional tagging methods, such as embedding QR codes on the surface or within the volume of parts, this approach requires no alteration to the printing process, as it utilizes naturally occurring microstructural characteristics. The proposed workflow involves the analysis of 3D micro-computed tomography data to identify specific voids that meet predefined identification criteria. This method is demonstrated on a batch of 24 parts manufactured with identical process parameters, proving capable of achieving unambiguous identification and authentication. By establishing a tamper-proof link between the physical part and its digital counterpart, this methodology effectively bridges the physical and digital realms. This not only enhances the traceability of additively manufactured parts but also provides a robust tool for integrating digital materials, parts databases, and product passports with their physical counterparts. KW - Authentication KW - Additive manufacturing KW - X-ray Computed Tomography KW - Digital fingerprint KW - Unique identification PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-630356 DO - https://doi.org/10.1016/j.matdes.2025.113986 SN - 1873-4197 VL - 254 SP - 1 EP - 12 PB - Elsevier Ltd. CY - Amsterdam AN - OPUS4-63035 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Huo, Wenjie A1 - Schmies, Lennart A1 - Gumenyuk, Andrey A1 - Rethmeier, Michael A1 - Wolter, Katinka T1 - Prediction of mean strain from laser beam welding images and detection of defects via strain curves based on machine learning N2 - With the advancement of machine learning, many predictions and measurements in visual tasks can be achieved by convolutional neural networks (CNNs). Solidification hot cracking is a significant defect in laser beam welding, commonly encountered in practical applications. Existing theories indicate that the formation of cracks is closely related to strain accumulation near the solidification front. In this paper, we first leverage supervised Regression networks to design CNNs that achieve real-time average strain estimation for each frame in the collected welding videos. Two different architectures are proposed and compared: the first model stacks two frames at a set interval and feeds them into the network, while the second model extracts image features individually and predicts the results by calculating the correlation between them. Each network has its own advantages in Terms of computational efficiency and accuracy. Finally, we further train a multilayer perceptron (MLP) classification model that can detect the occurrence of cracks based on the predicted strain behaviors. KW - Laser beam welding KW - Mean strain prediction KW - Solidification cracking detection Convolutional neural networks KW - Convolutional neural networks PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-644495 DO - https://doi.org/10.1016/j.optlastec.2025.113975 SN - 0030-3992 VL - 192, Part F SP - 1 EP - 8 PB - Elsevier Ltd. AN - OPUS4-64449 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Scharf-Wildenhain, R. A1 - Engelking, Lorenz A1 - Hälsig, A. A1 - Schröpfer, Dirk A1 - Kannengießer, Thomas A1 - Hensel, J. T1 - Effect of heat control on mechanical properties and residual stresses at the transition zone of component and substrate in hybrid DED‑arc manufacturing N2 - In hybrid additive manufacturing, components or semi-finished products manufactured by conventional primary forming are enhanced or modified by additive manufactured structures. However, systematic investigations focusing on the critical transition area between the specific properties of the substrate (like high-strength) and the additively manufactured component, made of specific filler material, are still lacking. The focus of the present study was to determine the influence of heat control on the Δt8/5 cooling time, the distortion, the mechanical properties, and the residual stresses in the transition area of hybrid-additive components. This contributed to the knowledge regarding the safe avoidance of cold cracking, excessive distortion, a reduction in yield stress, and the implementation of hybrid DED-arc manufacturing. The heat control was varied by means of heat input and working temperature such that the Δt8/5 cooling times corresponded to the recommended processing range. The heat input has a greater influence on the cooling time in the transition area than the working temperature. Working temperature and the total energy applied per layer have a significant effect on component distortion. The lowest working temperature of 100 °C in combination with the highest total energy per layer leads to significantly greater distortion compared to manufacturing with a high working temperature of 300 °C and low total energy per layer. In addition, the longitudinal residual compressive stresses in the sensitive transition area are reduced from − 500 MPa to approx. − 200 MPa by adjusting the working temperature from 100 to 300 °C. Such complex interactions must be clarified comprehensively to provide users with easily applicable processing recommendations and standard specifications for an economical hybrid additive manufacturing of components made, for example, of high-strength steels in the transition area. T2 - IIW Annual Assembly and International Conference CY - Rhodes Island, Greece DA - 07.07.2024 KW - Hybrid additive manufacturing KW - DED-arc KW - Heat control KW - High-strength metals KW - Residual stress PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-630415 DO - https://doi.org/10.1007/s40194-025-02036-z SN - 1878-6669 SP - 1 EP - 15 PB - Springer AN - OPUS4-63041 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -