TY - CONF A1 - Maierhofer, Christiane A1 - Ziegler, Mathias A1 - Kunert, M. A1 - Goldammer, M. T1 - Entwicklung von Referenzprobekörpern für die Standardisierung der Blitzthermografie N2 - Die aktive Thermografie wird in der Industrie zunehmend in verschiedenen Bereichen zur Qualitätssicherung, Zustandsdiagnose und Zustandsüberwachung eingesetzt. Bestehende Normen zur Thermografie beschreiben die Grundlagen, Geräte und Begriffe. In diesem Beitrag wird über ein Projekt berichtet, dessen Ziel die Erarbeitung einer Prüfnorm zur Blitzthermografie ist. Diese sollte neben der Auswahl geeigneter Gerätekomponenten, der Auswertungsverfahren und der Vorgehensweise bei der Prüfung auch die Beschreibung geeigneter Referenzprobekörper enthalten, die eine Bewertung der Messapparatur und eine Qualitätssicherung der Prüfung ermöglichen. T2 - Thermographie-Kolloquium 2011 CY - Stuttgart, Germany DA - 29.09.2011 KW - Aktive Thermografie KW - Blitzanregung KW - Prüfnorm KW - Referenzprobekörper PY - 2011 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-246230 SN - 978-3-940283-36-8 VL - 130 SP - 1 EP - 7 PB - Deutsche Gesellschaft für Zerstörungsfreie Prüfung (DGZfP) CY - Berlin AN - OPUS4-24623 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bartscher, M. A1 - Ehrig, Karsten A1 - Staude, Andreas A1 - Goebbels, Jürgen A1 - Neuschaefer-Rube, U. T1 - Application of an industrial CT reference standard for cast freeform shaped workpieces N2 - Industrial computed tomography (CT) today is an important method to analyze defects and to measure the geometry of technical products. The measurement capability of industrial CT often depends on the knowledge of the measurement errors being present. Only with this knowledge, effective corrections are possible by manufacturers, or adapted measurement procedures become possible for the customers. Thus, there is the strong need to have adequate reference standards both for the assessment of general dependencies and for the measurement of task-specific effects. Especially the latter are difficult to assess. This paper shows the application of a versatile dismountable workpiece-near reference body for the use with CT. The reference standard was made from a miniaturized cast aluminium (one-)cylinder head. It can be dismounted into four segments, each featuring reference geometries which enable a registration of CT measured and other reference datasets (e.g. from tactile CMM). The reference standard embodies complex freeform surfaces which are a challenging measurement task for CT and other sensors. Here the application of the reference standard is the study of the influence of material mixes. This is realized by adding pieces of other materials which disturb the mono-material measurement. Results of the application of the reference standard are presented using data from industrial micro-CT systems and CMM reference data. A special emphasis is given on the workflow of the data processing and the data analysis. T2 - International symposium on digital industrial radiology and computed tomography CY - Berlin, Germany DA - 20.06.2011 KW - Industrial reference standard KW - Computed tomographie KW - Freeform shaped workpieces PY - 2011 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-245532 SN - 978-3-940283-34-4 IS - DGZfP-BB 128 (We.4.3) SP - 1 EP - 12 PB - Deutsche Gesellschaft für zerstörungsfreie Prüfung e.V. (DGZfP) AN - OPUS4-24553 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Illerhaus, Bernhard A1 - Badde, Aurelia A1 - Michaelis, Matthias A1 - Berger, U. A1 - Onel, Yener A1 - Meinel, Dietmar A1 - Goebbels, Jürgen T1 - Einsatz von mobilen Röntgenuntersuchungsmethoden im Museum - Zwei Fallbeispiele N2 - Zwei Bildhauermodelle aus dem Georg-Kolbe-Museum Berlin standen zur Restaurierung an. Das kleinere, 'Lucino' (1920), 41cm, wurde hochauflösend mit CT gemessen, da mittels CT sowohl der Herstellungsprozeß einer Gipsstatue als auch der innere Zustand, wie Ergänzungen, Klebungen und Armierungen, festgestellt werden können. Aus den CT Bildern ergab sich eine für die vorher vermutete Gipszusammensetzung ungewöhnliche innere Struktur. Mit einer Freihand bedienten Röntgenpistole zur Messung der Röntgenfluoreszenz wurde daraufhin die Zusammensetzung des Materials der Statuette als Terracotta bestimmt. Durch den Einsatz von Helium als Spülmittel konnten auch leichte Materialien nachgewiesen und so eine Unterscheidung zwischen Gips und gebranntem Ton durchgeführt werden. Aus den CT Daten wurde eine virtuelle Darstellung der äußeren Geometrie gewonnen. Ein damit versuchsweise erstelltes Replik (Rapid Prototyping, 3D-Drucker, TU-Berlin) entsprach nicht den Anforderungen des Museums zur Erstellung einer Gußform für eine Bronzekleinserie der Statuette. Die zweite Statue, die 'Große Nacht' (1930) ist mit ihrer Größe von 2,12m und aufgrund des durch korrodierende Metallarmierung verursachten Schadensbildes nicht mehr transportfähig. Eine in-situ Untersuchung mit dem mobilen Tomographen, der in den 1980ern zur Untersuchung von Bäumen gebaut und jetzt mit einem modernen Flachdetektor und einer Röntgenröhre ausgestattet ist, wird vorgestellt. Die Möglichkeiten acder in-situ CT für große Skulpturen werden anhand der Ergebnisse diskutiert. T2 - DGZfP-Jahrestagung 2010 CY - Erfurt, Deutschland DA - 10.05.2010 KW - Mobile CT KW - Mobile RFA PY - 2010 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-246956 UR - https://www.ndt.net/?id=10149 SN - 978-3-940283-26-9 VL - 122 SP - 1 EP - 8 PB - Deutsche Gesellschaft für Zerstörungsfreie Prüfung (DGZfP) CY - Berlin AN - OPUS4-24695 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Dey, Anika A1 - Casperson, Ralf A1 - Pohl, Rainer A1 - Thomas, Hans-Martin T1 - Die Wirbelstromprüfung als Hilfsmittel für die Schieneninstandhaltung N2 - Die zerstörungsfreie Oberflächenprüfung an verlegten Eisenbahnschienen mit Wirbelstrom hat in den letzten Jahren durch ständige Weiterentwicklung und Verifizierung enorm an Bedeutung gewonnen. Es wurde u.a. angestrebt zuverlässige Planungsgrößen für den Einsatz von Instandhaltungsmaßnahmen zu erhalten, durch deren gezielten Einsatz Risswachstum unterbunden werden kann. Die Ursache für das Wachstum von Rissen in der Schiene liegt in der Materialermüdung des Werkstoffes infolge der Betriebsbelastungen im RadSchiene-Kontakt. Nach einer gewissen Beanspruchungsdauer kommt es an den Kontaktflächen der Fahrkante zu einer Kaltverfestigung des Schienenstahls. Durch fortschreitende Verfestigung des kontaktbeanspruchten Oberflächenbereichs der gehärteten Schicht wird der Werkstoff spröde und es bilden sich feine Risse aus. Die Risse wachsen anfangs unter einem flachen Winkel in das Schieneninnere hinein, neigen dann aber ab einem gewissen Stadium dazu in das Innere des Schienenkopfes abzukippen, was im Extremfall zu einem Schienenbruch führen kann. Diese Rollkontaktermüdungsrisse, auch genannt Head Checks, entstehen bevorzugt in der Fahrkante von bogenäußeren Schienen. Die Anwendung der Wirbelstromprüfung an der Schiene wurde bisher zur Ermittlung der Schädigungstiefe dieser Rollkontaktermüdungsrisse eingesetzt. Das Wirbelstromverfahren besitzt die Eigenschaft, sehr empfindlich auf alle Veränderungen der Materialeigenschaften an der Oberfläche zu reagieren. Daher wurde festgestellt, dass sich neben der Detektion von Rissen auch Fehler wie Eindrückungen oder Schlupfwellen, bis hin zu Materialveränderungen durch Schweißen oder Aufhärtungen in der Schienenoberfläche bestimmen lassen. Die Wirbelstromprüfung besitzt daher das Potenzial, mögliche Orte der Entstehung von Ermüdungsrissen in einem extrem frühzeitigen Stadium nachzuweisen. Ziel ist es, die rissgefährdeten Zonen schon im Zustand der Kaltverfestigung zu identifizieren. Dadurch können sich neue Aspekte für die präventive Schieneninstandhaltung ergeben. T2 - DGZfP-Jahrestagung 2010 - Zerstörungsfreie Materialprüfung ZfP in Forschung, Entwicklung und Anwendung CY - Erfurt, Germany DA - 10.05.2010 PY - 2010 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-214813 PB - Deutsche Gesellschaft für Zerstörungsfreie Prüfung (DGZfP) CY - Berlin AN - OPUS4-21481 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ehrig, Karsten A1 - Goebbels, Jürgen A1 - Meinel, Dietmar A1 - Paetsch, O. A1 - Prohaska, S. A1 - Zobel, Valentin T1 - Comparison of crack detection methods for analyzing damage processes in concrete with computed tomography N2 - Analyzing damages at concrete structures due to physical, chemical, and mechanical exposures need the application of innovative non-destructive testing methods that are able to trace spatial changes of microstructures. Here, the utility of three different crack detection methods for the analysis of computed tomograms of various cementitious building materials is evaluated. Due to the lack of reference samples and standardized image quality evaluation procedures, the results are compared with manually segmented reference data sets. A specific question is how automatic crack detection can be used for the quantitative characterization of damage processes, such as crack length and volume. The crack detection methods have been integrated into a scientific visualization system that allows displaying the tomography images as well as presenting the results. T2 - DIR 2011 - International symposium on digital industrial raidology and computed tomography CY - Berlin, Germany DA - 20.06.2011 KW - Crack detection KW - Computed tomography KW - Data visualization PY - 2011 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-243569 SN - 978-3-940283-34-4 IS - DGZfP-BB 128 (Poster 2) SP - 1 EP - 8 PB - Deutsche Gesellscahft für Zerstörungsfreie Prüfung e.V. (DGZfP) AN - OPUS4-24356 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Duffner, Eric A1 - Gregor, Christian A1 - Bohse, Jürgen T1 - Überwachung der Fertigungsqualität von Faserverbund - Druckbehältern mittels Schallemissionsprüfung N2 - Ziel der Untersuchung ist die Validierung einer Prüfmethodik zur Sicherung der Fertigungsqualität von Faserverbund – Druckbehältern unter realen Fertigungsbedingungen. Das Verfahren basiert auf Merkmalen und zulässigen Grenzwerten, die aus Schallemissionsverläufen bei der Erstdruckprüfung abgeleitet werden. Die Methodik konnte zuvor bereits erfolgreich an Faserverbund – Druckbehältern mit metallischem Liner getestet und patentiert werden. Mit den aktuellen Untersuchungen wurde die Möglichkeit des Erkennens von Fertigungsfehlern in Kohlenstofffaser/Glasfaser – Hybriddruckbehältern mit polymerem Liner evaluiert. Dazu wurden Faserverbund – Druckbehälter mittels Schallemissionsmessung bei einer hydraulischen Erstdruckprüfung überwacht, wie sie (ohne Schallemissionsprüfung) generell zur Qualitätssicherung nach der Fertigung von Faserverbund – Druckbehältern gefordert wird. An Druckbehältern aus einer Serienproduktion wurden die Schallemissionsverläufe registriert und die mittleren Merkmalswerte sowie deren Streuung als Referenz ermittelt. Diese werden mit den Schallemissionsverläufen von Druckbehältern mit gezielt eingebrachten Fertigungsfehlern verglichen. Bei den Fertigungsfehlern handelt es sich um Fehler, die in der Serienproduktion auftreten können und mit den Methoden der herkömmlichen Qualitätssicherung schwer oder gar nicht nachzuweisen sind. Alle untersuchten Druckbehälter wurden im Anschluss an die Erstdruckprüfung auf verschiedene Weise bis zum Versagen (Leckage, Bersten) beansprucht. Damit war es möglich, den tatsächlichen Einfluss der Fertigungsfehler auf den Berstdruck bzw. das Ermüdungsverhalten der Behälter zu verifizieren und die Aussagefähigkeit des Schallemissionsverfahrens zu beurteilen. T2 - 18. Kolloquium Schallemission CY - Wetzlar, Germany DA - 27.10.2011 KW - Faserverbund-Druckbehälter KW - Schallemissionsprüfung KW - Fertigungsüberwachung PY - 2011 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-247881 SN - 978-3-940283-37-5 IS - DGZfP-BB 131 (Vortrag 16) SP - 1 EP - 9 AN - OPUS4-24788 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Gaal, Mate A1 - Caldeira, Rui A1 - Bartusch, Jürgen A1 - Kupnik, M. T1 - Air-coupled ultrasonic ferroelectret receiver with additional DC voltage N2 - Highly sensitive air-coupled ultrasonic sensors are essential for various applications such as testing of composite materials. One of the major challenges for the development of air-coupled ultrasonic sensors is the impedance matching to air. With a lower acoustic impedance than the usual piezoelectric materials, charged cellular polypropylene film (cPP) offers better matching to air with a similar piezoelectric coefficient. The piezoelectric behaviour demonstrated by cPP comes from polarized air cells that create a permanent internal voltage. The sensitivity of the sensor varies with the application of an additional DC bias voltage. Thus, this work presents a cPP ultrasonic sensor with an improvement of up to 15 ± 1 dB on the signal-to-noise ratio. T2 - Eurosensors 2017 CY - Paris, France DA - 3.9.2017 KW - Ultrasonic KW - Air-coupled KW - Cellular polypropylene KW - Transducer KW - Ferroelectret PY - 2017 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-419009 DO - https://doi.org/10.3390/proceedings1040362 VL - 1 IS - 4 SP - Article 362, 1 EP - 4 AN - OPUS4-41900 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wachsmuth, Janne T1 - Wellenform basierte Quellenlokalisierung im Vergleich zu konventionellen Methoden N2 - Für eine 10 mm dicke Stahlplatte kann ein Bandpass so gesetzt werden, dass alle vorhandenen Wellenmoden mit derselben Schallgeschwindigkeit eintreffen. Anhand von Ortungsabweichungen und Ortungsunsicherheitswerten kann gezeigt werden, dass im Vergleich zu herkömmlichen Methoden der Quellenortung die Ortungsgenauigkeit durch eine Frequenzfilterung verbessert werden kann. T2 - 18. Kolloquium Schallemission CY - Wetzlar, Deutschland DA - 27.10.2011 KW - Schallemissionsprüfung KW - Ermüdungsrisswachstum KW - Korrosion PY - 2011 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-246612 SN - 978-3-940283-37-5 SP - 1 EP - 6 PB - DGZfP-BB 131 AN - OPUS4-24661 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Jaenisch, Gerd-Rüdiger A1 - Kolkoori, Sanjeevareddy A1 - Bellon, Carsten T1 - Quantitative simulation of back scatter X-ray imaging and comparison to experiments N2 - X-ray backscatter imaging is a well established NDT technique to inspect complex objects using only a single-sided access. In difference to conventional transmission X-ray radiography, the X-ray backscatter imaging utilizes the scattered radiation caused by the Compton scattering effect. In order to achieve high backscatter intensities from a test object, it is necessary to optimize the backscatter system parameters namely the angle between source and slit camera, the slit collimator system, the shielding between source and scatter camera, and the type of detector. In addition, the scatter phenomena in to the investigated object need to be understood. In this contribution, we present a Monte Carlo model McRay which considers all relevant single and multiple interactions of photons and electrons. This model can be used to simulate back scatter techniques. It allows not only calculating the scatter image for a given experimental setup but also registering the spectrum of the detected scattered photons. Both aspects are important to understand the imaging process, to interpret the results, and to optimize the backscatter camera investigated here. Additionally experimental results will be presented and compared with simulations. T2 - 19th World Conference on Nondestructive Testing CY - Munich, Germany DA - 13.06.2016 KW - Radiology KW - Back-scatter techniques KW - Simulation KW - Monte Carlo methods KW - Measurements PY - 2016 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-365897 SN - 978-3-940283-78-8 VL - 158 SP - 1 EP - 11 PB - Deutsche Gesellschaft für zerstörungsfreie Prüfung (DGZfP) CY - Berlin, Germany AN - OPUS4-36589 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Mishra, Kirti Bhushan A1 - Wehrstedt, Klaus-Dieter A1 - Krebs, Holger T1 - Boiling liquid expanding vapour explosion (BLEVE) of peroxy-fuels: Experiments and computational fluid dynamics (CFD) simulation N2 - Fire and explosion hazards associated with storage and transportation of flammable materials have been a matter of great interest in the recent times. BLEVE is a scenario that occurs when a closed fuel container is subjected to heat for a longer duration. Such events are disastrous to human beings and assets both. In the past there have been numerous studies on BLEVEs and fireballs of hydrocarbon fuels, e.g. kerosene, gasoline, LPG, LNG and others. Though, the fireballs of peroxy-fuels are not looked into detail as such. This article tries to overcome this lack of knowledge. Both, experimental investigation and CFD simulations are performed to measure and predict the fireball characteristics of a peroxy-fuel. Due to thermal decomposition in the liquid phase and active oxygen content a peroxy-fuel fireball burns at a very fast rate and emit higher thermal radiation whereas exhibits smaller diameter and elevation compared to hydrocarbons. That eventually leads to consideration of larger safety distances from them which are also verified by CFD results. KW - BLEVE KW - Hydrocarbons KW - Peroxy-fuels KW - Safety distances KW - CFD simulation PY - 2015 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-334184 DO - https://doi.org/10.1016/j.egypro.2015.02.082 SN - 1876-6102 VL - 66 SP - 149 EP - 152 PB - Elsevier Ltd. CY - Amsterdam AN - OPUS4-33418 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kraehnert, R. A1 - Ortel, Erik A1 - Paul, B. A1 - Eckhardt, B. A1 - Kanis, M. A1 - Liu, R. A1 - Antoniou, A. T1 - Electrochemically dealloyed platinum with hierarchical pore structure as highly active catalytic coating N2 - Micro structured reactors are attractive candidates for further process intensification in heterogeneous catalysis. However, they require catalytic coatings with significantly improved space-time yields compared to traditional supported catalysts. We report the facile synthesis of homogeneous nanocrystalline Pt coatings with hierarchical pore structure by electrochemical dealloying of amorphous sputter-deposited platinum silicide layers. Thickness, porosity and surface composition of the catalysts can be controlled by the dealloying procedure. XPS analysis indicates that the catalyst surface is primarily composed of metallic Pt. Catalytic tests in gas-phase hydrogenation of butadiene reveal the typical activity, selectivity and activation energy of nanocrystalline platinum. However, space time yields are about 13 to 200 times higher than values reported for Pt-based catalysts in literature. The highly open metallic pore structure prevents heat and mass transport limitations allowing for very fast reactions and reasonable stability at elevated temperatures. KW - Pt catalysts KW - Pt–Si layers KW - Scanning Electron Microscopy (SEM) KW - Transmission Electron Microscopy (TEM) KW - pore structure KW - electrochemical dealloying PY - 2015 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-351393 DO - https://doi.org/10.1039/C4CY00851K SN - 2044-4753 SN - 2044-4761 VL - 5 IS - 1 SP - 206 EP - 216 PB - RSC Publ. CY - Cambridge AN - OPUS4-35139 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Hemmann, Felix A1 - Agirrezabal-Telleria, Iker A1 - Jäger, Christian A1 - Kemnitz, E. T1 - Quantification of acidic sites of nanoscopic hydroxylated magnesium fluorides by FTIR and 15N MAS NMR spectroscopy N2 - Lewis and Brønsted sites were quantified in a series of weak acidic hydroxylated magnesium fluorides by Fourier transform infrared spectroscopy (FTIR) and solid state nuclear magnetic resonance spectroscopy (NMR) with pyridine as probe molecule. Molar extinction coefficients, which are necessary for quantitative FTIR measurements, were calculated by an easy approach. It utilizes the fact that both signals, used for the quantification by FTIR, are caused by the same deformation vibration mode of pyridine. Comparison of quantitative FTIR experiments and quantification by NMR shows that concentrations of acidic sites determined by FTIR spectroscopy have to be interpreted with caution. Furthermore, it is shown that the transfer of molar extinction coefficients from one catalyst to another may lead to wrong results. Molar extinction coefficients and concentrations of acidic sites determined by FTIR spectroscopy are affected by grinding and probably the particle size of the sample. High temperature during FTIR experiments has further impact on the quantification results. KW - Acidity KW - Fluoride catalyst KW - Infrared spectroscopy KW - Adsorption of pyridine KW - Molar extinction coefficient determination PY - 2015 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-351448 DO - https://doi.org/10.1039/C5RA15116C SN - 2046-2069 VL - 5 IS - 109 SP - 89659 EP - 89668 PB - RSC Publishing CY - London AN - OPUS4-35144 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Nguyen, Thi Yen A1 - Rademann, K. A1 - Emmerling, Franziska T1 - Direct evidence of polyamorphism in paracetamol N2 - While polymorphism is a common phenomenon in the crystallization processes of organic compounds, polyamorphism has gained importance only recently. Using sophisticated sample environments and applying in situ scattering methods and vibrational spectroscopy, the complete crystallization process of organic compounds from solution can be traced and characterized. Diffuse scattering from amorphous intermediates can be investigated by analyzing the atomic pair distribution function (PDF) to gain further insights into molecular pre-orientation. The crystallization behavior of paracetamol was studied exemplarily under defined, surface-free conditions. Based on the choice of the solvent, the formation of different polymorphs is promoted. The thermodynamically stable form I and the metastable orthorhombic form II could be isolated in pure form directly from solution. For both polymorphs, the crystallization from solution proceeds via a distinct amorphous precursor phase. PDF analyses of these different amorphous states indicate a specific pre-orientation of the analyte molecules introduced by the solvent. The resulting crystalline polymorph is already imprinted in these proto-crystalline precursors. Direct experimental evidence for the polyamorphism of paracetamol is provided. PY - 2015 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-351366 DO - https://doi.org/10.1039/C5CE01583A SN - 1466-8033 VL - 17 IS - 47 SP - 9029 EP - 9036 PB - Royal Society of Chemistry CY - London, UK AN - OPUS4-35136 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bellon, Carsten A1 - Gollwitzer, Christian A1 - Fratzscher, Daniel A1 - Ewert, Uwe A1 - Jaenisch, Gerd-Rüdiger T1 - Simulation of complex scan paths for 3D reconstruction N2 - X-ray computed tomography (CT) is a volumetric (3D) Imaging diagnostic method, well established in the medical field, and in industrial NDE as well. Developments in industrial CT aim to extent the applicability to complex structures, which do not allow the access of all directions. This are e.g. limited view, data and angle CT applications. New reconstruction algorithms are required on one side, and the accuracy has to be improved on the other side. Numerical Simulation can support such developments by providing well defined data sets for the testing of reconstruction algorithms. This approach of virtual CT is realized within the radiographic simulator aRTist, developed by BAM. The poster shows the possibilities of this tool to consider complex scan paths. Simulated data sets have been reconstructed by an versatile backprojection algorithm. T2 - International symposium on digital industrial radiology and computed tomography CY - Berlin, Germany DA - 20.06.2011 KW - Radiographie KW - Computer-Simulation KW - 3D-Rekonstruktion PY - 2011 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-243928 SN - 978-3-940283-34-4 IS - DGZfP-BB 128 (Poster 17) SP - 1 EP - 4 PB - Deutsche Gesellschaft für zerstörungsfreie Prüfung e.V. (DGZfP) AN - OPUS4-24392 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Abbott, A. P. A1 - Abolibda, T. Z. A1 - Davis, S.J. A1 - Emmerling, Franziska A1 - Lourdin, D. A1 - Leroy, E. A1 - Wise, W. R. T1 - Glycol based plasticisers for salt modified starch N2 - Starch is one of the most common and easily obtained natural polymers, making it attractive as a potential bio-based alternative to synthetic polymers. This study shows that a simple quaternary ammonium salt combined with urea or glycols forms effective modifiers that produce flexible plastics with good mechanical properties that are comparable to some polyolefin plastics. The processing conditions are shown to significantly affect the structure of the polymer which has a concomitant effect upon the mechanical and physical properties of the resulting plastic. Using a glycerol based modifier results in a totally sustainable and biodegradable material which can be injection moulded. KW - biodegradable material KW - flexible plastics KW - injection moulded PY - 2014 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-351426 DO - https://doi.org/10.1039/C4RA06220E SN - 2046-2069 VL - 4 IS - 76 SP - 40421 EP - 40427 PB - RSC Publishing CY - London AN - OPUS4-35142 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Gollwitzer, Christian A1 - Bellon, Carsten A1 - Deresch, Andreas A1 - Ewert, Uwe A1 - Jaenisch, Gerd-Rüdiger T1 - On POD estimations with radiographic simulator aRTist N2 - The computer simulation of radiography is applicable for different purposes in NDT such as for the qualification of NDT systems, the optimization of system parameters, feasibility analysis, model-based data interpretation, education and training of NDT/NDE personnel, and others. Within the framework of the European project PICASSO simulators will be adapted to support reliability assessments of NDT tasks. The radiographic simulator aRTist developed by BAM is well suited for this task. It combines analytical modelling of the RT inspection process with the CAD-orientated object description applicable to various industrial sectors such as power generation, aerospace, railways and others. The analytic model includes the description of the radiation source, the interaction of Radiation with the material of the part, and the detection process with special focus to DIR. To support reliability estimations the simulation tool is completed by a tool for probability of detection (POD) estimation. It consists of a user interface for planning automatic simulation runs with varying parameters, specifically defect variations. Further, an automatic image analysis procedure is included to evaluate the defect visibility and calculate the POD therefrom. T2 - International symposium on digital industrial radiology and computed tomography CY - Berlin, Germany DA - 20.06.2011 KW - Radiographie KW - Computersimulation KW - Probability of detection PY - 2011 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-245092 SN - 978-3-940283-34-4 IS - DGZfP-BB 128 (Tu.2.3) SP - 1 EP - 8 PB - Deutsche Gesellschaft für zerstörungsfreie Prüfung e.V. (DGZfP) AN - OPUS4-24509 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Sötebier, Carina A. A1 - Kutscher, D. J. A1 - Rottmann, L. A1 - Jakubowski, Norbert A1 - Panne, Ulrich A1 - Bettmer, J. T1 - Combination of single particle ICP-QMS and isotope dilution analysis for the determination of size, particle number and number size distribution of silver nanoparticles N2 - Single particle ICP-MS (spICP-MS) has gained great influence in the analysis of engineered nanoparticles (NPs) due to its simplicity, speed and ability to obtain a particle number size distribution. Despite its many advantages, the method is hampered by matrix effects affecting the sensitivity of the instruments. Consequently, over- or underestimated particle sizes might be obtained. To overcome these challenges, we present in this work the detection of both Ag isotopes with a quadrupole mass spectrometer for the application of isotopic dilution analysis (IDA) in combination with spICP-MS. Here, the isotopes are measured sequentially using the conventional spICP-MS integration time of 10 ms. Citrate stabilized Ag NPs of a spherical shape with the nominal diameters of 30, 40, 50 and 80 nm have been investigated. The experimental concept of adding ¹⁰⁹Ag+ solutions to the NP suspensions resulted in the NP Spikes being only visible in the ¹⁰⁷Ag trace. Therefore, a maximum of 45% of the particles was detected compared to that by conventional spICP-MS. A modified mass flow equation was applied to determine the particle sizes, particle size distributions and particle number concentrations of various Ag NPs. The addition of different spike concentrations between 0.5 and 4 mg L⁻¹ ¹⁰⁹Ag resulted in similar particle diameters, suggesting that the calculated diameter might be independent of the spike concentration. This would have the advantage that no size information would be needed before the analysis. By analyzing Ag NP suspensions in a simulated seawater matrix, we demonstrate its significant influence on the particle size determination using conventional spICP-MS. A lower transport efficiency of 6.1% was found in the matrix compared to 7.3% without the matrix. In our approach, the addition of the Matrix influenced the NP intensity stronger than the spike signal, resulting in slightly smaller diameters using IDA–spICP-MS with the matrix compared to the results without the matrix. On the other hand, the IDA–spICP-MS approach with the matrix can result in equivalent results for the particle sizes compared with conventional spICP-MS using suspensions without the matrix. Due to the lower instrument sensitivity in the matrix, a diameter of 30 nm was found to be close to the detection limit of the instrument. KW - Ag nanoparticles KW - Single particle ICP-MS KW - Matrix influence KW - Isotope dilution analysis PY - 2016 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-376490 DO - https://doi.org/10.1039/c6ja00137h SN - 0267-9477 VL - 31 IS - 10 SP - 2045 EP - 2052 AN - OPUS4-37649 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Neubert, Sebastian A1 - Pittner, Andreas A1 - Rethmeier, Michael T1 - Experimental determination of TRIP parameter K for mild- and high strength low alloy steels and a super martensitic filler material N2 - A combined experimental numerical approach is applied to determine the transformation induced plasticity (TRIP)-parameter K for different strength low-alloy steels of grade S355J2+N and S960QL as well as the super martensitic filler CN13-4-IG containing 13 wt% chromium and 4 wt% nickel. The thermo-physical analyses were conducted using a Gleeble® 3500 facility. The thermal histories of the specimens to be tested were extracted from corresponding simulations of a real gas metal arc weldment. In contrast to common TRIP-experiments which are based on complex specimens a simple flat specimen was utilized together with an engineering evaluation method. The evaluation method was validated with literature values for the TRIP-parameter. It could be shown that the proposed approach enables a correct description of the TRIP behavior. KW - Transformation induced plasticity (TRIP) KW - Phase transformation KW - High-strength low-alloy steel KW - Super martensitic filler material KW - Thermo physical simulation KW - Gleeble experiments PY - 2016 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-367297 DO - https://doi.org/10.1186/s40064-016-2474-0 VL - 5 IS - 575 SP - Paper 754, 1 EP - 16 PB - SpringerPlus AN - OPUS4-36729 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Tölle, Florian A1 - Gumenyuk, Andrey A1 - Gebhardt, Moritz Oliver A1 - Rethmeier, Michael T1 - Post-weld residual stress mitigation by scanning of a defocused laser beam N2 - High welding residual stresses can cause service life reducing consequences. Even though many processes have been developed to reduce these stresses, they are only applicable for wider welds and simple component geometries or are cost-intensive, respectively. The presented method uses a defocused beam after welding for heating the material regions on both sides of the weld. In this way, the welding stresses are decreased without contacting the surfaces using the available equipment. Different process parameters could be used depending on the component geometry and the laser power. The mechanism and the influence of the process parameters were investigated by FEM-simulation and experiments on S355J2+N steel and showed a stress reduction of about 73%. T2 - Lasers in Manufacturing 2011 - Proceedings of the Sixth International WLT Conference on Lasers in Manufacturing CY - Munich, Germany DA - 23.05.2011 KW - Residual stresses KW - Stress reduction KW - High energy beam welding KW - Post-weld heat treatment KW - Laser scanner optics PY - 2011 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-238482 DO - https://doi.org/10.1016/j.phpro.2011.03.052 SN - 1875-3892 VL - 12 IS - 1 SP - 410 EP - 418 PB - Elsevier CY - Amsterdam [u.a.] AN - OPUS4-23848 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Osterloh, Kurt A1 - Bellon, Carsten A1 - Hohendorf, Stefan A1 - Kolkoori, Sanjeevareddy A1 - Wrobel, Norma A1 - Nusser, A. A1 - Freitag, M. A1 - Bücherl, T. A1 - Bar, D. A1 - Mor, I. A1 - Tamin, N. A1 - Weiss-Babai, R. A1 - Bromberger, B. A1 - Dangendorf, V. A1 - Tittelmeier, K. T1 - Computed tomography with X-rays and fast neutrons for restoration of wooden artwork N2 - The objects of this investigation were sculptures taken from a ca. three hundred years old baroque epitaph of a church in Tonning, a town in Northern Germany. Around 1900 it was found in a disastrous state heavily damaged by wood-worm. At that time, the whole artwork was treated with the tar extract carbolineum as a remedy. Nowadays, this substance has been identified as carcinogenic, and its presence can be perceived by its stench and visually at certain spots on the surface where it has penetrated the covering paint. A gold-painted sculpture of a massive wooden skull was interrogated with X-rays and fast neutrons to investigate the internal distribution of the carbolineum. The X-ray tomography, with its excellent spatial resolution revealed galleries left over from the worm infestation in the outer areas and cracks in the central region. The golden color coating appeared as a thick and dense layer. In comparison the tomography with fast neutrons, though being of lower resolution and yet unresolved artefacts revealed sections of slightly different densities in the bulk of the wood. These differences we attribute to the differences in the distribution of the impregnant in the wood, visible due to its higher hydrogen content making it less transparent for neutrons. T2 - WCNR-10 - 10th World conference on neutron radiography CY - Grindelwald, Switzerland DA - 05.10.2014 KW - Computed tomography KW - Neutron radiology KW - Conservation of wooden artwork PY - 2015 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-323050 DO - https://doi.org/10.1016/j.phpro.2015.07.066 SN - 1875-3892 VL - 69 SP - 472 EP - 477 PB - Elsevier B.V. CY - Amsterdam AN - OPUS4-32305 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -