TY - CONF A1 - Theiler, Geraldine A1 - Cano Murillo, Natalia A1 - Sawae, Y. A1 - Shinmori, H. A1 - Hashimoto, H. A1 - Aoyagi, A. A1 - Dobbelaar, E. T1 - Towards sustainable and hydrogen compatible sealing materials N2 - Materialien auf PTFE-Basis werden in der Regel als Kolbenringe in Hochdruck- und/oder kryogenem Wasserstoff verwendet. In diesem Projekt werden neu formulierte und nachhaltigere Polymerwerkstoffe mit herkömmlichen Materialien verglichen. Auf Grundlage der tribologischen Ergebnisse werden vielversprechende Kandidaten zusammen mit Reibungsmechanismen sowohl bei Hochdruck- als auch bei Niedrigtemperatur-Wasserstoff vorgeschlagen. T2 - 66. GfT Tribologie-Fachtagung 2025 CY - Wernigerode, Germany DA - 29.09.2025 KW - Wasserstoff KW - Reibung KW - Verschleiß KW - Kolbenring KW - Dynamische Dichtung PY - 2025 VL - 09 SP - 1 EP - 4 AN - OPUS4-64314 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schaad, C. A1 - Tiebe, Carlo A1 - Groth, Katrina M. T1 - A Framework for Transforming Process Control System Data from a Hydrogen Fueling Station into HyCReD Data N2 - Reliability data for hydrogen infrastructure components is essential for developing Quantitative Risk Assessment (QRA) for these technologies, which in turn is necessary for a safer deployment and expansion of the hydrogen market. However, there is currently a lack of hydrogen component reliability data available for these systems, thus limiting the usefulness of insights obtained from these QRA. The Hydrogen Component Reliability Database (HyCReD) has been proposed as a tool for reliability data collection and as a source for future QRAs. In this paper, we develop a digital tool that automatically processes data coming from Process Control System (PCS) in a hydrogen fueling station, detects the relevant failure events for hydrogen systems during its operation, and then logs the event information into HyCReD. To build this tool, we first categorized the station components in hydrogen service, their specific failure modes, and the specific failure mechanisms that are relevant to a QRA. Then, we identified the data available in the station PCS and the methods available for diagnosing the relevant failure events. The resulting tool is divided into three steps: (1) PCS data collection through an API, (2) data analysis for the detection and diagnosis of new failure events, and (3) logging that event into HyCReD. Finally, we discuss the potential for expanding the detection and diagnosis to more complex failure modes present in a hydrogen fueling station. This digital tool is set for implementation and validation on an experimental hydrogen fueling site. The goal for this digital tool is to be applicable to every kind of hydrogen fueling station and to be extendable to similar hydrogen technologies. T2 - 35th European Safety and Reliability Conference (ESREL2025) and the 33rd Society for Risk Analysis Europe Conference (SRA-E 2025) CY - Stavanger, Norway DA - 15.06.2025 KW - Reliability data KW - Hydrogen safety KW - HyCReD KW - Hydrogen Component Reliability Database KW - Hydrogen fueling station KW - Hydrogen refuelling station KW - HRS PY - 2025 UR - https://rpsonline.com.sg/proceedings/esrel-sra-e2025/html/ESREL-SRA-E2025-P6264.html SN - 978-981-94-3281-3 DO - https://doi.org/10.3850/978-981-94-3281-3-procd SP - 2663 EP - 2670 PB - Research Publishing CY - Singapore AN - OPUS4-63532 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eberwein, Robert A1 - Hajhariri, Aliasghar A1 - Otremba, Frank A1 - Camplese, Davide A1 - Scarponi, Giordano E. A1 - Cozzani, Valerio A1 - Seidlitz, Holger T1 - Repeatable testing of a cryogenic storage tank with variable insulation material in fire like conditions N2 - For decarbonizing the energy industry and transport, cryogenic energy carriers have great potential. The storage takes place in tanks with thermal super-insulations, which are in application for decades, but there is only limited knowledge about its behaviour in a fire scenario. This represents a major incident that may generate extraordinary loads on the tank and its insulation system, and that eventually lead to a sudden tank failure. This paper presents a test rig called the Cryogenic High Temperature Thermal Vacuum Chamber (CHTTVC), which can be used to test typical thermal superinsulation’s under cryogenic and fire-like conditions in parallel. The test method makes it possible to measure the heat flow through the thermal superinsulation over time and to investigate the degradation behaviour of the insulation within a test. In the paper results from the first tests are presented. T2 - 18th Cryogenics 2025, IIR Conference CY - Prague, Czech Republic DA - 07.04.2025 KW - LH2 KW - LNG KW - Fire KW - Insulation KW - Safety PY - 2025 DO - https://doi.org/10.18462/iir.cryo.2025.0007 SP - 205 EP - 210 CY - Prag AN - OPUS4-63740 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tiebe, Carlo A1 - Detjens, Marc A1 - Fechner, A. A1 - Sielemann, S. A1 - Lorek, A. A1 - Wernecke, R. A1 - Stoltenberg, H. T1 - Development of a device for staged determination of water activity and moisture content N2 - Moisture content and water activity are important parameters for quality characterization of products like bulk materials, powders, granules. Thus, an exact determination is necessarily required in a wide range of industrial applications. Moisture of materials is the content of non-chemically bound water in a solid or liquid. Water activity (aW) is a characteristic/parameter of the non-chemically bound ("free") water in materials and is measured as humidity over a solid/liquid surface at constant temperature (equilibrium moisture content). It is an important parameter to characterize the quality of e. g. pharmaceutical and food products. In our contribution, we present the developed MOISHUM device for staged determination of water activity and moisture content of liquid and solid materials. T2 - Eurosensors 2018 CY - Graz, Austria DA - 09.09.2018 KW - Water activity KW - Moisture KW - Coulometric humidity sensor KW - MOISHUM PY - 2018 SN - 2504-3900 SP - 7253, 1 EP - 4 PB - MDPI AN - OPUS4-46210 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Detjens, Marc A1 - Tiebe, Carlo A1 - Banach, Ulrich A1 - Ritter, U. T1 - Ionische Flüssigkeiten als neuartige Sensorbeschichtung für coulometrische Spurenfeuchtesensoren N2 - Die Arbeit präsentiert erste Messungen mit coulometrischen Sensoren, die mit einer ionischen Flüssigkeit beschichtet sind. Diese Sensoren werden in der Industrie verwendet, um die Spurenfeuchte in unterschiedlichen Gasen zu messen. Normalerweise erfolgt eine Beschichtung der Sensoren mit Phosphorpentoxid und dessen Hydrolyseprodukte. In dieser Arbeit wurde stattdessen eine hygroskopische ionische Flüssigkeit benutzt. Die generierte Gasfeuchte für die Untersuchungen betrug bezogen auf die Frostpunkttemperatur -80 °C bis -30 °C, was gleichbedeutend mit einem Wasserdampf-Stoffmengenanteil von 0,5 μmol·mol-1 bis 376 μmol·mol-1 ist. Zusätzlich zu der Messung mit coulometrischen Sensoren erfolgte eine Referenzmessung der Gasfeuchte mittels eines Taupunkthygrometers. Erste Ergebnisse haben gezeigt, dass es möglich ist mit dieser Art der Beschichtung unterschiedliche Gasfeuchten zu messen. Aber es ergaben sich trotz gleicher Feuchte unterschiedliche Signalintensitäten bei den benutzen Sensoren und es zeigte sich eine Drift des Sensorsignales. T2 - Sensoren und Messsysteme CY - Nuremberg, Germany DA - 26.06.2018 KW - Spurenfeuchtemessung KW - Sensorbeschichtung KW - Elektrolyseverfahren KW - Ionische Flüssigkeiten PY - 2018 SN - 978-3-8007-4683-5 SN - 0932-6022 SP - 520 EP - 523 PB - VDE VERLAG GMBH CY - Berlin, Offenbach AN - OPUS4-45319 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Moufid, M. A1 - Tiebe, Carlo A1 - El Bari, N. A1 - Bartholmai, Matthias A1 - Bouchikhi, B. T1 - Combining of TD-GC-MS and home developed electronic nose for road traffic air monitoring N2 - In this work, we demonstrate the ability of an electronic nose system based on an array of six-semiconductor gas sensors for outdoor air quality monitoring over a day at a traffic road in downtown of Meknes city (Morocco). The response of the sensor array reaches its maximum in the evening of the investigated day which may due to high vehicular traffic or/and human habits resulting in elevated concentrations of pollutants. Dataset treatment by Principal Component Analysis and Discriminant Function Analysis shows a good discrimination between samples collected at different times of the day. Moreover, Support Vector Machines were used and reached a classification success rate of 97.5 %. Thermal Desorption-Gas Chromatography-Mass Spectrometry (TD-GC-MS) technique was used to validate the developed e-nose system by identifying the composition of the analyzed air samples. The discrimination obtained by e-nose system was in good agreement with the TD-GC-MS results. This study demonstrates the usefulness of TD-GC-MS and e-nose, providing high accuracy in discriminating outdoor air samples collected at different times. This demonstrates the potential of using the e-nose as a rapid, easy to use and inexpensive environmental monitoring system. T2 - 2021 IEEE International Conference on Design & Test of Integrated Micro & Nano-Systems (DTS) CY - Sfax, Tunisia DA - 07.06.2021 KW - GC-MS KW - Electronic nose KW - Gas sensors KW - Urban air monitoring PY - 2021 DO - https://doi.org/10.1109/DTS52014.2021.9498110 SP - 1 EP - 6 AN - OPUS4-54401 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Theiler, Geraldine A1 - Halder, Karabi A1 - Balasooriya, Winoj T1 - Effect of high-pressure hydrogen environment on the physical and mechanical properties of elastomers N2 - This paper deals with the exposure of HBNR rubbers to high pressure hydrogen (100 MPa) at 120 °C for 7 and 21 days under static conditions followed by characterization of their physical and mechanical properties. T2 - EHEC European Hydrogen Energy Conference 2022 CY - Madrid, Spain DA - 18.05.2022 KW - Rubbers KW - Hydrogen KW - Characterization PY - 2022 SP - 1 EP - 2 AN - OPUS4-62085 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Detjens, Marc A1 - Tiebe, Carlo A1 - Banach, Ulrich T1 - Influence of Gas Pressure on Coulometric Trace Humidity Measurement N2 - Planar coulometric sensors were investigated in humidified synthetic air at various absolute gas pressures, i. e. 2 bar, 5, bar, 10 bar, and 15 bar. Humidified gas flow at adjusted gas pressure was split into two flows, one passed a coulometric sensor and the other one passed a reference hygrometer after decompression. Both signals were recorded and then compared after calculation of resulting frost point temperature. Calculation is based on a calibration function obtained at ambient pressure. Comparison showed that an increasing pressure resulted in a higher derivation between sensor signal (calculated frost point temperature) and reference frost point temperature. At an absolute pressure of 2 bar the differences were minor in consideration of the uncertainty, however at 15 bar the differences were 6.77 K. Nevertheless, it was possible to measure the gas humidity at higher pressure with coulometric trace humidity sensors. T2 - 17th International Meeting of Chemical Sensors, IMCS 2018 CY - Vienna, Austria DA - 15.07.2018 KW - Gas pressure influence KW - Coulometric sensors KW - Trace humidity measurement PY - 2018 SN - 978-3-9816876-9-9 DO - https://doi.org/10.5162/IMCS2018/P2EC.7 SP - 715 EP - 716 PB - AMA Service GmbH CY - Wunstorf / Germany AN - OPUS4-45539 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Theiler, Geraldine A1 - Gradt, Thomas T1 - Friction and wear characteristics of polymers in gaseous and liquid N2 - In the present work it was shown that the the aim of the presented tests is to investigate polymer composites for their suitability for friction systems in gaseous and liquid hydrogen. T2 - 59. Tribologie-Fachtagung CY - Göttingen, Germany DA - 24.09.2018 KW - Friction KW - Wear KW - Polymer composites KW - Hydrogen KW - Cryogenic temperature PY - 2018 SN - 978-3-9817451-3-9 SP - 60/1 EP - 60/4 AN - OPUS4-46178 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Harwege, Finn A1 - Schmidt, Heiko A1 - Eberwein, Robert T1 - Testing of vacuum insulation panels for liquid hydrogen storage tanks N2 - Vacuum insulation panel (VIP) based insulation could present an alternative to the common double walled vacuum insulation for large liquefied Hydrogen (LH2) storage tanks. In this paper a brief introduction on VIPs and the envisioned design of VIP-based LH2-tank insulation is given. The design of a flat plate boil-off calorimeter for the testing of the insulation concept is shown, with regard to thermal design, mechanical design and instrumentation. Finally, an overview over the particular challenges for modelling VIP-based insulation and the proposed testing to be performed on the test rig is presented. T2 - 18th Cryogenics IIR International Conference CY - Prague, Czech Republic DA - 07.04.2025 KW - Liquefied Hydrogen KW - Insulation KW - Calorimeter KW - Vacuum Insulation Panel KW - LH2 PY - 2025 SN - 0151-1637 DO - https://doi.org/10.18462/iir.cryo.2025.0010 SN - 978-2-36215-053-1 VL - 2025 SP - 168 EP - 174 PB - ICCEX CY - Prag AN - OPUS4-62959 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schmidt, Martin A1 - Scheid, Marc A1 - Seifert, Alexander A1 - Böhme, Thilo A1 - Wehrstedt, Klaus-Dieter A1 - Bulin, Michael T1 - Bandbreiten sicherheitstechnischer Kenngrößen brennbarer Stäube im Gemeinsamen Stoffdatenpool Bund / Länder (GSBL) N2 - Die Beurteilung des Gefahrenpotentials brennbarer Stäube erfolgt üblicherweise mit Hilfe so genannter sicherheitstechnischer Kenngrößen (STK). Häufig werden hierfür in Datenbanken bereitgestellte Werte in der Vergangenheit untersuchter Stäube herangezogen. Insbesondere aufgrund stofflicher Unterschiede der untersuchten Stäube sind erhebliche Streuungen der ermittelten STK in Datenbanken enthaltener namentlich identischer Stäube festzustellen. Die Verwendung der Daten von Einzelstäuben kann daher zu unsicheren Einschätzungen hinsichtlich des Brand- und Explosionsschutzes führen. Vorgestellt wird ein Konzept, Stäube zu praxisrelevanten Gruppen zusammenzufassen und bewertete Bandbreiten sicherheitstechnischer Kenngrößen anzugeben. Die im Rahmen eines vom Sächsischen Landesamt für Umwelt, Landwirtschaft und Geologie, Dresden geförderten Vorhabens generierten Staubgruppen und zugehörigen Bandbreiten der STK stehen in der Datenbank GSBLpublic für die freie Nutzung zur Verfügung. T2 - 11. Fachtagung Anlagen-, Arbeits- und Umweltsicherheit CY - Köthen, Germany DA - 07.11.2013 KW - Sicherheitstechnische Kenngrößen KW - Stäube KW - Staubexplosionen KW - Datenbank PY - 2013 SN - 978-3-86011-058-4 IS - P-03 SP - 1 EP - 11 AN - OPUS4-29532 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Weimann, Karin A1 - Farago, Patrick A1 - Mayer, Felix ED - Angulo, Sergio ED - Landmann, Mirko T1 - New sources for secondary gypsum N2 - In order to protect natural gypsum deposits and to compensate for the decreasing amount of Flue Gas Desulfurization (FGD) gypsum it is necessary to develop and explore new sources of gypsum. For this purpose, the potentials of different gypsum wastes are investigated in the study “GipsRec 2.0”, funded by the Federal Ministry of Education and Research (Germany). On the one hand, the project worked on a new processing technology for gypsum fiberboards (GFB). While the recycling of gypsum plasterboards has already been carried out on an industrial scale for several years, the recycling of gypsum fiberboards (GFB) has proven to be challenging. Gypsum fiberboards from demolition sites and offcuts from GFB production were used for these investigations. The tests were conducted on a technical scale. Furthermore, various synthetic gypsums are being investigated with regard to their suitability for gypsum production. The analyses are carried out on production residues. In this project, a promising process for gypsum fiberboard recycling could be developed, as well as other waste gypsums are investigated and evaluated with regard to their potential as secondary raw material. In addition, selected process routes are assessed for their environmental impact using a life cycle assessment (LCA) approach. T2 - RILEM - V International Conference Progress of Recycling in the Built Environment CY - Weimar, Germany DA - 10.10.2023 KW - Gypsum recycling KW - Gypsum fiberboards and synthetic gypsum KW - Environmental evaluation PY - 2023 VL - V SP - 1 EP - 10 PB - RILEM Publications Sarl CY - Bagneux, France AN - OPUS4-60315 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Sterthaus, Jens A1 - Ballheimer, Viktor A1 - Kuschke, Christian A1 - Wille, Frank T1 - Numerical analysis of bolted trunnion systems of packages for radioactive materials N2 - Packages for the transport of radioactive material are generally equipped with particular components for crane operations and supporting the package during transport. As an example of such components the bolted trunnion system of heavy packages are analysed in this paper. According to the German guideline BAM-GGR 012 created by the BAM Federal Institute for Materials Research and Testing for analysis and assessment of bolted lid and trunnion Systems, the finite element (FE) method is to be used preferably in the analysis of such kind of structures to obtain more accurate and detailed Information about their stressing. The FE model of a trunnion System should include the trunnion itself, the bolts and an appropriate part of the packaging wall with necessary contact conditions on all interfaces between these components. The use of solid finite elements, which is generally recommended in the BAM-GGR 012 guideline, leads to local stress and strain fields as a result of the calculation. The modelling strategy, e.g. the way of modelling interaction between the components of the trunnion System, has an essential impact on these local values. The effect of different assumptions in a FE model is demonstrated in this paper using the calculation results for a reference trunnion System. The approaches for preparation and Interpretation of results in connection with local or nominal assessment criteria are discussed as well. T2 - ASME 2012 Pressure Vessels and Piping Division Conference - PVP 2012 CY - Toronto, Ontario, Canada DA - 15.07.2012 KW - Bolted trunnion KW - German guideline BAM-GGR 012 KW - Local stress and strain fields KW - Local and nominal assessment criteria PY - 2012 SP - 1 EP - 6 PB - American Society of Mechanical Engineers (ASME) CY - New York, NY AN - OPUS4-26835 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Steppan, Enrico A1 - Kromm, Arne A1 - Kannengießer, Thomas T1 - High-energy synchrotron study of the stress-strain behavior of hydrogen-charged high strength steel N2 - The ambition for light weight construction while simultaneously increasing the loading capacity is a main aim of many industries such as crane, vehicle, bridge construction, shipbuilding and plant construction. This aim is achieved by application of high strength structural steels with yield strengths of up to 1300 MPa. The plate thickness can be reduced and consequently the service load is increased. High strength structural steels are quenched and tempered and/or even thermo-mechanically processed. Their superior properties are due to precipitations formed by micro alloying elements finely dispersed in a martensitic matrix. The aim of this study was to observe the influence of hydrogen in the microstructure of high strength structural steel with the yield strength of 1300 MPa by using diffraction methods. Energy dispersive X-ray diffraction (EDXRD) available at the EDDI beam line of the HZB in Berlin Germany was utilized to compare the stress-strain behavior of samples exhibiting varying amounts of hydrogen during tensile loading. T2 - Visual-JW2012 - International Symposium on Visualization in Joining and Welding Science through Advanced Measurements and Simulation CY - Osaka, Japan DA - 28.11.2012 KW - High strength structural steel KW - Hydrogen diffusion KW - Hydrogen assisted cold cracking KW - Energy dispersive X-ray diffraction PY - 2012 IS - IWIS-17 SP - 228 EP - 229 PB - Joining and Welding Research Institute (JWRI) CY - Osaka AN - OPUS4-27396 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ohm, Katrin A1 - Baer, Wolfram ED - Grellmann, W. T1 - Einfluss der Verfahrenstechnik und der Werkstoffprüfung auf den im Zugversuch zu ermittelnden Verformbarkeitskennwert Agt von Betonstählen N2 - Die Streuung der Agt-Werte von Betonstahl bleibt durch die Variation der Prüfbedingungen (Temperatur, Geschwindigkeit) innerhalb der prüfnormseitig zulässigen Grenzen weitgehend unbeeinflusst. Gleichzeitig führt die Variation der Prüfbedingungen zu einer signifikanten, für die Produktabnahme relevanten Änderung des Niveaus von Agt. Die Auswertemethodik des Zugversuches (Festlegung der Höchstkraft, Wahl des Verfahrens zur Agt-Bestimmung) hat einen signifikanten Einfluss auf Niveau und Streuung von Agt. Es werden Empfehlungen zur Minimierung der Streuung von Agt gegeben. T2 - DVM-Tagung Werkstoffprüfung 2011 - Neue Entwicklungen in der Werkstoffprüfung - Herausforderungen an die Kennwertermittlung CY - Berlin, Germany DA - 01.12.2011 KW - Betonstahl KW - Zugversuch KW - Gesamtdehnung bei Höchstkraft KW - Kennwertstreuung KW - Prüfmethodik KW - Reinforcing steel KW - Tensile test KW - Percentage total extension at maximum force KW - Scatter of results KW - Test method PY - 2011 SN - 978-3-9814516-1-0 SN - 1861-8154 N1 - Serientitel: DVM-Bericht – Series title: DVM-Bericht IS - 643 SP - 279 EP - 284 AN - OPUS4-25068 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Viehrig, H.-W. A1 - Baer, Wolfram A1 - Gerwien, Peter A1 - Grundmann, N. A1 - Houska, M. A1 - Lucon, E. A1 - Mottitschka, T. A1 - Trubitz, P. T1 - Bestimmung der J-Risswiderstandskurve an einem zähen Reaktordruckbehälterstahl - Ergebnisse eines Round Robin Tests N2 - Die Bruchzähigkeit von Stählen kann im elastisch-plastischen Beanspruchungsbereich anhand von Risswiderstandskurven z.B. nach den Prüfnormen ISO 12135 und ASTM E1820 ermittelt werden, wobei die duktile Rissausbreitung mittels Mehr- oder Einprobenverfahren gemessen wird. Das Teilentlastungsverfahren ist das am weitesten verbreitete Einprobenverfahren zur Ermittlung von Risswiderstandskurven. Die Risswiderstandskurven wurden mit 1TC(T)-Proben aus einem Reaktordruckbehälterstahl mit dem Teilentlastungsverfahren von vier Prüflaboratorien gemessen und nach beiden Prüfnormen ausgewertet. Im Beitrag werden die möglichen Fehlerquellen bei der Anwendung des Teilentlastungsverfahrens und die Unterschiede bei der Auswertung nach beiden T2 - 45. Tagung des DVM-Arbeitskreises Bruchvorgänge CY - Berlin, Germany DA - 19.02.2013 KW - Duktiles Risswachstum KW - J-Integral KW - Teilentlastungsverfahren KW - Bruchzähigkeit KW - Ductile tearing KW - J integral KW - Unloading compliance KW - Fracture toughness KW - Bruchmechanik KW - Round Robin KW - Risswiderstandskurve PY - 2013 N1 - Serientitel: DVM-Bericht – Series title: DVM-Bericht VL - 245 SP - 91 EP - 100 AN - OPUS4-27912 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Baensch, Franziska A1 - Baer, Wolfram A1 - Chruscicki, Sebastian A1 - Habib, Abdel Karim A1 - Homann, Tobias A1 - Hussels, Maria-Teresa A1 - Prager, Jens A1 - Schmidt, Dirk A1 - Stajanca, Pavol A1 - Weltschev, Margit A1 - Wossidlo, Peter T1 - Feasibility study - Continuous monitoring of pipes using distributed acoustic and fibre optic sensors N2 - The feasibility study „AGIFAMOR. Ageing infrastructures – distributed acoustic monitoring of pipes” is an interdisciplinary research project at BAM internally financed from 2015 to 2018. Therefore, the quite young fibre optic sensing technology of distributed acoustic sensing (DAS) was investigated to possibly be extended towards a global condition monitoring system for pipelines operating in real time. DAS is a highly dynamic fibre optic sensing technology based on the method of coherent optical time domain reflectometry (C-OTDR). DAS allows capturing strain changes in the range of kHz. For the experimental work, the most suitable application yielding an optimum sensitivity was proven by wrapping a standard single-mode silica fibre around the pipe. The DAS sensitivity was investigated regarding the detection of 1) incidents that initiate propagation of acoustic waves in the pipe wall, 2) changes inside the pipeline causing altered flow and 3) damage development in the pipe wall. Therefore, several testing setups in laboratory as well as in real scale were realized. For comparison purposes, experiments were accompanied by acoustic emission analyses and by measurements with accelerometers. DAS was found to be very sensitive to gas ignition and its propagation across the pipe. Furthermore, the ability of DAS to detect and localize acoustic signals associated with pipeline leakage was demonstrated. The detection of crack formation and propagation within the pipe wall by means of DAS was studied during bending tests on several pipe segments, but was not proven so far with certainty. As expected, these studies turned out as the most difficult challenge due to the random occurrence and transient nature of microscopic damage phenomena. T2 - Proceedings of the International Symposium on Structural Health Monitoring and Nondestructive Testing CY - Saarbrücken, Germany DA - 04.10.2018 KW - Accelerometers KW - Acoustic emission KW - Fibre optic acoustic sensing KW - Continous monitoring KW - Bending tests on pipe segments KW - Leak detection PY - 2018 SP - Paper 21 AN - OPUS4-46375 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Baer, Wolfram ED - Yu, S. ED - Feng, X.-Q. T1 - Experimental requirements of small and large scale dynamic fracture mechanics testing N2 - The paper deals with experimental requirements of dynamic fracture mechanics tests in general with special focus on ductile cast iron materials. This is based on instructions for dynamic measurement techniques provided by the standards ASTM E 1820 and BS 7448-3 which were compared and rated. The low blow multiple specimen technique using a drop tower was investigated for crack resistance curve determination on SE(B)25x25 specimens. It was shown that no detrimental effects should be expected from the second impact of the rebounded striker. Strain gage instrumentations for direct force measurement according to the standards provided different results. The ASTM position should be preferred. Important conclusions were drawn concerning hidden friction in drop towers from a comparison of electro-optically measured displacement and calculations from force-time record. Full blow large scale tests on SE(B)140x280 specimens were performed using a servo-hydraulic test system to determine dynamic fracture toughness values. Different strain gage instrumentations were compared with respect to their force measurement capability. For displacement measurement only a non-contact electro� optical camera technique was applicable. An appropriate method of instrumentation was identified whose results show good agreement with numerical simulations of the tests. It can be concluded that the recommendations of the test standards provide different results. Therefore, they must not simply be transferred to the own specific test requirements. It is regarded absolutely essential for dynamic fracture mechanics tests in general that all measuring techniques are being validated in advance. T2 - ICF13 - 13th International conference on fracture CY - Beijing, China DA - 16.06.2013 KW - Dynamic fracture mechanics testing KW - Ductile cast iron KW - Measurement PY - 2013 SN - 978-988-12265-2-5 SP - 1 EP - 10 AN - OPUS4-28738 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Stajanca, Pavol A1 - Baensch, Franziska A1 - Baer, Wolfram A1 - Chruscicki, Sebastian A1 - Homann, Tobias A1 - Seifert, Stefan A1 - Schmidt, Dirk A1 - Weltschev, Margit A1 - Wossidlo, Peter A1 - Habib, Abdel Karim T1 - Monitoring of pipes by distributed acoustic fibre optic sensors – A large-scale test on a pipeline under realistic operation condition N2 - The monitoring of oil and gas pipelines by means of distributed fibre optic sensors is becoming common. The most recent development in the field of fibre optic sensing is the distributed acoustic sensing (DAS), which allows to detect and to localize third party threats to pipelines. For this purpose, fibre optic telecommunication cables located close to the pipelines are usually used. However, DAS carries a far greater potential for continuous condition monitoring of pipelines. The interdisciplinary research project AGIFAMOR (Ageing Infrastructures – Fibre Optic Monitoring of Pipes) at BAM investigates a new technical approach to extend the application field of DAS towards the detection and localization of acoustic signals that indicate critical alterations and certain damage scenarios originated from within the pipeline or the pipe wall. Therefore, the optical fibre sensors are applied onto the pipe itself and the application procedure towards an optimal acoustic signal transduction is optimized. A number of laboratory scale experiments were performed focusing on the signal transmission of acoustic signals as well as the detection of damages in the pipe wall by means of DAS. Furthermore, real-scale tests on a pipeline DN100 of 38m length have been carried out at the BAM test site for technical safety (BAM-TTS) to study the detection and localization of leaks and of changing flow profiles due to corrosion or sedimentation processes. T2 - 13th Pipeline Technology Conference CY - Berlin, Germany DA - 12.03.2018 KW - Pipeline monitoring KW - Distributed acoustic sensing KW - Fiber optic sensing PY - 2018 SN - 2198-428X SP - Poster session, paper 9, 1 EP - 8 PB - EITEP (Euro Institute for Information and Technology Transfer in Environmental Protection) CY - Hannover AN - OPUS4-44519 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Holzwarth, Marcel A1 - Baer, Wolfram A1 - Mayer, Uwe A1 - Weihe, Stephan T1 - Investigation of the Master Curve Concept for Ferritic Ductile Cast Iron N2 - Within fracture mechanics safety assessment for steels in nuclear technology, the probabilistic master curve (MC) concept according to ASTM E1921 is currently used for quasi-static loading conditions as a supplement to the established deterministic ASME reference curve concept. However, for ductile cast iron (DCI), a systematic review of potential modifications to the assumptions and the procedure according to ASTM E1921 and an associated validation are still lacking. For this reason, the application of the fracture mechanics MC concept to ferritic ductile cast iron is being investigated in a recently started joint research project between MPA Stuttgart and BAM Berlin. According to the IAEA guidelines SSG 26, the safety assessment of DCI containers for transport as well as storage of radioactive materials is based on the fracture mechanics criterion of general crack initiation exclusion. Within this context, the focus of the current research project is on the further development of brittle fracture safety assessment methods. Therefore, a methodology shall be established to determine and assess dynamic fracture toughness values of DCI in the ductile-to-brittle transition regime, using samples extracted from a component. For the experimental program, a DCI material will be produced as it is generally used for transport and storage containers. A basic mechanical-technological material characterization consisting of tensile, Charpy and Pellini tests is planned and a comprehensive fracture mechanics test program was compiled covering dynamic testing of DC(T)9, C(T)25, C(T)50, SE(B)10, SE(B)25, and SE(B)140 specimens. Numerical analyses of different specimen geometries and test setups are planned to investigate the influences of stress triaxiality and loading rate. Throughout the experimental program, the microstructure-property relationship will be investigated based on quantitative metallographic and fractographic analyses. Finally, different MC assessment strategies will be considered and modifications will be made if necessary. T2 - 21st International Symposium ASTM/ESIS Symposium on Fatigue and Fracture Mechanics CY - Washington, DC, USA DA - 08.11.2023 KW - Ductile Cast Iron KW - Dynamic Fracture Toughness KW - Cleavage Fracture KW - Master Curve Concept PY - 2023 SP - 1 EP - 5 PB - ASTM International CY - West Conshohocken, PA AN - OPUS4-59064 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Holzwarth, Marcel A1 - Baer, Wolfram A1 - Mayer, Uwe A1 - Weihe, Stefan T1 - Master Curve-Auswertungen und Untersuchung des Größeneffekts für c(t)-proben - Aktuelle Erkenntnisse zur Untersuchung des Master Curve Konzepts für ferritisches Gusseisen mit Kugelgraphit bei dynamischer Beanspruchung N2 - Ausgehend vom Stand des Regelwerkes und der Forschung wird in einem BMUV-Verbundprojekt zwischen der MPA Stuttgart und der BAM Berlin die Anwendung des Master Curve (MC)-Konzepts auf ferritisches Gusseisen mit Kugelgraphit (DCI) untersucht. Ziel des Verbundprojekts ist die Anwendbarkeit des MC-Konzepts näher zu untersuchen und ggf. Modifikationen vorzunehmen, um eine Bewertungsmethode für die dynamische Bruchzähigkeit von DCI im Übergangsbereich zu erarbeiten. Auf den Jahrestagungen 2023 und 2024 des DVM-AK Bruchmechanik und Bauteilsicherheit wurden bereits der Forschungsansatz sowie erste Ergebnisse des Projekts MCGUSS präsentiert. Der Beitrag für die diesjährige Tagung soll nun MC-Auswertungen und den Größeneffekt für C(T)-Proben aus DCI diskutieren. T2 - 57. Tagung des DVM-Arbeitskreises Bruchmechanik und Bauteilsicherheit CY - Köln, Germany DA - 18.02.2025 KW - Versuche KW - Master Curve KW - Bruchmechanik KW - Dynamische Beanspruchung KW - Gusseisen mit Kugelgraphit PY - 2025 DO - https://doi.org/10.48447/BR-2025-495 SP - 123 EP - 129 PB - DVM-Verlag CY - Berlin AN - OPUS4-62555 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Holzwarth, Marcel A1 - Mayer, Uwe A1 - Baer, Wolfram T1 - Investigating the Applicability of the Master Curve Concept for Ductile Cast Iron – Early Results for 2 Different Test Temperatures N2 - Based on the state-of-the-art research and regulations, the application of the fracture mechanics master curve (MC) concept to ferritic ductile cast iron (DCI) is being investigated in a joint research project between MPA Stuttgart and BAM Berlin. This paper outlines the research approach, the planned investigations and first results of the experimental program. T2 - 8th SEDS Workshop: Safety of Extended Dry Storage CY - Garching, Germany DA - 15.05.2024 KW - Dynamic fracture KW - Brittle fracture KW - Ductile cast iron KW - Master Curve PY - 2024 SP - 1 EP - 4 AN - OPUS4-60013 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schneider, Ronald A1 - Rogge, Andreas A1 - Thöns, S. A1 - Bismut, E. A1 - Straub, D. ED - Caspeele, Robby ED - Taerwe, Luc ED - Frangopol, Dan M. T1 - A sampling-based approach to identifying optimal inspection and repair strategies for offshore jacket structures N2 - Identifying optimal inspection and repair strategies for offshore jacket structures is a challenging task. We pre-sent an approach, which is based on recent developments in the field of risk-based operation and maintenance planning at the structural system level. The approach utilizes heuristics to define inspection and repair strate-gies at the system level and to reduce the search space of possible strategies. For each defined strategy, the expected service life cost of inspection, repair and failure is evaluated based on simulated inspection and re-pair histories. Subset simulation is applied to compute the conditional repair and failure probabilities required for this analysis. It also forms the basis for simulating inspection and repair histories. The strategy that mini-mizes the expected service life cost is the optimal one in the set of pre-selected strategies. The underlying condition and performance model accounts for the stochastic dependence among the deterioration states of the different structural elements and the structural redundancy. The approach is demonstrated in a case study considering a jacket-type frame. In this study, we essentially vary the inspection interval, the minimum num-ber of inspected components and the target reliability, and identify the combination that minimizes the ex-pected total service life cost. T2 - The sixth international symposium on life-cycle civil engineering (IALCCE 2018) CY - Ghent, Belgien DA - 28.10.2018 KW - Offshore steel structures KW - Fatigue KW - Reliability KW - Risk KW - Inspection planning PY - 2019 SN - 978-1-138-62633-1 SN - 978-1-315-22891-4 SP - 1081 EP - 1088 PB - Taylor & Francis Group CY - London AN - OPUS4-46434 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Völzke, Holger T1 - Stand bei den Behälterbauartprüfungen für das Endlager Konrad N2 - Die Verfügbarkeit von Behältern für die Entsorgung nicht Wärme entwickelnder radioaktiver Abfälle im Endlager Konrad stellt ein wesentliches Element des nationalen Entsorgungskonzeptes für diese Abfallart dar. Grundlage für die Verfügbarkeit geeigneter Behälter sind typspezifische Bauartprüfungen, auf deren Grundlage eine Eignungs-feststellung in Form eines Prüfzeugnisses durch die Bundesgesellschaft für Endlagerung mbH (BGE), vormals Bundesamt für Strahlenschutz (BfS), erfolgt. Die Prüfgrundlagen sind in den durch das BfS (heute BGE) veröffent-lichten „Anforderungen an endzulagernde radioaktive Abfälle“ (Endlagerungsbedingungen) sowie der zugehörigen „Produktkontrolle radioaktiver Abfälle, radiologische Aspekte“ (PK) verankert. Die Eignungsfeststellung für eine Be-hälterbauart ist gleichzeitig die Grundlage für eine Behälterserienfertigung entsprechend den im Prüfzeugnis veran-kerten Spezifikationen und Randbedingungen. Mit den Gesetzen zur Neuordnung der Organisationsstruktur im Bereich der Endlagerung (Mitte 2016) und zur Neuordnung der Verantwortung in der kerntechnischen Entsorgung (Mitte 2017) mit der Finanzierung des Kern-energieausstiegs wurden wesentliche Weichenstellungen im Hinblick auf den anstehenden Rückbau der bereits stillgelegten und in den kommenden Jahren noch stillzulegenden deutschen Kernkraftwerke vorgenommen. Bezüg-lich der nicht Wärme entwickelnden radioaktiven Abfälle führt dies zu einer spürbaren Intensivierung der Anstren-gungen zur Bereitstellung qualifizierter Gebinde für das Endlager Konrad, das nach aktueller Planung bis 2027 sei-nen Einlagerungsbetrieb aufnehmen soll. Dies wiederum führt zu einer erheblichen Verdichtung der Verfahren zur Behälterbauartprüfung, die allen Seiten (Antragsteller, BGE, Gutachter) erhebliche Anstrengungen abfordert. Die Bundesanstalt für Materialprüfung und –forschung (BAM) ist auf Grundlage des Kap. 7 der o. g. „Produktkon-trolle …“ (PK) von der BGE mit den Behälterbauartprüfungen für das Endlager Konrad beauftragt. Hierbei ist eine Vielzahl von Anforderungen zu berücksichtigen, wozu neben den Anforderungen an Abfallbehälter gemäß Kap. 5 der Endlagerungsbedingungen weitere Anforderungen an die Verpackung (Kap. 3.2.2 PK), Kenngrößen (Kap. 3.5.1 PK) und schließlich die eigentliche Prüfung von Behältern/Verpackungen zählt (Kap. 7 PK). Letzteres beinhaltet die umfassende Behälterbeschreibung und –spezifikation, die Behälterauslegung, die thermischen und mechanischen Baumusterprüfungen (z.B. Brand- und Fallprüfungen), und schließlich die qualitätssichernden Maßnahmen für Her-stellung und Betrieb der Behälter. Neben der klassischen Bauartprüfung neuer Behältertypen spielt auch die Prü-fung bereits hergestellter Behälter, sog. Altbehälter, eine wesentliche Rolle, da sich etliche tausend Gebinde bereits in der Zwischenlagerung befinden und nach Möglichkeit für das Endlager Konrad qualifiziert werden sollen. Dieser Beitrag berichtet aktuell über den Umfang und Stand der laufenden Bauartprüfungen bei der BAM unter Be-rücksichtigung der besonderen Herausforderungen und der zuletzt erzielten Fortschritte. Dabei erfordert die paral-lele Bearbeitung der zahlreichen Verfahren einen verstärkten Koordinierungsbedarf hinsichtlich vergleichbarer fach-licher Aspekte sowie hinsichtlich Priorisierung und Ressourceneinsatz. Bei den experimentellen Nachweisen (Fall- und Brandversuche) betrifft das hinsichtlich der Nutzung der Versuchseinrichtungen bei der BAM die Koordination mit anderen Prüfaufträgen, wie z. B. verkehrsrechtliche Baumusterprüfungen. Schließlich erfordern diverse Fach-fragen zur Interpretation der Anforderungen aus Endlagerungsbedingungen und Produktkontrolle intensive Abstim-mungsprozesse zwischen BAM, BGE und Antragstellern. Wichtige Ergebnisse mit übergeordneter Bedeutung wer-den in Form erläuternder Fachnotizen durch die BGE veröffentlicht und können so bei zukünftigen Antragsverfahren berücksichtigt werden. T2 - KONTEC 2019 CY - Dresden, Germany DA - 27.03.2019 KW - Endlager KW - Container KW - Bauartprüfung KW - Konrad PY - 2019 SP - Paper 017, 205 EP - 212 PB - Kontec GmbH CY - Hamburg AN - OPUS4-47667 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kullolli, Borana A1 - Baeßler, Matthias A1 - Cuéllar, Pablo A1 - Rica, S. A1 - Rackwitz, F. T1 - An enhanced interface model for friction fatigue problems of axially loaded piles N2 - The shaft bearing capacity often plays a dominant role for the overall structural behaviour of axially loaded piles in offshore deep foundations. Under cyclic loading, a narrow zone of soil at the pile-soil interface is subject to cyclic shearing solicitations. Thereby, the soil may densify and lead to a decrease of confining stress around the pile due to microphenomena such as particle crushing, migration and rearrangement. This reduction of radial stress has a direct impact on the shaft capacity, potentially leading in extreme cases to pile failure. An adequate interface model is needed in order to model this behaviour numerically. Different authors have proposed models that take typical Interface phenomena in account such as densification, grain breakage, normal pressure effect and roughness. However, as the models become more complex, a great number of material parameters need to be defined and calibrated. This paper proposes the adoption and transformation of an existing soil bulk model (Pastor- Zienkiewicz) into an interface model. To calibrate the new interface model, the results of an experimental campaign with the ring shear device under cyclic loading conditions are here presented. The constitutive model shows a good capability to reproduce typical features of sand behaviour such as cyclic compaction and dilatancy, which in saturated partially-drained conditions may lead to liquefaction and cyclic mobility phenomena. T2 - Conference: OMAE CY - Glasgow, Scotland, UK DA - 09.06.2019 KW - Soil-structure interaction KW - Interface PY - 2019 VL - 2019 SP - Article Number: UNSP V001T10A013 PB - ASME CY - Glasgow, Scotland AN - OPUS4-48444 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Geißler, Peter A1 - Schwarz, Johannes A1 - Cuéllar, Pablo A1 - Hüsken, Götz A1 - Baeßler, Matthias A1 - Kühne, Hans-Carsten A1 - Morrone, C. T1 - Compaction grouting to improve the pile bearing capacity in non-cohesive soil N2 - The aim of an ongoing research project is to develop a design approach for typical offshore driven piles (e.g. Jacket piles) based on the application of injections by compaction grouting directly at the pile shaft. The paper aims to present the results of laboratory and in-situ tests, which reveal the efficiency and the promising potential of the optimised foundation concept for a more economic dimensioning of pile foundations and to increase their bearing capacity in non-cohesive soil at any moment after installation. T2 - Twenty-ninth International Ocean and Polar Engineering Conference CY - Honolulu, HI, USA DA - 16.06.2019 KW - Offshore Pile Foundation KW - Compaction Grouting KW - Grout KW - Injection Sequence KW - Tensile Capacity PY - 2019 SN - 978-1-880653-85-2 SN - 1098-6189 VL - II SP - 2178 EP - 2184 PB - International Society of Offshore and Polar Engineers (ISOPE) CY - Cupertino, California, USA AN - OPUS4-48505 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schönfelder, Thorsten A1 - Müller, Lars A1 - Komann, Steffen A1 - Wille, Frank ED - Schönfelder, Thorsten T1 - Design assessment of a dual purpose cask for damaged spent nuclear fuel N2 - German package design approvals were granted recently for dual purpose casks (DPC) intended for loading with encapsulated damaged spent nuclear fuel (DSNF). Comprehensive assessment procedures were carried out by the authority BAM with respect to the mechanical and thermal package design, the activity release of radioactive material and quality assurance aspects for manufacturing and operation of each packaging. The objective of each procedure was to verify the Package Design Safety Report (PDSR) and the relevant guidelines fulfils the requirements of the IAEA regulations. Previous approvals of German SNF package designs consider mainly standard fuel assemblies with defined specifications and properties for transport and interim storage. Due to the nuclear power phase-out in Germany all kinds of SNF, e.g. damaged spent fuel rods shall be packed in DPC now. Therefore specific requirements shall be considered in accordance with international experiences including IAEA technical reports. The main requirement for DSNF is a tight encapsulation with specific defined properties under transport and storage conditions. Due to the interim storage period of currently up to 40 years the encapsulation with DSNF in the casks shall also be long term durable. Thus specific loading and drying procedures are necessary and had to be qualified during the approval process. BAM assessed these drying procedures and could confirm the long-term behaviour of the encapsulation and the suitability of the drying equipment. This special equipment was qualified in a “cold handling”. In addition, it was shown that the behaviour of the test equipment used in the qualification process was comparable with the original equipment, e.g. test fuel rods or test encapsulation. In the development of the drying process, experience was obtained in how to put the requirements of the IAEA regulations and related IAEA technical reports into practice. The paper gives an overview of approval assessment and testing experience made by BAM and point out the main resulting requirements on drying processes for these kinds of encapsulations with DSNF. T2 - Proceedings of the 19th International Symposium on the Packaging and Transportation of Radioactive Materials PATRAM 2019 CY - New Orleans, USA DA - 04.08.2019 KW - Assessment KW - Dual purpose cask KW - Spent nuclear fuel PY - 2019 SP - Paper 1204, 1 EP - 10 AN - OPUS4-48685 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Linnemann, Konrad A1 - Müller, Lars A1 - Schönfelder, Thorsten A1 - Komann, Steffen A1 - Wille, Frank T1 - Authority Experience during Design Approval Procedure for Packages Loaded with Special Encapsulations for Damaged Spent Nuclear Fuel N2 - The first German package design approval certificate for a dual purpose cask intended for loading with damaged spent nuclear fuel was issued recently. BAM as part of the competent authority system in Germany carried out a comprehensive assessment procedure with respect to the mechanical and thermal design, the release of radioactive material and the quality assurance aspects of manufacturing and operation. Packages for the transport and storage of radioactive material have been assessed by BAM for many years, thus the common assessment procedure is well-known and good practice. Up to now only SNF without defects or HLW with well-defined properties were designated for long-term Interim storage and transports afterwards. Due to Germany’s nuclear phase out all other kinds of spent nuclear fuel in particular damaged spent nuclear fuel shall be packed as well. Damaged spent nuclear fuel needs a tight closure with Special encapsulations and clearly defined properties in Germany. In addition, these encapsulations shall be long-term durable, because they are not accessible after loading in a packaging within periodical inspections. The main difference to Standard package components is that encapsulations with a permanent closure achieve their specified conditions not after manufacturing but only during operation, after loading and closing. To ensure compliance with the specific conditions, special measures for quality assurance are necessary during operation of each encapsulation, e.g. drying and sealing, which were assessed by BAM. The present paper gives an overview of the conducted assessment from BAM and point out the findings concerning to the special closure lid of the approved encapsulation, which is screwed and welded. A wide verification concept is necessary to show the specific tightness under transport conditions. Together with quality assurance measures during first operation steps these encapsulations with damaged spent nuclear fuel can be handled like standard fuel assemblies in approved package designs. T2 - International Conference on the Management of Spent Fuel from Nuclear Power Reactors CY - Vienna, Austria DA - 24.06.2019 KW - Transport package KW - Design approval KW - Spent nuclear fuel KW - Special encapsulation PY - 2019 SP - 1 EP - 9 AN - OPUS4-48749 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Feldkamp, Martin A1 - Quercetti, Thomas A1 - Wille, Frank T1 - Fire reference test for IAEA package thermal testing in a propane gas fire test facility N2 - Packages for the transport of radioactive material shall withstand severe accidents. Therefore, the IAEA Regulations define different test scenarios to cover severe hypothetical accident conditions. One of these tests defined in detail is the thermal test, mainly consisting of a 30 minute fully engulfing 800 °C pool fire or an equally severe fire test. The heat fluxes into the package are of significant importance and depend substantially on the fire characteristics and the surface temperature of the package. In order to investigate the heat fluxes over a wide range of surface temperatures during a propane gas fire test and to get information about local fire impact a fire reference package, representing the outer geometry of a specific type of transport cask for radioactive waste, was designed. A closed steel sheet cylinder with a wall thickness of 10 mm was chosen as fire reference package. The cylinder was filled with refractory insulation material and instrumented with thermocouples distributed all over the cylinder. The local steel sheet temperatures measured allow the determination of local as well as global heat fluxes as a function of time and surface temperature. With this fire reference package three open-air propane gas fire tests were performed at BAM’s open air fire test stand. The flame exposure time period was changed for the different fire tests. Furthermore, the wind conditions changed between and during the tests. Test stand parameters like wind shield location and propane gas volume flow were chosen constant for the three tests. The test results were used to determine the changes of heat flux into the fire reference package in relation to the package surface temperature. This data also allows the calculation of local characteristics of the propane gas fire as there are the flame temperature, the fire convection coefficient and the radiation exchange coefficient in a first approach. The recently conducted tests provide an initial picture of local fire characteristics of the propane gas fire test facility. The test shows that the propane gas fire covers the IAEA-fire over a wide range of surface temperatures with the chosen test stand parameters. T2 - 19th International Symposium on the Packaging and Transportation of Radioactive Materials PATRAM 2019 CY - New Orleans, LA, USA DA - 04.08.2019 KW - Fire test KW - Propane gas KW - Calorimetric test KW - IAEA fire testing PY - 2019 SP - Paper 1141, 1 EP - 10 AN - OPUS4-48840 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zencker, Uwe A1 - Simbruner, Kai A1 - Völzke, Holger T1 - Brittle failure of spent fuel claddings under long-term dry interim storage conditions – Preliminary analysis N2 - The evaluation of cladding integrity is a major issue to be demonstrated in Germany for extended interim storage periods up to 100 years and subsequent transportation considering operational and accidental conditions with respect to reactor operation, cask drying and dry interim storage. The chemical reaction between the zirconium fuel cladding and the cooling water in water-cooled reactors produces hydrogen and zirconium oxide. Hydrogen diffuses into the cladding and precipitates as zirconium hydrides when the solubility limit is reached, preferably oriented in hoop direction. At high temperatures during vacuum drying procedures, the hydrides can dissolve. Over a succeeding period of slow cooling with existing hoop stress the hydrides precipitate again, but partly reoriented along the radial direction of the cladding. This change of microstructure in combination with a decreasing temperature (0.5...2 K/year) during (extended) interim storage and additional mechanical load by handling procedures or under accident conditions could lead to a potential cladding embrittlement and consequently increased failure probability. The current research project BRUZL (Fracture mechanical analysis of spent fuel claddings under long-term dry interim storage conditions) has been launched by BAM to investigate potential sudden brittle failure of spent fuel claddings at small deformation under long-term dry interim storage conditions and is presented. T2 - IAEA International Conference on the Management of Spent Fuel from Nuclear Power Reactors CY - Vienna, Austria DA - 24.06.2019 KW - Ageing Management KW - Cladding Embrittlement KW - Extended Storage KW - Ring Compression Test KW - Spent Nuclear Fuel PY - 2019 SP - Paper IAEA-CN-272/49, 1 EP - 8 AN - OPUS4-48869 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Palkowski, Carsten A1 - von Schwarzenberg, Stefan A1 - Simo, Anne T1 - Dynamic testing to better reflect real use for the seasonal performance of air conditioners N2 - In this contribution, a dynamic test method to determine the seasonal performance of invertertype air conditioners has been developed and verified. In comparison to current test standards, where test modes for fixing the compressor speed are required, a dynamic approach is applied with unfixed compressor speed and thus better reflects the performance of air conditioners under real operating conditions. The dynamic tests are conducted in two calorimeter chambers. The indoor chamber is kept at a constant temperature whereas the outdoor chamber is subjected to a temperature profile based on the climate BIN-distribution, representing the reference cooling demand. The proposed dynamic test considers the dynamic control of an air conditioner and delivers results which could indicate the units' performance in the field. T2 - 25th International Congress of Refrigeration 2019 CY - Montréal, Canada DA - 25.09.2019 KW - Seasonal Performance Factor KW - Inverter-type Air Conditioner KW - Dynamic Test Method KW - Real Use Behavior PY - 2019 SN - 978-2-36215-035-7 SN - 1025-9031 SP - 672, 3891 EP - 3899 PB - International Institute of Refrigeration IIR CY - Paris AN - OPUS4-48865 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zencker, Uwe A1 - Qiao, Linan A1 - Völzke, Holger T1 - Fracture mechanical analysis of a cylindrical cast iron cask N2 - The safety evaluation of cask components made of ductile cast iron includes investigations to prevent brittle fracture. Generally, ductile cast iron is endangered by brittle fracture especially at low temperatures (down to -40°C) and in combination with existing crack-like material defects. An applicable method is the assessment of fracture resistance using fracture mechanics according to the IAEA guidelines. The approach is based on the prevention of fracture initiation. For application of these principles for drop loads, account must be taken both of dynamic stresses within the component and dynamic material behavior. Basically, the dynamic stress intensity factor of postulated pre-existing crack-like defects is compared with the dynamic fracture toughness of the material. Applicable numerical and experimental methods for the safety assessment of cask components are demonstrated for the case of an artificially pre-cracked cylindrical cast iron cask which undergoes dynamic loading conditions as result of the hard impact between the cask and a concrete target. The proposed evaluation procedure is a combination of numerical and experimental steps. Exemplarily, the calculated stress intensity factor is compared with measured fracture toughness values from single edge notched bending specimens. T2 - 19th International Symposium on the Packaging and Transportation of Radioactive Materials (PATRAM 2019) CY - New Orleans, LA, USA DA - 04.08.2019 KW - Ductile Cast Iron KW - Brittle Fracture KW - Cylindrical Cask PY - 2019 SP - Paper 1209, 1 EP - 7 AN - OPUS4-48914 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Johann, Sergej A1 - Kohlhoff, Harald A1 - Gawlitza, Kornelia A1 - Bell, Jérémy A1 - Mansurova, Maria A1 - Tiebe, Carlo A1 - Bartholmai, Matthias T1 - Semi-automatic Gas Measurement Device Based on Fluorescent Multi-gas Sensors N2 - This paper describes the development of a semi-automatic gas measurement device presenting potentially a broad range of applications, noteworthy in the agricultural sector. Non-reversible fluorescent molecular sensors were designed and syn-thesized. Upon, integration into a hydrogel matrix with an optimal ratio of co-solvents, the sensors reacting selectively to ammonia were illuminated by excitation light to produce a concentration-correlated fluorescence emission. An automated mechanical-elec-trical device initiates a given gas mixture and thus simulates con-centrations similar to a threshold value. The aim of this project is to develop a sensor or a low-cost method which can monitor low concentrations of harmful gases and aid in their elimination or regulation in livestock housing, barns or stables. T2 - IEEE Sensors 2019 CY - Montreal, Canada DA - 27.10.2019 KW - gas analysis KW - fluorescence KW - embedded sensor KW - spectroscopy KW - environment KW - agricultural economy PY - 2019 SN - 978-1-7281-1634-1 SP - 88 EP - 92 PB - IEEE AN - OPUS4-49506 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hüllmann, Dino A1 - Neumann, Patrick P. A1 - Scheuschner, Nils A1 - Bartholmai, Matthias A1 - Lilienthal, A.J. T1 - Experimental Validation of the Cone-Shaped Remote Gas Sensor Model N2 - Remote gas sensors mounted on mobile robots enable the mapping of gas distributions in large or hardly accessible areas. A challenging task, however, is the generation of threedimensional distribution maps from these gas measurements. Suitable reconstruction algorithms can be adapted, for instance, from the field of computed tomography (CT), but both their performance and strategies for selecting optimal measuring poses must be evaluated. For this purpose simulations are used, since, in contrast to field tests, they allow repeatable conditions. Although several simulation tools exist, they lack realistic models of remote gas sensors. Recently, we introduced a model for a Tunable Diode Laser Absorption Spectroscopy (TDLAS) gas sensor taking into account the conical shape of its laser beam. However, the novel model has not yet been validated with experiments. In this paper, we compare our model with a real sensor device and show that the assumptions made hold. T2 - IEEE Sensors 2019 CY - Montreal, Canada DA - 27.10.2019 KW - Remote gas sensor model KW - TDLAS KW - Gas dispersion simulation PY - 2019 SN - 978-1-7281-1634-1 SP - 104 EP - 107 PB - IEEE AN - OPUS4-49548 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Brandt, S. A1 - Müller, B. A1 - de Lima Vasconcelos, S. A1 - Plehn, W. A1 - Brozowski, F. A1 - Horn, Wolfgang A1 - Sattler, M. T1 - Präzisierung der Geruchsprüfung für Bauprodukte nach DIN ISO 16000-28 – Untersuchung von Vergleichsmaßstäben N2 - Bauprodukte, die in Innenräumen verwendet werden, sollten die Gesundheit und das Wohlbefinden der Personen die sich darin aufhalten nicht durch das Ausdünsten von Geruchsstoffen stören. Die DIN ISO 16000-28 „Bestimmung der Geruchsstoffemissionen aus Bauprodukten mit einer Emissionsprüfkammer“ (DIN ISO 16000-28) beschreibt umfassend die Möglichkeiten der Geruchsprüfung. In Verbindung mit der Anwendung der VDI-Richtlinie 4302 Blatt 1 „Geruchsprüfung von Innenraumluft und Emissionen aus Innenraummaterialien“ (VDI 4302 Blatt 1) ist sie zur Bewertung der empfundenen Intensität von Bauprodukten mit Vergleichsmaßstab geeignet (Umweltbundesamt 2015). In einem vom Umweltbundesamt (UBA) geförderten Forschungsprojekt der Hochschule für Technik und Wirtschaft Berlin (HTW Berlin) und der Bundesanstalt für Materialforschung und –prüfung (BAM) wurden erstmals verschiedene Vergleichsmaßstäbe miteinander verglichen. Ziel des derzeitigen Folgeprojektes ist nun, Mindestanforderungen an Vergleichsmaßstäbe zu erarbeiten, welche die Reproduzierbarkeit der Ergebnisse erhöhen und mit denen die Norm konkretisiert werden kann. Dieser Beitrag stellt die Untersuchungen und Ergebnisse des ersten Projektes und die Schlussfolgerungen für die Durchführung des zweiten Projektes dar. T2 - 12. Fachkongress der Arbeitsgemeinschaft ökologischer Forschungsinstiute (AGÖF) CY - Hallstadt (Bamberg), Germany DA - 17.10.2019 KW - Geruch KW - Emission KW - Bauprodukte KW - VOC KW - Emissionskammer PY - 2019 SN - 978-3-930576-11-1 VL - 12. Fachkongress SP - 214 EP - 223 PB - Arbeitsgemeinschaft ökologischer Forschungsinstiute (AGÖF) e. V. CY - Springe-Eldagsen AN - OPUS4-49702 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Artinov, Antoni A1 - Bakir, Nasim A1 - Bachmann, Marcel A1 - Gumenyuk, Andrey A1 - Na, S.-J. A1 - Rethmeier, Michael T1 - On the search for the origin of the bulge effect in high power laser beam welding N2 - The shape of the weld pool in laser beam welding plays a major role to understand the dynamics of the melt and its solidification behavior. The aim of the present work was its experimental and numerical investigation. To visualize the geometry of the melt pool in the longitudinal section a butt joint configuration of 15 mm thick structural steel and transparent quartz glass was used. The weld pool shape was recorded by means of a high-speed video camera and two thermal imaging MWIR and VIS cameras. The observations show that the dimensions of the weld pool vary depending on the depth. The regions close to the surface form a teardrop shaped weld pool. A bulge-region and its temporal evolution were observed approximately in the middle of the depth of the weld pool. Additionally, a transient numerical simulation was performed until reaching a steady state to obtain the weld pool shape and to understand the formation mechanism of the observed bulging phenomena. A fixed keyhole with an experimentally obtained shape was used to represent the full-penetration laser beam welding process. The model considers the local temperature field, the effects of phase transition, thermo-capillary convection, natural convection and temperature-dependent material properties up to evaporation temperature. It was found that the Marangoni convection and the movement of the laser heat source are the dominant factors for the formation of the bulging-region. Good correlation between the numerically calculated and the experimentally observed weld bead shapes and the time-temperature curves on the upper and bottom surface were found. T2 - International Congress on Applications of Lasers & Electro-Optics (ICALEO®) CY - Orlando, USA DA - 14.10.2018 KW - Bulging effect KW - High power laser beam welding KW - Numerical modelling KW - Solidification cracking PY - 2019 SP - 1 EP - 8 AN - OPUS4-47139 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Theiler, Geraldine A1 - Gradt, Thomas T1 - High performance polymer materials for tribological applications in hydrogen and methane N2 - The development of hydrogen technologies is a key strategy to reduce greenhouse gas emission worldwide. Power-to-Gas is a challenging solution, in which hydrogen and methane can be used in mobility, industry, heat supply and electricity generation applications. This presentation deals with the tribological behaviour of polymer materials in hydrogen and methane, both in gas and in liquefied form. T2 - ECOTRIB 2019, MaTri'19 CY - Vienna, Austria DA - 12.06.2019 KW - Slidng wear KW - Polymer materials KW - Hydrogen KW - Methane PY - 2019 SN - 978-3-901657-60-3 SP - 228 EP - 229 AN - OPUS4-48253 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schirdewahn, S. A1 - Spranger, Felix A1 - Hilgenberg, Kai A1 - Merklein, M. ED - M., Oldenburg ED - J., Hardell ED - D., Caellas T1 - Tribological performance of localized dispersed X38CrMoV5-3 surfaces for hot stamping of Al-Si coated 22MnB5 sheets N2 - Over the last years, the weight of modern car bodies has risen significantly due to the increasing customers’ demand for comfort and safety equipment. However, this ongoing trend leads to an increasing fuel consumption and thus to higher carbon dioxide emissions. In order to counteract these problems, hot stamping has been established in the automotive industry as a key technolo-gy for lightweight construction, regarding the manufacturing of safety-relevant car body compo-nents. Hot stamped parts are commonly made out of boron-manganese steel 22MnB5, which is initially austenized and subsequently formed and quenched in one process step. As a result, geo-metrical complex structures with an ultimate tensile strength of 1500 MPa are generated. The surfaces of the workpieces are coated with an Al-Si layer to avoid oxide scale formation and to ensure corrosion protection. However, the coating system leads to an increased adhesive wear on the tool surface due to the high thermo-mechanical tool stresses. Therefore, a time and cost con-suming rework of the hot stamping tools is required. The aim of this study is to increase the tribological performance of hot stamping tools by using a laser implantation process. This tech-nique allows the ma-nufacturing of separated, elevated and dome-shaped microstructures on the tool surface in consequence of a localized dispersing of hard ceramic particles by pulsed laser radiation. The generated surface features offer great potential for reducing the tribological load, due to their high hardness and wear resistance. For this purpose, the friction coefficient of un-modified and laser implanted tool surfaces were examined and compared by using a modified pin-on-disk test. In addition, the surfaces were analyzed by optical measurements in order to quantify the amount of wear. T2 - 7th International Conference on Hot Sheet Metal Forming of High-Performance Steel CHS2-2019 CY - Lulea, Sweden DA - 02.06.2019 KW - Laser implantation KW - Surface texturing KW - X38CrMoV5-3 KW - TiB2 KW - Hot-Stamping PY - 2019 VL - 2019 SP - 357 EP - 364 AN - OPUS4-48285 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Artinov, Antoni A1 - Karkhin, V. A1 - Bakir, Nasim A1 - Meng, Xiangmeng A1 - Bachmann, Marcel A1 - Gumenyuk, Andrey A1 - Rethmeier, Michael T1 - Lamé curves approximation for the assessment of the 3-D temperature distribution in keyhole mode welding processes N2 - A novel approach for the reconstruction of an equivalent volumetric heat source from a known weld pool shape is proposed. It is based on previously obtained weld pool geometries from a steady-state thermo-fluid dynamics simulation. Hereby the weld pool dimensions are obtained under consideration of the most crucial physical phenomena, such as phase transformations, thermo-capillary convection, natural convection and temperature-dependent material properties. The algorithm provides a time and calibration efficient way for the reproduction of the weld pool shape by local Lamé curves. By adjusting their parameters, the identification of the finite elements located within the weld pool is enabled. The heat input due to the equivalent heat source is assured by replacing the detected nodes’ temperature by the melting temperature. The model offers variable parameters making it flexible and adaptable for a wide range of workpiece thicknesses and materials and allows for the investigation of transient thermal effects, e.g. the cooling stage of the workpiece. The calculation times remain acceptably short especially when compared to a fully coupled process simulation. The computational results are in good agreement with performed complete-penetration laser beam welding experiments. T2 - ICALEO 2019 - 38th International congress on applications of lasers & electro-optics CY - Orlando, FL, USA DA - 07.10.2019 KW - Weld pool shape approximation KW - Keyhole mode laser beam welding KW - Numerical simulation KW - Superelliptic Lamé curves PY - 2019 UR - http://icaleo.conferencespot.org/2019-proceedings?qr=1 SN - 978-1-940168-1-42 SP - Paper # Macro 1002 AN - OPUS4-49310 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Barthel, Maria A1 - Rübner, Katrin A1 - Kühne, Hans-Carsten T1 - Aktivierung von Papierasche zur Nutzung als Bindemittelkomponente N2 - In Deutschland fallen jährlich 20 Millionen Tonnen Altpapier an. 75 % davon werden dem Recyclingprozess zugeführt. Dabei bleiben Prozessrückstände wie Deinkingschlämme, Sortierrückstände und Faserreststoffe übrig. Zusammengefasst als Papierschlamm verwerten die Recycler diesen Reststoff thermisch in dezentralen Heizkraftwerken. Die dabei anfallende Papierasche hat mit den Anteilen der Hauptoxide von 59 M.-% CaO, 22 M.-% SiO2 und 13 M.-% Al2O3 eine ähnliche chemische Zusammensetzung wie Portlandzement, wobei sich die Mineralphasen unterscheiden. Durch eine Aktivierung der Papierasche können jedoch hydraulisch aktive Phasen wie Mayenit (C7A12) und Belit (C2S) erzeugt werden. Die Mineralphase Mayenit reagiert schnell mit Wasser zu Calciumaluminathydraten, wodurch der Bindemittelleim schnell ansteift. Die festigkeitsbildenden Calciumsilicathydrate (CSH) in Bindemittelleimen entstehen bei einer späteren Reaktion von Belit mit Wasser. Zur Aktivierung dient eine hydrothermale Calcinierung. Dabei wird Papierasche mit einer Aktivatorlösung (Wasser oder KOH) gemischt und bei 200 °C hydrothermal behandelt, wobei sich Hydratphasen ausbilden. Diese Zwischenprodukte dehydratisieren durch eine anschließende Calcinierung zu reaktiven Calciumsilicaten und Calciumaluminaten. Wie sich die Parameter des Aktivierungsprozesses auf die Mineralphasen auswirken, war Fokus der Untersuchungen. Mit thermogravimetrischen Analysen der Zwischenprodukte konnten die Reaktionsprodukte nach dem hydrothermalen Prozessschritt bestimmt werden. Den größten Einfluss auf den Mineralphasenbestand hat hierbei die Alkalität der Aktivatorlösung. Im zweiten Prozessschritt, der Calcinierung, ist die Temperatur der wesentliche Faktor für die Ausbildung reaktiver Phasen. Die Ergebnisse kalorimetrischer Untersuchungen an Leimen aus den calcinierten Proben dienten der Auswahl der optimalen Calcinierungstemperatur. Die gesamte Reaktionswärme war für die Proben, welche bei einer Calcinierungstemperatur zwischen 700-800 °C hergestellt wurden, am höchsten. T2 - GDCH-Tagung Bauchemie CY - Aachen, Germany DA - 30.09.2019 KW - Papierasche KW - Zement KW - Hydrothermale Calcinierung KW - Bindemittel PY - 2019 SN - 978-3-947197-13-2 VL - 54 SP - 16 EP - 24 CY - Aachen AN - OPUS4-49312 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mohr, Gunther A1 - Seeger, Stefan A1 - Hilgenberg, Kai T1 - Measurement of particle emissions in Laser Powder Bed Fusion (L-PBF) processes and its potential for in-situ process monitoring N2 - Laser Powder Bed Fusion (L-PBF) is a promising additive manufacturing (AM) technology for metal part production especially for complex and lightweight structures or functional designs. In L PBF processes several by-products including welding plume and its condensates, spatter and ejected powder are generated during laser exposure. Investigations of micro- and nano-sized by-products have received little attention in literature. This study focuses on the analysis of particle emissions in L PBF of 316L stainless steel using a scattered light aerosol spectrometer and a fast mobility particle sizer spectrometer during the process which allows for in-situ analysis of particle sizes in the range of 6 nm to 100 µm. A distinct correlation of emission signals to part position can be revealed. In addition, a significant influence of laser scanning vector directions on emission signals is presented. Furthermore, differing powder layer thicknesses can be recognised by deviations in emission signals. T2 - Euro PM 2019 CY - Maastricht, The Netherlands DA - 13.10.2019 KW - Plume KW - Laser Powder Bed Fusion (L-PBF) KW - Additive Manufacturing (AM) KW - Spatter KW - Fume KW - Particle gas emission KW - Aerosol measurements PY - 2019 SP - 1 EP - 7 AN - OPUS4-49388 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Werner, Tiago ED - Madia, Mauro ED - Zerbst, Uwe T1 - Experimental investigation on cyclic R-curves for additively manufactured 316L steel N2 - The present study deals with the experimental characterization of short crack propagation in SLM (selective-laser-melting) manufactured stainless steel. More specifically, the determination of cyclic R-curves is discussed. This describes the dependency of the crack propagation threshold on crack growth during the short crack propagation stage. For metals, the threshold, starting at a material-intrinsic value, increases until it reaches a value independent of the crack length due to crack closure phenomena which build up at that stage. The cyclic R-curve, when used in the frame of a cyclic R curve analysis, characterizes the resistance of a material to fatigue crack growth and the ability to arrest a physically short crack. Thus, it is the link between classical fatigue and fracture mechanics. In the high-cycle-fatigue range, the short crack propagation stage dominates the overall lifetime, i.e., the number of cycles until failure. Below the fatigue limit crack arrest of hitherto propagable micro-cracks will occur. The effort for the experimental characterization of the short fatigue crack propagation behavior and the cyclic R-curve is very high compared to experiments on long crack propagation. A very exact measurement of crack extension is required, since small increments need to be depicted. Pre-cracking must leave a closure free initial crack, since closure must be build up only by the cyclic R-curve. The closure-free status is achieved by compression pre-cracking. The aim of the present study is an insight into the influence of an AM process on the short crack propagation threshold. Cyclic R-curves are experimentally determined at different load-ratios for 316L austenitic steel specimens produced by SLM and conventional manufacturing. Residual stresses are measured in the crack plane and their influence on the cyclic R-curve is discussed. T2 - ESIAM19 CY - Trondheim, Norway DA - 09.09.2019 KW - Fatigue crack growth KW - Additive Manufacturing KW - 316L KW - Cyclic R-curve KW - Laser Powder Bed Fusion KW - AM KW - L-PBF PY - 2019 SP - 1 EP - 8 AN - OPUS4-49416 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Spranger, Felix A1 - Schirdewahn, S. A1 - Kromm, Arne A1 - Merklein, M. A1 - Hilgenberg, Kai T1 - On the influence of tib2, tic and tin hard particles on the microstructure of localized laser dispersed aisi d2 tool steel surfaces N2 - The control of friction and wear is a major concern in many industrial applications. A promising method for a tailored surface modification is the so-called laser implantation technique. This method combines surface texturing and material optimization in one processing step by a localized dispersing of hard ceramic particles using pulsed laser radiation. Wear resistant, protruding micrometric features (implants) with defined geometry can be created in deterministic pattern where needed on highly stressed surfaces, i.e. on forming or cutting tools. However, in order to maintain the implants over the tool’s lifetime, a suitable selection of hard ceramic particles is a prerequisite. They must provide a defect-free Metal Matrix Composite with a high share of homogeneously distributed particles and especially a high implant hardness. In this study TiN, TiC and TiB2 hard particles were compared as implant materials for the first time. By a systematic variation of the pulse power and pulse duration, their dispersing behavior and influence on the material properties of AISI D2 tool steel was investigated. Although all powder materials had grain sizes smaller than 10 µm, it was possible to disperse them by pulsed laser radiation and to obtain defect-free protruding implants. The highest share of dispersed particles (~64 %) was observed for TiB2. By scanning electron microscopy and energy dispersive X-ray spectroscopy, it was also shown that a significant share of the pre-placed particles was dissolved by the laser beam and precipitated as nanometer sized particles within the matrix during solidification. These in-situ formed particles have a decisive influence on the material properties. While the TiN and TiC implants have shown maximum hardness values of 750 HV1 and 850 HV1, the TiB2 implants have shown the highest hardness values with more than 1600 HV1. By X-ray diffraction, it was possible to ascribe the lower hardness values of TiC and TiN implants to high amounts of retained austenite in the metal matrix. By implanting TiB2, the formation of retained austenite was successfully suppressed due to the in-situ formation of TiC particles, which was proven by electron backscatter diffraction. In conclusion, all the implant materials are basically suitable for laser implantation on AISI D2 tool steel. However, TiB2 has shown the most promising results. T2 - 38th International Congress on Applications of Lasers & Electro-Optics CY - Orlando, FL, USA DA - 07.10.2019 KW - Laser implantation KW - Surface texturing KW - AISI D2 KW - TiB2 PY - 2019 SN - 978-1-940168-1-42 SP - 1 EP - 10 AN - OPUS4-49317 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hemmleb, M. A1 - Bettge, Dirk ED - Petzow, G. T1 - In-situ Messung der 3D-Topografie von Bruchflächen im REM N2 - Die Abbildung von Bruchflächen im Rasterelektronenmikroskop (REM) liefert hochaufgelöste Bilddaten, die für die mikrofraktografische Bewertung von Bruchmechanismen unerlässlich sind. Die Ermittlung von Bruchmechanismen ist oft ein wichtiger Teil von Schadensanalysen zur Ermittlung der Bruchursache. Durch den Abbildungsprozess im REM gehen räumliche Informationen im Normalfall größtenteils verloren und können daher nicht zur Präzisierung des Bruchmechanismus herangezogen werden. Um räumliche Informationen von Probenoberflächen im REM zu erfassen, gibt es verschiedene Methoden. Die für die Ermittlung der 3D-Topografie bereits länger eingeführten Verfahren mittels Proben- oder Strahlkippung können die Berechnung des Oberflächenmodells erst nach der seriellen Aufnahme mehrerer Bilder vornehmen. Mit der Verwendung eines segmentierten Rückstreudetektors ist dagegen die Erzeugung eines 3D-Oberflächenmodells während der Bildaufnahme praktisch in Echtzeit möglich. Die Probentopografie wird gleichzeitig mit dem Bildeinzug dargestellt und gespeichert. T2 - Metallographietagung 2019 CY - Dresden, Germany DA - 18.09.2019 KW - Fraktografie KW - Schadensanalyse KW - Topografie KW - 3D KW - REM PY - 2019 SN - 978-3-88355-417-4 VL - 2019/53 SP - 175 EP - 180 PB - DGM AN - OPUS4-49332 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Artinov, Antoni A1 - Karkhin, V. A1 - Bachmann, Marcel A1 - Rethmeier, Michael T1 - Mathematical modeling of the geometrical differences between the weld end crater and the steady-state weld pool N2 - The geometrical characteristics of the weld end crater are commonly used for the validation of numerical results in welding simulation. A semi-analytical model calculating the cooling stage of the welding process after the moving energy source is turned off has been developed. A solution for various combinations of heat sources and workpieces has been found. The theoretical limits for the heat transfer of the absorbed energy during cooling in a thin plate and a semi-infinite body were studied. It is shown that after turning off the energy source, an additional melting of the base material in longitudinal direction may occur. The developed technique is applied to complete-penetration keyhole laser beam welding of a 2 mm thick austenitic chromium-nickel 316L steel plate at a welding speed of 20 mm/s and a laser power of 2.3 kW. The results show a theoretical increase of the weld end crater length in comparison to the length of the steady-state weld pool of up to 19 %. A shift of the centre of the end crater, in which the solidification of the liquid metal ends, towards the tail of the end crater relative to the axis of the heat source at the time of its termination, was computed. The speed and the direction of crystallization of the molten material in the weld pool and the end crater were found to be different. A good agreement between the computational results and the welding experiments was achieved. T2 - ICALEO 2019 - The International Congress on Applications of Lasers & Electro-Optics (Proceedings) CY - Orlando, FL USA DA - 07.10.2019 KW - Keyhole mode welding KW - Weld pool shape KW - End-crater KW - Heat conduction PY - 2019 UR - http://icaleo.conferencespot.org/2019-proceedings?qr=1 SN - 978-1-940168-1-42 SP - 1 EP - 8 AN - OPUS4-49344 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Brunner-Schwer, C. ED - Graf, B. ED - Schreiber, F. ED - Rethmeier, Michael T1 - Highspeed-Plasma-Laser Cladding (HPLC) als hybrides Beschichtungsverfahren: Evaluierung des Einsatzpotentials für hohe Prozessgeschwindigkeiten N2 - Das Plasma-Pulver-Auftragschweißen ist ein Verfahren, dass hohe Auftragraten ermöglicht, jedoch auch eine erhöhte thermische Belastung des Bauteiles verursacht. Laser-Pulver- Auftragschweißen hingegen erreicht eine hohe Präzision und eine geringe Aufmischung, erfordert jedoch ein kostspieliges Hochleistungslasersystem und erreicht im Vergleich nur geringe Auftragraten, was zu hohen Verarbeitungskosten führt. Eine Kopplung von Laser- und Lichtbogenenergie in einer gemeinsamen Prozesszone zielt darauf ab, die jeweiligen Vorteile beider Technologien zu nutzen. Dies betrifft insbesondere die Effizienz der Wärmeausnutzung und der Nutzung des Zusatzwerkstoffs. Es wird ein Plasma-Laser-Hybrid-Prozess als Highspeed-Plasma-Laser-Cladding-Technologie (HPLC) für Beschichtungs- sowie Instandsetzungszwecke vorgestellt. Gezeigt werden Ergebnisse mit Prozessgeschwindigkeiten von 10 m/min bei Laserleistungen von 2 kW, dabei können Flächenraten von mehr als 1 m2/h erreicht werden. Effiziente Beschichtungen von großen Flächen, beispielsweise auf rotationssymmetrischen Bauteilen stellen ein relevantes Anwendungsfeld für diesen Technologieansatz dar. Die Nickelbasislegierung Inconel 625 wird als Korrosionsschutzwerkstoff eingesetzt. Im Rahmen der Verfahrensprüfung werden die hergestellten Beschichtungen einer EDX Messung unterzogen. Prozesscharakteristische Kenngrößen wie z.B. die Auftragrate werden vorgestellt und vor dem Hintergrund wirtschaftlicher Kennzahlen diskutiert. Zusätzlich werden die Aufmischung, Spurgeometrie und Wärmeeinflusszone der Spuren und Schichten ausgewertet. Im Vergleich zum Laser-Pulver-Auftragschweißen werden Spuren bei hohen Prozessgeschwindigkeiten mit einer hohen Auftragrate erzeugt. T2 - DVS Congress 2019 CY - Rostock, Germany DA - 16.09.2019 KW - Highspeed-plasma-laser-cladding KW - Korrosionsschutz KW - Laser KW - Plasma KW - Auftragschweißen PY - 2019 SP - n.b. AN - OPUS4-49364 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Voigt, Marieke A1 - von Werder, Julia A1 - Meng, Birgit ED - Caprai, V. ED - Brouwers, H. J. H. T1 - Investigation of the zonation of thermally treated ultra high performance concrete N2 - Ultra high performance concrete (UHPC) is characterised by its high compressive strength of more than 150 MPa and its high durability. Due to thermal treatment at 90°C a strength comparable to the 28-days-strength can be achieved immediately after the treatment and in some cases can be even further increased up to 30 %. The explanations for the increase in strength are the accelerated hydration of the clinker minerals and the intensified pozzolanic reaction contributing to a denser microstructure and hence, a high performance in compressive strength. Former research shows that thermal treatment can lead to inhomogeneities in form of a visible zonation within the cross-section. The width of the margin increases with shorter pre-storage time before the thermal treatment and with omitting protective measures against desiccation during the treatment. Specimens exhibiting a zonation typically show a lower compressive strength compared to the undisturbed reference whereas changes in chemistry, mineral content and microstructure were not reported in detail. In this study the zonation of thermally treated UHPC is investigated with respect to its chemistry, mineral composition and microstructure to allow predictions on durability and strength development. Measurements show a change in pore sizes, minerals phase composition and element distribution leading to the visible zonation and weaker bending tensile strength compared to the reference. T2 - 2nd International Conference of Sustainable Building Materials CY - Eindhoven, Netherlands DA - 12.08.2019 KW - UHPC KW - Thermal treatment KW - Zonation KW - Desiccation KW - Microstructure KW - Durability PY - 2019 VL - 2 SP - 185 EP - 193 AN - OPUS4-49479 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Babutzka, Martin A1 - Burkert, Andreas A1 - Heise, Svenja A1 - Heyn, A. T1 - Korrosionsuntersuchungen mit gelartigen Elektrolyten an Zink - Eine innovative Prüfmethodik N2 - Ein neuer Ansatz bei elektrochemischen Korrosionsuntersuchungen kann durch den Einsatz von gelartigen Elektrolyten als Alternative zu wässrigen Prüfelektrolyten beschritten werden. Gelartige Elektrolyte ermöglichen minimalinvasive Untersuchungen an natürlich gebildeten Zinkdeckschichten. Dadurch können korrosionsrelevante Kennwerte ermittelt werden, die Aussagen zur Deckschichtbildung und zur Stabilität von atmosphärisch gebildeten Deckschichten erlauben. In diesem Beitrag wird anhand verschiedener Untersuchungen an Reinzink der Mehrwert von gelartigen Elektrolyten für die Korrosionsforschung und -prüfung verdeutlicht. Darüber hinaus werden neue Erkenntnisse zur Deckschichtbildung von Zink unter atmosphärischen Bedingungen vorgestellt. T2 - GfKORR-Jahrestagung 2019 CY - Frankfurt a. M. DA - 12.11.2019 KW - Zink KW - Gelartige Elektrolyte KW - Korrosionsuntersuchungen KW - Deckschichtbildung PY - 2019 SN - 978-3-935406-71-0 SP - 53 EP - 64 AN - OPUS4-49642 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Weise, Frank T1 - AKR an Betonfahrbahndecken - ausgewählte Einflussgrößen und neuartige AKR-Vermeidungsstrategie N2 - In den letzten Jahren sind im deutschen Bundesautobahnnetz vermehrt Schäden an vor 2005 hergestellten Betonfahrbahndecken aufgetreten, die mit einer Alkali-Kieselsäure-Reaktion (AKR) in Verbindung gebracht werden. Vor diesem Hintergrund werden in diesem Beitrag zunächst die Voraussetzungen und ausgewählte Einflussgrößen für eine schädigende AKR aufgezeigt. Besondere Aufmerksamkeit wird dabei der Rolle des Tausalzeintrags durch den Winterdienst bei Betonfahrbahndecken geschenkt. So wird mit Löseversuchen in 1 M KOH-Lösung zweier Gesteinskörnungen bei 80 °C gezeigt, dass mit zunehmender NaCI-Zugabe die Löslichkeit von SiÖ2 zunimmt und die von AI2O3 eine Verminderung erfährt. Basierend auf dem so exemplarisch erbrachten Nachweis für die Verstärkung der schädigenden AKR durch das Tausalz wird die Notwendigkeit und Richtigkeit der Durchführung von AKR-Betonversuchen mit Alkalizufuhr im ARS 04/2013 zur zukünftigen Vermeidung von AKR-Schäden an Betonfahrbahndecken im Rahmen von Neubau- und Erneuerungsmaßnahmen im Bundesfernstraßennetz belegt. Zusätzlich durchgeführte WS-Grundprüfungen nach dem ARS 04/2013 mit den beiden Gesteinskörnungen der Löse versuche veranschaulichen, dass die nach der Alkali- Richtlinie des DAfStb als unbedenklich eingestuften Gesteinskörnungen bei den Betonversuchen mit Alkalizufuhr durchaus als alkaliempfindlich bewertet werden können. Dies wiederum führt zu einer Verminderung der für den Betonstraßenbau verfügbaren Gesteinskörnungen. Vor diesem Hintergrund wird nach neuartigen AKR-Vermeidungsstrategien gesucht, die auch eine Verwendung der als grenzwertig alkaliempfindlich eingestuften Gesteinskörnungen erlaubt. Einen möglichen Lösungsansatz stellt in diesem Kontext die Innenhydrophobierung des Fahrbahndeckenbetons dar. Es soll so durch die Behinderung des Feuchte- und Tausalzeintrags in den Beton der AKR-Schädigungsprozess signifikant vermindert werden. Für die Bewertung der Leistungsfähigkeit der Innenhydrophobierung zur Vermeidung bzw. Verminderung einer schädigenden AKR in Betonfahrbahndecken wird zurzeit im Aufträge der BASt an der BAM ein Forschungsvorhaben bearbeitet. Im Rahmen dieses Beitrags werden erste Ergebnisse dieses Projekts vorgestellt. So wird exemplarisch an einem Oberbeton (D > 8)/Unterbeton und einem Oberbeton 0/8 mit einer alkaliempfindlichen Gesteinskörnung der Einfluss zweier Hydrophobierungsmittel auf die Frisch- und Festbetoneigenschaften ganzheitlich aufgezeigt und bewertet. Bei Letzteren stehen zunächst die mechanischen und hygrischen Parameter sowie der Frost-Tausalzwiderstand im Vordergrund. In einem weiteren Schritt wird der Einfluss beider Hydrophobierungsmittel auf die schädigende AKR mittels AKR-Betonversuchen mit Alkalizufuhr beleuchtet. Dabei gelangen ergänzend zur Beurteilung des Tausalzeintrags die Laser-Induced Breakdown Spectroscopy (LIBS) und zur Bewertung der Ausprägung der AKR und sekundären Ettringitbildung (SEB) die Dünnschliffmikroskopie zum Einsatz. T2 - 9. Betonfachtagung 2019 CY - Berlin, Germany DA - 12.11.2019 KW - AKR KW - Betonfahrbahn KW - Innenhydrophobierung KW - Tausalzeintrag KW - AKR-Betonversuche PY - 2019 SN - 978-3-7640-0633-4 SP - 159 EP - 176 AN - OPUS4-50056 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schnell, A. A1 - Rübner, Katrin A1 - Ihlenfeldt, Toni A1 - Vöge, M. T1 - Leichtgranulate aus heterogenen Bau- und Abbruchabfällen N2 - Mineralische Bauabfälle stellen in den Industrienationen den größten Abfallstrom dar. Allein in Deutschland fallen jährlich mehr als 50 Mio. Tonnen Bauschutt an, der hauptsächlich aus Beton- und Mauerwerkbruch besteht. Dabei nehmen die Verwertungs- und Recyclingquoten bei den bereits etablierten herkömmlichen Einsatzgebieten für aufbereitete Bau- und Abbruchabfälle mit zunehmender Heterogenität des Materials ab. Ein höherwertiges Recycling mit dem Ziel das aufbereitete Material beispielsweise in Betonprodukten einzusetzen erfolgt heute in Deutschland lediglich im Rahmen von Pilotprojekten. So können die groben Körnungen des Betonbruchs als rezyklierte Gesteinskörnung im Beton eingesetzt werden. Besonders eingeschränkte Verwertungsmöglichkeiten liegen für Mauerwerkbruch vor, einem Gemisch aus Beton, Ziegel, Kalksandstein, Porenbeton, Mörtel, Natursteinen und anderen mineralischen Bestandteilen. Die Ursache hierfür ist neben der heterogenen Zusammensetzung des Materials auch dessen feine Kornverteilung, die durch den bei der mechanischen Aufbereitung zwangsläufig anfallenden Feinkornanteil von 30 bis über 40 Prozent bedingt ist. Defizite in der Verwertung bestehen also besonders bei heterogenen feinkörnigen Gemischen. Hier müssen Ansätze gefunden werden, um eine hochwertige Wiederverwertung zu ermöglichen. Dafür ist eine möglichst gute Trennung der einzelnen Materialfraktionen ein bewährter Ansatz. Während Metalle mittels Band- und Wirbelstromabscheidern und leichte Fremdbestandteile über Windsichtung und Dichtesortierung ausgetragen werden können, ist eine Trennung der Materialien Ziegel, Mörtel und Beton, insbesondere für die feinen Fraktionen, derzeit technologisch und wirtschaftlich nicht umsetzbar. Ein rohstoffliches Recycling dieser heterogen zusammengesetzten Abfälle unter Nutzung ihrer chemisch-mineralogischen Zusammensetzung ohne eine vorherige Trennung in die einzelnen Materialfraktionen bietet sich als Alternative an. Ergebnisse zur Herstellung von Leichtgranulaten aus Mauerwerkbruch und Tonen in einem thermischen Prozess ähnlich der Blähtonherstellung wurden bereits mehrfach veröffentlicht. Diese Recycling-Granulate (RCG) könnten unter anderem als leichte Gesteinskörnung für Betone verwendet werden. T2 - 24. Tagung Siedlungsabfallwirtschaft Magdeburg CY - Magdeburg, Germany DA - 18.09.2019 KW - Leichte Gesteinskörnungen KW - Bau- und Abbruchabfälle KW - Mauerwerkbruch KW - Recycling PY - 2019 VL - 2019 SP - 89 EP - 94 PB - Otto-von-Guericke-Universität Magdeburg CY - Magdeburg AN - OPUS4-50189 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -