TY - CONF A1 - Wander, Lukas T1 - Assessment and validation of various flow cell designs for quantitative online NMR spectroscopy N2 - Compact nuclear magnetic resonance (NMR) instruments make NMR spectroscopy and relaxometry accessible in industrial and harsh environments for reaction and process control. Robust field integration of NMR systems have to face explosion protection or integration into process control systems with short set-up times. This paves the way for industrial automation in real process environments. The design of failsafe, temperature and pressure resistant flow through cells along with their NMR-specific requirements is an essential cornerstone to enter industrial production plants and fulfill explosion safety requirements. NMR-specific requirements aim at full quantitative pre-magnetization and acquisition with maximum sensitivity while reducing sample transfer times and dwell-times. All parameters are individually dependent on the applied NMR instrument. Luckily, an increasing number of applications are reported together with an increasing variety of commercial equipment. However, these contributions have to be reviewed thoroughly. The performance of sample flow cells commonly used in online analytics and especially for low-field NMR spectroscopy was experimentally and theoretically investigated by 1H-NMR experiments and numerical simulations. Here, we demonstrate and discuss an automated test method to determine the critical parameters of flow through cells for quantitative online NMR spectroscopy. The setup is based on randomized setpoints of flow rates in order to reduce temperature related effects. Five flow cells and tubings were assessed and compared for high-field as well as low-field NMR spectrometers. T2 - Small Molecule NMR Conference (SMASH) CY - Baveno, Italy DA - 17.09.2017 KW - Online NMR spectroscopy KW - Reaction monitoring KW - Flow cell KW - Process control KW - SMASH PY - 2017 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-419485 UR - http://www.smashnmr.org/conference/program AN - OPUS4-41948 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bronsert, Jeffrey T1 - Assessment and optimisation of bridge transition zones on the basis of a numerical model for train-track-bridge interaction T2 - EURODYN 2014 IX International Conference on Structural Dynamics CY - Oporto, Portugal DA - 2014-06-30 PY - 2014 AN - OPUS4-31154 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Thöns, Sebastian T1 - Assessment and monitoring of reliability and robustness of offshore wind energy converters T2 - ESREL 2008 CY - Valencia, Spain DA - 2008-09-22 PY - 2008 AN - OPUS4-18076 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rücker, Werner A1 - Rohrmann, Rolf T1 - Assessment and Damage Detection for Offshore Wind Turbines and Infrastructures T2 - IRIS - Current Praxis Workshop CY - Thessaloniki, Greece DA - 2009-03-30 PY - 2009 AN - OPUS4-20663 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tütken, T. A1 - Tatzel, Michael A1 - Vogl, Jochen A1 - Rosner, M. T1 - Assessing δ26Mg in bioapatite as proxy for faunivory N2 - Knowledge about feeding behavior is essential to determine trophic interactions and reconstruct predator-prey relationships in modern and past foodwebs. Traditionally, nitrogen isotopes (δ15N) of collagen are used to quantify the ingestion of animal protein, however collagen usually does not preserve over geological time scales. To infer the diet of extinct vertebrates from fossil material more resistant dietary proxies such as Ca and Mg isotopes are needed, which are major elements in the bioapatite of bones and teeth. Magnesium is a bio-essential element that replaces calcium in the bioapatite lattice and bone and enamel δ26Mg values of extant mammals increase systematically along the foodchain [1, 2]. The existing δ26Mg data, however, is scarce, in particular with respect to carnivores, thus still limiting the capability of this dietary proxy to reliably determine trophic differences between plant- and animal-feeders. To better constrain trophic-level effects recorded in Mg isotopes, we analyzed δ26Mg of bioapatite from modern mammals with a focus on faunivores, both carnivores and as yet unexplored insectivores. The trophic level effect of δ26Mg is influenced by the geological substrate which causes isotope variability in δ26Mg of faunal remains between different ecosystems [1, 2]. Therefore, as first-order proxy for sample provenance and to assess potential influences of the bedrock substrate of the animals´ habitats on δ26Mg of bones and teeth, we measured the 87Sr/86Sr on the same specimens. This information will enable us to refine trophic level effects and determine whether δ26Mg can be used to distinguish different faunivores isotopically. This will be of paramount importance for dietary reconstructions of trophic niches in fossil foodwebs. [1] Martin et al. (2014) Geochmica Cosmochimica Acta 130, 12-20. [2] Martin et al. (2015) Proceedings of the National Academy of Sciences 112, 430-435. T2 - Goldschmidt CY - Paris, France DA - 13.08.2017 KW - Magnesium stable isotopes KW - Isotope fractionation KW - Trophic level KW - 87Sr/86Sr KW - Provenance PY - 2017 AN - OPUS4-41535 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Thöns, Sebastian T1 - Assessing the Value of Structural Health Monitoring T2 - ICOSSAR 2013, 11th International Conference on Structural Safety & Reliability CY - New York, NY, USA DA - 2013-06-16 PY - 2013 AN - OPUS4-28820 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bruno, Giovanni T1 - Assessing the safety of new technologies: Summary of Project AGIL N2 - In Additive Manufacturing everybody is talking about Free Form, Unconventional Design, Re-thinking Components, “Think out of the box”. However, there are a few outstanding question: a) What are the material properties ? They certainly differ from literature values for conventional materials; b) How about the microstructure? It is different from conventional materials. Does it stay so with ageing? How does it form? c) Do we properly take residual stress into account? We often blame them for our ignorance about failure scenarios. d) Do we apply tailored heat treatments? Very often, we follow conventional schedules… This talk describes the summary of the efforts carried out within the BAM Project AGIL. At BAM, we aimed to thoroughly investigate the microstructure and how it evolves as a function of load and temperature (service), to determine the material properties after different process and service conditions, to properly determine residual stress and the way it impacts mechanical properties and component performance, to properly quantify the impact of (unavoidable?) defects, and to determine heat treatments tailored to the process-specific material (stress relieve, microstructure homogenization etc.). The Project AGIL was and is intimately coupled with the project ProMoAM, dealing with online monitoring of AM processes. T2 - Workshop In-situ Monitoring and Microstructure Development in Additive Manufactured Alloys CY - Online meeting DA - 19.04.2021 KW - Mechanical properties KW - Additive manufacturing KW - Residual Stress KW - Microstructure KW - Fatigue KW - Creep PY - 2021 AN - OPUS4-52581 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schartel, Bernhard T1 - Assessing the performance of intumescent coatings using bench-scaled cone calorimeter T2 - European Coatings Conference - Fire Retardant Coatings CY - Berlin, Germany DA - 2006-09-14 PY - 2006 AN - OPUS4-13780 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ávila Calderón, Luis T1 - Assessing the low cycle fatigue behaviour of additively manufactured Ti-6Al-4V: Challenges and first results N2 - The understanding of process-microstructure-property-performance (PMPP) relationships in additive manufacturing (AM) of metals is highly necessary to achieve wide-spread industrial application and replace conventionally manufactured parts, especially regarding safety-relevant applications. To achieve this understanding, reliable data and knowledge regarding material’s microstructure-property relationships (e.g. the role of defects) is needed, since it represents the base for future more targeted process optimizations and more reliable calculations of performance. However, producing reliable material data and assessing the AM material behaviour is not an easy task: big challenges are e.g. the actual lack of standard testing methods for AM materials and the occasional difficulties in finding one-to-one comparable material data for the conventional counterpart. This work aims to contribute to end this lack of reliable material data and knowledge for the low cycle fatigue behaviour of the most used titanium alloy in aerospace applications (Ti-6Al-4V). For this purpose, two sets of test specimens were investigated. The first set was manufactured from cylindrical rods produced by an optimized DED-L process and the second was manufactured from a hot formed round bar. The test specimens were cyclically loaded until failure in the low-cycle-fatigue (LCF) regime. The tests were carried out according to ISO 12106 between 0.3 to 1.0 % axial strain amplitude from room temperature up to 400°C. The LCF behaviour is described and compared between materials and with literature values based on cyclic deformation curves and strain-based fatigue life curves. Besides, the parameters of Manson-Coffin-Basquin relationship were calculated. The microstructures (initial and after failure) and fracture surfaces were comparative characterized. Thereby, the focus lied on understanding the role of grain morphology and defects on the failure mechanisms and fatigue lifetimes. For this latter characterization, optical microscopy (OM), scanning electron microscopy (SEM) and micro computed tomography (µCT) were used. T2 - 4th International Symposium on Fatigue Design and Material Defects CY - Online meeting DA - 26.05.2020 KW - Ti-6Al-4V KW - Additive manufacturing KW - Low cycle fatigue KW - Micro computed tomography KW - Microstructure PY - 2020 AN - OPUS4-50893 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wan, Wei T1 - Assessing the FRET Acceptor Potential of Various BODIPY Dyes for Europium as the FRET Donor T2 - International Bunsen Discussion Meeting on Förster Resonance Energy Transfer in Life Sciences CY - Göttingen, Germany DA - 2011-03-27 PY - 2011 AN - OPUS4-23937 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Saif-Ur-Rehman, Saif-Ur-Rehman T1 - Assessing Structural Failure in Extrusion-based 3D Concrete Printing Using Plasticity Models N2 - 3D concrete printing (3DCP) brings automation in construction, reduces material usage, increases design flexibility, and eliminates the need for formwork. However, it is a complex process involving various parameters that are often defined by trial and error. This can lead to unforeseen failures during the print, such as buckling or yielding. Computational modeling can be used in the design stage to predict and prevent failure, during printing for real-time process control, and afterwards to assess how variations during printing affect the final structure. The structural failure during the print is primarily governed by how concrete behaves at the material level, making the choice of constitutive model crucial. Plasticity models are commonly used to assess buildability, with the Mohr-Coulomb criterion being a widely used approach [1]. However, its suitability for modeling fresh concrete for 3DCP, under such loading conditions and varying material properties is still an open research question. Furthermore, experimental studies have shown that fresh concrete exhibits non-linear behavior before failure [2], which is usually not considered in structural simulations of 3DCP. This work investigates the influence of plasticity models on different structural failure modes observed in 3DCP, specifically elastic buckling and plastic collapse. The non-linear behavior of fresh concrete is accounted for by incorporating non-linear isotropic hardening into the plasticity models. A Von-Mises plasticity model and a Mohr-Coulomb model with a hyperbolic smooth approximation are implemented, both incorporating non-linear hardening. An objective stress rate formulation is adopted to consider geometric non-linearity for accurate buckling predictions. As freshly deposited layers structurate over time, an age-dependent model is implemented to capture the stiffness and strength evolution of printed layers. To simulate the layer-by-layer process, a pseudo-density-based activation method is used, allowing sequential activation of layers as printing progresses. Model parameters are identified for different ages using Bayesian inference via inverse finite element modeling by numerically replicating stress-strain data from uniaxial compression tests on samples at different ages. Printing simulations are conducted for thin-walled and cylindrical structures, demonstrating the influence of choice of plasticity model on buckling behavior and material failure. T2 - The Fifth International Conference on Simulation for Additive Manufacturing (SIM-AM 2025) CY - Pavia, Italy DA - 9.09.2025 KW - 3D Concrete Printing KW - Material Modeling KW - Plasticity KW - Simulation PY - 2025 AN - OPUS4-64361 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Saif-Ur-Rehman, Saif-Ur-Rehman T1 - Assessing Structural Failure in Extrusion-based 3D Concrete Printing Using Plasticity Models N2 - 3D concrete printing (3DCP) brings automation in construction, reduces material usage, increases design flexibility, and eliminates the need for formwork. However, it is a complex process involving various parameters that are often defined by trial and error. This can lead to unforeseen failures during the print, such as buckling or yielding. Computational modeling can be used in the design stage to predict and prevent failure, during printing for real-time process control, and afterwards to assess how variations during printing affect the final structure. The structural failure during the print is primarily governed by how concrete behaves at the material level, making the choice of constitutive model crucial. Plasticity models are commonly used to assess buildability, with the Mohr-Coulomb criterion being a widely used approach. However, its suitability for modeling fresh concrete for 3DCP, under such loading conditions and varying material properties is still an open research question. Furthermore, experimental studies have shown that fresh concrete exhibits non-linear behavior before failure, which is usually not considered in structural simulations of 3DCP. This work investigates the influence of plasticity models on different structural failure modes observed in 3DCP, specifically elastic buckling and plastic collapse. The non-linear behavior of fresh concrete is accounted for by incorporating non-linear isotropic hardening into the plasticity models. A Von-Mises plasticity model and a Mohr-Coulomb model with a hyperbolic smooth approximation are implemented, both incorporating non-linear hardening. An objective stress rate formulation is adopted to consider geometric non-linearity for accurate buckling predictions. As freshly deposited layers structurate over time, an age-dependent model is implemented to capture the stiffness and strength evolution of printed layers. To simulate the layer-by-layer process, a pseudo-density-based activation method is used, allowing sequential activation of layers as printing progresses. Model parameters are identified for different ages using Bayesian inference via inverse finite element modeling by numerically replicating stress-strain data from uniaxial compression tests on samples at different ages. Printing simulations are conducted for thin-walled and cylindrical structures, demonstrating the influence of choice of plasticity model on buckling behavior and material failure T2 - 11th GACM Colloquium on Computational Mechanics 2025 CY - Braunschweig, Germany DA - 21.09.2025 KW - 3D concrete printing KW - Von-Mises plasticity KW - Mohr-Coulomb plasticity KW - Constitutive modeling KW - Non-linear hardening KW - Objective stress rate KW - Finite element modeling KW - Bayesian inference PY - 2025 AN - OPUS4-64360 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Westin, Elin T1 - Assessing ferrite content in duplex stainless weld metal: WRC '92 predictions vs. practical measurements N2 - The weldability of stainless steels is largely controlled by the chemical composition, and alloys with ferritic or ferritic-austenitic solidification show the highest resistance to hot cracking. As the resulting phase balance also affects the final properties, it may be beneficial to both foresee and measure the weld metal ferrite content. The WRC ’92 constitution diagram is currently the most accurate prediction tool available, but it does not take the cooling rate into consideration and the precision may be less accurate for stainless steels with high ferrite numbers (FN). This study aims to assess the reliability of the WRC ’92 diagram for weld metals with FN > 50. The chemical composition was altered through gas tungsten arc welding (GTAW) of UNS S32205 with ER347 filler wire that had been PVD-coated with either niobium (Nb), copper (Cu), nickel (Ni), manganese (Mn), carbon (C), or silicon (Si). The actual ferrite content was evaluated using image analysis, FERITSCOPE® and X-ray diffraction (XRD). While predictions from the WRC ’92 diagram were deemed acceptable for Ni, Si, and Mn, notable deviations were observed for Nb, Cu, and C. The FeriteScope exhibited a consistent trend with image analysis, albeit with slightly higher FN values, wider scatter, and the conversion factor from FN to vol.-% is open for discussion. The lowest accuracy and largest spread were obtained using non-contact XRD, rendering it unsuitable for ferrite measurements of welds. These findings underscore the need for improved prediction tools and appropriate measurement methods for assessing ferrite content in duplex weld metals. T2 - Annual Assembly and International Conference CY - Rhodes, Greece DA - 07.07.2024 KW - Duplex steel KW - Ratio austenite / ferrite KW - WRC diagram PY - 2024 AN - OPUS4-60771 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Assessing ferrite content in duplex stainless steel weld metals: WRC '92 predictions vs. practical measurements N2 - The weldability of stainless steels is largely controlled by the chemical composition, and alloys with ferritic or ferritic-austenitic solidification show the highest resistance to hot cracking. As the resulting phase balance also affects the final properties, it may be beneficial to both foresee and measure the weld metal ferrite content. The WRC ’92 constitution diagram is currently the most accurate prediction tool available, but it does not take the cooling rate into consideration and the precision may be less accurate for stainless steels with high ferrite numbers (FN). This study aims to validate the reliability of the WRC ’92 diagram for weld metals with FN > 50. The chemical composition was altered through gas tungsten arc welding (GTAW) of UNS S32205 with ER347 filler wire that had been PVD-coated with either niobium (Nb), copper (Cu), nickel (Ni), manganese (Mn), carbon (C), or silicon (Si). The actual ferrite content was assessed using image analysis, FERITSCOPE® and X-ray diffraction (XRD). While the WRC ’92 diagram predictions were deemed accurate to acceptable for Ni, Si, and Mn, notable deviations were observed for Nb, Cu, and C. The FeriteScope exhibited a consistent trend with image analysis, though the values were higher, and scatter was wider, and the conversion factor is open for discussion. The lowest accuracy and largest spread were obtained using non-contact XRD, rendering it unsuitable for ferrite measurements of welds. T2 - IIW Intermediate Meeting Comission IX-H CY - Incheon, Republic of Korea DA - 12.03.2024 KW - Duplex Stainless Steel KW - Ferrite KW - WRC 92 PY - 2024 AN - OPUS4-59750 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Andresen, Elina T1 - Assessing dissolution of upconverting nanoparticles by TEM, EDXS, potentiometry and fluorometry N2 - Inorganic lanthanide-doped upconversion nanoparticles (UCNP) constitute an emerging class of near-infrared (NIR)-excitable luminescent reporters for bioimaging, fluorescence assays, sensors in bioanalysis, and optical thermometry as well as phosphors for photovoltaic and security applications.1 However, the use of UCNPs in bioimaging and cellular studies requires biocompatible particles. One possible cause of UCNP toxicity is the release of potentially harmful fluoride fluoride and lanthanide ions as revealed by dilution studies in aqueous environments, particularly under high dilution conditions.2-5 To address this issue, suitable surface coatings preventing such effects in combination with fast screening methods suited for online in situ analysis are desired. Here we present a systematic study of differently sized β-NaYF4:Yb,Er nanocrystals stabilized with different surface coatings and different hydrophilic ligands varying in binding strength to the surface atoms in various aqueous environments at different temperatures. T2 - E-MRS Fall Meeting 2021 CY - Online meeting DA - 20.09.2021 KW - Dissolution KW - Nanomaterial KW - Upconversion nanoparticle KW - Lanthanide KW - Photoluminescence PY - 2021 AN - OPUS4-56231 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Resch-Genger, Ute T1 - Assessing different types of silica networks for the complete protection of nir luminescent molecular rubies from oxygen quenching in air N2 - The application of emerging luminophores such as near-infrared (NIR) emissive earth-abundant chromium(III) (CrIII) complexes and triplet-triplet annihilation upconversion (TTA-UC) systems in air as optical reporters for bioimaging or photonic materials for energy conversion requires simple and efficient strategies for their complete protection from luminescence quenching by oxygen. Therefore, we explored the influence of sol-gel synthesis routes on the oxygen protection efficiency of the resulting core and core/shell silica nanoparticles (SiO2 NPs), utilizing the molecular ruby-type luminophores CrPF6 ([Cr(ddpd)2](PF6)3; ddpd = N,N’-dimethyl- N,N’-dipyridin-2-ylpyridin-2,6-diamine) and CrBF4 ([Cr(ddpd)2](BF4)3) with their oxygen-dependent, but polarity-, proticity-, viscosity-, and concentration-independent luminescence as optical probes for oxygen permeability. The sol-gel chemistry routes we assessed include the classical Stöber method and the underexplored larginine approach, which relies on the controlled hydrolysis of tetraethoxysilane (TEOS) in a biphasic cyclohexane/water system with the catalyst l-arginine. As demonstrated by luminescence measurements of air- and argon-saturated dispersions of CrPF6- and CrBF4-stained SiO2 NPs of different size and particle architecture, utilizing the luminescence decay kinetics of argon-saturated solutions of CrPF6 and CrBF4 in acetonitrile (ACN) as benchmarks, only SiO2 NPs or shells synthesized by the l-arginine approach provided complete oxygen protection of the CrIII complexes under ambient conditions. We ascribe the different oxygen shielding efficiencies of the silica networks explored to differences in density and surface chemistry of the resulting nanomaterials and coatings, leading to different oxygen permeabilities. Our l-arginine based silica encapsulation strategy can open the door for the efficient usage of oxygen-sensitive luminophores and TTA-UC systems as optical reporters and spectral shifters in air in the future. T2 - eMRS Strasbourg CY - Strasbourg, France DA - 26.05.2025 KW - Quality assurance KW - Fluorescence KW - Nano KW - Particle KW - Synthesis KW - Quantum yield KW - NIR KW - Mechanism KW - Characterization KW - Electron microscopy KW - Silica KW - Oxygen sensing KW - Surface KW - Doping KW - Lifetime KW - Cr(III) complex PY - 2025 AN - OPUS4-63300 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schulz, Anne-Christine T1 - Assessing co-selection of biocide and antibiotic resistance in wastewater microbial communities N2 - Biocides are used for a wide range of purposes, including disinfectants or preservatives. Biocides play a major role in the prevention of microbial infections in healthcare and animal husbandry. The use of biocides often leads to the discharge of active biocidal substances into wastewater streams, causing the exposure of wastewater microbial communities to subinhibitory concentrations. In turn, it is known that wastewater treatment plants (WWTP) are hotspots for antibiotic resistant bacteria. Since similar mechanisms confer resistance to biocides and antibiotics, exposure to biocides can result in co-selection of antibiotic resistant bacteria in WWTP due to biocides. Here, we investigate the magnitude and the drivers of co-selection of antibiotic resistance in natural wastewater microbial communities upon biocide exposure. Microbial communities will be sampled at the WWTP Ruhleben in Berlin and characterized regarding their biocide and antibiotic resistance. Changes in the resistance level after exposure to different biocides will be determined by enumerating resistant and non-resistant E. coli and heterotrophic bacteria on selective plates with and without several biocides and antibiotics. Moreover, we are establishing a synthetic community comprising about 100 environmental E. coli isolates each with different antimicrobial resistance traits. Each isolate will be tagged with a unique DNA-barcode. All isolates will be pooled and exposed to different biocides at various concentrations. The barcode labeling enables us to determine the abundance of each isolate at the beginning and end of the experiment by transposon-tag sequencing. The project results will inform risk assessment of the effects of biocidal residues on antimicrobial resistance selection in WWTP. The project is part of the BIOCIDE consortium funded within the call on Aquatic pollutants by JPI-AMR, JPI-OCEANS and JPI-WATER. T2 - 6th International Symposium onn the Environmental Dimension of Antibiotic Resistance - EDAR 6 CY - Gothenburg, Sweden DA - 22.09.2022 KW - Antibiotic resisitance KW - Biocide KW - Wastewater KW - Risk assesment PY - 2022 AN - OPUS4-56796 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Gallo, Emanuela T1 - Assessing Cable Reaction to Fire by New Intermediate-Scale Method T2 - FRPM 2015, 15th European Meeting on Fire Retardancy and Protection of Materials CY - Berlin, Germany DA - 2015-06-22 PY - 2015 AN - OPUS4-33629 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hinchliffe, Daniel T1 - Assesing the Ecodesign Review Process T2 - Global Conference of Cleaner Production and Sustainable Consumption CY - Sitges, Spain DA - 2015-11-01 PY - 2015 AN - OPUS4-34918 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Otremba, Frank A1 - Romero Navarrete, J. A. T1 - Assesing rail damage in turns due to lateral load transfer N2 - A testing procedure is proposed and used, to estimate the rail damage potentials of variations in both, the height of the cargo´s center of gravity and the railway car suspension´s spring constant. The experimental setup consisted of a tilt table that slowly exerted an increasing lateral acceleration on a two-axle bogie-type vehicle equipped with a spring supported container. The potential damaging effect derived from the resulting lateral load transfer, was assessed on the basis of the fourth-power law. Results suggest that the cargo having a higher center of gravity could be more damaging to the outside rail when compared with the effect of the shorter center of gravity of the cargo, in arrange from0.94% to 3.17%, as a function of the spring constant of the suspension. Consequently, and comparatively, there would be a long-term damaging effect on the rail when having a cargo with a higher center of gravity, so that specific cargo, having a high center of gravity, would be more aggressive to the infrastructure. On the other hand, for the range of time rate changes of the lateral acceleration, it was not found a consistent trend regarding the effect of the value of the spring constant on the magnitude of the load transfers. T2 - ASME 2024 CY - Portland, OR, USA DA - 17.11.2024 KW - Rail demage KW - Lateral load transfer PY - 2024 AN - OPUS4-61784 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. T1 - Aspekte eines umfassenden Sicherheitskonzepts für Treibgasspeichersysteme T2 - Abschlusskolloquium zum Vorhaben "CNG-Fahrzeuge" des BMU, BAM CY - Berlin, Germany DA - 2003-11-18 PY - 2003 AN - OPUS4-6023 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. T1 - Aspekte einer digitalen Lebenslaufakte (Impulsvortrag) N2 - Durch Einsatz neuer Technologien im Transport von komprimiertem Wasserstoff konnte eine Verdreifachung des Nutzlastverhältnisses erreicht werden. Diese neuen Speicher auf den Transportfahrzeugen müssten aber anders auf ihre Sicherheit überprüft werden, als dies heute gefordert wird. Mit dem Markthochlauf Wasserstoff vervielfacht sich zudem die Anzahl der Transporteinheiten. Da sich im Zuge der neuen H2-Transportfahrzeuge aber auch die Anzahl der einzelnen Speicher pro Fahrzeug etwa verzwanzigfacht hat, kommen die Kapazitäten für die erforderliche wiederkehrende Prüfung an ihre Grenzen. Dies könnte evtl. durch eine entsprechende Erhöhung der Prüfkapazitäten gelöst werden. Da dies aber weder praktisch machbar ist noch technisch wirklich sinnvoll, müssen alternative Ansätze z.B. durch digital erfasste zerstörungsfreie Prüfkonzepte gesucht werden. Hierzu bedarf es aber einer Lebenslaufakte, die beginnend von der Definition einer Bauweise über die Baumusterprüfung, Zulassung, Herstellung, erstmalige Prüfung, Verwendung und wiederkehrenden oder begleitenden Prüfungen bis zum Verschrotten alle Daten erfassen und verwalten kann. Eine solche Lebenslaufakte könnte auch als eine Art digitaler Produktpass (DPP) verstanden werden. T2 - QI-digital Forum 2023 CY - Berlin, Germany DA - 10.10.2023 KW - Wasserstoffspeicher KW - Lebenslaufakte KW - Digitaler Produktpass DPP KW - Wiederkehrende Prüfung KW - Lebensdauerüberwachung PY - 2023 AN - OPUS4-58559 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kalbe, Ute T1 - Aspekte der Versuchsplanung von Säulenversuchen - Möglichkeiten der Optimierung und Fallbeispiele T2 - Anwendertreffen Elutionsverfahren im Boden- und Abfallbereich, BAM CY - Berlin, Germany DA - 2010-11-09 PY - 2010 AN - OPUS4-22396 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Völzke, Holger T1 - Aspekte der sicherheitstechnischen Begutachtung von Zwischen- und Endlagerbehältern T2 - 1. RAM-Behältersicherheitstage 2009 CY - Berlin-Horstwalde, Germany DA - 2009-03-26 PY - 2009 AN - OPUS4-19149 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Scharf, Holger T1 - Aspekte der Qualitätssicherung bei der Herstellung und Anwendung von Referenzmaterialien für die Analytik von Sedimenten und Böden T2 - 7. Chemisches Kolloquium der Bundesanstalt für Gewässerkunde CY - Berlin, Germany DA - 1997-11-04 PY - 1997 AN - OPUS4-3311 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Subaric-Leitis, Andreas T1 - Aspekte der Prüfung und Kalibrierung von Martenshärteprüfgeräten im Makrobereich T2 - VMPA-Arbeitskreis Prüfmaschinen und Prüfgeräte CY - Oberaula, Germany DA - 2010-06-17 PY - 2010 AN - OPUS4-22459 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Subaric-Leitis, Andreas T1 - Aspekte der Messunsicherheitsbestimmung in der Härteprüfung T2 - 5. Zwick-Roell-Härte-Symposium CY - Ulm, Germany DA - 2011-07-05 PY - 2011 AN - OPUS4-24959 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wille, Frank T1 - Aspekte der Konzeption der sicherheitstechnischen Nachweisführung - Mechanische Nachweisführung innerhalb der verkehrsrechtlichen Bauartprüfung T2 - 2. RAM-Behältersicherheitstage 2010, BAM CY - Berlin, Germany DA - 2010-03-18 PY - 2010 AN - OPUS4-23148 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Auersch, Lutz T1 - Aspekte der Erschütterungsprognose bei Bahnlinien: Quasi-Statik und Achsfolge, unregelmäßiger Schotter und Boden, Wellenausbreitung bei Tunneln und Besonderheiten bei Bürogebäuden N2 - Erschütterungen, die durch Eisenbahnverkehr erzeugt werden, breiten sich durch den Erdboden aus und regen benachbarte Gebäude zu Schwingungen an. Es wurde ein Prognoseverfahren für Bahnerschütterungen ent-wickelt, das mit einfachen Modellen schnell Ergebnisse liefert. Dies sind physikalische Modelle, zum Beispiel 1-dimensionale Modelle mit Übertragungsmatrizen für die Fahrzeug-Fahrweg-Boden-Wechselwirkung und für die Gebäude-Boden Wechselwirkung. Damit werden die komplexen Verhältnisse bei der Emission (dem Zusammen¬wirken von Fahrzeug und Fahrweg), bei der Transmission durch den homogenen oder geschichteten Boden und bei der Immission in Gebäuden näherungsweise erfasst. In (Auersch, 2020) wird gezeigt, dass diese einfachen Prognosemodelle die Ergebnisse von detaillierten Modellen wie der Finite-Element-Randelement-Methode für das Gleis, die Wellenzahlintegrale für den Boden und 3-dimensionale Finite-Element-Modelle für das Gebäude gut wiedergeben können. Dies entspricht auch der Absicht, die Prognosemodelle aus den Ergebnissen der Detailmodelle abzuleiten. Die drei Prognoseteile werden getrennt berechnet, aber es werden physikalisch sinn¬volle Schnittstellen verwendet. Für die Emission und Transmission sind es die auf den Untergrund wirkenden Erregerkräfte von Fahrzeug und Fahrweg, für die Transmission und Immission sind es die Freifeldamplituden des Bodens. T2 - 17. D-A-CH-Tagung Erdbebeningenieurwesen und Baudynamik CY - Online meeting DA - 16.09.2021 KW - Erschütterungen KW - Emission KW - Transmission KW - Immission PY - 2021 AN - OPUS4-53314 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Subaric-Leitis, Andreas T1 - Aspekte der Ergebnisunsicherheit im Prüfwesen T2 - 260. PTB-Seminar: Berechnung der Messunsicherheit - Empfehlungen für die Praxis CY - Berlin, Germany DA - 2011-03-21 PY - 2011 AN - OPUS4-24958 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. A1 - Duffner, Eric T1 - Aspekte der Bauteilprüfung, Bauteilsicherheit und Zulassung im Kompetenzzentrum H2SAFETY@BAM N2 - Der Vortrag zeigt den Weg des Themas Wasserstoff von Adolf Martens bis zum Kompetenzzentrum H2SafetyBAM, die zugehörigen Kompetenzfelder, deren Ziele und verantwortliche Personen. Der Hauptteil reflektiert den Aspekt des Markthochlaufes von Wasserstofftechnologien und zeigt einen Maßnahmenkatalog von der Risikosteuerung über die Konsequenzbegrenzung bis zu probabilistische Ansätzen in der Bewertung von Prüfergebnissen und der Wirkung von Mindestanforderungen. T2 - DVGW-Kongress H2-Sicherheit CY - Online meeting DA - 26.02.2022 KW - Wasserstoffspeicher KW - Markthochlauf KW - Monte-Carlo-Simulation KW - Druck-Volumen-Produkt KW - Alterung PY - 2022 AN - OPUS4-54609 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. T1 - Aspekte der Bauteilprüfung, Bauteilsicherheit und Zulassung im Kompetenzzentrum H2Safety N2 - Der Vortrag stellt das Kompetenzzentrum H2Safety der BAM vor und zeigt Aspekte besonderer Kompetenz des Zentrums mit Blick auf das Kompetenzfeld TestCert. Beginnend mit dem H2-Unfall auf dem Tempelhofer Feld in 1894 wird dargestellt welche Bedeutung Sicherheitsfragen zu Wasserstoff für das Kompetenzzentrum H2Safety haben. Danach wird die Struktur und die Arbeitsschwerpunkte erläutert und die verantwortlichen Personen kurz vorgestellt. Das Kompetenzfeld TestCert wird vertieft erläutert und hier insbesondere auf Sicherheitsaspekte des Markthochlaufes hingewiesen. Darauf aufbauend werden die statistischen Aspekte eines Markthochlaufes wie auch die der Streuung einer Population und deren Alterung dargelegt. Zuletzt kommt der Hinweis auf das Potential der Bewertung von Baumusterprüfkriterien mithilfe der Monte-Carlo-Simulation. T2 - DVGW Kongress "H2 Sicherheit" CY - Online meeting DA - 27.01.2021 KW - H2Safety@BAM KW - Markthochlauf KW - Sicherheit KW - Zuverlässigkeit KW - Alterung KW - Zulassungskriterium PY - 2021 AN - OPUS4-53152 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Baer, Wolfram T1 - Aspekte der analytischen bruchmechanischen Bauteilbewertung N2 - Am Beispiel eines abgesetzten zylindrischen Bauteils (Achsschenkel) werden Probleme der analytischen bruchmechanischen Bauteilbewertung diskutiert. Als Basis-philosophie wird ein Fail Safe-Kriterium (kontrolliertes Versagen) angesetzt. Die Forderung ist, dass sich der Achsschenkel, bevor er bricht, in einem Ausmaß plastisch verformen kann, bei dem der Fahrer bemerkt, dass mit seinem Fahrzeug etwas nicht in Ordnung ist. Um das zu gewährleisten, muss der Werkstoff einen bestimmten Riss-widerstand aufweisen. Dazu werden im hier vorgestellten ersten Teil des Projektes mittels FEM Rissspitzenbeanspruchungen in Abhängigkeit von der Auslenkung des Zylinders und angenommener Rissgrößen ermittelt. Diese finden als Zielgrößen in der weiteren Analyse Anwendung. Da eine einfach umzusetzende Lösung angestrebt wird, werden zusätzlich analytische Rechnungen an Ersatzgeometrien (halbunendliche Platte und Vollzylinder), aber mit den realen Spannungen am Bauteil durchgeführt. Es zeigt sich, dass die Ergebnisse wegen des Steifigkeitsunterschieds zwischen Bauteil und Ersatzgeometrie unvertretbar konservativ sind. Alternativ wird ein hybrides Konzept vorgestellt, für das die Modellparameter mittels FEM bestimmt werden. Es liefert sehr genaue Ergebnisse. Im Rahmen der analytischen Rechenvorschrift können die Lösungen auf andere Werkstoffe übertragen werden, ohne dass zusätzliche FEM-Analysen notwendig sind. T2 - 54. Tagung des DVM-Arbeitskreises Bruchmechanik und Bauteilsicherheit CY - Online meeting DA - 22.02.2022 KW - Bauteilbewertung KW - Fail-safe KW - Analytisches Modell KW - FEM PY - 2022 AN - OPUS4-54408 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Völzke, Holger T1 - Aspects on Long Term Storage of Used Nuclear Fuel and High Active Waste in Germany T2 - PATRAM 2010 (16th Internationl Symposium on the Packaging and Transport of Radioactive Material) CY - London, England DA - 2010-10-03 PY - 2010 AN - OPUS4-22239 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - von Oertzen, Alexander T1 - Aspects of the pyrotechnics directive in Europe T2 - Treffen zur Europäischen Pyrotechnikrichtlinie, organisiert vom italienischen Pyrotechnikverband CY - Città Sant'Angelo, Italy DA - 2007-03-10 PY - 2007 AN - OPUS4-14647 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Linnemann, Konrad T1 - Aspects of spent fuel behavior assessment for transport packages N2 - Transport packages for spent nuclear fuel have to be assessed with respect to specific transport conditions which are defined in the safety regulations of the International Atomic Energy Agency. In general, gastight fuel rods constitute the first barrier of the containment system. The physical state of the spent fuel and the fuel rod cladding as well as the geometric configuration of the fuel assemblies are important inputs for the evaluation of the package safety under transport conditions. The objective of this paper is to discuss the methodologies accepted by BAM for the authority assessment of spent fuel behavior within the package design approval procedure of German package designs. In particular, cracks or failures in the fuel rod cladding can occur under regulatory transport conditions. These defects can cause the release of gas, volatiles, fuel particles or fragments into the package cavity and have to be considered properly in the safety analysis. Another issue is the transport of defective fuel rods. One concept is to use special canisters which can be handled like fuel assemblies. This concept requires additional assessment concerning drying, sealing and the mechanical and thermal design of such canisters. The package as a mechanical system is characterized by a complex set of interactions, e.g. between the fuel rods within the assembly as well as between the fuel assemblies, the basket, and the cask containment. This complexity together with the limited knowledge about the material properties and the variation of the fuel assemblies regarding cladding material, burn-up and the operation history makes an exact mechanical analysis of the fuel rods nearly impossible. The simplified approaches to consider conservatively spent fuel behavior currently accepted by BAM are presented here. T2 - International Conference on the Management of Spent Fuel from Nuclear Power Reactors: An Integrated Approach to the Back End of the Fuel Cycle CY - Wien, Austria DA - 15.06.2015 KW - Transport packages KW - Spent fuel assessment PY - 2005 AN - OPUS4-38101 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Linnemann, Konrad T1 - Aspects of spent fuel behavior assessment for transport packages N2 - Transport packages for spent nuclear fuel have to be assessed with respect to specific transport conditions. The physical state of the spent fuel and the fuel rod cladding as well as the geometric configuration of the fuel assemblies are important inputs for the evaluation of the package safety. The objective of this paper is to discuss the methodologies accepted by BAM for the authority assessment of spent fuel behavior within the package design approval procedure. T2 - SNL/BAM Workshop 2015 CY - Berlin, Germany DA - 29.10.2015 KW - Transport packages KW - Spent fuel assessment PY - 2015 AN - OPUS4-38103 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Reiche, I. T1 - Aspects of Safety Assessments for Package Designs with Additional Equipment T2 - 14th Int. Symposium on the Packaging and Transportation of Radioactive Materials (PATRAM) CY - Berlin, Germany DA - 2004-09-20 PY - 2004 AN - OPUS4-6027 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Nehrig, Marko T1 - Aspects of Gas Generation Caused by Residual Water inside ILW Packages T2 - Ramtrans 2015 10th International Conference on Radioactive Materials Transport and Storage CY - Oxford, UK DA - 2015-05-19 PY - 2015 AN - OPUS4-33450 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zekhnini, Khalid A1 - Seifert, Lando T1 - Aspects of corrosion protection in the maritime sector– Focus of Current research of BAM for H2Mare N2 - Germany has set itself the task of becoming a world leader in the field of green hydrogen technologies and is promoting the transition to a hydrogen economy. The H2Mare flagship project is exploring the offshore production of green hydrogen and other power-to-X products. One of the most important goals is the safe and cost-efficient operation of offshore infrastructures, where a service life of at least 25 years is aimed at. However, the corrosive environment towards metallic materials presents challenges in marine areas. The atmosphere at one location could be affected by the distance to the sea level and does not have the same corrosivity for all exposed kinds of materials. The research of the durabilitty of different materials and corrosion protection systems by weathering campaigns and laboratory experiments aims to close this gap of knowledge. BAM‘s mandate is to make the data available to the responsible operators through standardisation to ensure safety and cost efficiency. T2 - H2Mare Conference 2024 CY - Berlin, Germany DA - 06.06.2024 KW - Atmospheric Corrosion KW - Offshore KW - Wind energy KW - Marine Corrosion KW - Laboratory Container KW - Corrosion protecting system KW - Sediment KW - Green Hydrogen PY - 2024 AN - OPUS4-60225 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bremser, Wolfram T1 - Aspects of Certified Reference Materials T2 - ECA International Workshop on Reference Standards CY - Berlin, Germany DA - 2003-11-13 PY - 2003 AN - OPUS4-3692 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Feldkamp, Martin T1 - Aspects of Assessment of Packages with Wood Filled Impact Limiters during Fire Tests N2 - Packages for the transport of radioactive material are often equipped with impact limiters consisting of wood, encapsulated by steel sheets. These impact limiters shall ensure that the transport casks meet the mechanical and thermal IAEA regulatory test requirements. According to the accident conditions of transport it is mandatory to expose the specimens to a cumulative effect by mechanical and thermal impacts. The mechanical tests consist of a free drop from 9 m onto a flat unyielding target and a 1 m drop onto a puncture bar. After damage caused by mechanical test sequences the package has to withstand a severe fire scenario. Corresponding to the IAEA advisory material it is required that the impact attitudes for the 9 m drop test and for the puncture test have to be such as to produce maximum damage, taking into account the thermal test. Moreover, any damage, which would give rise to increased radiation or loss of containment or affect the confinement system after the thermal test, should be considered. During and following the thermal test, the specimen shall not be artificially cooled and any combustion of materials of the package shall be permitted to proceed naturally. Different works from the French Institute for Radiological Protection and Nuclear Safety (IRSN) and BAM show that additional energy supply from a pre-damaged impact limiter to the cask could occur. This effect should be considered within the safety assessment of the containment. Thermal effects at the closure system of the cask, which might result in an elevated activity release, have to be excluded. BAM conducted small scale tests with wood filled metal buckets showing continuing combustion processes during the cooling down phase. These test results are presented. As not much is known about smouldering processes in wood filled impact limiters, it is highly complex to define pre-damage of impact limiters, which are conservative, regarding the maximum damaging energy flow from the impact limiter to the containment system. More research has to be done to develop models to examine the effects of smouldering impact limiters on the containment of packages for the transport of radioactive material. Aspects of assessment and its difficulties are shown. BAM as a competent authority for the approval of transport casks for radioactive material in Germany operates the test facilities to examine the issue of mechanical damage, combustion and heat transfer for such kind of package systems. For this purpose the knowledge from real drop tests with casks of a mass partly over 100 tons was transferred to a test application. A thermal test will take place with a wood filled test specimen with a diameter of about 2.3 meters. The aim is to understand the phenomena of smouldering under the consideration of relevant regulatory boundary conditions. The process of smouldering is described with regard to the requirements in the thermal assessment of safety of packages for the transport of radioactive material. Requirements concerning the pre-damage of packages for the maximum damage of impact limiters are discussed. Parameters influencing the smouldering process are identified. T2 - WM 2017 Conference CY - Phoenix, Arizona, USA DA - 05.03.2017 KW - Fire test KW - Wood KW - Combustion KW - Smouldering KW - Smoldering KW - Impact limiter KW - Shock absorber KW - Thermal test KW - IAEA PY - 2017 AN - OPUS4-43170 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Peplinski, Burkhard T1 - Aspects of accuracy in the application of X-ray and neutron diffraction techniques to ceramics and catalysts T2 - Workshop "Accuracy in X-ray powder diffraction" of the Researsh Institute of Standards and Science (KRISS) CY - Daejeon, South Korea DA - 2002-11-19 PY - 2002 AN - OPUS4-3753 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zencker, Uwe T1 - ASME-Regelwerksentwicklung zu numerischen Nachweismethoden N2 - Es wird über die Weiterentwicklung des ASME (American Society of Mechanical Engineers) – Regelwerks berichtet. Relevant für das Design von Behältern ist ASME BPVC (ASME Boiler and Pressure Vessel Code) Section III Division 3. In den ASME BPVC in der Fassung von 2015 wurden dehnungsbasierte Bewertungskriterien aufgenommen. Eine dehnungsbasierte Bewertung erfordert die genaue Kenntnis der aufgetretenen Dehnungen, d.h. speziell möglichst genaue numerische Berechnungen der Behälterbeanspruchungsszenarien. Daher sind regulatorische Vorgaben notwendig für die Vorbereitung, Durchführung und Auswertung numerischer Simulationen. In einer Arbeitsgruppe (ASME Special Working Group on Computational Modeling for Explicit Dynamics) werden dazu Leitlinien für die Anwendung numerischer Berechnungsverfahren entwickelt. Im Vortrag werden diese Leitlinien vorgestellt. T2 - 5. RAM-Behältersicherheitstage CY - Berlin, Germany DA - 16.03.2016 KW - ASME KW - Regelwerk KW - Leitlinien KW - Numerische Nachweismethoden KW - Numerische Berechnungsverfahren PY - 2016 AN - OPUS4-35991 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Stahl, E. T1 - ASHES-nutrient recycling from the thermo-chemical processing of waste bagasse and straw - Clips from a German-Brazilian collaborative research project N2 - The challenge of the project ASHES is focused on the recycling of nutrients from residues of thermochemical processing of by-products of sugar cane industry (bagasse/straw) in Brazil to increase the energy efficiency of thermal conversion and to enable the recycling of process ashes as fertilisers. Dry lignocellulosic biomass (straw, bagasse) are combusted, gasified and subsequently combined with post-thermochemical treatment in the AshDec process to increase the plant availability of phosphorus. Different fertilizer formulations are granulated/pelletized and tested regarding their storage/handling characteristics. T2 - Biomass Ash 2018 CY - Kopenhagen, Denmark DA - 06.06.2018 KW - Bagasse KW - Nutrient KW - Recycling PY - 2018 AN - OPUS4-45652 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Simon, Franz-Georg T1 - Aschen und Schlacken aus der Abfallverbrennung; Gefährlich oder nicht? N2 - In Deutschland fallen aktuell pro Jahr über 5 Mio. Tonnen Hausmüllverbrennungs-aschen (HMVA) an. Eine Verwertung dieser Aschen und Schlacken ist in Deutschland möglich und findet überwiegend im Deponiebau statt. Für die Verwertung sind in der Ersatzbaustoffverordnung Eluatgrenzwerte für Schwermetalle und einige andere Parameter vorgesehen. Der Umgang mit HMVA könnte durch eine Einstufung als gefährlicher Abfall erschwert werden. Maßgeblich für die Einstufung eines Abfalls als gefährlich oder ungefährlich sind die gefahrenrelevanten Eigenschaften HP 1 bis HP 15 nach Anhang III der Richtlinie 2008/98/EG über Abfälle mit dort festgelegten Konzentrationsgrenzen. Für HMVA ist im Wesentlichen nur der Parameter HP 14 (Ökotoxizität) von Bedeutung. Dafür sind entscheidend die Gehalte an chemischen Verbindungen mit den Gefahrenhinweiscodes (hazard statement code, HSC) H400, H410, H411, H412 und H413. Eine detaillierte Diskussion zu den übrigen Gefahreneigenschaften bei HMVA findet sich in der Literatur. Die Einstufung als gefährlicher Abfall erfolgt nach festgelegten Rechenregeln. Die BAM bearbeitet ein durch das UBA gefördertes Forschungsprojekt zur Erfassung und Bewertung von Analysedaten zu Aschen und Schlacken aus Abfallverbrennungsanlagen. Die Ergebnisse des Vorhabens sollen bei der Weiterentwicklung des vorhandenen Konzeptes für eine bundeseinheitlichen Untersuchung und abfallrechtlichen Einordnung von Aschen und Schlacken aus deutschen Abfallverbrennungsanlagen unterstützend herangezogen werden. Im Vortrag werden Verfahren zur quantitativen Bestimmung der einstufungsrelevanten Verbindungen vorgestellt: 1.) der Praxisleitfaden von ITAD und IGAM, 2.) Methode basierend auf der Bioverfügbarkeit und 3.) Methode basierend auf Speziierungsanalyse. T2 - Jahrestreffen 2023 der DECHEMA-Fachgruppen AuW und TRO CY - Dresden, Germany DA - 06.03.2023 KW - Rostasche KW - Speziierungsanalyse KW - Abfallbehandlung PY - 2023 AN - OPUS4-57346 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Simon, Franz-Georg T1 - Aschen und Schlacken aus der Abfallverbrennung im Lichte der Ersatzbaustoffverordnung N2 - Im Rahmen eines vom Umweltbundesamt geförderten Forschungsprojekts wurde untersucht, ob die Abtrennung der Feinfraktion (0-2 mm) eine Verbesserung der umweltrelevanten Eigenschaften bewirkt und somit HMVA-1 erreicht werden kann. In Deutschland wird die Rostasche durch Nassentschlackungssysteme aus dem Feuerraum ausgetragen. Durch den Kontakt mit Wasser setzen direkt hydraulische Reaktionen ein, die eine vollständige Abtrennung der Feinfraktion unmöglich machen. Das wurde bereits in den 1990er Jahren erkannt und führte zur Entwicklung des ABB InRec Verfahrens mit Trockenentaschung als ersten Verfahrensschritt. Auch damals war das Ziel eine möglichst inerte Rostasche für die Verwertung zu erzeugen. In den letzten Jahren wurden in der Schweiz Trockenentaschungssystem installiert, hier vor allem um die Rückgewinnung von elementaren Metallen auch in der Feinfraktion zu verbessern. Welche Potenziale sich dabei erschließen lassen, wurde in einem anderen UBA-Projekt untersucht. Im Rahmen unserer Arbeiten wurde versuchsweise trockene Rostasche an einer Anlage in Süddeutschland genommen und im Labor untersucht. Im Vortrag werden die Ergebnisse zum Auslaugverhalten und zur Gefahreneigenschaft HP14 (Ökotoxizität) vorgestellt. T2 - Jahrestreffen 2024 der DECHEMA-Fachgruppen Abfallbehandlung und Wertstoffrückgewinnung (AuW) und Gasreinigung (GAS) CY - Dresden, Germany DA - 25.03.2024 KW - Rostasche KW - Ersatzbaustoffe PY - 2024 AN - OPUS4-59985 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rübner, Katrin T1 - Aschen aus dem Altpapierrecycling N2 - Sortierrückstände, Faserreststoffe und Schlämme aus der Altpapieraufbereitung und dem Deinking werden gegenwärtig entweder deponiert oder einer energetischen Verwertung zugeführt. Es gibt Bemühungen, die Reststoffe kontrolliert bei Temperaturen zwischen 700 °C und 800 °C zu calcinieren, um dadurch direkt einen metakaolinhaltigen puzzolanisch wirkenden Zementbestandteil oder Betonzusatzstoff herzustellen. Üblicherweise erfolgt die Verbrennung der Papierreststoffe aber beim Papierrecycler bzw. –hersteller in dezentralen Heizkraftwerken, in denen mittels Kraft-Wärme-Kopplung Strom, Wärme und Dampf erzeugt werden. Der auf die Strom- und Wärmeerzeugung optimierte Prozess verläuft bei Temperaturen von 950°C bis 1000 °C. Dabei bilden sich aus dem amorphen Metakaolin bereits wieder inerte Verbindungen. Pro Tonne verbranntem Papierreststoff fallen etwa 240 kg Papierasche (PA) in Form einer Mischung aus Kessel- und Elektrofilteraschen an. Die Papierasche wird etwa zu 16 % in der Ziegelherstellung und zu 52 % in der Rohmehlproduktion der Zementindustrie kostenpflichtig entsorgt. Mit 26 % werden große Anteile der Papierasche deponiert. Mit den Zielen der Anhebung der Verwertungsquote der Papierasche, der Reduzierung der Entsorgungskosten und einer qualitativ höherwertigen Verwendung der Asche unter Ausnutzung ihrer spezifischen Eigenschaften, stehen Papieraschen im Mittelpunkt verschiedener Forschungsarbeiten. Die in den Untersuchungen verwendete Papierasche liegt als feinkörniges Material in einem breiten Kornband mit Partikelgrößen zwischen 0,5 µm und 100 µm vor. In Abhängigkeit von der Materialcharge beträgt die Feststoffdichte der Asche 2,63-2,67 g/cm³ und ihre spezifische Oberfläche liegt bei 2,6-5,0 m²/g. Die Papierasche kommt mit den Anteilen der Hauptoxide von 49-59 M.-% CaO, 22-28 M.-% SiO2 und 13-14 M.-% Al2O3 der Zusammensetzung eines Portlandzements nahe, sie ist jedoch etwas kalkärmer und tonerdereicher. In Abhängigkeit von der Herstellungs- und Lagerungshistorie enthält sie zwischen 3 M.-% und 15 M.-% Freikalk (CaO). Mittels Röntgenbeugungsanalyse werden Calcit (CaCO3), Gehlenit (Ca2Al(AlSi)O7), Portlandit (Ca(OH)2) und Belit (Ca2SiO4), Quarz (SiO2) und Talk Mg3Si4O10(OH)2 als Hauptmineralphasen der Papierasche identifiziert. In einigen PA-Chargen werden zusätzlich Freikalk (CaO), Tricalciumaluminat (Ca3Al2O6) und geringe amorphe Anteile gefunden. Aufgrund dieser Eigenschaften werden von der Papierasche auch hydraulische Eigenschaften erwartet, die eine Verwendung als Bindemittel allein oder Bindemittelkomponente im Gemisch mit Portlandzement oder anderen Zusatzstoffen nahe legen. Erste Untersuchungen an der Papierasche dienten der mineralogischen, chemischen, umweltanalytischen und betontechnologischen Charakterisierung der Papierasche, von Zement-PA- und Flugasche-PA-Gemischen. Anschließende Studien befassten sich mit dem Einsatz von Papierasche als Zementzumahlstoff, Zusatz in erdfeuchten Betonen und als Bodenverfestigungsmittel. Im Vortrag werden die wesentlichen Ergebnisse der Forschungsarbeiten vorgestellt und die Einsatzmöglichkeiten der Papierasche als Baustoff im Hinblick auf ihre technologische und nachhaltigkeitsbezogene Eignung bewertet. T2 - Workshop Ressourcen und Recycling im Themenfeld Umwelt CY - Berlin, Germany DA - 18.01.2017 KW - Papierasche KW - Altpapierrecycling KW - Baustoff KW - Bindemittelersatz PY - 2017 AN - OPUS4-39200 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rübner, Katrin T1 - Aschen aus dem Altpapierrecycling N2 - Sortierrückstände, Faserreststoffe und Schlämme aus der Altpapieraufbereitung und dem Deinking werden gegenwärtig entweder deponiert oder einer energetischen Verwertung zugeführt. Es gibt Bemühungen, die Reststoffe kontrolliert bei Temperaturen zwischen 700 °C und 800 °C zu calcinieren, um dadurch direkt einen metakaolinhaltigen puzzolanisch wirkenden Zementbestandteil oder Beton-zusatzstoff herzustellen. Üblicherweise erfolgt die Verbrennung der Papier-reststoffe aber beim Papierrecycler bzw. –hersteller in dezentralen Heizkraftwerken, in denen mittels Kraft-Wärme-Kopplung Strom, Wärme und Dampf erzeugt werden. Der auf die Strom- und Wärmeerzeugung optimierte Prozess verläuft bei Temperaturen von 950°C bis 1000 °C. Dabei bilden sich aus dem amorphen Metakaolin bereits wieder inerte Verbindungen. Pro Tonne verbranntem Papierrest-stoff fallen etwa 240 kg Papierasche (PA) in Form einer Mischung aus Kessel- und Elektrofilteraschen an. Die Papierasche wird etwa zu 16 % in der Ziegel-herstellung und zu 52 % in der Rohmehlproduktion der Zementindustrie kostenpflichtig entsorgt. Mit 26 % werden große Anteile der Papierasche deponiert. Mit den Zielen der Anhebung der Verwertungsquote der Papierasche, der Re-duzierung der Entsorgungskosten und einer qualitativ höherwertigen Verwendung der Asche unter Ausnutzung ihrer spezifischen Eigenschaften, stehen Papieraschen im Mittelpunkt verschiedener Forschungsarbeiten. Die in den Untersuchungen verwendete Papierasche liegt als feinkörniges Material in einem breiten Kornband mit Partikelgrößen zwischen 0,5 µm und 100 µm vor. In Abhängigkeit von der Materialcharge beträgt die Feststoffdichte der Asche 2,63-2,67 g/cm³ und ihre spezifische Oberfläche liegt bei 2,6-5,0 m²/g. Die Papierasche kommt mit den Anteilen der Hauptoxide von 49-59 M.-% CaO, 22-28 M.-% SiO2 und 13-14 M.-% Al2O3 der Zusammensetzung eines Portlandzements nahe, sie ist jedoch etwas kalkärmer und tonerdereicher. In Abhängigkeit von der Herstellungs- und Lagerungshistorie enthält sie zwischen 3 M.-% und 15 M.-% Freikalk (CaO). Mittels Röntgenbeugungsanalyse werden Calcit (CaCO3), Gehlenit (Ca2Al(AlSi)O7), Portlandit (Ca(OH)2) und Belit (Ca2SiO4), Quarz (SiO2) und Talk Mg3Si4O10(OH)2 als Hauptmineralphasen der Papierasche identifiziert. In einigen PA-Chargen werden zusätzlich Freikalk (CaO), Tricalciumaluminat (Ca3Al2O6) und geringe amorphe Anteile gefunden. Aufgrund dieser Eigenschaften werden von der Papierasche auch hydraulische Eigenschaften erwartet, die eine Verwendung als Bindemittel allein oder Bindemittelkomponente im Gemisch mit Portlandzement oder anderen Zusatzstoffen nahe legen. Erste Untersuchungen an der Papierasche dienten der mineralogischen, chemischen, umweltanalytischen und betontechnologischen Charakterisierung der Papierasche, von Zement-PA- und Flugasche-PA-Gemischen sowie der PA als Bodenverfestigungsmittel. Eine umfangreiche Studie befasste sich mit dem Einsatz von Papierasche als Bindemittel. Untersucht wurde die Mineralphasen- und Festigkeitsentwicklung nach einer Aktivierung mit Wasser oder 2 mol/l NaOH- bzw. KOH-Lösungen. In einer Arbeit zur Herstellung eines zementfreien reststoffbasierten Bindemittels wurde unter anderem die CaO-reiche Papierasche als Ausgangsmaterial ausgewählt. Durch eine hydrothermale Behandlung von PA-Wasser-Gemischen mit anschließender Calcinierung wird die Asche hydraulischen aktiviert. Dabei bildet sich als Zwischenprodukt Calciumsilcathydrat (CSH), das durch die nachfolgende Calcinierung zu hydraulisch aktivem Belit dehydratisiert. In einem anderen Anwendungspfad dient die Papierasche als alleiniger Ausgangsstoff oder als Kalklieferant im Gemisch Papierasche/Mauerwerkbruch zur Herstellung leichter Granulate mit Rohdichten von 1,5-2,0 g/cm³. Dabei erfolgt nach einer Granulierung des Ausgangsmehls eine Erhärtung in einem Autoklav bei 200 °C und 1,6 MPa in gesättigter Wasserdampfatmosphäre. Während des hydrothermalen Prozesses bilden sich CSH-Phasen, die die beim Granulieren vorgeprägte Mikrostruktur der Granulate weiter beeinflussen. Neben der Verwendung als leichte Gesteinskörnung wird auch eine Anwendung als Speicher-medium, Filtermaterial oder Adsorptions- bzw. Puffermittel getestet. Im Vortrag werden die wesentlichen Ergebnisse der Forschungsarbeiten vorgestellt und die Einsatzmöglichkeiten der Papierasche als Baustoff im Hinblick auf ihre technologische und nachhaltigkeitsbezogene Eignung bewertet. T2 - Fachtagung Recycling R'16 CY - Weimar, Germany DA - 19.09.2016 KW - Papierasche KW - Recycling KW - Bindemittel KW - Zementersatz KW - Baustoff PY - 2016 AN - OPUS4-37636 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Adam, Christian T1 - Ascheentsorgung - Acker oder Deponie? T2 - 4. Fachtagung Verfahren & Werkstoffe für die Energietechnik, "Biomasse & Abfall - Regionale Brennstoffe richtig nutzen" CY - Sulzbach-Rosenberg, Germany DA - 2008-06-11 PY - 2008 AN - OPUS4-17507 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Röthke, A. T1 - As good as or even better than ID-ICP-MS? High accuracy ICP OES determination of 1 g/kg mercury solutions N2 - To establish the SI traceability of the element content w(Hg) of a gravimetrically prepared 1 g/kg mercury solution, the latter was compared to a primary reference solution by means of high accuracy inductively coupled plasma optical emission spectrometry (ICP OES) measurements. For this purpose, the ICP OES bracketing method previously described [1] was improved to yield a relative expanded uncertainty of the mercury element content of Urel(w(Hg)) = 0.5 % (with k = 2) associated with the comparison of two monoelemental solutions. In case of mercury, such a small uncertainty was achieved for the first time. Before, in general, such small uncertainties were only reported applying isotope dilution methods performed with MC-ICP-MS. However, for mercury solutions at this concentration range, several dilution steps are necessary to prepare the samples for ID-MC-ICP-MS. The sum of the uncertainty contributions stemming from the dilution steps, as well as the intrinsic difficulties of measuring mercury at low concentrations, result in an overall uncertainty of the ICP-MS measurements, which is comparable to or even larger than those, achieved with the ICP OES method applied. We will present details of the sample preparation as well as of the dedicated ICP OES measurement approach, which were crucial to achieve such a small measurement uncertainty. The newly developed method was successfully applied in the context of the development and production of elemental solution chemical reference standards (CRS), which are distributed by the EDQM. The CRS are intended to support measurements required by the European Pharmacopoeia, which has recently incorporated a new international guideline for the control of elemental impurities in medicinal products. T2 - ICP-MS Anwendertreffen CY - Berlin, Germany DA - 03.09.2018 KW - Traceability KW - Mercury solution PY - 2018 AN - OPUS4-46218 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Despinasse, Marie-Claire T1 - Arylphosphates and phosphazene flame retardants in Polycarbonate / Acrylonitrile-Butadiene-Styrene blends T2 - 13th European Meeting on Fire Retardant Polymers, FRPM CY - Alessandria, Italy DA - 2011-06-26 PY - 2011 AN - OPUS4-24068 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bellon, Carsten T1 - Artistlib - remote control the radiographic simulator aRTist from Python N2 - The software aRTist is a simulation tool for the generation of realistic radiographs of virtual radiographic superstructures. With radiographic simulations, virtual component models can be scanned as in a computed-tomography scanner. In modern radiography, simulation has become an important tool to minimize cost- and time-intensive measurements. It is increasingly used to optimize techniques for complex applications, to support the method developments, and for educational purposes. With Artistlib, we have started the development of a programming interface to support use cases where the interactive use of the graphical user interface is not suitable. The open-source Python library is intended to remote control and automate the radiographic simulator aRTist. T2 - 10th International Symposium on Digital Industrial Radiography and Computed Tomography (DIR 2025) CY - Paris, France DA - 01.07.2025 KW - Computed Tomography KW - Numerical Simulation PY - 2025 AN - OPUS4-63703 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bellon, Carsten T1 - aRTist – An Industrial-Radiology Simulator Using Tcl/Tk & VTK N2 - Industrial radiography or Radiographic Testing (RT) is a method of non-destructive testing where many types of manufactured components can be examined to verify the internal structure and integrity of the specimen. The computer program aRTist can generate synthetic radiographs from a virtual RT test set-up. In the field of industrial radiology simulation is used, e.g. to optimize techniques for complex applications, to support the preparation of written procedures, and for education purposes. The simulator aRTist combines analytical and Monte Carlo methods to efficiently model the radiation transport. The program comes with a graphical user interface written in Tcl/Tk. In combination of Tcl/Tk and the 3D capabilities of the visualization toolkit (VTK) a practical and convenient simulator has been realized. This will be illustrated by discussing application scenarios of classical radiography, X-ray computer tomography, and X-ray backscatter imaging. Additionally, some insight to the software implementation of the simulator will be given. T2 - EuroTCL 2017, 15th European Tcl/Tk User Meeting CY - Berlin, Germany DA - 08.07.2017 KW - Simulation KW - Radiography KW - Computed tomography PY - 2017 AN - OPUS4-43153 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Jaenisch, Gerd-Rüdiger T1 - aRTist - radiographic simulation for industrial application T2 - 6th International Exhibition and Conference for Non-Destructive Testing and Technical Diagnostics CY - Moscow, Russia DA - 2007-05-15 PY - 2007 AN - OPUS4-14827 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Jaenisch, Gerd-Rüdiger T1 - aRTist - analytical RT inspection simulation tool for industrial application T2 - 17. WCNDT (World Conference on NDT) CY - Shanghai, China DA - 2008-10-25 PY - 2008 AN - OPUS4-18150 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Jaenisch, Gerd-Rüdiger T1 - aRTist - analytical RT inspection simulation tool T2 - 45th Annual British Conference on NDT CY - Stratford-upon-Avon, England DA - 2006-09-12 PY - 2006 AN - OPUS4-13979 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bellon, Carsten T1 - aRTist - analytical RT inspection simulation tool T2 - International Symposium on Digital Industrial Radiology and Computed Tomography DIR 2007 CY - Lyon, France DA - 2007-06-25 PY - 2007 AN - OPUS4-15473 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wachtendorf, Volker T1 - Artificial weathering including acidic deposition T2 - 3rd European Weathering Symposium CY - Kraków, Poland DA - 2007-09-12 PY - 2007 AN - OPUS4-15907 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lauer, Franziska T1 - Artificial pollen grain mixtures analyzed with multivariate MALDI-TOF MS imaging N2 - Anemophilous plants produce pollen grains, which have to be monitored to provide an information network for persons suffering from an allergy. The current conventional characterization and identification of pollen is performed by time-consuming microscopic examinations on the basis of the genus-specific pollen shape and size. These examinations are in need of proficient researchers, are not statistically validated, and additionally rely on relatively inaccurate observations of the pollination process. A variety of new analytical approaches have been proposed in order to develop a fast and reliable pollen identification using specific molecular information. Recently, matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF MS) was initially applied for the rapid investigation of such complex biological samples. The combination of the obtained patterns of pollen mass spectra and multivariate statistics provide a powerful tool for identifying taxonomic relationships. Here promising results obtained by the reduction and optimization of sample preparation prior to MALDI-TOF MS mapping are presented. Based on a novel application of conductive carbon tape as target, the signal information of the species-specific mass peak patterns of pollen was enhanced. This leads to a clear separation in a subsequent pattern analysis, which is important when analyzing pollen grains in natural species mixtures. As a proof-of-concept, artificial pollen mixtures were investigated by MALDI imaging and evaluated by innovative multivariate data analysis strategies, to assign individual pollen species in the mixtures. Our results can be used to improve the taxonomic differentiation and identification of pollen species and might be useful for the development of a routine method to identify pollen based on mass spectrometry. T2 - ANAKON 2017 CY - Tübingen, Germany DA - 03.04.2017 KW - Sample pretreatment KW - MALDI-TOF MS KW - HCA and PCA imaging KW - Pollen PY - 2017 AN - OPUS4-39989 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lukas, M. T1 - Artificial plastic aging as a framework for microplastics ecotoxicity evaluation N2 - Microplastics are widely distributed in aquatic and terrestrial environments, up to now less is known on toxicological impacts under realistic conditions. Research so far has focused mainly on the impacts on organisms by fresh plastic fragments or beats. However, plastic materials found in the environment are mainly a mixture of different polymers and additives and particularly degraded during aging processes. Although especially oxidized degradation products might escape from plastic materials during aging, there is a lack of information on potentially adverse effects on aquatic biota. The latter is of particular interest as oxidized chemicals become more water soluble due to higher polarity and are more bio-available, therefore. The present study focused on plastic leachates of polystyrene (PS) and polylactic acid (PLA), which were derived from alternating stress by hydrolysis and UV radiation. Test specimen of PS, PLA or PS/PLA blends (each 50 %) were alternatingly maintained in water at 45 °C for five days and UV radiated at 45 °C for two days, for in total six weeks. Ecotoxicological effects of potentially generated degradation products of plastic materials in the storage water (mineral water, pH: 7.2) were detected by algae growth inhibition tests with Desmodesmus suspicatus and photosystem II inhibition tests with Raphidocelis subcapitata. Results clearly indicate inhibitory effects on algae growth by contaminants in the storage water of stressed plastic materials with increasing growth inhibition of proceeding hydrolysis and UV stress times. Here, different plastics cause variable responses of algal growth. First chemical analyses indicate dissolved monomers and their oxidation products of plastic materials as possible driver of detected ecotoxicological effects, since detected microplastic particles do not seem to harm algae. The existing data highlight the relevance of plastic aging as a framework for microplastic ecotoxicity evaluation and allow a proof of concept. T2 - 37. DGL-Tagung, Universität Konstanz CY - Konstanz, Germany DA - 19.09.2022 KW - Microplastic KW - Ecotoxicity PY - 2022 AN - OPUS4-55870 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lukas, M. T1 - Artificial Plastic Ageing as a Framework for Microplastics Ecotoxicity Evaluation N2 - Microplastics are widely distributed in aquatic and terrestrial environments, up to now less is known on toxicological impacts under realistic conditions. Research so far has focused mainly on the impacts on organisms by fresh plastic fragments or beats. However, plastic materials found in the environment are mainly a mixture of different polymers and particularly degraded during aging processes. Although especially oxidized degradation products might escape from plastic materials during aging, there is a lack of information on potentially adverse effects on aquatic biota. The latter is of particular interest as oxidized chemicals become more water soluble due to higher polarity and are more bio-available, therefore. The present study focussed on plastic leachates of polystyrene (PS) and polylactic acid (PLA), which were derived from alternating stress by hydrolysis and UV radiation. Test specimen of PS, PLA or PS/PLA blends (each 50 %) were alternatingly maintained in water at 45 °C for five days and UV radiated at 45 °C for two days, for in total six weeks. Ecotoxicological effects of potentially generated degradation products of plastic materials in the storage water (mineral water, pH: 7.2) were detected by algae growth inhibition tests with Desmodesmus suspicatus and photosystem II inhibition tests with Raphidocelis subcapitata. Results clearly indicate inhibitory effects on algae growth by contaminants in the storage water of stressed plastic materials with increasing growth inhibition of proceeding hydrolysis and UV stress times. Here, different plastics cause variable responses of algal growth. First chemical analyses indicate dissolved monomers and their oxidation products of plastic materials as possible driver of detected ecotoxicological effects, since detected microplastic particles do not seem to harm algae. The existing data highlight the relevance of plastic aging as a framework for microplastic ecotoxicity evaluation and allow a proof of concept. T2 - SETAC 2023 CY - Dublin, Ireland DA - 30.04.2023 KW - Microplastics KW - Ecotoxicity KW - Plastic aging KW - Algae growth inhibition tests PY - 2023 AN - OPUS4-57501 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kowarik, Stefan T1 - Artificial intelligence, the end of the world, and surface science N2 - Artificial intelligence (AI), machine learning, and neural networks have revolutionized fields such as self-driving cars or machine translation. Indeed, AI has progressed so far that scientists such as Stephen Hawking now fear that it may destroy humankind altogether. So, let’s get started and use AI in surface science. Here we train neural networks to use raw measurement data as input and immediately return the desired output parameters. We discuss the example of X-ray reflectivity measurements of ultrathin films, which contain reciprocal space information and must traditionally be fitted with dynamic scattering theory. Instead, we train the neural network with simulated X-ray data of multilayer structures and then apply it to measurement data. The neural network yields high accuracy results, is robust against noise, and performs significantly faster than fitting algorithms in real-time experiments. The presented neural network data analysis is becoming increasingly attractive, because free software has become very accessible and specialized computer chips (NPU) are currently being rolled out. T2 - DPG Früjahrstagung CY - Berlin, Germany DA - 12.03.2018 KW - X-ray reflectivity KW - AI KW - Machine learning KW - Neural network PY - 2017 AN - OPUS4-44602 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Völker, Christoph T1 - Artificial intelligence in NDT (AI NDT) a networking workshop N2 - Data-driven research is considered the new paradigm in science. In this field, data is the new resource from which knowledge is extracted that is too complex for traditional methods. Several factors such as national funding and advances in information technology, are driving the development. In particular, the creation of databases and the analysis of data with artifical intelligence are playing an important role in establishing the new paradigm. However, there are numerous challenges that must be overcome to realize the full potential of data-driven methods. This talk sets the stage for the upcoming workshop by reviewing some of the historical developments and the current state of data-driven science in NDT and materials science. T2 - Workshop on Artificial Intelligence in NDT (AI-NDT) CY - Online meeting DA - 30.10.2020 KW - Data Science KW - Materials Informatics KW - NDT PY - 2020 AN - OPUS4-51812 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Radtke, Martin T1 - Artificial intelligence for spectroscopy examples from BAMline N2 - Various applications for artificial intelligence in the context of spectroscopy will be presented. in particular, examples from bamline will be featured. After a short introduction to synchrotron radiation, artificial intelligence algorithms for the quantification of X-ray fluorescence measurement are discussed. In the second example, information retrieval by natural language processing is reviewed. As a last example the reconstruction of measurements with the X-ray color camera and coded apertures is presented. T2 - Seminar Strahlenphysikalische Anwendungen in Technik und Medizin CY - ATi Wien, Austria DA - 22.01.2020 KW - Machine learning KW - Natural language processing KW - Neural networks KW - Synchrotron KW - BAMline PY - 2020 AN - OPUS4-51891 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Fricke, F. A1 - Meyer, Klas T1 - Artificial Intelligence for Mass Spectrometry and Nuclear Magnetic Resonance Spectroscopy N2 - Mass Spectrometry (MS) and Nuclear Magnetic Resonance Spectroscopy (NMR) are critical components of every industrial chemical process as they provide information on the concentrations of individual compounds and by-products. These processes are carried out manually and by a specialist, which takes a substantial amount of time and prevents their utilization for real-time closed-loop process control. This paper presents recent advances from two projects that use Artificial Neural Networks (ANNs) to address the challenges of automation and performance-efficient realizations of MS and NMR. In the first part, a complete toolchain has been developed to develop simulated spectra and train ANNs to identify compounds in MS. In the second part, a limited number of experimental NMR spectra have been augmented by simulated spectra to train an ANN with better prediction performance and speed than state-of-theart analysis. These results suggest that, in the context of the digital transformation of the process industry, we are now on the threshold of a possible strongly simplified use of MS and MRS and the accompanying data evaluation by machine-supported procedures, and can utilize both methods much wider for reaction and process monitoring or quality control. T2 - 2021 Design, Automation & Test in Europe Conference & Exhibition (DATE) CY - Online meeting DA - 01.02.2021 KW - Industry 4.0 KW - Cyber-Physical Systems KW - Artificial Neural Networks KW - Mass Spectrometry KW - Nuclear Magnetic Resonance Spectroscopy PY - 2021 UR - www.date-conference.com AN - OPUS4-52181 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hübert, Thomas T1 - Artificial fruits - post harvest online monitoring of agricultural food by measuring humidity and temperature T2 - TEMPMEKO+ISHM 2010 (Joint International Symposium on Temperature, Humidity, Moisture and Thermal Measurements in Industry and Science) CY - Portorož, Slovenia DA - 2010-05-31 PY - 2010 AN - OPUS4-21368 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kästner, Claudia T1 - Artificial Digestion of Colloidal Silver Monitored by Small-Angle X-Ray Scattering N2 - In the last decade the utilization of silver nanoparticles in consumer related products is enhanced. Therefore, many studies focus on investigations regarding their toxicological potential. This includes investigations concerning uptake, distribution and excretion of the particles. So far, little attention was paid to changes of physical and chemical properties in the human body. During processes like digestion, the question arises whether they can pass this barrier in a nanoscale form. In this study we analytically monitored the changes in the size distribution of colloidal silver during an artificial digestion process with the help of small angle x-ray scattering (SAXS). Therefore, we synthesized polyacrylic acid stabilized ultra-small silver nanoparticles with a radius of 3 nm and a size distribution width of 18%. The artificial digestion process mimics the gastro-intestinal passage and simulates the oral, gastric and small intestinal conditions. Additionally, food components like oil, starch, glucose and skimmed milk powder are used to provide a preferably realistic environment. In absence of any food components the low pH initiates aggregation of the particles in the stomach. However, the particles unexpectedly stabilize in a defined cluster form with a mean radius of 12 nm. By the use of the food components oil and starch we observed that the particles are dispersed again. Now we found a bimodal size distribution of primary particles and aggregates. In contrast to that, with skimmed milk powder only a slight aggregation occurs in the stomach. In the gastric tract the particle distribution is stabilized at a mean volume weighted radius of 5 nm. Hence, skimmed milk powder acts as a colloidal stabilizer. For comparison we also used silver nitrate as a control substance. Surprisingly, we observed a formation of nanoparticles already in the saliva. During the digestion process the distribution narrows and finally in the intestine it shows a stable distribution with a mean volume weighted radius of 3 nm and a small fraction of aggregates. These results indicate that the silver nanoparticles can pass the digestion process in a nanoscale form but undergo a transformation in the size distribution. However, even from pure silver nitrate nanoparticle formation can be observed. This sketches a complex mechanism in which not only food components but also silver ions cause changes in nanoparticle size and aggregation. T2 - 6th International Colloids Conference CY - Berlin, Germany DA - 19.06.2016 KW - SAXS KW - Artificial digestion KW - Silver nanoparticles PY - 2016 AN - OPUS4-36888 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Sieg, H. T1 - Artificial digestion of aluminium-containing nanomaterials and their effects on the gastrointestinal tract in vitro N2 - Although aluminium is one of the most common elements in the biosphere, up to now little is known about its impact on human health. aluminium and its chemical derivatives are highly abundant in food, food contact materials and consumer products. Humans are exposed to aluminium via the gastrointestinal tract (GI tract). Exposition can change substantially due to consumer behavior since aluminium is also a compound of numerous food additives. Recently, aluminium exposition is increasingly considered to cohere with cancer and neurodegenerative disorders. Lately, due to an increasing attentiveness on this topic, limiting values for food additives have been tightened by the EFSA. However, cellular effects of aluminium and especially aluminium-containing nanomaterials, that represent a significant part of chemicals found in food products, are widely unknown and in the focus of our research activities, for example in the bilateral SolNanoTOX project. We established an in vitro simulation system of the GI tract, where nanomaterials undergo the different physiological, chemical and proteinbiochemical conditions of saliva, gastric juice and the intestine. The artificially digested nanomaterials, as well as soluble aluminium chloride as ionic control substance, were subjected to several analytical and biochemical methods to characterize their change of appearance and their cytotoxic effects on intestinal cellular models. We observed the fate of the nanomaterials during typical pH-values of saliva, gastric and intestinal juice with Dynamic light scattering measurements and ICP-MS in the single particle mode. After observable disappearance at pH 2 the particles recovered in the simulated intestinal fluid. The simulation of the GI tract, mainly the change of pH settings, can lead to a certain chemical activation of aluminium that can increase bioavailability in the intestine after oral uptake of aluminium-containing food products. In vitro assays like CTB, MTT and cellular impedance measurements showed that there were no acute cytotoxic effects measurable after a period up to 48h after incubation, comparable to undigested particles. In contrast, high amounts of aluminium ions showed synergistic effects on cell viability compared to non-digested aluminium ions. Although toxicological potential of Al ions to healthy tissue appears to be low, increased hazardous potential cannot be ruled out to pre-damaged tissue and can have a relevance in risk assessment for special consumer groups with for example chronical intestinal inflammation or dietary eating behavior combined with high exposure to Al-containing food products. T2 - 82nd Annual Meeting of the German Society for Experimental and Clinical Pharmacology and Toxicology CY - Berlin, Germany DA - 29.02.2016 KW - Nanoparticles KW - Digestion KW - SAXS KW - Cytotoxicity PY - 2016 AN - OPUS4-36026 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Isecke, Bernd T1 - Art der Korrosion T2 - Deutscher Verband für Schweißtechnik DVS Sektion Berlin CY - Brandenburg, Germany DA - 2006-01-28 PY - 2006 AN - OPUS4-12144 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Arroyo-Abad, Uriel T1 - Arsenolipids in marine fish: Occurence and Perspective T2 - Anakon 2015 CY - Graz, Austria DA - 2015-03-23 PY - 2015 AN - OPUS4-33647 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Arroyo-Abad, Uriel T1 - Arsenolipids in marine fish: Occurence and Perspective T2 - CANAS - Colloquium Analytische Atomspektroskopie CY - Leipzig, Germany DA - 2015-03-08 PY - 2015 AN - OPUS4-33648 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Piechotta, Christian T1 - Arsenolipide im Hering - Eine Quelle für kanzerogene Arsenverbindungen im Urin? T2 - ANAKON 2013 CY - Essen, Germany DA - 2013-03-04 PY - 2013 AN - OPUS4-27858 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Arroyo-Abad, Uriel T1 - Arsenolipid pattern in fresh cod liver: application of RP-HPLC with simultaneous ICP-MS and ESI-Q-TOF-MS detection T2 - Metallomics 2013 CY - Oviedo, Spain DA - 2013-07-08 PY - 2013 AN - OPUS4-28774 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lischka, Susanne T1 - Arsenobetainbestimmung in Fisch mittels LC-ESI-MS/MS T2 - CIA CY - Berlin, Germany DA - 2011-09-26 PY - 2011 AN - OPUS4-24419 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lischka, Susanne T1 - Arsenobetainanalytik unter Einsatz eines 13C-markierten Kalibrierstandard für Elektrospray-Massenspektrometrie T2 - Doktorandenseminar des AK Separation Science der GDCh CY - Hohenroda, Germany DA - 2012-01-08 PY - 2012 AN - OPUS4-25662 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kappler, A. T1 - Arsenic redox transformation by humanic substances and Fe minerals T2 - Ninth International Symposium on the Geochemistry of the Earth's Sureface (GES-9) CY - Boulder, CO, USA DA - 2011-06-01 PY - 2011 AN - OPUS4-25154 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Piechotta, Christian T1 - Arsenic and Mercury speciation in fish T2 - GSF Speciation 2008 CY - Munich, Germany DA - 2008-05-25 PY - 2008 AN - OPUS4-17790 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Piechotta, Christian T1 - Arsen- und Quecksilberspezies in Fisch T2 - 4. Conference über Ionenanalyse, Technische Universität Berlin CY - Berlin, Germany DA - 2007-03-12 PY - 2007 AN - OPUS4-14307 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Swart, Claudia T1 - Arsen in Wasser: Quellen, Bestimmung und Entfernung der verschiedenen Spezies T2 - Innovationsforum-Nanobasierte Umwelttechnik CY - Jena, Germany DA - 2006-11-09 PY - 2006 AN - OPUS4-13777 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wachtendorf, Volker T1 - Arrhenius-Ansatz zur Lebensdauervorhersage aus künstlichen Bewitterungsversuchen T2 - 41. Jahrestagung der GUS 2012 - Umwelteinflüsse erfassen, simulieren, bewerten CY - Stutensee, Germany DA - 2012-03-14 PY - 2012 AN - OPUS4-25627 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hufschläger, Daniel A1 - Gaal, Mate A1 - Gohlke, Dirk A1 - Weise, Matthias A1 - Szewieczek, A. A1 - Hillger, W. A1 - Ilse, D. T1 - Array-Prüfköpfe für luftgekoppelte Ultraschallprüfung N2 - Seit Jahren stellt die luftgekoppelte Ultraschallprüfung eine etablierte Alternative zur konventionellen Prüfung von Leichtbaukomponenten aus den Bereichen Luft- und Raumfahrt sowie Automotive dar. Im Gegenteil zur flüssigkeitsgekoppelten Prüfung in Kontakt oder im Tauchbecken ist sie weniger invasiv und bietet daher zeitliche und finanzielle Anreize. Normalerweise wird die luftgekoppelte Prüfung mit Einzelelementschwingern in Durchschallung realisiert, wohingegen die Gruppenstrahlertechnik bereits Industriestandard im Bereich der Kontakttechnik darstellt. Die damit verbundenen Vorteile wie die aktive Fokussierung oder, die gezielte Manipulation des Einschallwinkels zur Anregung von geführten Wellen, finden im Bereich der luftgekoppelten Prüfung dabei noch wenig Anwendung. Im Rahmen dieses Beitrags stellen wir die ersten Zwischenergebnisse des geförderten Projektes „PALUP – Phased- Array-Technik für Luftultraschall-Prüfungen“ vor. Ziel des Projektes ist die Entwicklung von Mehrelementschwingern auf Basis von zellulären Kunststoffen, die Entwicklung einer dedizierten Pulserstufe im Kilovoltbereich, sowie die nötige rauscharme messtechnische Auswertung jedes Einzelelements. T2 - DGZfP Jahrestagung CY - Kassel, Germany DA - 23.05.2022 KW - Phased array KW - Air-coupled ultrasound PY - 2022 AN - OPUS4-54996 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Krenzer, Julius A1 - Mueller, Thomas T1 - Aroyl-S,N-ketene acetal based bichromophores exhibiting energy transfer and aggregation induced (dual) emission N2 - A series of aroyl-S,N-ketene acetal based bichromophores is readily synthesized by Buchwald-Hartwig amination and Ullmann reaction in moderate to good yields. The aminated aroyl-S,N-ketene acetals are emissive in the solid state and in the aggregate, but not in solution, thus, they are AIEgens (aggregation induced emission chromogens). Aggregation is induced by fractional alternation of the solvent mixture, here by increasing the water fraction of ethanol/water mixtures. For most derivatives, the emission upon induced aggregation stems solely from the aroyl-S,N-ketene acetal chromophore, regardless whether excitation occurs at the absorption maximum of the triarylamine or the aroyl-S,N-ketene acetal. Therefore, a pronounced energy transfer from the triarylamine donor to the aroyl-S,N-ketene acetal acceptor can be inferred. The color of the emission can be controlled by choosing the para-aroyl substituent. A partial energy transfer could also be observed for some bichromophores, leading to aggregation-induced dual emission (AIDE). In addition, four examples of aminated diaroyl-S,N-ketene acetals were added to the compound library. The electron-withdrawing properties of the additional aroyl group provide a bathochromic shift of the emission band of the aroyl-S,N-ketene acetal. These bichromophores also show AIDE and in one case even aggregation-induced white light emission as a result of additive color mixing. T2 - Beilstein Symposium on pi-Conjugated Molecules and Materials CY - Limburg, Germany DA - 07.11.2023 KW - aggregation-induced dual emission (AIDE) PY - 2023 AN - OPUS4-59006 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Epping, Ruben T1 - Aroma Sensing of Truffles N2 - The aim of this project is to develop a mobile technical device to search for truffles. This way, truffles can be harvested faster, cheaper and more efficiently compared to the current method using dogs. For this purpose, suitable marker substances in the aroma of ripe truffles were identified using analytical-chemical methods. The collected data was used to create aroma profiles of different truffle species. The specificity of possible marker substances was confirmed with a truffle dog study. The hypothesis “If trained truffle dogs recognize the substances as supposed truffles in the context of an experiment, they can be regarded as specific” was made. The results show that the truffle aroma is mainly characterized and perceived by dogs by dimethyl sulfide and dimethyl disulfide. For the concentration measurement of these markers in the ambient air, we are currently building our own detector. The Challenge is to get a fast measurement with a very low limit of detection at the same time. The device will resemble a metal detector in terms of shape and handling and be particularly suitable for mobile use. The R&D cooperation project between the Federal Institute for Materials Research and Testing (BAM) and sglux GmbH thus enables truffles to be harvested professionally and systematically. This brings the technical advances that have revolutionized agriculture over the last hundred years to truffle cultivation for the first time. T2 - Adlershofer Forschungsforum CY - Berlin, Germany DA - 11.11.2022 KW - Truffle KW - Volatile organic compounds KW - Gas chromatography KW - Canine olfactometry PY - 2022 AN - OPUS4-56301 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ramanujam, Maalolan T1 - Argon Plasma Treatment of Polymers - Trapping of Radicals by Nitric Oxidegassing T2 - Plasma Surface Engineering 2010 CY - Garmisch-Partenkirchen, Germany DA - 2010-09-13 PY - 2010 AN - OPUS4-23244 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bonnerot, Olivier T1 - Are X-rays safe for manuscripts’ materials? N2 - In the last decade, applications of X-rays to the study of manuscripts significantly spread in both diversity and extent. They range from writing material analysis, mostly with X-ray fluorescence (XRF), permitting non-invasive characterization of inks and pigments used, to the investigation of the origin of writing supports. In addition, XRF mapping has proved to be an invaluable tool for recovering erased text. Finally, computed-tomography (CT) has shown potential in virtually unrolling rolls, making text readable without using-damaging mechanical methods. Despite their growing use, little attention has been paid to the side effects of such analytical tools. We observed irreversible parchment colour changes during some experiments on dead-sea scrolls with synchrotron radiation sources. Furthermore, partial photo-reduction of iron under high intensity beam during X-ray absorption near edge structure spectroscopy (XANES) measurements of iron-gall ink on paper has been reported several times [5,6]. Such phenomena have mostly been overlooked so far, although there is an increasing awareness of the necessity to study them. We conducted experiments at the Deutsches Elektronen-Synchrotron (DESY) facilities to investigate X-ray induced structural alteration of paper and parchment to see whether the presence of absorption centres (ink and pigments) has an impact. In addition to better understanding degradation processes, we are aiming to define an appropriate methodology of analysis of manuscripts with a tolerable risk of damage. The first results concerning X-ray induced damage of cellulose materials have already been presented at the Synchrotron Radiation and Neutrons in Art and Archaeology (SR2A). We are focusing here on the results on parchment materials. T2 - Cultural and Natural Heritage Workshop CY - Grenoble, France DA - 22.01.2020 KW - X-rays KW - Manuscripts KW - Parchment KW - Synchrotron PY - 2020 AN - OPUS4-50305 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schönhals, Andreas T1 - Are the termal Tg and the segmental dynamics in polymer thin films fully interdependent T2 - Broadband Dielectric Spectroscopy and its Applications CY - Leipzig, Germany DA - 2012-09-03 PY - 2012 AN - OPUS4-26866 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lohrer, Christian T1 - ARE SHELLS "SAFETY" DISTANCES "SAFE"? T2 - 15th International Symposium on Fireworks CY - Bordeaux, France DA - 2015-09-21 PY - 2015 AN - OPUS4-33862 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schröpfer, Dirk A1 - Kromm, Arne T1 - Are residual stresses influenced by a mill scale? - Welding Residual Stresses in Quenched and Tempered and Thermo-Mechanically Hot Rolled High Strength Steels T2 - 9th European Conference on Residual Stresses CY - Troyes, France DA - 2014-07-07 PY - 2014 AN - OPUS4-31031 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wawrzyn, Eliza T1 - Are novel aryl phospates competitors for BDP in halogen-free flame retarded PC/ABS/PTFE blend? T2 - Polymers for Advanced Technologies 2011 CY - Lodz, Poland DA - 2011-10-02 PY - 2011 AN - OPUS4-24439 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Jaenisch, Gerd-Rüdiger T1 - Are Monte Carlo Model Applicable to Radiological Techniques? T2 - National Seminar on NDE of the Indian Society for Non-Destructive Testing CY - Kolkata, India DA - 2005-12-02 PY - 2005 AN - OPUS4-11437 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Liebner, Christian T1 - Are microreaction devices inherently safe? An investigation on gas phase explosion propagation limits T2 - 13th International Symposium on Loss Prevention and Safety Promotion in the Process Industries CY - Bruges, Belgium DA - 2010-06-06 PY - 2010 AN - OPUS4-21391 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Behrendt, S. T1 - Archäometrische Untersuchungen an Stuckartefakten zur Klärung von Alter, Herkunft und Authentizität T2 - Mu Tec, Internationale Fachmesse für Museums- und Ausstelltechnik CY - Leipzig, Germany DA - 2010-11-18 PY - 2010 AN - OPUS4-22008 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Behrendt, S. T1 - Archäometrische Untersuchungen an Stuckartefakten zur Klärung von Alter, Herkunft und Authentizität T2 - Tagung Archäometrie und Denkmalpflege CY - Bochum, Germany DA - 2010-09-15 PY - 2010 AN - OPUS4-22009 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Paz, B. T1 - Archäometrische Untersuchungen an Glasfragmenten aus abbasidischer Zeit T2 - Jahrestagung Archäometrie und Denkmalpflege 2013 CY - Weimar, Germany DA - 2013-09-25 PY - 2013 AN - OPUS4-29784 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hahn, Oliver T1 - Archäometrie und Denkmalpflege 2003 T2 - Archäometrie und Denkmalpflege, Kurzberichte 2003, Staatliche Museen zu Berlin CY - Berlin, Germany DA - 2003-03-12 PY - 2003 AN - OPUS4-3305 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hahn, Oliver T1 - Archäometrie contra Restaurierung - die Beduetung der Naturwissenschaften bei der Entscharfung eines Konfliktes T2 - Jahrestagung Archäometrie und Landesamt für Denkmalpflege CY - Mainz, Deutschland DA - 2015-03-25 PY - 2015 AN - OPUS4-32911 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Reinholz, Uwe T1 - Archäometrie an der BAMline T2 - Lange Nacht der Wissenschaften, BAM, BESSY II CY - Berlin, Germany DA - 2010-06-05 PY - 2010 AN - OPUS4-21379 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rabin, Ira T1 - Archeometry of the Dead Sea Scrolls T2 - Laboratorii Nazionali del Sud, INFN CY - Catania, Italy DA - 2009-03-18 PY - 2009 AN - OPUS4-19669 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rabin, Ira T1 - Archaeometry of the Dead Sea Scrolls T2 - SBL International Meeting CY - London, England DA - 2011-07-04 PY - 2011 AN - OPUS4-24280 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -