TY - CONF A1 - Xu, W. A1 - Zscherpel, Uwe A1 - Peng, J. A1 - Luo, L. A1 - Gao, X. A1 - Li, J. T1 - Investigation on Wall Thickness Ranges Using Digital Radiography for Tangential Projection Technique N2 - X-ray testing is based on the attenuation of X-rays when passing through matter. Image detectors acquire the X-ray information which is defined by the local penetrated wall thickness of the tested sample. By X-ray absorption in the detector and following read-out and digitization steps a digital image is generated. As detectors a radiographic film and film digitization, a storage phosphor imaging plate and a special Laser scanner (Computer Radiography - CR) or a digital detector array (DDA) can be used. The digital image in the computer can then be further analyzed using many types of image processing. In the presented work the automated evaluation of wall thickness profiles are investigated using a test steel pipe with 9 different wall thicknesses and various X-ray voltages and different filter materials at the tube port and intermediate between object and detector. In this way the influence of different radiation qualities on the accuracy of the automated wall thickness evaluation depending on the penetrated wall thickness of the steel pipe was investigated. T2 - 10th International Conference on Information Optics and Photonics CY - Beijing, China DA - 08.07.2018 KW - Image evaluation KW - Computed radiography (CR) KW - Digital Detector Array (DDA) KW - Tangential radiography KW - Wall thickness measurement PY - 2018 SN - 978-1-51062580-8 DO - https://doi.org/10.1117/12.2506324 SN - 0277-786X VL - 10964 SP - Article Number: UNSP 109645B PB - SPIE CY - Bellingham, WA AN - OPUS4-47346 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Herrmann, Ralf A1 - Rabe, J. A1 - Marx, S. ED - Baeßler, Matthias ED - Möller, G. ED - Rogge, Andreas ED - Schiefelbein, N. T1 - Datenmanagement und –analyse von kontinuierlichen Datenströmen bei Offshore Windparks N2 - Mit der Errichtung und der Inbetriebnahme des Windpark alpha ventus wurden umfangreiche Messungen an den Tragstrukturen und den Umgebungsparametern durchgeführt. Im Projekt Gigawind life wurde im TP1 ein Datenmanagementsystem zur kontinuierlichen und periodisch fortgeführten Datenauswertung für große Datenbestände (Big Data) entworfen und realisiert. Anhand von Performanceuntersuchungen konnte eine Verkürzung der Rechenzeit um den Faktor 10 in einem Rechencluster erreicht werden. Unter Anwendung einer Datenpipeline nach dem Publish/Subscribe Prinzip wird eine skalierbare Datenschnittstelle für Monitoringdaten vorgeschlagen. T2 - Messen im Bauwesen 2018 CY - Berlin, Germany DA - 13.11.2018 KW - Datenmanagement KW - Big Data KW - Windenergie PY - 2018 SN - 978-3-9818564-1-5 VL - 2018/1 SP - 89 EP - 98 PB - Bundesanstalt für Materialforschung und -prüfung (BAM) CY - Berlin AN - OPUS4-46918 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Uckert, Danilo A1 - Kühn, Hans-Joachim A1 - Matzak, Kathrin A1 - Rehmer, Birgit A1 - Skrotzki, Birgit T1 - Ermüdungsverhalten des warmfesten austenitischen Gusseisens EN-GJSA-XNiSiCr35-5-2 bei hoher Temperatur N2 - Die warmfeste austenitische Gusseisenlegierung EN-GJSA-XNiSiCr35-5-2 (häufig auch als Ni-Resist D-5S bezeichnet) wurde hinsichtlich ihres mechanischen Verhaltens bei hoher Temperatur charakterisiert. Dazu wurden (isotherme) niederzyklische (LCF-) und (nicht-isotherme) thermomechanische Ermüdungsversuche (TMF) zwischen Raumtemperatur und 900 °C durchgeführt. Diese Ergebnisse dienten (zusammen mit weiteren Versuchsdaten) der Kalibrierung werkstoffmechanischer Modelle. Bei den höchsten Prüftemperaturen wurde Schädigung in Form von Kriechen beobachtet und metallographisch dokumentiert. T2 - Langzeitverhalten warmfester Stähle und Hochtemperaturwerkstoffe CY - Dusseldorf, Germany DA - 30.11.2018 KW - Kriechen KW - LCF KW - Lebensdauer KW - Ni-Resist KW - Schädigung KW - TMF PY - 2018 SN - 978-3-00-061694-5 SP - 29 EP - 38 CY - Düsseldorf AN - OPUS4-46919 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Butz, Adam A1 - Fedelich, Bernard A1 - Rehmer, Birgit A1 - Skrotzki, Birgit A1 - Schmitz, Sebastian ED - Moninger, G. T1 - Risserkennung an Bohrlochproben: Numerische Voruntersuchung für eine neuartige Methode zur Rissformerkennung T1 - Crack Detection on Borehole Specimens: Numerical pre-examination for a novel crack shape detection method N2 - Es konnte anhand einer numerischen Voruntersuchung gezeigt werden, dass anhand der kombinierten Auswertung der im Versuch verwendeten Sensorik eine Einteilung der unter Ermüdung in Bohrlochproben auftretenden Rissformen in verschiedene Hauptkategorien (Eckriss, Oberflächenriss, Durchgangsriss) möglich ist. N2 - When fatigued specimens with a hole are to be investigated regarding crack growth, it may be the case that the shape of the crack can’t be identified with sufficient certainty. If marking the fracture surface e.g. using beach marks is not possible, a method is required that nevertheless allows for the determination of the crack shape in order to calculate the corresponding fracture mechanics parameters. This paper describes a numerical pre-study for a method that allows for the classification of cracks in a sample featuring a drill hole into one of three crack shape classes based on the combined evaluation of various types of test data. T2 - Tagung Werkstoffprüfung 2018 CY - Bad Neuenahr, Germany DA - 06.12.2018 KW - Crack KW - LCF KW - Data Fusion KW - Risse KW - Rissform KW - Datenfusion PY - 2018 VL - 2018 SP - 249 EP - 254 AN - OPUS4-46976 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wilsch, Gerd A1 - Gottlieb, Cassian A1 - Günther, Tobias A1 - Millar, Steven ED - Forde, Mike T1 - Application of laser induced breakdown spectroscopy N2 - A big part of the infrastructure is made of concrete, which is a multiphase system made of cement, aggregates, water and pores. Concrete is often used in combination with steel as reinforced concrete. Environmental influences, especially the ingress of harmful ions in combination with the ingress of water, trigger different damage processes which reduce the designed lifetime of a structure. The ingress of chlorides from de-icing salt or sea water leads to corrosion of the reinforcement. In addition, the carbonation of the concrete may trigger the corrosion of the reinforcement. The ingress of alkalis from deicing salts may cause the expansion of the amorphous silica aggregates (alkali-silica reaction) through formation of a swelling gel of calcium silicate hydrate if water is present. The ingress of sulphates may cause spalling of the concrete surface due to ettringite formation. For the standard procedure in civil engineering cores are taken, cut in slices, grinded and the obtained homogenized powder is solved in acid and investigated by standard procedures. BAM has developed the LIBS technique for the 2D evaluation of the chemical composition of concrete. The technique is established for automated laboratory use with high numbers of samples to investigate transport processes of harmful species (Cl-, CO2 , SO4 2-and alkalis) in concrete. Information about ingress depth and the quantitative values are important to estimate the remaining lifetime of the infrastructure. LIBS is a surface technique. To get information about the ingress depth, a drill core has to be taken and cut in the middle. The measurements are carried out at the cross section. The main advantages of LIBS are the direct measurement on the surface of the concrete, fast analysis (sample rate 100 Hz) with a spatial resolution of up to 100 µm, the consideration of the heterogeneity of the concrete and the possibility of automated measurements which save a lot of manpower and time. As an example the investigation of ingress profiles for standard diffusion and migration tests in civil engineering takes hours in comparison to just a few minutes using LIBS. At the same time a 2D-evaluation provides information about hot spots of elemental concentration which may not be found by standard methods. The state of the art of LIBS technique for applications in civil engineering will be presented, including typical results of 2D investigation of concrete in laboratory. The performance is also demonstrated by examples for onsite applications using a mobile LIBS system. The road map to standardization is presented as well. T2 - Structural Faults + Repair-2018 CY - Edinburgh, UK DA - 15.05.2018 KW - Sulphate KW - Chloride KW - Concrete KW - LIBS PY - 2018 SN - 0-947644-86-5 DO - https://doi.org/10.25084/sfr.2018.0030 SP - 1 EP - 7 PB - University of Edinburgh CY - Edinburgh AN - OPUS4-46947 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Algernon, D. A1 - Arndt, R.W. A1 - Denzel, W. A1 - Ebsen, B. A1 - Feistkorn, S. A1 - Friese, M. A1 - Große, C.U. A1 - Kathage, S. A1 - Keßler, S. A1 - Köpp, Christian A1 - Küttenbaum, Stefan A1 - Lohse, C. A1 - Maack, Stefan A1 - Niederleithinger, Ernst A1 - Schickert, M. A1 - Schröder, G. A1 - Taffe, A. A1 - Timofeev, Juri A1 - Walther, A. A1 - Wilcke, M. A1 - Wolf, J. A1 - Wöstmann, Jens T1 - Test specimen concepts in regard to quality assurance and validation of nondestructive testing in civil engineering N2 - The process of ensuring reliability of NDT applications contains various aspects, such as determining the performance and probability of success, the uncertainty in measurement, the provision of clear and functional procedures and ensuring the correct application accordingly. Test specimens have become powerful elements in supporting many of these aspects. Within the committee for NDT in Civil Engineering (NDT-CE) of the German Society for Nondestructive Testing (DGZfP), the subcommittee on Quality Assurance (UA-QS) therefore addresses the design and the integration of test specimens in the quality assurance process. Depending on the specific purpose, the requirements on test specimens can vary significantly based on the defined simulated scenario. The most prominent purposes of test specimens might be seen in providing references for inspection systems in regard to function control, calibration and validation. Further aspects can be parametric studies, basic investigation of physical principles related to NDT or a simplified and therefore comprehensive demonstration of inspection concepts (e.g. for teaching purposes). The specific purpose of a test specimen dictates the requirements regarding its conception, including the exact design, the material or the fabrication accuracy and the conditioning. In the development of a general guideline by the UA-QS for application-specific procedures and their validation, the use of test specimens is addressed and specific concepts for the design of test specimens are made. This includes the analysis of the measurement process regarding any given application, deriving an adequate calibration approach for it and designing test specimens (calibration specimens) accordingly. Furthermore, it includes the validation of the procedure taking into account all conditions related to the specific application in the field. The validation requires a statistically sufficient number of trials. Thorough evaluation of each trial can only be established if the ground-truth is known. Therefore, test specimens providing a realistic but controlled simulation of the inspection problem are valuable and indispensable elements in the validation process. The requirement of being fully realistic will often not be possible to fulfill due to practical restrictions. Any aspect that cannot be included in the simulation realistically needs to be simulated conservatively. This again, requires a sufficient understanding of the inspection principle and technique to ensure conservativeness. Among other quality-assurance-related aspects, the UA-QS establishes concepts and guidelines regarding sound and efficient approaches for the specific purposes of test specimens. This subcommittee brings together representatives of different Groups along the entire value chain of NDT-CE, including researchers, practitioners, manufacturers and clients. They all work together in establishing a common understanding and level of quality assurance in the industry. T2 - SMT and NDT-CE 2018 CY - New Brunswick, NJ, USA DA - 27.08.2018 KW - Quality assurance KW - Procedure KW - Reliability KW - Validation KW - Reference specimen PY - 2019 UR - https://asnt.org/smt18papers SN - 978-1-57117-456-7 VL - 11/19 SP - 39 EP - 48 PB - The American Society for Nondestructive Testing, Inc. CY - Columbus, OH, USA AN - OPUS4-47240 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Burkert, Andreas A1 - Babutzka, Martin T1 - Korrosionsschutz durch Deckschichtbildung und Passivität N2 - Metallene Konstruktionswerkstoffe reagieren infolge ihres thermodynamisch instabilen Zustandes mehr oder weniger stark mit Stoffen aus der Umgebung. Eine große Rolle bei diesen Reaktionen spielt das Feuchtigkeitsangebot an der Metalloberfläche, welches nicht zwingend mit einem sichtbaren Wasserfilm einhergehen muss. An der Atmosphäre bilden sich an sauberen Metalloberflächen bei etwa 80 % relativer Luftfeuchte, bei versalzten Oberflächen auch schon ab etwa 25 % r. F., Feuchtfilme aus. Im Feuchtfilm laufen grundsätzlich die gleichen elektrochemischen Reaktionen ab, wie diese von wässrigen Medien bekannt sind. Dabei geht das Metall zunächst in Ionenform und in nachgelagerten Reaktionen in einen thermodynamisch stabilen Zustand in Form unterschiedlichster Oxid- und Hydroxidverbindungen über. Die so entstehenden Korrosionsprodukte können im Feuchtigkeitsfilm begrenzt löslich oder unlöslich sein und lagern sich auf den Oberflächen der Konstruktionswerkstoffe häufig als feste Korrosionsprodukte ab bzw. wachsen dort auf. Je nachdem wie die Korrosionsprodukte strukturell zum Untergrund passen, können sich dichte, sehr gut haftende Schichten ausbilden oder poröse, dicke Schichten ohne nennenswerte Haftung aufwachsen. Wachsen dichte, porenfreie Schichten mit guter Haftung auf, die im umgebenden Medium unlöslich sind, wird die weitere Auflösung des Metalls stark gehemmt. Man spricht dann von der Ausbildung schützender Deckschichten bzw. von Passivschichten auf welcher der Korrosionsschutz und damit die Dauerhaftigkeit vieler Konstruktionswerkstoffe beruhen. Kaesche bezeichnete die Passivität sehr treffend als „optimalen Grenzfall des Korrosionsschutzes durch Schichten von Korrosionsprodukten“. Aus technischer Sicht hält Kaesche eine Unterscheidung von Deckschichten bzw. Passivschichten für nicht zwingend erforderlich, da beide die Korrosionsgeschwindigkeit in gleichem Maß herabsetzen können. Die Übergänge zwischen den meist dickeren und dadurch sichtbaren Deckschichten und den meist dünnen, nicht sichtbaren Passivschichten sind fließend. T2 - 18. Tagung "Korrosionsschutz in der maritimen Technik" CY - Hamburg, Germany DA - 30.01.2019 KW - Korrosionsschutz KW - Überzüge KW - Deckschichten KW - Passivität PY - 2019 SN - 978-3-935406-70-3 VL - 18 SP - 25 EP - 38 AN - OPUS4-47307 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Abraham, O. A1 - Niederleithinger, Ernst A1 - Chapeleau, X. A1 - Klikowicz, P. A1 - Brühwiler, E. A1 - Bassil, A. A1 - Wang, Xin A1 - Chakraborty, J. A1 - Bayane, I. A1 - Leduc, D. A1 - Salamak, M. A1 - Katunin, A. A1 - Sørensen, J.D. T1 - Addressing the need to monitor concrete fatigue with nondestructive testing: Results of infrastar European project N2 - Fatigue is one of the most prevalent issues, which directly influences the service life expectancy of concrete structures. Fatigue has been investigated for years for steel structures. However, recent findings suggest that concrete structures may also be significantly subjected to fatigue phenomena that could lead to premature failure of certain structural elements. To date, fatigue of reinforced concrete has been given little focus. Knowledge on the influence factors and durability/capacity effects on this material should be improved. Current technological means to measure fatigue in civil structures like bridges and wind turbines (both onshore and offshore) are outdated, imprecise and inappropriate. Meanwhile, this topic has got much more attention as time-variant loading on concrete structures plays an increasing role, e.g. in bridges with increasing traffic and heavier trucks, and for wind turbines for renewable energy production, e.g. for offshore wind turbine support structures affected by wind and waves. The European Innovative Training Networks (ITN) Marie Skłodowska-Curie Actions project INFRASTAR (Innovation and Networking for Fatigue and Reliability Analysis of Structures - Training for Assessment of Risk) provides research training for 12 PhD students. The project aims to improve knowledge for optimizing the design of new structures as well as for more realistic verification of structural safety and more accurate prediction of the remaining fatigue lifetime of existing concrete structures. First, the INFRASTAR research framework is detailed. Then it will be exemplified through the presentation of the major results of the four PhD students involved in the work package dealing with auscultation and monitoring. This includes the development and improvement of Fiber Optics (FO) and Coda Wave Interferometry (CWI) for crack sizing and imagery, new sensor technologies and integration, information management, monitoring strategy for fatigue damage investigation and lifetime prediction. T2 - SMT and NDT-CE 2018 CY - New Brunswick, NJ, USA DA - 27.08.2018 KW - Concrete KW - Fatigue KW - Crack KW - Monitoring KW - Non-destructive testing PY - 2019 UR - https://asnt.org/smt18papers SN - 978-1-57117-456-7 VL - 11/19 SP - 2 EP - 13 PB - The American Society for Nondestructive Testing, Inc. CY - Columbus, OH, USA AN - OPUS4-47237 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Niederleithinger, Ernst A1 - Wiggenhauser, Herbert T1 - The LAUS: First Applications of a New System for Ultrasonic Imaging of Very Concrete Structures N2 - The LAUS (Large Aperture Ultrasonic System) has been developed to image very thick concrete structures, which are not accessible for commercial systems. The device and the corresponding software is the result of joint Research of BAM, an ultrasonic instrument manufacturer and University of Kassel, Germany. It consists of 12 separate Arrays of 32 point-contact shear wave transducers each, which can be deployed in flexible configurations. Each array is combined with battery and transmitter, receiver and wireless communication electronics. Three case histories are presented. First the system was deployed on a 5-m thick heavily reinforced foundation slab. The reflection of the slab’s bottom was imaged clearly. In addition, a multiple reflection was registered, thus giving hope that even thicker elements might be imaged by the instrument. Second, the LAUS was used to investigate a massive bridge girder where a heavy rainstorm during concreting had led to imperfections that were visible after removing the formwork was removed. The LAUS could image tendon ducts in 1.8m depth and the backwall closely behind them. Some limited areas showed blurred reflections and were checked by drill holes; these areas were affected by diffuse damage which could be repaired by injections. Third, a large retaining wall was checked for thickness. Meanwhile, the LAUS has been used in underground waste deposits (nuclear and other) for quality assurance of sealing plugs. A confirmed penetration depth of about 7 m has been reached. T2 - SMT and NDT-CE 2018 CY - New Brunswick, NJ, USA DA - 27.08.2018 KW - LAUS (Large Apertur Ultrasonic System) KW - Ultrasonic echo KW - Deep penetration KW - Concrete PY - 2019 UR - https://asnt.org/smt18papers SN - 978-1-57117-456-7 VL - 11/19 SP - 208 EP - 213 PB - The American Society for Nondestructive Testing, Inc. CY - Columbus, OH, USA AN - OPUS4-47238 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Algernon, D. A1 - Arndt, R.W. A1 - Denzel, W. A1 - Ebsen, B. A1 - Feistkorn, S. A1 - Friese, M. A1 - Große, C.U. A1 - Kathage, S. A1 - Keßler, S. A1 - Köpp, Christian A1 - Küttenbaum, Stefan A1 - Lohse, C. A1 - Maack, Stefan A1 - Niederleithinger, Ernst A1 - Schickert, M. A1 - Schröder, G. A1 - Taffe, A. A1 - Timofeev, Juri A1 - Walther, A. A1 - Wilcke, M. A1 - Wolf, J. A1 - Wöstmann, Jens T1 - NDT procedures in relation to quality assurance and validation of nondestructive testing in civil engineering N2 - The field of non-destructive testing of civil structures (NDT-CE) has been continuously growing. Due to the complexity and diversity of civil constructions as well as the heterogeneity of concrete, specific standards or guidelines for the application of modern NDT-CE are still missing. The development of individual solutions is the current approach, which is just as challenging as it is common for NDT-CE. With the increasing development and commercialization of NDT-CE technology, the group of practitioners is growing. To ensure a good level of quality in the industry, it appears necessary to establish adequate means. Naturally, the performance of NDT-CE methods regarding a specific application is strongly dependent on choosing the most suitable inspection technique and applying it correctly, generally referred to as the inspection procedure in the field of NDT. There are well-defined guidelines regarding procedure documentation and handling in many fields of NDT (e.g. nuclear, aerospace or automotive) according to the high importance of procedures in assuring a successful and reliable application. For a long time, this has not always been the case with NDT-CE, which is still considered a unique discipline of NDT. Part of the reason for that might be the young development state of NDTCE, the heterogeneity of building materials like concrete, timber or masonry as a material and the diversity of civil structures. In consequence, NDT-CE procedure development is considered challenging. Among other aspects, addressed in the subcommittee on Quality Assurance (UA-QS) within the committee for NDT-CE of the German Society for Nondestructive Testing (DGZfP), part of its work aims at establishing an adequate basis for NDT-CE procedure development. While some of the highly developed approaches from other industries are taken into consideration, they need to be analyzed regarding their suitability for NDT-CE and adapted accordingly. For a procedure to be as defined as possible, it needs to contain sufficient information, such as the scope and limitations regarding material, geometry and condition of the test object, inspection parameters, calibration, data acquisition, analysis criteria as well as requirements regarding the inspection personnel. For a successful implementation in the field, it is important to define the specific procedure as precisely as possible. Despite the necessity of a great amount of information to be included, the procedure needs to be suitable for efficient field application. The UA-QS is developing a guideline for NDT-CE procedures suitable for application in this field of NDT to ensure correct and reproducible application. To demonstrate and evaluate this concept, specific examples of procedures are also produced. In particular, the UA-QS has developed a procedure for the detection and positioning of tendon ducts using Ground Penetrating Radar (GPR). This procedure is tested regarding the practical applicability in a roundrobin on a defined type of reference test block. T2 - SMT and NDT-CE 2018 CY - New Brunswick, NJ, USA DA - 27.08.2018 KW - Quality assurance KW - Procedure KW - Reliability KW - Validation KW - Reference specimen PY - 2019 UR - https://asnt.org/smt18papers SN - 978-1-57117-456-7 VL - 11/19 SP - 31 EP - 38 PB - The American Society for Nondestructive Testing, Inc. CY - Columbus, OH, USA AN - OPUS4-47239 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wöhlecke, Andreas ED - Al-Akel, S. T1 - Aktuelle Diskussionen aus dem Fachbeirat der BAM N2 - Vor nun 30 Jahren im Jahre 1989 wurde die erste Zulassung für eine Kunststoffdichtungsbahn von der BAM auf der Grundlage des „Niedersächsischen Dichtungserlasses“ erteilt. Vor ungefähr 10 Jahren wurde die BAM mit dem Erscheinen der Deponieverordnung (DepV) mit der Zulassung von Geokunststoffen, Polymeren und Dichtungskontrollsystemen beauftragt. Wir möchten dies zum Anlass nehmen, an dieser Stelle den viele ehrenamtlichen Experten des Fachbeirats und seiner Arbeitsgruppen für ihren Einsatz und die Unterstützung zu danken. Darüber hinaus soll über aktuelle Arbeitsthemen und Entwicklungen im Fachbeirat berichtet werden. So soll in einer Sondersitzung des Fachbeirats über die Entlassung aus der Nachsorgephase beim Einsatz von Geokunststoffprodukten in Böschungen diskutiert werden. Es ist geplant, in einer Unterarbeitsgruppe eine Sitzung über die Fremdüber¬wachung in der Produktion abzuhalten. Darüber hinaus werden Änderungen in den Zulassungsrichtlinien für Kunststoff Dichtungsbahnen und Kunststoff Dränelemente kurz vorgestellt. In der Zwischenzeit wurde auch die abschließende Zulassungsrichtlinie für Geogitter verabschiedet. Neue Fragestellungen sind hier entstanden. Unter welchen Voraussetzungen können Geogitter in Zwischenabdichtungen eingesetzt werden. Bisher können diese Produkte formal nur in Oberflächenabdichtungen eingesetzt werden. Auch auf diese beiden Themen soll im Folgenden in Kürze eingegangen werden. T2 - 15. Leipziger Deponiefachtagung CY - Leipzig, Germany DA - 05.03.2019 KW - Deponie KW - Abdichtungssysteme KW - Geogitter PY - 2019 SN - 978-3-943443-48-6 VL - 15 SP - 29 EP - 40 PB - HTWK Leipzig CY - Leipzig AN - OPUS4-47490 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Spranger, Felix A1 - Hilgenberg, Kai A1 - Rethmeier, Michael T1 - Anwendung der Laserimplantation zur Strukturierung verschleißgefährdeter Werkzeuge N2 - In einer Vielzahl technischer Anwendungen spielt die Aufrechterhaltung eines definierten Reibungs- und Verschleißverhaltens zwischen bewegten Oberflächen für die Sicherheit und Funktionalität eine entscheidende Rolle. Die Oberflächentechnik versucht durch geeignete Verfahren die Randschichten zu ertüchtigen, um Reibung und Verschleiß zu kontrollieren. Eine Verbesserung der Materialeigenschaften kann durch flächige Beschichtungen erreicht werden. Zusätzlich ermöglichen Oberflächenstrukturierungen breite Möglichkeiten zur Beeinflussung des Schmierungszustandes bzw. der Kontaktbedingungen. Neben Negativstrukturen bieten ebenfalls erhabene Mikrostrukturen großes Potenzial zur Beeinflussung des tribologischen Verhaltens. Ihr Einsatz ist aber aufgrund der besonderen Verschleißproblematik erhabener Strukturen momentan limitiert, so dass in der Regel zusätzliche verschleißreduzierende Beschichtungen notwendig werden. In diesem Beitrag wurde das Verfahren der Laserimplantation angewandt, mit dem erhabene und separierte Oberflächenstrukturen hoher Verschleißfestigkeit in einem Fertigungsschritt erzeugbar sind. Das Verfahren basiert auf einem lokalisierten Dispergieren von Hartstoffpartikeln. Hierfür wurde erstmalig ein gepulster Faserlaser mit hoher Strahlqualität zur Erzeugung punkt- und linienförmiger Mikrostrukturen angewandt. Versuche wurden auf dem Kaltarbeitsstahl X153CrMoV12 unter Anwendung von Titandiborid als Hartstoff durchgeführt. Anhand von Härtemessungen konnte gezeigt werden, dass sowohl punkt- als auch linienförmige Strukturen mit Härten über 1000 HV1 und einer feinkörnigen Mikrostruktur mit feinverteilten Hartstoffpartikeln herstellbar sind. Des Weiteren war es möglich, die Implantgeometrien, welche an Querschliffen und durch Weißlichtinterferometeraufnahmen erfasst wurden, durch die Pulsleistung und Pulsdauer zu steuern. T2 - 38. Assistentenseminar der WGF CY - Rabenau, Germany DA - 06.09.2017 KW - Laserimplantation PY - 2018 SN - 978-3-96144-028-3 VL - 342 SP - 24 EP - 33 CY - Düsseldorf AN - OPUS4-47295 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Aidagulov, Gallyam A1 - Qiu, Xiangdong A1 - Brady, Dominic A1 - Abbad, Mustapha A1 - Onel, Yener A1 - Ewert, Uwe T1 - New insights into carbonate matrix stimulation from high-resolution 3D images of wormholes obtained in radial acidizing experiments N2 - We analyzed the results of high-energy X-ray CT scans for three 20×16×16 in. block samples of Indiana limestone from our recent radial acidizing experiments with HCl. CT scans were done for complete samples, and 3D images of internal dissolution patterns were built. Each 3D image consists of submillimeter-size voxels to capture fine details of individual wormholes. The obtained 3D images of acidized blocks allow us to observe from various angles the details of the wormholes obtained in the three experiments, which demonstrated wide pore-volume-to-breakthrough (PVBT) range with three different injection rates. Also, variation of the CT number reveals the presence of depositional layers in all block samples, and the obtained CT images were used to interpret the effect that rock layers might have on wormhole penetration at different injection rates. Further, the built voxel models were used to calculate the radial distributions of dissolved rock volume, which otherwise are not obvious for such complex branched structures as wormholes. We observed how varied experimental conditions affected those distributions. The radial distributions were found very similar across the samples, which suggested the way to detect the effective wormhole penetration depth. T2 - SPE Kingdom of Saudi Arabia Annual Technical Symposium and Exhibition CY - Dammam, Saudi Arabia DA - 23.04.2018 KW - Carbonate matrix stimulation KW - High-energy X-ray CT KW - XL-CT KW - Analysis of wormholes PY - 2018 DO - https://doi.org/10.2118/192366-MS SP - SPE-192366-MS, 1 EP - 19 AN - OPUS4-46654 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wöhlecke, Andreas T1 - Die Zulassung von Geokunststoffen nach der deutschen Deponieverordnung N2 - Seit dem Erscheinen der Deponieverordnung (DepV) bedürfen Geokunststoffe, Polymere und Dichtungskontrollsysteme einer Zulassung durch die BAM, wenn diese in deutschen Deponieabdichtungssystemen eingesetzt werden sollen. Die DepV ermöglicht den Einsatz verschiedener Komponenten. Sie stellt dabei allgemeine Anforderungen an die Geokunststoffprodukte auf. Dadurch beschreibt sie den Stand der Technik für Geokunststoffe, die in deutschen Abdichtungen eingesetzt werden. Diese Anforderungen werden durch die Zulassungsrichtlinien der BAM in konkrete technische Spezifikationen überführt. In dem Beitrag wird eine Übersicht über die Produkte und die entsprechenden Anforderungen gegeben. Zudem soll erläutert werden, durch welche Qualitätsmanagementmaßnahmen eine gleichbleibende Qualität und Funktionserfüllung der Produkte gewährleistet wird. T2 - 14. DEPONIEWORKSHOP Liberec - Zittau 2018 CY - Liberec, Czech Republic DA - 15.11.2018 KW - Deponie KW - Geokunststoffe KW - Polymere KW - Dichtungskontrollsysteme PY - 2018 VL - 14 SP - 149 EP - 158 PB - Technische Universität Liberec, Hochschule Görlitz/Zittau CY - Liberec, Tschechien AN - OPUS4-46660 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Koclega, Damian A1 - Radziszewska, A. A1 - Kranzmann, Axel T1 - The influence of the aggressive environments on the Inconel 686 coating in high-temperature corrosion experiments N2 - This work presents the microstructure and chemical composition of oxide scales created on Ni – base coating after corrosion experiments in aggressive gases and ashes. The Inconel 686 coating applied on the low carbon steel 13CrMo4-5 was performed by a CO2 laser cladding process. The experiments were carried out in oxidizing gas atmospheres containing O2, COx, SOx. The second Variation of corrosion experiments were performed in a reducing atmosphere with ashes containing elements such as: Na, Cl, Ca, Si, C, Fe, Al etc. After 240 h and 1.000 h corrosion experiments the oxide scales on the substrate and overlay were created in both cases. The sulfur compounds were found on the top of the coating surface (EPMA) and also higher contents of silica compounds were revealed on specimens covered by ashes during the experiments. The microstructure and chemical composition of the clad and scales were investigated by means of a light microscope and an electron microscope (SEM)equipped with an EDS detector. T2 - 50. Kraftwerkstechnisches Kolloquium CY - Dresden, Germany DA - 23.10.2018 KW - Nickel based coatings KW - Inconel 686 KW - High temperature corrosion PY - 2018 SP - 599 AN - OPUS4-46590 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schnell, A. A1 - Rübner, Katrin A1 - Ihlenfeldt, Toni A1 - Vöge, M. A1 - Ludwig, H.-M. ED - Ludwig, H.-M. T1 - Leichtbetone mit Recycling-Granulaten aus Mauerwerkbruch-Ton-Mischungen N2 - Mineralische Bauabfälle stellen in den Industrienationen den größten Abfallstrom dar. Allein in Deutschland fallen jährlich mehr als 50 Mio. Tonnen Bauschutt an, der hauptsächlich aus Beton- und Mauerwerkbruch besteht. Dabei nehmen die Verwertungs- und Recyclingquoten bei den bereits etablierten herkömmlichen Einsatzgebieten für aufbereitete Bau- und Abbruchabfälle mit zunehmender Heterogenität des Materials ab. Ein höherwertiges Recycling mit dem Ziel das aufbereitete Material in hochwertigen Betonprodukten einzusetzen erfolgt heute in Deutschland lediglich im Rahmen von Pilotprojekten. So können die groben Körnungen des Betonbruchs als rezyklierte Gesteinskörnung im Beton eingesetzt werden. Besonders eingeschränkte Verwertungsmöglichkeiten liegen für Mauerwerkbruch vor, einem Gemisch aus Beton, Ziegel, Kalksandstein, Porenbeton, Mörtel, Natursteinen und anderen mineralischen Bestandteilen. Die Ursache hierfür ist neben der heterogenen Zusammensetzung des Materials auch dessen feine Kornverteilung, die durch den bei der mechanischen Aufbereitung zwangsläufig anfallenden Feinkornanteil von 30 bis über 40 Prozentbedingt ist. Defizite in der Verwertung bestehen also besonders bei heterogenen feinkörnigen Gemischen. Hier müssen Ansätze gefunden werden, um eine hochwertige Wiederverwertung zu ermöglichen. Dafür ist eine möglichst gute Trennung der einzelnen Materialfraktionen ein bewährter Ansatz. Während Metalle mittels Band- und Wirbelstromabscheidern und leichte Fremdbestandteile über Windsichtung und Dichtesortierung ausgetragen werden können, ist eine Trennung der Materialien Ziegel, Mörtel und Beton, insbesondere für die feinen Fraktionen, derzeit technologisch und wirtschaftlich nicht umsetzbar. Ein rohstoffliches Recycling dieser heterogen zusammengesetzten Abfälle unter Nutzung ihrer chemisch-mineralogischen Zusammensetzung ohne eine vorherige Trennung in die einzelnen Materialfraktionen bietet sich als Alternative an. Ergebnisse zur Herstellung von Leichtgranulaten aus Mauerwerkbruch und Tonen in einem thermischen Prozess ähnlich der Blähtonherstellung wurden bereits mehrfach veröffentlicht. Diese Recycling-Granulate (RCG) sollen unter anderem als leichte Gesteinskörnung für Betone verwendet werden. Gegenstand dieses Beitrags sind Ergebnisse aus dem Verbundforschungsprojekt „RC-Leichtgranulate“ zum Einsatz der RCG in Leichtbeton. T2 - ibausil 2018 - 20. Internationale Baustofftagung CY - Weimar, Germany DA - 12.09.2918 KW - Recycling KW - Mauerwerkbruch KW - Leichte Gesteinskörnungen KW - Recyclinggranulat KW - Leichtbeton KW - Ton PY - 2018 SN - 978-3-00-059950-7 VL - 2 SP - 2-381 EP - 2-388 PB - F.A. Finger-Institut für Baustoffkunde CY - Weimar AN - OPUS4-46697 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bakir, Nasim A1 - Artinov, Antoni A1 - Bachmann, Marcel A1 - Gumenyuk, Andrey A1 - Rethmeier, Michael T1 - About the origin of solidification cracking in laser welded thick-walled structures N2 - In this study, a three-dimensional CFD-simulation model was developed to simulate the fluid flow in the weld pool. The CFD-model showed a bulging region in the middle of the depth, which is separated from the top surface and bottom surface by two narrowing regions. It can be concluded that the interaction of the movement of the laser source with the Marangoni vortex leads to a teardrop shape at the upper and bottom surface of the workpiece. Additionally, it shows that the bulging in the weld is a result of the backflows on the upper and lower sides due to the thermo-capillary-driven flows. The weld pool shape was used as a heat source in a two-dimensional thermomechanical model, which allows a highly accurate transformation of the weld pool dimensions obtained from the CFD model. This developed technique allows the consideration of physical aspects, which cannot be considered when using traditional heat sources. The mechanical model has shown that the chronological order of the solidification of the weld has a significant influence on the nature and distribution of the stresses in the weld. High tensile stress has been observed in the bulging region, i.e. in the susceptible region for solidification cracking, when compared to the other narrowing regions, which show compressive stress. T2 - 4th International Conference on Welding and Failure Analysis of Engineering Materials CY - Aswan, Egypt DA - 19.11.2018 KW - Laser beam welding KW - Solidification cracking KW - Numerical simulation KW - Weld pool geometry KW - CFD-model KW - FE-model PY - 2018 SP - W-6, 1 EP - 10 CY - Aswan, Egypt AN - OPUS4-46735 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Siayah, A. A1 - El-Batahgy, A. A1 - Khafagi, S. A1 - Gumenyuk, Andrey A1 - Gook, S. A1 - Rethmeier, Michael T1 - A study on shielded metal arc welding of 9%Ni steel using non-conventional ferritic welding electrode for LNG facilities N2 - The present research work aims at clarification of the effect of the welding electrode type on the mechanical properties of SMA welded joints of 9%Ni steel plates. Properties of produced SMA welded joints were evaluated using different non-destructive and destructive investigation methods. In comparison with the conventionally used Ni-based welding electrode ENiCrMo-3 (AWS A5.11), an experimentally produced non-conventional ferritic welding electrode with 11%Ni (ENi11-Company specification) has resulted in a better combination of the mechanical properties of SMA welded joints of this steel type for critical cryogenic applications. Besides, a positive economic impact for the experimentally produced non-conventional ferritic welding electrode, due to its lower cost, could be another attractive aspect. T2 - 4th International Conference on Welding and Failure Analysis of Engineering Materials CY - Aswan, Egypt DA - 19.11.2018 KW - 9%Ni steel, KW - SMAW KW - Conventional Ni-based austenitic welding electrode KW - Mechanical properties KW - Ferritic welding electrode PY - 2018 SP - W-21, 1 EP - 3 AN - OPUS4-46736 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - El-Batahgy, A. A1 - Gook, S. A1 - Gumenyuk, Andrey A1 - Rethmeier, Michael T1 - Effect of laser-beam and hybrid-laser-arc welding parameters and filler metal on microstructure and mechanical properties of thick heat-treated steel X8ni9+Qt640 for cryogenic service N2 - The present research work encloses results of experimental investigations of the interaction between welding process parameters for laser-beam and hybrid-laser-arc as well as type of the filler metal and the achievable mechanical properties of the weld joints on steel grade X8Ni9+QT640 for cryogenic service containing 9% nickel. The results obtained contribute to the development and conversion in the industrial practice a new laser beam-based welding technology for the automated manufacturing of facilities for the liquefaction, storage and the transport of natural gases (LNG facilities). The results show, that the martensitic microstructure of the laser weld metal including low amount of retained austenite not exceeding 3.5% leads to the relatively low V-notch impact energy. The remarkable heterogeneity in the chemical composition of the weld metal through the weld thickness could be recognized in the case of hybrid-laser-arc welding with ERNiCrMo-3 austenitic filler metal, what also led to insufficient impact toughness of the weld metall. The most promising results could be achieved by using 11%Ni filler wire, which is similar to the base metal and provides a homogeneous microstructure with uniform distribution of Ni through the weld seam. It is remarkable, that a correlation between Charpy impact toughness and wire feeding speed and respectively process heat input exists. The highest toughness values were 134±58 J at -196C. The both laser as well as laser-hybrid welds passed the tensile test. The failure stress of 720±3 MPa with a fracture location in the base material was achieved for all samples tested. T2 - 4th International Conference on Welding and Failure Analysis of Engineering Materials CY - Aswan, Egypt DA - 19.11.2018 KW - Hybrid-laser-arc welding KW - Laser-beam welding, KW - Cryogenic steel KW - Microstructure KW - Tensile strength PY - 2018 SP - W-29, 1 EP - 10 AN - OPUS4-46738 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Romero-Navarrete, José A. A1 - Otremba, Frank A1 - Lozano -Guzmán, A. A. T1 - Commidities and rail damage N2 - A roll-plane simplified model, representing the suspended body-cargo of a railway car, was developed to simulate thedynamic response of a railway car while subjectedto lateral acceleration derived from its traveling along curved tracks. The model provides the means to calculate the suspension forces, which are supposed to be transmitted to the bogie´s wheelset. For the analysis of the potential effect of such forces on the railway fatigue life, different performance measures were considered, under different concepts. A family of curves were produced to analyze the effect of the height of the center of gravity of the body-cargo system, on the different performance measures. The resultingdiagramswereused to assess the rail damage potentials offour different railway cars. Results suggest that the height of the center of gravity, associated to the different types of railway cars, nonlinearly and strongly affects the fatigue lifeof the rail, with the double stack car being the moreinfrastructure-aggressive. In this respect, experimental evidence should be provided about such remarkable effects, so as to supportsome operational recommendationsthat shouldbe taken to mitigate these effects, including, for example, the regulation of the traveling speed of some vehicles. T2 - IMECE 2018 International Mechanical Engineering Congress and Exposition CY - Pittsburgh, PA, USA DA - 09.11.2018 KW - Commidities KW - Rail KW - Damage PY - 2018 SP - 86008-1 EP - 86008-6 PB - ASME AN - OPUS4-46650 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Gluth, Gregor A1 - Sturm, Patrick A1 - Greiser, Sebastian A1 - Jäger, Christian A1 - Kühne, Hans-Carsten ED - Wang, J. ED - Kriven, W. ED - Fey, T. ED - Colombo, P. ED - Weber, W.J. ED - Amoroso, J. ED - Fahrenholtz, W.G. ED - Shimamura, K. ED - Halbig, M. ED - Kirihara, S. ED - Wu, Y. ED - Shurgart, K. T1 - One-part geopolymers and aluminosilicate gel-zeolite composites: factors influencing microstructure and engineering properties N2 - Mixing and curing of geopolymers and related alkali-activated materials without storage and handling of highly alkaline solutions possesses advantages regarding safety and economic viability. One possible approach is to produce these materials from solid silica feedstocks and solid sodium aluminate, and subsequent mixing with water. We present a comparison between geopolymers and aluminosilicate gel-zeolite composites synthesized by this route from different silica feedstocks (by-product silica from chlorosilane production, microsilica, rice husk ash) and with different SiO2/Al2O3 ratios, using results from XRD, NMR, SEM, thermal analysis, mechanical and acid resistance testing. The use of rice husk ash favors formation of a fully amorphous geopolymer with high strength. Utilization of the other silica feedstocks leads to formation of aluminosilicate gel-zeolite composites, the amount and kind of zeolites depending on the feedstock and the SiO2/Al2O3 ratio. These composites show beneficial dehydration behavior, viz. no distinct dehydration step of thermal strain, with the phase assemblage after heating to 1000°C controlled by the starting composition. Mortars produced from both, the geopolymers as well as the composites, exhibit high resistance to sulfuric acid attack, making them promising materials for the construction and the repair of industrial and sewer structures. T2 - 42nd International Conference on Advanced Ceramics and Composites CY - Daytona Beach, FL, USA DA - 21.01.2018 KW - Alkali-activated materials KW - One-part geopolymers KW - Sulfuric acid resistance KW - High-temperature resistance PY - 2019 DO - https://doi.org/10.1002/9781119543381.ch17 VL - 39 IS - 3 SP - 183 EP - 196 PB - John Wiley & Sons AN - OPUS4-47282 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rübner, Katrin A1 - Schnell, A. A1 - Ihlenfeldt, Toni A1 - Vöge, M. ED - Martins, I. M. ED - Ulsen, C. ED - Villagran, Y. T1 - Lightweight concrete with recycling aggregates made from masonry rubble and rubble-clay mixtures N2 - Structural lightweight concrete is a construction material composed primarily of lightweight aggregates (LWA), cement and water. Most LWA are produced by thermal treatment of natural raw materials such as clay and shale today. In addition to the high energy costs thereby incurred, the availability of suitable raw materials is limited. An alternative is the use of recycling LWA made from mineral construction and demolition waste. Recycling LWA made from masonry rubble and rubble-clay mixtures were studied in two different research projects. The technology pursues the idea of feedstock recycling, which means the recycling is based on the chemical and mineralogical composition of the masonry rubble and clay. The recycling LWA are produced in a multistage manufacturing process by thermal hardening in laboratory and pilot scale. Their particle bulk densities and particle strengths vary between 600 and 2000 kg/m³ and 1.5 and 13 MPa, respectively. Their equivalence to traditional LWA was proven in comprehensive tests of the aggregates themselves as well as the mortars and concretes made therefrom. Our contribution reports on the results of the characterization of the recycling aggregates compared to expanded clays and the studies on LWA concretes. T2 - IV International Conference Progress of Recycling in the Built Environment CY - Lisbon, Portugal DA - 11.10.2018 KW - Lightweight aggregates (LWA) KW - Recycling aggregates KW - Lightweight concrete KW - Masonry rubble KW - Recycling PY - 2018 SN - 978-2-35158-208-4 VL - 2018/PRO 124 SP - 323 EP - 331 PB - RILEM Publications S.A.R.L. CY - Paris, France AN - OPUS4-47315 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kutz, Philipp A1 - Otremba, Frank A1 - Werner, Jan A1 - Sklorz, Christian T1 - Development of a Single Walled Tank under Cryogenic Conditions made of Composite N2 - The use of glass-fiber reinforced plastic (GRP) can reduce the weight of tanks significantly. By replacing steel with GRP in tanks for gases (propane, etc.) a weight reduction of up to 50 % was reached. In this project not only the material should be optimized, but also the design. Previous tanks consist of a double-walled structure with an insulation layer between the two shells (e.g. vacuum). Goal of this project is to realize a single-walled construction of GRP with an insulation layer on the outside. To determine the temperature dependent material values, two different experiments are performed: In the first experiment, temperature dependent material properties of liquid nitrogen found in literature research are validated in a simple setup. The level of liquid nitrogen in a small jar is measured over the experiment time. Numerical simulation shows the change of nitrogen level with sufficient precision. In the second experiment, a liquid nitrogen is applied on one side of a GRP plate. Temperature is measured with thermocouples on top and bottom of the GRP plate, as well as in the middle of the plate. By use of numerical simulation, temperature dependent thermal conductivity is determined. In the third experiment, a test stand is designed to examine different insulation materials. In this test stand, the insulation material can easily be changed. A numerical simulation, in which the determined material data is used, is performed as well for this test stand. The experiments show, that GRP can be used in cryogenic environments. Multiphase simulations are a suitable tool to describe the energy absorption of thermal energy due to thermal phase change. Results on different insulation materials will follow. T2 - IMECE 2018 CY - Pittsburgh, PA, USA DA - 09.11.2018 KW - Lightweight design KW - Thermal properties of GRP KW - Liquid nitrogen KW - LNG PY - 2018 UR - http://proceedings.asmedigitalcollection.asme.org/proceeding.aspx?articleID=2722335 SN - 978-0-7918-5214-9 DO - https://doi.org/10.1115/IMECE2018-86365 VL - 9 SP - V009T12A019 PB - ASME AN - OPUS4-47321 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Heckel, Thomas A1 - Casperson, Ralf A1 - Rühe, Sven A1 - Mook, Gerhard T1 - Signal processing for non-destructive testing of railway tracks N2 - Increased speed, heavier loads, altered material and modern drive systems result in an increasing number of rail flaws. The appearance of these flaws also changes continually due to the rapid change in damage mechanisms of modern rolling stock. Hence, interpretation has become difficult when evaluating non-destructive rail testing results. Due to the changed interplay between detection methods and flaws, the recorded signals may result in unclassified types of rail flaws. Methods for automatic rail inspection (according to defect detection and classification) undergo continual development. Signal processing is a key technology to master the challenge of classification and maintain resolution and detection quality, independent of operation speed. The basic ideas of signal processing, based on the Glassy-Rail-Diagram for classification purposes, are presented herein. Examples for the detection of damages caused by rolling contact fatigue also are given, and synergetic effects of combined evaluation of diverse inspection methods are shown. T2 - QNDE - Annual Review of Progress in Quantitative Nondestructive Evaluation CY - Provo, UT, USA DA - 16.07.2017 KW - Rail KW - Inspection KW - Train KW - Ultrasound KW - Signal KW - Processing PY - 2018 DO - https://doi.org/10.1063/1.5031528 VL - 1949 SP - 030005-1 EP - 030005-7 AN - OPUS4-47217 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Beckmann, Jörg A1 - Spranger, Holger A1 - Ewert, Uwe T1 - THz Applications for Non-Destructive Testing N2 - Up to now THz-TDS-systems aren’t considered to be nondestructive testing facilities for large scale industrial applications, despite it was proven that they provide a comprehensive set of quality parameters. A practical approach to bring THz-TDS in addition to already existing testing systems into the industrial mainstream is systematic development of future test procedures and test facilities for dielectrics. For this purpose polyeth-ylene test specimen with introduced artefacts were designed, to evaluate the detection sensitivity of Time of Flight measurements based on dielectrics. SAFT reconstructed tomograms are presented which visualize the sizes and location of artificially introduced flaws. T2 - 2017 Far East NDT New Technology & Application Forum (FENDT) CY - XI'an, China DA - 22.06.2017 KW - THz radiation KW - Dielectric materials KW - Image reconstruction KW - Terahertz synthetic aperture PY - 2018 DO - https://doi.org/10.1109/FENDT.2017.8584511 VL - 12 SP - 272 EP - 276 PB - IEEE Conference Publication CY - USA AN - OPUS4-47220 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Feldkamp, Martin A1 - Quercetti, Thomas A1 - Wille, Frank T1 - Fire reference test for IAEA package thermal testing in a propane gas fire test facility N2 - Packages for the transport of radioactive material shall withstand severe accidents. Therefore, the IAEA Regulations define different test scenarios to cover severe hypothetical accident conditions. One of these tests defined in detail is the thermal test, mainly consisting of a 30 minute fully engulfing 800 °C pool fire or an equally severe fire test. The heat fluxes into the package are of significant importance and depend substantially on the fire characteristics and the surface temperature of the package. In order to investigate the heat fluxes over a wide range of surface temperatures during a propane gas fire test and to get information about local fire impact a fire reference package, representing the outer geometry of a specific type of transport cask for radioactive waste, was designed. A closed steel sheet cylinder with a wall thickness of 10 mm was chosen as fire reference package. The cylinder was filled with refractory insulation material and instrumented with thermocouples distributed all over the cylinder. The local steel sheet temperatures measured allow the determination of local as well as global heat fluxes as a function of time and surface temperature. With this fire reference package three open-air propane gas fire tests were performed at BAM’s open air fire test stand. The flame exposure time period was changed for the different fire tests. Furthermore, the wind conditions changed between and during the tests. Test stand parameters like wind shield location and propane gas volume flow were chosen constant for the three tests. The test results were used to determine the changes of heat flux into the fire reference package in relation to the package surface temperature. This data also allows the calculation of local characteristics of the propane gas fire as there are the flame temperature, the fire convection coefficient and the radiation exchange coefficient in a first approach. The recently conducted tests provide an initial picture of local fire characteristics of the propane gas fire test facility. The test shows that the propane gas fire covers the IAEA-fire over a wide range of surface temperatures with the chosen test stand parameters. T2 - 19th International Symposium on the Packaging and Transportation of Radioactive Materials PATRAM 2019 CY - New Orleans, LA, USA DA - 04.08.2019 KW - Fire test KW - Propane gas KW - Calorimetric test KW - IAEA fire testing PY - 2019 SP - Paper 1141, 1 EP - 10 AN - OPUS4-48840 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Palkowski, Carsten A1 - von Schwarzenberg, Stefan A1 - Simo, Anne T1 - Dynamic testing to better reflect real use for the seasonal performance of air conditioners N2 - In this contribution, a dynamic test method to determine the seasonal performance of invertertype air conditioners has been developed and verified. In comparison to current test standards, where test modes for fixing the compressor speed are required, a dynamic approach is applied with unfixed compressor speed and thus better reflects the performance of air conditioners under real operating conditions. The dynamic tests are conducted in two calorimeter chambers. The indoor chamber is kept at a constant temperature whereas the outdoor chamber is subjected to a temperature profile based on the climate BIN-distribution, representing the reference cooling demand. The proposed dynamic test considers the dynamic control of an air conditioner and delivers results which could indicate the units' performance in the field. T2 - 25th International Congress of Refrigeration 2019 CY - Montréal, Canada DA - 25.09.2019 KW - Seasonal Performance Factor KW - Inverter-type Air Conditioner KW - Dynamic Test Method KW - Real Use Behavior PY - 2019 SN - 978-2-36215-035-7 SN - 1025-9031 SP - 672, 3891 EP - 3899 PB - International Institute of Refrigeration IIR CY - Paris AN - OPUS4-48865 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zencker, Uwe A1 - Simbruner, Kai A1 - Völzke, Holger T1 - Brittle failure of spent fuel claddings under long-term dry interim storage conditions – Preliminary analysis N2 - The evaluation of cladding integrity is a major issue to be demonstrated in Germany for extended interim storage periods up to 100 years and subsequent transportation considering operational and accidental conditions with respect to reactor operation, cask drying and dry interim storage. The chemical reaction between the zirconium fuel cladding and the cooling water in water-cooled reactors produces hydrogen and zirconium oxide. Hydrogen diffuses into the cladding and precipitates as zirconium hydrides when the solubility limit is reached, preferably oriented in hoop direction. At high temperatures during vacuum drying procedures, the hydrides can dissolve. Over a succeeding period of slow cooling with existing hoop stress the hydrides precipitate again, but partly reoriented along the radial direction of the cladding. This change of microstructure in combination with a decreasing temperature (0.5...2 K/year) during (extended) interim storage and additional mechanical load by handling procedures or under accident conditions could lead to a potential cladding embrittlement and consequently increased failure probability. The current research project BRUZL (Fracture mechanical analysis of spent fuel claddings under long-term dry interim storage conditions) has been launched by BAM to investigate potential sudden brittle failure of spent fuel claddings at small deformation under long-term dry interim storage conditions and is presented. T2 - IAEA International Conference on the Management of Spent Fuel from Nuclear Power Reactors CY - Vienna, Austria DA - 24.06.2019 KW - Ageing Management KW - Cladding Embrittlement KW - Extended Storage KW - Ring Compression Test KW - Spent Nuclear Fuel PY - 2019 SP - Paper IAEA-CN-272/49, 1 EP - 8 AN - OPUS4-48869 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schönfelder, Thorsten A1 - Müller, Lars A1 - Komann, Steffen A1 - Wille, Frank ED - Schönfelder, Thorsten T1 - Design assessment of a dual purpose cask for damaged spent nuclear fuel N2 - German package design approvals were granted recently for dual purpose casks (DPC) intended for loading with encapsulated damaged spent nuclear fuel (DSNF). Comprehensive assessment procedures were carried out by the authority BAM with respect to the mechanical and thermal package design, the activity release of radioactive material and quality assurance aspects for manufacturing and operation of each packaging. The objective of each procedure was to verify the Package Design Safety Report (PDSR) and the relevant guidelines fulfils the requirements of the IAEA regulations. Previous approvals of German SNF package designs consider mainly standard fuel assemblies with defined specifications and properties for transport and interim storage. Due to the nuclear power phase-out in Germany all kinds of SNF, e.g. damaged spent fuel rods shall be packed in DPC now. Therefore specific requirements shall be considered in accordance with international experiences including IAEA technical reports. The main requirement for DSNF is a tight encapsulation with specific defined properties under transport and storage conditions. Due to the interim storage period of currently up to 40 years the encapsulation with DSNF in the casks shall also be long term durable. Thus specific loading and drying procedures are necessary and had to be qualified during the approval process. BAM assessed these drying procedures and could confirm the long-term behaviour of the encapsulation and the suitability of the drying equipment. This special equipment was qualified in a “cold handling”. In addition, it was shown that the behaviour of the test equipment used in the qualification process was comparable with the original equipment, e.g. test fuel rods or test encapsulation. In the development of the drying process, experience was obtained in how to put the requirements of the IAEA regulations and related IAEA technical reports into practice. The paper gives an overview of approval assessment and testing experience made by BAM and point out the main resulting requirements on drying processes for these kinds of encapsulations with DSNF. T2 - Proceedings of the 19th International Symposium on the Packaging and Transportation of Radioactive Materials PATRAM 2019 CY - New Orleans, USA DA - 04.08.2019 KW - Assessment KW - Dual purpose cask KW - Spent nuclear fuel PY - 2019 SP - Paper 1204, 1 EP - 10 AN - OPUS4-48685 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Niederleithinger, Ernst A1 - Abraham, Odile A1 - Larose, Eric T1 - A review on ultrasonic monitoring of concrete: coda wave interferometry and beyond N2 - The propagation of ultrasonic waves in concrete is affected by its micro- and macro-structure, geometry and properties as well as external influences as stress, temperature or moisture. In addition, age and degradation have a strong influence. Therefore, Ultrasound has been used to monitor concrete samples and structures since decades. However, early applications using conventional techniques as time-of flight or changes in amplitudes have been limited to detect changes in a late stage close to serviceability or ultimate load states. Around 2000, several new, more sensitive techniques adopted from geophysics or other field of material sciences have been introduced to research in ultrasonic monitoring of concrete. The most discussed methodologies are coda wave interferometry, a technique which allows to detect very subtle changes from repeated ultrasonic measurements. Nonlinear acoustic techniques help to identify e. g. cracks even in an inhomogeneous background. Both techniques can be combined. This paper reviews methods and results achieved so far on the laboratory scale and with full scale models the directions for future research and application is given as well. T2 - QNDE 2019 CY - Portland, OR, USA DA - 14.07.2019 KW - Ultrasound KW - Coda wave interferometry KW - Concrete KW - Nonlinear KW - Monitoring PY - 2019 SP - Paper 1234 AN - OPUS4-48686 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lugovtsova, Yevgeniya A1 - Johannesmann, S. A1 - Henning, B. A1 - Prager, Jens T1 - Analysis of Lamb wave mode repulsion and its implications to the characterisation of adhesive bonding strength N2 - Lamb waves are widely used for non-destructive evaluation of material parameters as well as for detection of defects. Another application of Lamb waves is quality control of adhesive joints. Researchers are currently investigating shear horizontal and zero-group velocity modes for characterisation of the adhesive bonding strength. In a new approach, Lamb wave mode repulsion is used to obtain the coupling strength between different layers to characterise the adhesive bonding strength. The modes of the individual layers become coupled in the multilayered systems forming particular regions, the so-called mode repulsion regions. This study investigates these modes and their interaction in two-layered plate-like structures with varying coupling strength both numerically, with the Scaled Boundary FEM, and experimentally T2 - International Congress on Ultrasonics CY - Bruges, Belgium DA - 03.09.2019 KW - Lamb waves KW - Multi-layered system KW - Adhesive joint KW - Mechanical strength KW - Scaled Boundary FEM PY - 2019 SP - 1 EP - 4 AN - OPUS4-48911 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zencker, Uwe A1 - Qiao, Linan A1 - Völzke, Holger T1 - Fracture mechanical analysis of a cylindrical cast iron cask N2 - The safety evaluation of cask components made of ductile cast iron includes investigations to prevent brittle fracture. Generally, ductile cast iron is endangered by brittle fracture especially at low temperatures (down to -40°C) and in combination with existing crack-like material defects. An applicable method is the assessment of fracture resistance using fracture mechanics according to the IAEA guidelines. The approach is based on the prevention of fracture initiation. For application of these principles for drop loads, account must be taken both of dynamic stresses within the component and dynamic material behavior. Basically, the dynamic stress intensity factor of postulated pre-existing crack-like defects is compared with the dynamic fracture toughness of the material. Applicable numerical and experimental methods for the safety assessment of cask components are demonstrated for the case of an artificially pre-cracked cylindrical cast iron cask which undergoes dynamic loading conditions as result of the hard impact between the cask and a concrete target. The proposed evaluation procedure is a combination of numerical and experimental steps. Exemplarily, the calculated stress intensity factor is compared with measured fracture toughness values from single edge notched bending specimens. T2 - 19th International Symposium on the Packaging and Transportation of Radioactive Materials (PATRAM 2019) CY - New Orleans, LA, USA DA - 04.08.2019 KW - Ductile Cast Iron KW - Brittle Fracture KW - Cylindrical Cask PY - 2019 SP - Paper 1209, 1 EP - 7 AN - OPUS4-48914 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Winkler, Nicolas P. A1 - Neumann, Patrick P. A1 - Hüllmann, Dino A1 - Kohlhoff, Harald A1 - Bartholmai, Matthias A1 - Bennetts, V. H. A1 - Lilienthal, A. J. T1 - Remote Gas Sensing with Multicopter-Platforms N2 - This presentation gives an introduction to the gas-sensitive aerial robots developed at BAM, including various application examples in the field of mobile robot olfaction: gas source localization and gas distribution mapping. T2 - Zweites Innovationsforum "Autonome, mobile Dienste; Services für Mobilität" CY - Berlin, Germany DA - 04.06.2019 KW - Tunable Diode Laser Absorption Spectroscopy (TDLAS); UAV-REGAS KW - Localization of gas sources KW - Mobile Robot Olfaction KW - Nano UAV Swarm KW - Tomographic reconstruction of gas plumes PY - 2019 UR - http://modisem.de/files/Ereignisse/2019-06/Innovationsforum_Downloads/IF2_2019_Tagungsband_WEB.pdf SN - 978-3-942709-22-4 N1 - Tagungsband auf Deutsch, Beitrag auf Englisch. VL - 2019 SP - 24 EP - 34 AN - OPUS4-48699 LA - mul AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wasmer, Paul A1 - Bulling, Jannis A1 - Prager, Jens T1 - Ultrasonic sensor based on phononic crystals N2 - An essential task in many industries, e.g. food, petrol or chemical industry, is the precise and accurate characterization of liquids. Therefore, the development of innovative in-line sensors is of great interest. New concepts based on periodic structures, so-called phononic crystals (PnCs), are an interesting idea for the design of innovative sensors. A PnC-based sensor can be designed by introducing a resonance inside a bandgap, a frequency region where no wave propagation is allowed. High-Q measurement systems using PnCs are already reported in the literature. However, existing designs cannot be implemented into a piping system directly, but need special fittings, openings or by-passes to be in contact with the liquid. To circumvent this issue, we develop a new sensor based on PnCs, which can be directly implemented as part of the piping system. For this purpose, we use a PnC consisting of hollow cylinders with a periodic change of the outer diameter. A bandgap could be found for the described geometry without fluid in simulation and measurement. However, simulations show, that a bandgap for fluid-filled cylinders can only be obtained for quasi-longitudinal modes. Hence, we propose a mode selective excitation for the sensor. T2 - ICA 2019 CY - Aachen, Germany DA - 09.09.2019 KW - Phononic crystal KW - Ultrasound PY - 2019 SN - 978-3-939296-15-7 SN - 2226-7808 SN - 2415-1599 SP - 969 EP - 976 AN - OPUS4-48860 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rockenhäuser, Christian A1 - von Hartrott, P. A1 - Metzger, M. A1 - Skrotzki, Birgit T1 - Digital material representation of precipitation coarsening in alloy 2618A for the lifetime assessment of radial compressor wheels N2 - The concept of digital material representation is introduced and the aluminium alloy 2618A is discussed as an example of this concept regarding the simulation of material ageing based on nanoscaled precipitates. T2 - Microscopy Conference 2019 (MC2019) CY - Berlin, Germany DA - 01.09.2019 KW - Alloy 2618A KW - Aluminium KW - Digital material representation KW - Transmission electron microscopy KW - Material degradation PY - 2019 SP - 183 EP - 184 AN - OPUS4-48885 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Auersch, Lutz ED - Lombaert, G. ED - Degrande, G. T1 - Predicted and measured amplitude-speed relations of railway ground vibrations at four German sites with different test trains N2 - The present contribution evaluates four measuring series made by the Federal Institute of Material Research and Testing for the relations between train speed and ground vibration amplitudes. This experimental evaluation is supported by the simulation of the train passages at the different sites by using appropriate excitation mechanisms and forces as well as layered soil models which have been derived from impact measurements at each site. T2 - 13th International Workshop on Railway Noise and Vibration CY - Leuven, Belgium DA - 16.09.2019 KW - Train speed KW - Ground vibration KW - Excitation forces KW - Layered soils PY - 2019 SP - 1 EP - 8 PB - KU Leuven CY - Leuven AN - OPUS4-49440 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Auersch, Lutz ED - Adam, C. T1 - Bahnerschütterungen bei verschiedenen Böden und Zuggeschwindigkeiten – Messungen in Deutschland, Österreich und der Schweiz N2 - Die Bundesanstalt für Materialforschung und -prüfung hat in den letzten 30 Jahren an vielen Orten Bahnerschütterungen gemessen. Dabei wurden immer auch Versuche zur Bestimmung der Bodeneigen-schaften durchgeführt, meist mit Hammeranregung, gelegentlich auch mit Schwingeranregung. Es werden verschiedene Auswertemethoden wie Seismogramm-Montage, Spektrale Analyse (SASW), Multistation Analysis of Surface Waves (MASW), f,v-Analyse (Dispersion aus zweifacher Fourier-Analyse), Spatial AutoCorrelation (SPAC, hier auch für deterministische Quellen) vorgestellt. Durch Approximation der frequenzabhängigen Wellengeschwindigkeiten (Dispersion) oder der gemessenen Übertragungsfunktionen erhält man ein passendes Bodenmodell. Zu diesem Bodenmodell kann man dann die Übertragungsfunktionen für Hammer- und Zuganregung berechnen. Mit allgemeinen oder spezifischen Achslastspektren werden dann die Bahnerschütterungen prognostiziert und mit den Messergebnissen verglichen. Bei etlichen Messorten, insbesondere in der Schweiz, wurden deutliche Merkmale einer Bodenschichtung beobachtet. Es ergibt sich eine deutliche Reduktion der tiefen Frequenzanteile durch den steifen unterliegenden Halbraum. Die weiche Deckschicht bestimmt das hochfrequente Verhalten. Hier bewirkt die Materialdämpfung des Bodens oft einen starken Amplitudenabfall, sowohl mit der Entfernung als auch mit der Frequenz. Für den verbleibenden mittelfrequenten Anteil wurde an mehreren Messorten die Amplituden-Fahrgeschwindigkeits-Gesetzmäßigkeiten untersucht. Es gibt konstante bis stark ansteigende Amplituden, und es zeigt sich auch hier, dass der geschichtete Boden von entscheidender Bedeutung ist. T2 - 16. D-A-CH Tagung Erdbebeningenieurwesen & Baudynamik (D-A-CH 2019) CY - Innsbruck, Austria DA - 26.09.2019 KW - Wellengeschwindigkeit KW - Dispersionsmessung KW - Bodenübertragungsfunktion KW - Bahnerschütterungen KW - Zuggeschwindigkeit PY - 2019 SP - 1 EP - 8 PB - Universität Innsbruck CY - Innsbruck AN - OPUS4-49441 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ramirez Caro, Alejandra A1 - Pauli, Jutta A1 - Mota, Berta A1 - Crasselt, Claudia A1 - Artemeva, Elena A1 - Schmidt, Wolfram A1 - Resch-Genger, Ute T1 - A Spectroscopic Study of the Superplasticizer Effect on Early Cement Hydration N2 - Organic/inorganic mixtures were prepared from ordinary Portland cement (OPC), water (w/c 0.22), a fluorescent dye in aqueous solution (stable at alkaline pH; BAM-I), and two different comb shape polycarboxylates (PCEs), i.e., high charge (PCE-HC) and low charge (PCE-LC), respectively. Rheological and calorimetric measurements were performed prior to optical studies in order to select PCE concentrations. Absorption and fluorescence spectroscopy of the system OPC + BAM-I (CBAM-I) revealed maxima of dye BAM-I located at 645 nm and 663 nm, respectively. In presence of PCE-HC and PCE-LC, these mixtures displayed a small red shift in reflectance and a faster decrease in intensity compared to studies with CBAM-I; however, only slight differences were observed between the different PCEs. With time, all systems exhibited a decrease in intensity of BAM-I in absorption/reflectance and emission. This could be caused by dye adsorption and possibly decomposition when in contact with cement particles or hydration products. T2 - The Sixth International Symposium on Nanotechnology in Construction (NICOM6) CY - Hong Kong, China DA - 02.12.2018 KW - Cement KW - Optical Spectroscopy KW - Dye KW - Hydration PY - 2018 SP - 1 EP - 9 AN - OPUS4-49378 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bresch, Harald A1 - Schmidt, Alexandra A1 - Bachmann, V. A1 - Kämpf, K. A1 - Kuhlbusch, T. A1 - Schwirn, K. A1 - Völker, D. ED - Bosse, H. ED - Buhr, E. ED - Dziomba, T. ED - Hodoroaba, Vasile-Dan ED - Klein, T. ED - Krumrey, M. T1 - OECD Test Guideline on particle size and size distribution of manufactured nanomaterials N2 - The properties of nanomaterials are influenced not only by their chemical composition but also by physical properties (such as size, geometry and crystal structure). For the reliable determination and assessment of behaviour and effects of nanomaterials as well as for the determination of the exposure of humans and environment a comprehensive physical-chemical characterization of nanomaterials is essential. This is an important prerequisite to identify them as nanomaterials and to interpret and compare test results and - in future – to forecast interaction and effects of nanomaterials. In 2006, the OECD launched a sponsorship program for the testing of nanomaterials in which 11 nanomaterials were thoroughly investigated using a variety of methods. The aim of the project was, among other things, to find out where problems occur and where there are gaps in the measurement and test procedures and where are changes required. An important outcome of the sponsorship program was the finding that the OECD Test Guidelines should in several cases be extended to the specific needs in testing of nanomaterials. The existing standardized test methods of the OECD for physical-chemical characterization have not been developed for nanomaterials in particular. A high demand for an extension of the test guidelines was identified. Germany complied with the OECD's request in 2017 and has agreed to extend the “Test Guideline on Particle Size Distribution / Fiber Length and Diameter Distributions Test Guideline” for Manufactured Nanomaterials (MN). UBA commissioned BAM and BAuA with the preparation of the Test Guideline. The aim of the project is the development of a harmonized test protocol for a valid and reproducible determination of particle size and size distribution which is one of the most relevant physical-chemical properties for MNs. Different measuring methods provide different results for the size distribution of the particles. This is caused by the different measuring principles of the methods. Each method measures a specific parameter that ultimately determines particle size. First, the measured quantity differs for each method (Scattered light intensity, 2D image / projection, electric mobility, etc.). Second, the calculated diameters of the MN may differ (Feret Diameter, Area Projection, Mobility Diameter, Aerodynamic Diameter, Hydrodynamic Diameter). Third, a measuring method provides a size distribution which is measured either mass-based, surface-based or number-based. A conversion between the results requires additional parameters and thus possibly increases the measurement error. In addition to the technical differences, the individual parameters are strongly influenced by the structure and material of the nanoparticles. For example, a surface functionalization can lead to very different results in the size distribution. The suitability of measurement methods differs with the material of the MN. As a result, two very different results can be measured for the particle size distribution using two different methods, which are nevertheless both correct. Several large projects in recent years therefore concluded that nanomaterials should be characterized by at least two complementary method. Imaging techniques are regarded as one of these methods for the characterization, the complementary methods are supposed to be statistical methods. The different results for the size distribution of nanomaterials become problematic for the registration of new MN. A comparable and reproducible size distribution is a prerequisite for a standardized registration. In the future, the particle size distribution in the EU will also decide on the classification of a substance as a nanomaterial or as a non-nanomaterial. Especially in borderline cases, a standardized and comparable measurement methodology is therefore essential. T2 - NanoWorkshop 2018: Workshop on Reference Nanomaterials CY - Berlin, Germany DA - 14.05.2018 KW - OECD KW - Guideline KW - Particle size distribution KW - Nano KW - Prüfrichtlinie PY - 2019 SN - 978-3-95606-440-1 DO - https://doi.org/10.7795/110.20190412 SN - 0179-0609 VL - F-61 SP - 125 EP - 132 PB - Physikalisch-Technische Bundesanstalt CY - Braunschweig und Berlin AN - OPUS4-49511 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kämpf, K. A1 - Bachmann, V. A1 - Bresch, Harald A1 - Schmidt, Alexandra A1 - Kuhlbusch, T. A1 - Schwirn, K. A1 - Völker, D. ED - Bosse, H. ED - Buhr, E. ED - Dziomba, T. ED - Hodoroaba, Vasile-Dan ED - Klein, T. ED - Krumrey, M. T1 - OECD Test Guideline on particle size and particle size distribution of manufactured nanomaterials: simultaneous measurement of length and diameter of fibers N2 - The new OECD test guideline will address the following four main steps in the determination of the length and width distributions of fibers: sample preparation, image acquisition, data evaluation and uncertainty analysis. As the sample preparation has to be optimized for each material, general quality criteria will be given in the protocol. For full visibility of a fiber the appropriate resolution has to be chosen. In the data evaluation the length and diameter of each fiber will be determined concurrently to allow for application of different regulatory definitions. The quality of the results critically depends on the sample preparation as well as the data evaluation. In this step the classification rules have to be formulated and followed accurately in order to optimize reproducibility of the method. The SOP will be validated in an international round robin test, which is planned for 2018/2019. T2 - NanoWorkshop 2018: Workshop on Reference Nanomaterials CY - Berlin, Germany DA - 14.05.2018 KW - OECD KW - Nano KW - Guideline KW - Particle size distributuion KW - Prüfrichtlinie PY - 2019 SN - 978-3-95606-440-1 DO - https://doi.org/10.7795/110.20190412 SN - 0179-0609 VL - F-61 SP - 302 EP - 302 PB - Physikalisch-Technische Bundesanstalt CY - Braunschweig und Berlin AN - OPUS4-49514 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schwirn, K. A1 - Völker, D. A1 - Ahtianinen, J. A1 - Schmidt, Alexandra A1 - Bresch, Harald A1 - Kämpf, K. A1 - Bachmann, V. A1 - Kuhlbusch, T. ED - Bosse, H. ED - Buhr, E. ED - Dziomba, T. ED - Hodoroaba, Vasile-Dan ED - Klein, T. ED - Krumrey, M. T1 - OECD Test Guidelines development for chemicals safety assessment of nanomaterials N2 - The OECD test guidelines (TGs) for testing chemicals have been widely used for regulatory purposes all over the world since the establishment of the Mutual Acceptance of Data (MAD) principle in 1984. This MAD principle ensures that, if a chemical is tested under the Good Laboratory Practice (GLP) conditions accordingly to an OECD TG, the data should be accepted in all OECD countries. The TGs have been developed, harmonized, internationally validated (round robin tests) and adopted by OECD countries to be used for the physical-chemical characterisation, fate estimation, and hazard identification for risk assessment of various chemicals. In addition to the TGs, OECD Guidance Documents (GDs) usually provide guidance on how to use TGs and how to interpret the results. These GDs do not have to be fully experimentally validated, and hence they are not under MAD, but they are based on relevant published scientific research. But are the existing TGs and the related GDs applicable and adequate for the regulatory testing of nanomaterials? In general, for nanomaterials it is accepted that most of the "endpoints" or more precisely measurement variables are applicable. However, for some endpoints new or amended TGs are needed. In addition, several GDs are needed to give more precise advice on the test performance in order to gain regulatory relevant data on nanomaterials. T2 - NanoWorkshop 2018: Workshop on Reference Nanomaterials CY - Berlin, Germany DA - 14.05.2018 KW - OECD KW - Nano KW - Guideline KW - Nanomaterials KW - Prüfrichtlinie PY - 2019 SN - 978-3-95606-440-1 DO - https://doi.org/10.7795/110.20190412 SN - 0179-0609 VL - F-61 SP - 279 EP - 279 PB - Physikalisch-Technische Bundesanstalt CY - Braunschweig und Berlin AN - OPUS4-49515 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kasch, Thomas A1 - Woitzek, Andreas T1 - Beurteilungsmöglichkeiten nichtmetallischer Materialien für den Einsatz in Sauerstoff N2 - Nichtmetallische Materialien dürfen generell als Gleitmittel, Dichtungsmaterialien, Flanschdichtungen und Füllflüssigkeiten nur dann in Sauerstoffanwendungen eingesetzt werden, wenn sie sicherheitstechnisch für die entsprechenden Betriebsbedingungen geeignet sind. Genormte Prüfverfahren sowie weitere Untersuchungsmöglichkeiten wie die Sauerstoff- Druckstoßprüfung, die Bestimmung der Zündtemperatur in verdichtetem Sauerstoff, die Untersuchung des Alterungsverhaltens, die Flanschprüfung sowie die Prüfung des Reaktionsverhaltens des Materials mit flüssigem Sauerstoff bei mechanischer Einwirkung sollen dies gewährleisten und können auch bei der BAM durchgeführt werden. Die vorhandenen Prüfungen und Beurteilungskriterien verursachen jedoch manchmal Probleme, wenn es um die Übertragbarkeit auf die tatsächliche, praktische Anwendung oder um die Interpretation von Prüfergebnissen geht. Der Vortrag stellt diesbezüglich die BAM- Sicherheitsphilosophie vor. T2 - Deutsche Industriearmaturen Messe & Fachmesse für Dichtungstechnik CY - Bochum, Germany DA - 09.10.2019 KW - Beurteilungskriterien KW - Sauerstoff KW - Prüfverfahren KW - Untersuchungsmöglichkeiten der BAM, Chargenprüfung PY - 2019 SP - 33 EP - 37 PB - Vulkan-Verlag GmbH CY - Essen AN - OPUS4-49523 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Nerger, Deborah A1 - Hille, Falk A1 - Moosavi, Robabeh A1 - Grunwald, Marcel A1 - Redmer, Bernhard A1 - Kühn, T. A1 - Hering, M. A1 - Bracklow, F. T1 - Improved tomographic investigation for impact damage characterization N2 - Reinforced concrete (RC) is used as structural material in most diverse civil engineering applications. For the variability of its physical properties it is still an engineering challenge to meet all necessary requirements for the prediction of dynamic effects under impact loading. In this paper, investigations are shown within the scope of quantifying and evaluating the damage caused by an impact. The experimental investigations are performed in the field of low- and medium-velocity impact. The chosen flat nose shape results in small penetrations on the top side and scabbing on the bottom side. The plate is scanned with an adapted planar tomographic examination after the impact, and the damage is analysed, afterwards. Cracks and spalling are made visible with a reconstruction. The numerical model validated on the tomographic results justifies the application for further predictions of the damage description. T2 - 25th International Conference on Structural Mechanics in Reactor Technology - SMIRT25 CY - Charlotte, NC, USA DA - 04.08.2019 KW - Impact KW - Damage characterization KW - Planar tomography KW - Numeric simulation KW - Reinforced concrete structure PY - 2019 SP - Paper Div 5 S8, 1 EP - 9 AN - OPUS4-49541 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Askar, Enis A1 - Schröder, Volkmar A1 - Göpfert, T. A1 - Winterleitner, E. A1 - Schwarze, M. T1 - Safety related properties of low-GWP refrigerants N2 - Most fluorinated hydrocarbons that shall replace refrigerants with high GWP, like R134a, are flammable. For evaluating inertization measures for explosion protection, flammability of low-GWP refrigerants R1234yf, R32 and R1132a blended with carbon dioxide, nitrogen and argon were studied experimentally in a closed autoclave at atmospheric conditions. Furthermore, a calculation method was adapted to reduce the experimental costs for flammability studies on these gas mixtures. For igniting R1234yf in the closed autoclave a newly developed ignition system was used that allows generating electric arcs with high ignition energy. Gas mixtures containing the mildly flammable R1234yf and R32 could be inerted by adding much less inert gas than mixtures containing R1132a, which is more similar to unfluorinated hydrocarbons regarding the explosion regions. By using the adapted model of constant adiabatic flame temperature profiles estimating the explosion limits of fluorinated hydrocarbons was possible with similar accuracy as for unfluorinated hydrocarbons. Keywords: Explosion Protection, Inertization, Flammability, HFOs, HFC., R1234yf, R32, R1132a T2 - 25th IIR Internationa Congress of Refrigeration CY - Montreal, Canada DA - 24.08.2019 KW - Explosion Protection KW - Inertization KW - Flammability KW - HFOs KW - R1234yf KW - R1132a KW - R32 KW - HFC PY - 2019 SN - 978-2-36215-035-7 DO - https://doi.org/10.18462/iir.icr.2019.0767 SN - 1025-9031 SP - 1 EP - 9 AN - OPUS4-49546 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Krietsch, Arne A1 - Dufaud, O. A1 - Santandrea, A. A1 - Vignes, A. A1 - Perrin, L. A1 - Laurent, A. T1 - Some keys considerations when evaluating explosion severity of nanopowders N2 - Protection from explosion events requires the determination of key safety parameters like lower explosion limit. maximum Explosion over-pressure. and maximum rate of pressure rise. These Parameters are routinely obtained through standard tests performed typically either in a 20 L -sphere or a 1 m3-container. But several aspects are worth a closer investigation. Firstly, the test apparatus must be able to disperse a fairly uniform dust cloud. However. previous investigations showed that actually the current dispersion System can be improved. Secondly, the influence of humidity on the explosivity is not considered in current standards. lt is just stated that the relative humidity should be checked and noted down. though some provisions exist in American standards. Thirdly. the ignition delay time is sometimes modified to study the impact of the dust cloud turbulence on flame propagation but is often misunderstood. Maybe these aspects have not been thoroughly considered for micron powders. However. in the case of nanopowders. the importance of these influencing factors was shown in order to duly evaluate explosion parameters. Experimental evidences confirm these aspects and alternative solutions will be presented. T2 - Loss Prevention Symposium 2019 CY - Delft, Netherlands DA - 16.06.2019 KW - Nanopowders KW - Dust explosion KW - Safety characteristics PY - 2019 SN - 978-88-95608-72-3 SN - 2283-9216 VL - 75 SP - 1 EP - 6 PB - AIDIC AN - OPUS4-49547 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hüllmann, Dino A1 - Neumann, Patrick P. A1 - Scheuschner, Nils A1 - Bartholmai, Matthias A1 - Lilienthal, A.J. T1 - Experimental Validation of the Cone-Shaped Remote Gas Sensor Model N2 - Remote gas sensors mounted on mobile robots enable the mapping of gas distributions in large or hardly accessible areas. A challenging task, however, is the generation of threedimensional distribution maps from these gas measurements. Suitable reconstruction algorithms can be adapted, for instance, from the field of computed tomography (CT), but both their performance and strategies for selecting optimal measuring poses must be evaluated. For this purpose simulations are used, since, in contrast to field tests, they allow repeatable conditions. Although several simulation tools exist, they lack realistic models of remote gas sensors. Recently, we introduced a model for a Tunable Diode Laser Absorption Spectroscopy (TDLAS) gas sensor taking into account the conical shape of its laser beam. However, the novel model has not yet been validated with experiments. In this paper, we compare our model with a real sensor device and show that the assumptions made hold. T2 - IEEE Sensors 2019 CY - Montreal, Canada DA - 27.10.2019 KW - Remote gas sensor model KW - TDLAS KW - Gas dispersion simulation PY - 2019 SN - 978-1-7281-1634-1 SP - 104 EP - 107 PB - IEEE AN - OPUS4-49548 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Otremba, Frank A1 - Romero-Navarrete, José A. ED - Otremba, Frank ED - Romero-Navarrete, José A. T1 - Sloshing in Vertical Circular Tanks and Earthquakes Perturbations N2 - A simplified formulation is proposed in this paper to assess the proximity of the earthquake-related Perturbation frequencies to the natural sloshing frequencies of the liquid contained in vertical cylindrical tanks. The methodology is based upon an existing gravity-waves approach, which was developed for rectangular cross-section reservoirs, and is extended in this paper to analyze circular cross-section tanks. The experimental outputs of this paper show that the existing methodology correlates at 100% with experimental data in the case of rectangular containers; while the corresponding average error in the case of a conical container and a cylindrical container is 7% and 9.1 %, respectively. The full diameter of the cross section was considered. The use of sovalidated methodology to full scale tanks, suggests that cylindrical vertical tanks with a capacity lower than 700 m3, could be exposed to a resonance excitation when subjected to earthquake motions, regardless of the fill level. T2 - WCECS 2019 CY - San Francisco, CA, USA DA - 22.10.2019 KW - Sloshing KW - Tanks KW - Earthquake KW - Perturbation PY - 2019 SP - 1 EP - 6 PB - IA ENG CY - San Francisco AN - OPUS4-49407 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mohr, Gunther A1 - Seeger, Stefan A1 - Hilgenberg, Kai T1 - Measurement of particle emissions in Laser Powder Bed Fusion (L-PBF) processes and its potential for in-situ process monitoring N2 - Laser Powder Bed Fusion (L-PBF) is a promising additive manufacturing (AM) technology for metal part production especially for complex and lightweight structures or functional designs. In L PBF processes several by-products including welding plume and its condensates, spatter and ejected powder are generated during laser exposure. Investigations of micro- and nano-sized by-products have received little attention in literature. This study focuses on the analysis of particle emissions in L PBF of 316L stainless steel using a scattered light aerosol spectrometer and a fast mobility particle sizer spectrometer during the process which allows for in-situ analysis of particle sizes in the range of 6 nm to 100 µm. A distinct correlation of emission signals to part position can be revealed. In addition, a significant influence of laser scanning vector directions on emission signals is presented. Furthermore, differing powder layer thicknesses can be recognised by deviations in emission signals. T2 - Euro PM 2019 CY - Maastricht, The Netherlands DA - 13.10.2019 KW - Plume KW - Laser Powder Bed Fusion (L-PBF) KW - Additive Manufacturing (AM) KW - Spatter KW - Fume KW - Particle gas emission KW - Aerosol measurements PY - 2019 SP - 1 EP - 7 AN - OPUS4-49388 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Artinov, Antoni A1 - Bachmann, Marcel A1 - Karkhin, Victor A1 - Rethmeier, Michael ED - Sommertisch, C. ED - Enzinger, N. ED - Mayr, P. T1 - A novel approach for calculating the thermal cycle of a laser beam welding process using a stationary CFD model N2 - This work aims to find the thermal cycles during and after fusion welding through simulation by first calculating the resulting local temperature field in the quasi-stationary part of the process. Here complete-penetration keyhole laser beam welding with a laser power of 18 kW on a 15 mm thick slab of a low-alloyed steel at a welding speed of 2 m/min is considered. In order to physically depict the laser material interaction a multi-physics numerical model including the effects of phase transformation, thermo-capillary convection, natural convection and temperature-dependent material properties up to evaporation temperature is developed. It uses a fixed keyhole geometry with a right truncated circular cone shape to introduce the laser beam energy to the workpiece. In a subsequent study, the resulting local temperature field is then used as an equivalent heat source in order to predict the unsteady thermal cycle during and after fusion welding. The translational movement of the laser beam through the workpiece is represented by a moving mesh approach. For the simulation, stationary heat transfer and fluid dynamics are described by a system of strongly coupled partial differential equations. These are solved with the commercial finite element software COMSOL Multiphysics 5.0. The results of the numerical simulation are validated by experiments, where the weld bead shapes and the thermal cycles show good correlation. T2 - 12th International Seminar "Numerical Analysis of Weldability" CY - Graz, Austria DA - 24.09.2018 KW - Equivalent heat source KW - Process simulation KW - Laser beam welding KW - Transient heat transfer KW - Moving mesh PY - 2019 SN - 978-3-85125-616-1 VL - 12 SP - Chapt. VI, 694 EP - 710 PB - Verlag der Technischen Universität Graz AN - OPUS4-48817 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rockenhäuser, Christian A1 - Piesker, Benjamin A1 - Heidl, Daniel A1 - Skrotzki, Birgit T1 - Influence of prestraining on the aging response of an Al-Cu-Li alloy N2 - The influence of prestraining on the aging response of an Al-Cu-Li alloy is investigated by preparation of different strain states (3 %, 4 %, 6 %) of the initial aging state. The Brinell hardness of the subsequently aged samples (up to 60 h aging time) was measured and it was found that the increasing dislocation concentration in the 3 different initial states leads to faster hardness increases and slightly higher maximum hardness. T2 - Microscopy Conference 2019 (MC2019) CY - Berlin, Germany DA - 01.09.2019 KW - Al-Cu-Li alloys KW - hardness KW - coarsening PY - 2019 SP - 186 EP - 187 PB - Deutsche Gesellschaft für Elektronenmikroskopie (DGE) CY - Dresden AN - OPUS4-48918 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hüllmann, Dino A1 - Neumann, Patrick P. A1 - Monroy, J. A1 - Lilienthal, A. J. T1 - A realistic remote gas sensor model for three-dimensional olfaction simulations N2 - Remote gas sensors like those based on the Tunable Diode Laser Absorption Spectroscopy (TDLAS) enable mobile robots to scan huge areas for gas concentrations in reasonable time and are therefore well suited for tasks such as gas emission surveillance and environmental monitoring. A further advantage of remote sensors is that the gas distribution is not disturbed by the sensing platform itself if the measurements are carried out from a sufficient distance, which is particularly interesting when a rotary-wing platform is used. Since there is no possibility to obtain ground truth measurements of gas distributions, simulations are used to develop and evaluate suitable olfaction algorithms. For this purpose several models of in-situ gas sensors have been developed, but models of remote gas sensors are missing. In this paper we present two novel 3D ray-tracer-based TDLAS sensor models. While the first model simplifies the laser beam as a line, the second model takes the conical shape of the beam into account. Using a simulated gas plume, we compare the line model with the cone model in terms of accuracy and computational cost and show that the results generated by the cone model can differ significantly from those of the line model. T2 - 2019 IEEE International Symposium on Olfaction and Electronic Nose (ISOEN) CY - Fukuoka, Japan DA - 26.05.2019 KW - Remote gas sensor KW - Gas detector KW - TDLAS KW - Sensor modelling PY - 2019 SN - 978-1-5386-8327-9 SN - 978-1-5386-8328-6 DO - https://doi.org/10.1109/ISOEN.2019.8823330 SP - 1 EP - 3 PB - IEEE AN - OPUS4-48919 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Neumann, Patrick P. A1 - Hirschberger, Paul A1 - Baurzhan, Zhandos A1 - Tiebe, Carlo A1 - Hofmann, Michael A1 - Hüllmann, Dino A1 - Bartholmai, Matthias T1 - Indoor air quality monitoring using flying nanobots: Design and experimental study N2 - In this paper, we introduce a nano aerial robot swarm for Indoor Air Quality (IAQ) monitoring applications such as occupational health and safety of (industrial) workplaces. The robotic swarm is composed of nano Unmanned Aerial Vehicles (UAVs), based on the Crazyflie 2.0 quadrocopter, and small lightweight Metal Oxide (MOX) gas sensors for measuring the Total Volatile Organic Compound (TVOC), which is a measure for IAQ. An indoor localization and positioning system is used to estimate the absolute 3D position of the swarm similar to GPS. A test scenario was built up to validate and optimize the swarm for the intended applications. Besides calibration of the IAQ sensors, we performed experiments to investigate the influence of the rotor downwash on the gas measurements at different altitudes and compared them with stationary measurements. Moreover, we did a first evaluation of the gas distribution mapping performance. Based on this novel IAQ monitoring concept, new algorithms in the field of Mobile Robot Olfaction (MRO) are planned to be developed exploiting the abilities of an aerial robotic swarm. T2 - 2019 IEEE International Symposium on Olfaction and Electronic Nose (ISOEN) CY - Fukuoka, Japan DA - 26.05.2019 KW - Indoor air quality KW - Nano aerial robot KW - Aerial robot olfaction KW - Swarm KW - Gas detector PY - 2019 SN - 978-1-5386-8327-9 SN - 978-1-5386-8328-6 DO - https://doi.org/10.1109/ISOEN.2019.8823496 SP - 1 EP - 3 PB - IEEE AN - OPUS4-48920 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Widjaja, Martinus Putra A1 - Joannes, S. A1 - Bunsell, A. A1 - Mair, Georg A1 - Thionnet, A. T1 - The Application of a Reduced Volume Method for the Simulation of the Characterisation of a Carbon Fibre Pressure Vessel N2 - The developed model has certain limitations of the element size to be used in the simulation to characterise the strength of composite materials. A reduced volume method is proposed in order to reduce the number of degree of freedom of the finite element simulation.This study has revealed certain configuration to be followed to speed up the computation time. T2 - The 18th European Conference on Composite Materials CY - Athens, Greece DA - 24.06.2018 KW - Composite pressure vessel KW - Fibre break KW - Integral range KW - Representative volume element PY - 2018 SP - 1193-892 AN - OPUS4-48927 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Grelle, Tobias A1 - Probst, Ulrich A1 - Wolff, Dietmar A1 - Jaunich, Matthias A1 - Völzke, Holger T1 - Investigations on the long-term behavior of metal seals for dual purpose casks N2 - In Germany, spent nuclear fuel and high active waste from reprocessing is stored in transport and storage containers with double lid systems that are equipped with metal seals completing the primary sealing barrier. The tasks of the Bundesanstalt für Materialforschung und -prüfung (BAM) within the interim storage licensing procedures ruled by the German Atomic Energy Act include the long-term safety evaluation of the container design regarding the permanently safe enclosure of the inventory. In order to generate a knowledge base for the safety evaluation, research regarding the long-term behavior of the critical components is performed. So far, the containers are licensed for an interim storage period of 40 years. However, due to significant delays in establishing a final repository, the required time span for interim storage is expected to increase significantly. Thus, a widespread investigation program is run to gain systematic data on the long-term behavior of the seals and to develop prediction models. Long-term seal investigations consider the development of their restoring seal force, their useable resilience and their achievable leakage rate caused by aging at temperatures ranging from room temperature up to 150 °C. This year, the total time span of the tests reaches 10 years. Furthermore, seal segments are aged at the selected temperatures for up to 300 days. From these segments additional information on the sealing behavior, changes of the seal contact and the material behavior is gained. This contribution deals with the current results of the long-term seal investigations at BAM. Furthermore, insights of the more in-depth component and material investigations of the metal seals with focus on the seal contact development are discussed and the ongoing work aiming for an analytical description of the thermo-mechanical aging effects on metal seals are presented. T2 - 19th International Symposium on the Packaging and Transportation of Radioactive Materials PATRAM 2019 CY - New Orleans, LA, USA DA - 04.08.2019 KW - Metal seal KW - Radioactive waste containers KW - Creep KW - Long-term behaviour PY - 2019 SP - 1 EP - 6 AN - OPUS4-49019 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Sklorz, Christian A1 - Balke, Christian A1 - Otremba, Frank T1 - Fire protection systems for above-ground storage tanks N2 - Liquefied propane gas (LPG) tanks in a fully engulfing accidental fire experience a fast increase in internal pressure. The result is often a Boiling Liquid Expanding Vapor Explosion (BLEVE) that can result in a large fireball and flying debris over a radius of more than 100 meters. In the last 30 years BAM has carried out more than 30 real scale fire tests on propane storage vessels across three test sites. The primary research goal was to identify systems that can delay or prevent a BLEVE. Early studies started with water deluge systems, and have since moved on to consider alternative protection systems. It has been shown that an unprotected vessel fails within 10 minutes or less. Tests with different oil and propane fueled fires have given an overview on possible real accidents involving full-engulfing scenarios. LPG tanks of various sizes (2.7 m³, 3.6 m³, 4.8 m³, 6.7 m³) were used with different filling levels. Numerous protection systems, ranging from active systems like water systems to passive thick- and thin-film layers. Also, the degree of thickness of these layers was variated. Pressure relief valves (PRV) have also been investigated, both alone and in combination with protection systems. This paper gives an overview of the work performed by BAM in the field of BLEVE prevention of protecting system since the last 30 years. It has been shown that e.g. with a full applied coating degree on the tank with and without PRV can be reached an exposition in a test fire scenario a duration of more than 60min. For partly coated tanks with and without PRV the duration time is like an unprotected vessel. Furthermore, it could be shown that the active water system also protects with technically correct design. T2 - Loss Prevention 2019 CY - Delft, Niederlande DA - 16.06.2019 KW - Fire KW - Protection systems KW - Propane storage tanks PY - 2019 SN - 978-88-95608-72-3 VL - 75 SP - 1 EP - 6 AN - OPUS4-49021 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Torge, Manfred ED - Brion, I. ED - Alloteau, F. ED - Lehuede, P. ED - Majerus, O. ED - Caurant, D. T1 - The effect of particle deposition and climate on glass degradation N2 - Medieval stained-glass windows are protected by an outside gazing system in many churches.The interspace between the original and the protective glass is ventilated with air from the indoor or exterior environment, where dust and particles can move.Cascade impactor measurements and SEM/EDX analyses of sampled dust were carried to determine the dust composition. The effect of particles on model glass samples was investigated in climate chambers under accelerated weathering conditions. The results from in situ measurements and laboratory tests were combined to evaluate the potential effect of particulate matter on historic stained-glass Windows. T2 - International Symposium on Glass Degradation in Atmospheric Conditions CY - Paris, France DA - 15.11.2017 KW - Medieval-stained glass KW - Protective glazing KW - Cascade impector KW - Simulation PY - 2019 SN - 9782705697945 SP - 223 EP - 224 PB - hermann CY - Paris AN - OPUS4-49023 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Le, Quynh Hoa A1 - Bäßler, Ralph A1 - Schiller, B.N. A1 - Beck, M. A1 - Bettge, Dirk T1 - On the corrosion behaviour of co 2 injection pipe steels: role of cement N2 - Carbon Capture and Storage (CCS) is identified as an excellent technology to reach the target of CO2 reduction. However, the safety issue and cost-effectiveness hinder the future of CCS. For the reliability and safety issues of injection wells, the corrosion resistance of the materials used needs to be determined. In this study, representative low-cost materials including carbon steel 1.8977 and low alloyed steel 1.7225 were investigated in simulated pore water at 333 K and under CO2 saturation condition to represent the worst-case scenario: CO2 diffusion and aquifer fluid penetration. These simulated pore waters were made from relevant cement powder to mimic the realistic casing-cement interface. Electrochemical studies were carried out using the pore water made of cement powder dissolved in water in comparison with those dissolved in synthetic aquifer fluid, to reveal the effect of cement as well as formation water on the steel performance. Two commercially available types of cement were investigated: Dyckerhoff Variodur® and Wollastonite. Variodur® is a cement containing high performance binder with ultra-fine blast furnace slag which can be used to produce high acid resistance concrete. On the other hand, Wollastonite is an emerging natural material mainly made of CaSiO3 which can be hardened by converting to CaCO3 during CO2 injection. The results showed the pH-reducing effect of CO2 on the simulated pore water/aquifer (from more than 10 to less than 5) leading to the active corrosion process that happened on both 1.8977 and 1.7225. Electrochemical characterization showed negative free corrosion potential and polarisation curves without passive behaviors. The tested coupons suffered from pitting corrosion, which was confirmed by surface analysis. Interestingly, basing on the pit depth measurements from the tested coupons and the hardness of cement powder, it is suggested that Variodur® performed better than Wollastonite in both aspects. The electrochemical data was compared to that resulted from exposure tests to give a recommendation on material selection for bore-hole construction. T2 - EUROCORR 2019 CY - Sevilla, Spain DA - 09.09.2019 KW - Cement KW - Carbon capture KW - Corrosion and storage (CCUS) technology KW - Utilization KW - Carbon steel KW - Crevice corrosion PY - 2019 SP - Paper 200597, 1 EP - 4 PB - SOCIEMAT CY - Madrid, Spain AN - OPUS4-49109 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bakenecker, A. A1 - Topolniak, Ievgeniia A1 - Lüdtke-Buzug, K. A1 - Pauw, Brian Richard A1 - Buzug, T. T1 - Additive manufacturing of superparamagnetic micro-devices for magnetic actuation N2 - 3D microstructures with sub-micron resolution can be manufactured in additive manner applying multi-photon laser structuring technique. This paper is focused on the incorporation of superparamagnetic iron oxide nanoparticles into the photoresist in order to manufacture micrometer-sized devices featuring a magnetic moment. The aim of the project is to achieve untethered actuation of the presented objects through externally applied magnetic fields. Future medical application scenarios such as drug delivery and tissue engineering are targeted by this research. T2 - Additive Manufacturing Meets Medicine 2019 CY - Lübeck, Germany DA - 12.09.2019 KW - MPI KW - Two-Photon Polymerization KW - Magnetic swimmers KW - MPLS PY - 2019 UR - www.journals.infinite-science.de/ammm DO - https://doi.org/10.18416/AMMM.2019.1909S09T06 SP - 153 EP - 154 PB - Infinite Science Publishing AN - OPUS4-49114 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mirtsch, Mona A1 - Blind, K. ED - Jacobs, K. ED - Morone, P. T1 - Exploring the Diffusion of an ISMS Standard N2 - This paper introduces and discusses the applicability of Web Mining of Firm Websites to explore the Diffusion of Management System Standards using the example of an ISMS Standard. T2 - EURAS Conference CY - Rome, Italy DA - 13.06.2019 KW - Management System Standard KW - Information Security KW - Web Mining PY - 2019 SN - 978-3-95886-282-1 VL - 24 SP - 329 EP - 348 PB - Verlagshaus Mainz GmbH CY - Aachen, Germany AN - OPUS4-49031 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schraut, Katharina A1 - Adamczyk, Burkart A1 - Simon, Sebastian A1 - von Werder, Julia A1 - Meng, Birgit A1 - Stephan, D. A1 - Kargl, F. A1 - Adam, Christian T1 - Formation and chemical stabilisation of tricalcium-silicate during solidification from the melt of post-treated metallurgical slags N2 - Tricalcium-silicate (C3S) or Alite is the most important mineral in Portland cement. Since pure tricalcium-silicate is only stable above temperatures of 1250 °C, its decomposition has to be prevented technically by fast cooling after the sintering process. At room temperature, the decomposition velocity is very slow so that metastable tricalcium-silicate is obtained. Although the mechanisms of clinker phase formation during burning process of Portland cement in a rotary kiln were solved and improved over the years, in view of possible economic and ecological benefits current projects aim to produce clinker phases from metallurgical slags. Recent studies discovered that the mineral phase which remained after a reducing treatment and separation of formed metallic iron from molten Linz-Donawitz (LD-) slags contained about 60 wt.% Alite despite it was cooled slowly. Because the results could be verified using slags from different origins and varying cooling velocities a chemical stabilisation of the Alite can be assumed. First tests in mortars indicate that workability, hardening and solid state properties are comparable with an ordinary Portland cement. An application of the observed phenomenon in cement production requires enhanced knowledge about formation and stabilisation conditions of Alite during crystallisation from melts in contrast to the sintering reactions in conventional Portland cement production. Therefore, this study focuses on the stabilisation mechanisms of Alite in consolidating melts. Samples from different melting experiments are analysed to determine stabilising factors. T2 - 15th International Congress on the Chemistry of Cement CY - Prag, Czech Republic DA - 16.09.2019 KW - Tricalcium-silicate KW - Portland Cement KW - Alite KW - Steelmaking slag PY - 2019 SP - Paper 492, 1 EP - 10 AN - OPUS4-49050 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Müller, Karsten A1 - Quercetti, Thomas A1 - Borch, Jörg-Peter T1 - Fire tests of RAM packages and containers under high thermal load N2 - Fire testing is an essential part of the hypothetical, cumulative mechanical and thermal test conditions that shall guarantee package safety in severe accidents. Within regulatory approval of transport or storage packages for radioactive material, specific thermal load tests are required in accordance to licensing conditions and international standards, respectively. The specifications of these thermal tests are based on test conditions with equivalent heat input to that of a hydrocarbon fuel fire. In the past, light heating oil, diesel or kerosene was mostly used as the fuel to generate the pool fire. In accordance with IAEA regulations for a fire in an accident, the temperature of 800 °C over a period of 30 minutes must be fulfilled. Furthermore, the delivery acceptance criteria for containers in nuclear waste repositories could reach for example average temperatures of 800 °C during a period of one hour in combination with defined requirements on activity release. BAM as a scientific and technical German federal government institute operates an open air Technical Safety Test Site for experimental investigations of dangerous good and its containment. In this areal a large fire test facility is under operation. Liquid Propane is utilized as fuel which is pumped via pipelines from a central storage tank to the fire exposed test facility areas. In the ring burner system, the gas is released from nozzles, and ignited by ignition burners. The paper includes examples of fire test performance with prototypes of a transport package and a storage container, respectively. In preparation of the thermal load, calorimeter tests have been performed using test specimens of appropriate size and behavior. For the fire test scenario is demonstrated that the IAEA thermal test requirements are fulfilled. T2 - 19th International Symposium on the Packaging and Transportation of Radioactive Materials PATRAM 2019 CY - New Orleans, LA, USA DA - 04.08.2019 KW - IAEA Thermal Test KW - Thermal package testing KW - Transport package KW - Container for radioactive waste PY - 2019 SP - Paper 1298, 1 EP - 6 AN - OPUS4-49093 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wille, Frank A1 - Debruyne, M. A1 - Eckert, B. A1 - Gauthier, F. A1 - Ben Ouaghrem, K. A1 - Le Bars, I. A1 - Jouve, A.-C. A1 - Cordier, N. T1 - Assessment of safety demonstrations relative to packages containing UF6 N2 - The safety demonstrations realized by applicants in the case of approval request for the package designs containing enriched UF6 have to take into account some specific technical issues. Concerning the shipment of enriched UF6, the package designs consist in general of a filled 30B cylinder surrounded by an overpack. The description of the content, considering the UF6 origin, i.e. natural or reprocessed, shall be clearly justified especially when the UF6 isotopic composition exceeds the limits specified in ASTM standards. Concerning the containment of the UF6, the applicant shall demonstrate in all conditions of transport the leak-tightness of the valve and plug of the cylinders filled with enriched UF6. In this regard, when mechanical justifications are based on numerical calculations, the absence of contact between these components of the cylinder and the internal surfaces of the overpack after the regulatory drop tests shall be shown to respect the IAEA regulations. Furthermore, the representativeness of the ballast used to simulate the behaviour of the UF6 loaded within the cylinder shall be justified if drop tests are performed. The representativeness of the ballast should also be justified for numerical calculations. In addition, the applicant shall demonstrate that the melting temperature of the valve and the plug, including the tinned joint, will not be exceeded during the regulatory fire test. Finally, specific provisions relative to the use of plugs and the maintenance of cylinders should be included in the safety analysis report. T2 - 19th International Symposium on the Packaging and Transportation of Radioactive Materials PATRAM 2019 CY - New Orleans, LA, USA DA - 04.08.2019 KW - Valve KW - Fire test KW - Content simulation KW - UF6 KW - Intumescent material PY - 2019 SP - Paper 1208, 1 EP - 8 AN - OPUS4-49094 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wille, Frank A1 - Ballheimer, Viktor A1 - Apel, Andreas A1 - Kuschke, Christian A1 - Moutarde, M. A1 - Desnoyers, B. A1 - Kalinina, E. A1 - Ammerman, D. T1 - ISO-Standard and IAEA guidance material for package load attachment Points - Current approaches and developments N2 - For transport package design and operation according to the IAEA regulations, the package shall be securely stowed and its retention system shall be capable to withstand load conditions of routine transport. The supporting IAEA Advisory Material SSG-26 provides information how to do that. Up to now package designers in different countries use other load factors for the design of attachment points than those specified in the IAEA guidance material. In particular the acceleration values vary between different countries and lead to difficulties during the validation of foreign approval certificates. Therefore the IAEA started a discussion process to review the existing guidance text. An international working group was constituted in 2013. Representatives came from different stakeholders, e.g. transport operators, competent authorities and modal organizations. The discussions concluded especially on the transport conditions which has to be considered for stowage design, including on the one hand the relevance of the load factors used for strength and fatigue analysis and on the other hand the criteria which have to be considered for the attachment points. The proposed acceleration values will be compared to those measured during recent multi-modal testing by Sandia National Laboratories that measured the acceleration levels experienced by a spent fuel flask during heavy-haul truck, sea, and rail transport. The ISO standard 10276 is dealing with the load attachment systems of packages as well. This standard considers the trunnion design, manufacturing and operational aspects. The regular standard revision phase started in 2017. An expert group discussed new state-of-the-art technology, different analysis approaches for strength and fatigue analysis and proposed revised text for the ISO standard for international discussion. The finite-element analysis approach incl. appropriate acceptance criteria are described and referenced. The paper describes relevant tie-down aspects, gives background argumentation relevant to analysis approaches, and tries to support harmonized application of the revised IAEA guidance material and the future revised ISO standard. T2 - 19th International Symposium on the Packaging and Transportation of Radioactive Materials PATRAM 2019 CY - New Orleans, LA, USA DA - 04.08.2019 KW - Load attachment KW - Stowage KW - Trunnion KW - Bolt design KW - Retention KW - Acceleration KW - Transport KW - Load cycles PY - 2019 SP - Paper 1130, 1 EP - 10 AN - OPUS4-49095 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Komann, Steffen A1 - Reiche, I. A1 - Ramsay, J. A1 - Pilecki, L. A1 - Hirose, M. A1 - Fukuda, T. A1 - Moutarde, M. A1 - Fiaccabrino, V. A1 - Malesys, P. A1 - Nöring, R. T1 - Development of the IAEA safety guide_format and content of the package design safety report_PDSR for the transport of radioactive material N2 - Since 2005, several European countries, coordinated by the European Association of Competent Authorities (EACA), have been developing a guide on contents and structure of the documentation demonstrating the compliance with the regulations for packages for the transport of radioactive material (package design safety report, PDSR). This guide has been periodically improved, considering feedback from Designers and authorities. Taking into account the successful application of this guide in Europe, in 2013 the International Atomic Energy Agency (IAEA) decided to establish a similar guide as an IAEA document for promotion of worldwide use. The development of this IAEA guide started from the latest version of the European PDSR guide. In 2016/2017, during a 120-day review period, comments on the draft were received from member states and international organizations. These were incorporated into the draft in a series of meetings in 2017. In another meeting in December 2018 the draft was updated to be in line with the latest revision of the IAEA Regulations for the Safe Transport of Radioactive Material (SSR-6). In this process the draft has been improved significantly, regarding structure as well as implementation of a graded approach depending on the package type, and clarified. This paper points to the major considerations in developing the guide and important improvements over the last version of the European PDSR guide. T2 - 19th International Symposium on the Packaging and Transportation of Radioactive Materials PATRAM 2019 CY - New Orleans, LA, USA DA - 04.08.2019 KW - IAEA KW - Safety report KW - Radioactive material KW - European Guide KW - Guidance material KW - Package types KW - Package design PY - 2019 SP - Paper 1172, 1 EP - 7 AN - OPUS4-49097 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Aristia, Gabriela A1 - Le, Quynh Hoa A1 - Bäßler, Ralph T1 - Effect of CO2 gas on carbon steel corrosion in an acidic-saline based geothermal fluid N2 - Geothermal energy is one of the most promising energy resources to replace fossil fuel. To extract this energy, hot fluids of various salts and gases are pumped up from a geothermal well having a certain depth and location. Geothermal wells in volcanic regions often contain highly corrosive CO2 and H2S gases that can be corrosive to the geothermal power-plants, which are commonly constructed of different steels, such as carbon steel. This research focuses on the corrosion behaviour of carbon steel exposed to an artificial geothermal fluid containing CO2 gas, using an artificial acidic-saline geothermal brine as found in Sibayak, Indonesia. This medium has a pH of 4 and a chloride content of 1,500 mg/L. Exposure tests were conducted for seven days at 70 °C and 150 °C to simulate the operating temperatures for low and medium enthalpy geothermal sources. Surface morphology and cross-section of the specimens from the above experiments were analysed using scanning electron microscope (SEM) and energy dispersive X-ray (EDX). Electrochemical tests via open circuit potential (OCP) and electrochemical impedance spectroscopy (EIS) were performed to understand the corrosion processes of carbon steel in CO2-containing solution both at 70 °C and 150 °C. Localized corrosion was observed to a greater extent at 70 °C due to the less protectiveness of corrosion product layer compared to that at 150 °C, where FeCO3 has a high corrosion resistance. However, a longer exposure test for 28 days revealed the occurrence of localized corrosion with deeper pits compared to the seven-day exposed carbon steel. In addition, corrosion product transformation was observed after 28 days, indicating that more Ca2+ cations incorporate into the FeCO3 structure. T2 - EUROCORR 2019 CY - Sevilla, Spain DA - 09.09.2019 KW - Carbon steel KW - CO2 KW - EIS KW - Geothermal KW - Corrosion PY - 2019 SP - Paper 200245, 1 EP - 5 CY - Madrid, Spain AN - OPUS4-49099 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Crasselt, Claudia A1 - Schmidt, Wolfram A1 - Sturm, Heinz T1 - Influence of rheology modifying admixtures on early hydration of cementitious suspensions N2 - The presence of polycarboxylate ether (PCE) based superplasticizers (SPs) has enormous influence on the early hydration of cement. C3A as the most reactive phase of Portland cement plays a significant role in early hydration reactions and affects the rheological performance. Therefore, this paper presents experimental results about the influence of delayed addition of PCEs on the Hydration of cement and C3A-gypsum pastes investigated by isothermal heat flow calorimetry. Complementary in-situ XRD was carried out on C3A pastes to analyze hydration and phase changes related to the addition of PCE. Cement pastes with a delayed addition of PCE showed less Retardation compared to simultaneous addition. The alteration caused by PCE is much more pronounced for C3A-gypsum mixes. With a delayed addition of SP, the hydration of C3A is less retarded or even accelerated. It is obvious that there is less retardation the later the addition of SP. Furthermore, the PCE alter the hydration of C3A when added delayed and exhibit changes in kinetics and hydration rates. XRD results showed that more C3A is dissolved in the presence of PCE. Also, the gypsum depletion occurs earlier in the presence of PCE and even faster with delayed addition. Without PCE AFm starts to form just after the gypsum depletion. However, in the presence of PCE AFm already starts to form at the beginning of the hydration. Due to the faster gypsum depletion in the presence of PCE, also the transformation from ettringite into AFm begins earlier, but takes longer as without SP. T2 - 15th International Congress on the Chemistry of Cement CY - Prague, Czech Republic DA - 16.09.2019 KW - Cement KW - C3A KW - Early hydration KW - Polycarboxylate ether (PCE) KW - Delayed addition PY - 2019 SP - 1 EP - 8 AN - OPUS4-49104 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - von Oertzen, Alexander T1 - New Standardisation Tasks under the European Explosives Directive: Electronic Detonators, On-site Mixed Explosives N2 - Since the early drafting of the European standards for civil explosives, harmonised under directive 93/15/EEC and 2014/28/EU, blasting technology has developed notably. This is particularly evident for electronic detonators and electronic firing systems, and the EU commission agreed to initiate a standardisation initiative, also noting that the currently existing document on electronic detonators is “only” a Technical Specification (CEN/TS). This paper addresses the current activities in the area of standardisation. The EU is about to launch a formal standardisation request to cover the most recent technological developments not addressed by the current standards. The request would also include various adjustments of references to the new Directive for civil explosives, and in addition the task of developing a Technical Specification for on-site mixed explosives and corresponding manufacturing units. The latter has been included to address the nowadays frequently found mobile production on the basis of ammonium nitrate prills or emulsions. T2 - EFEE 10th anniversary World Conference on Explosives and Blasting CY - Helsiniki, Finland DA - 15.09.2019 KW - On-site mixed Explosives KW - Technical Specification KW - Harmonised Standards KW - Standardisation KW - Electronic Detonators PY - 2019 SN - 978-0-955029-6-6 SP - 215 EP - 219 PB - EFEE European Federation of Explosives Engineers AN - OPUS4-49107 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Auster, Jürgen A1 - Müller, Karsten A1 - Gründer, K.-P. T1 - Dynamic impact tests on materials & components of RAM packages - Advanced experimental and measurement methods N2 - In accident scenarios of transport packages or hypothetical crashes of containers in a storage facility or repository, the materials resistance against dynamic failure of the involved components is a deciding factor for package and container integrity during the handling, transport and storage for each type of radioactive material. For example, different dynamic impact tests on containers and components like lid sealing systems and specimens made of ductile cast iron and shock-absorbing materials are carried out by BAM. In order to perform dynamic impact tests with packages and its parts BAM operates two free-fall drop test facilities with maximum capacities of 200 t and 55 t, and a test bench for guided drop tests. This latter drop test machine enables a clearly specified component loading by a precisely positioned test object or drop weight and has been used recently for numerous investigations. The paper gives an overview of the wide range of experimental testing methods carried out within guided Impact and bending tests. Examples of methodological challenges are presented, especially such experimental analysis of dynamic impact conditions. In addition to known applied methods of dynamic, non-contact displacement measurements like high-speed 3-D surface deformation a recently patented 2-D tracking method is presented. By means of in-situ determination of fracture parameters with relevance to the materials stress intensity factor, the method has been successfully applied for a typical specimen geometry. Also shown are the possibility of detecting in-situ He-leakage rates on laterally impact loaded lid sealing systems as well as a method of acceleration sensor-temperature control under test conditions in the low temperature range. T2 - 18th International Symposium on the Packaging and Transportation of Radioactive Materials PATRAM 2019 CY - New Orleans, LA, USA DA - 04.08.2019 KW - Dynamic impact tests KW - Materials KW - RAM packages KW - Advanced experimental KW - Measurement methods PY - 2019 SP - Paper 1374, 1 EP - 10 AN - OPUS4-49067 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rolle, Annette A1 - Ballheimer, Viktor A1 - Neumeyer, Tino A1 - Wille, Frank T1 - Application of leakage rates measured on scaled cask or component models to the package containment safety assessment N2 - The containment systems of transport and storage casks for spent fuel and highlevelradioactive waste usually include bolted lids with metallic or elastomeric seals. The mechanical and thermal loadings associated with the routine, normal and accident conditions of transport can have a significant effect on the leak tightness of such containment system. Scaled cask models are often used for providing the required mechanical and thermal tests series.Leak tests have been conducted on those models. It is also common practice to use scaled component tests to investigate the influence of deformations or displacements of the lids and the seals on the standard leakage rate as well as to study the temperature and time depending alteration of the seals. In this paper questions of the transferability of scaled test results to the full size design of the containment system will be discussed. T2 - 19th International Symposium on the Packaging and Transportation of Radioactive Materials PATRAM 2019 CY - New Orleans, LA, USA DA - 04.08.2019 KW - Leakage rate KW - Transport packages KW - Seals KW - Radioaktive PY - 2019 SP - Paper 1147, 1 AN - OPUS4-49053 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Komann, Steffen A1 - Ballheimer, Viktor A1 - Quercetti, Thomas A1 - Scheidemann, Robert A1 - Wille, Frank T1 - Design assessment by bam of a new package design for the transport of snf from a german research reactor N2 - For disposal of the German research reactor of the Technical University Munich FRM II a new transport and storage cask design was under approval assessment by the German authorities. The Bundesanstalt für Materialforschung und -prüfung (BAM) assessed the mechanical and thermal package safety and performed drop tests. The activity release approaches and subjects of quality assurance and surveillance for manufacturing and operation of the package were assessed by BAM as well. The cask body is made of ductile cast iron and closed by two bolted lid systems with metal seals. The material of the lids is stainless steel. On each end of the cask a wood-filled impact limiter is installed to reduce impact loads to the cask under drop test conditions. In the cavity of the cask a basket for five spent fuel assemblies is arranged. For the safety case a combination of experimental testing and analytical/numerical calculations were applied. In total, four drop tests were carried out at the BAM large drop test facility. Two tests were carried out as a full IAEA drop test sequence consisting of a 9m drop test onto an unyielding target and a 1m puncture bar drop test. The other two drop test were performed as single 9m drop tests and completed by additional analyses for considering the effects of an IAEA drop test sequence. The main objectives of the drop tests were the investigation of the integrity of the package and its safety against release of radioactive material as well as the test of the fastening system of the impact limiters. Furthermore, the acceleration and strain signals measured during the tests were used for the verification of Finite-Element-Analysis (FEA) used for the safety analysis of the package design. The finite-element models incorporated in the package design safety report include the cask body, the lid system, the inventory and the impact limiters with the fastening system. In this context special attention was paid to the modeling of the encapsulated wood-filled impact limiters. Additional calculations using the verified numerical models were done by the applicant and assessed by BAM to investigate e.g. the brittle fracture of the cask body made of ductile cask iron within the package design approval procedure. This paper describes the package design assessment from the view of the competent authority BAM including the applied assessment strategy, the conducted drop tests and the additional calculations by using numerical and analytical methods. T2 - 19th International Symposium on the Packaging and Transportation of Radioactive Materials PATRAM 2019 CY - New Orleans, LA, USA DA - 04.08.2019 KW - Numerical modelling KW - Drop test KW - Assessment method KW - Ductile cast iron KW - Package design KW - Experimental testing PY - 2019 SP - Paper 1176, 1 AN - OPUS4-49054 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Neumann, Martin A1 - Schilling, O. A1 - Kuschke, Christian A1 - Darnstädt, A. A1 - Schubert, Sven A1 - Günther, U. A1 - Wille, Frank T1 - Requirements for management systems for manufacturing of transport packages: the new revision of BAM-GGR 011 guideline N2 - In accordance with IAEA SSR-6 para 306 a management system shall be established and implemented to ensure compliance with the relevant provisions of the IAEA regulations. BAM has issued an update of the guideline: the BAM-GGR 011. The new revision describes necessary quality assurance measures for design, manufacture, testing, documentation, use, maintenance and inspection of packagings for package designs requiring competent authority approval for the transport of radioactive material. The measures can be categorised as system-related and design-related. They are independently approved and monitored by the German competent authority BAM and its authorised expert (BAM/T). The qualification of the organisation applying for the design approval certificate is reviewed in the context of the design approval procedure. The quality assurance measures for manufacture consist of three main steps. Pre-assessment of manufacturing documents such as quality plans, specifications etc., Manufacturing inspections according the pre-assessed documents and inspection before commissioning including documentation review. Periodic inspections during operation as well as relevant specifications for use and maintenance ensure that the properties specified in the approval certificate are preserved over the package life time. Special provisions for the return on experience regarding operational feedback for design, manufacture, use, maintenance and inspection are given. Special focus shall be given here to the rearranged and meanwhile established system of manufacturing inspections. This includes more transparent roles for a) the Producers authorised inspection 11282 representative, b) the independent inspection expert (S), acting on behalf of the manufacturer with acceptance of BAM, and c) BAM or its authorised expert (BAM/T). Additional attention shall be drawn to the management of deviations during manufacturing and provisions for maintenance and periodic inspections. T2 - 19th International Symposium on the Packaging and Transportation of Radioactive Materials PATRAM 2019 CY - New Orleans, LA, USA DA - 04.08.2019 KW - Quality assurance KW - Transport KW - Manufacturing KW - Surveillance KW - Radioactive material PY - 2019 SP - Paper 1128, 1 AN - OPUS4-49059 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Maierhofer, Christiane A1 - Krankenhagen, Rainer A1 - Röllig, Mathias A1 - Rehmer, Birgit A1 - Gower, M. A1 - Baker, G. A1 - Lodeiro, M. A1 - Aktas, A. A1 - Knaszovicka, L. A1 - Blahut, A. A1 - Monte, C. A1 - Adibekyan, A. A1 - Gutschwager, B. T1 - Characterisation of artificial defects in CFRP and GFRP sheets designed for energy applications using active thermography N2 - The increased use of fibre-reinforced plastic (FRP) composites for improved efficiency and reliability in energy related applications e.g. wind and marine turbine blades, nacelles, oil and gas flexible risers, also increases the demand for innovative non-destructive testing technologies. Thus, in order to achieve increased acceptance of suited and optimized non-destructive testing (NDT) methods in industry, the European Metrology Research Programme (EMRP) project ENG57 Validated Inspection Techniques for Composites in Energy Applications (VITCEA) deals with the development and validation of innovative NDT technologies. In this contribution, results concerning thermographic investigations at test specimens during tensile loading and active thermography testing after tensile loading are presented. Additionally, the determination of the optical properties (relative transmittance and directional spectral emissivity) of CFRP and GFRP test specimens is described. T2 - Conference QIRT 2016 CY - Gdansk, Poland DA - 04.07.2016 KW - Active thermography KW - CFRP KW - GFRP KW - Validation of methods PY - 2016 UR - http://qirt.gel.ulaval.ca/archives/qirt2016/papers/076.pdf DO - https://doi.org/10.21611/qirt.2016.076 SN - 2371-4085 SP - Paper 076, 527 EP - 536 CY - Quebec, Canada AN - OPUS4-37512 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Straße, Anne A1 - Gumenyuk, Andrey A1 - Rethmeier, Michael T1 - Nahteigenschaftsverbesserung von dickwandigen laserstrahlgeschweißten Duplexblechen mittels pulveraufgetragenen Pufferschichten N2 - Duplexstähle finden aufgrund ihrer Eigenschaften, wie der guten Korrosionsbeständigkeit, einer hohen Festigkeit bei gleichzeitig guter Duktilität häufig industrielle Anwendung. Durch die hohen Abkühlraten beim Laserstrahlschweißen weisen Schweißnähte jedoch anstelle eines ausgeglichenen Duplexgefüges einen deutlich erhöhten Ferritanteil, im Vergleich zum Basiswerkstoff, auf. Dies führt zu einer verringerten Duktilität sowie Korrosionsbeständigkeit. Um dieses Problem zu lösen, wurde ein Prozess entwickelt, der auf einer Kantenbeschichtung mit nickelhaltigem Zusatzmaterial der zu fügenden Bleche mittels Laser-Pulver-Auftragschweißen (LPA) basiert. Die resultierenden Schweißnähte wurden zerstörend anhand von Schliffbildern, EDX-Aufnahmen, Härtemessungen und Kerbschlagbiegeversuchen geprüft. T2 - 40. Assistentenseminar der Füge- und Schweißtechnik CY - Braunlage, Germany DA - 25.09.2019 KW - Laser-Pulver-Auftragschweißen; Laserstrahlschweißen, Duplex, Pufferschichten PY - 2020 VL - 357 SP - 131 EP - 140 PB - DVS Media CY - Düsseldorf AN - OPUS4-50144 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Brunner-Schwer, C. ED - Graf, B. ED - Schreiber, F. ED - Rethmeier, Michael T1 - Highspeed-Plasma-Laser Cladding (HPLC) als hybrides Beschichtungsverfahren: Evaluierung des Einsatzpotentials für hohe Prozessgeschwindigkeiten N2 - Das Plasma-Pulver-Auftragschweißen ist ein Verfahren, dass hohe Auftragraten ermöglicht, jedoch auch eine erhöhte thermische Belastung des Bauteiles verursacht. Laser-Pulver- Auftragschweißen hingegen erreicht eine hohe Präzision und eine geringe Aufmischung, erfordert jedoch ein kostspieliges Hochleistungslasersystem und erreicht im Vergleich nur geringe Auftragraten, was zu hohen Verarbeitungskosten führt. Eine Kopplung von Laser- und Lichtbogenenergie in einer gemeinsamen Prozesszone zielt darauf ab, die jeweiligen Vorteile beider Technologien zu nutzen. Dies betrifft insbesondere die Effizienz der Wärmeausnutzung und der Nutzung des Zusatzwerkstoffs. Es wird ein Plasma-Laser-Hybrid-Prozess als Highspeed-Plasma-Laser-Cladding-Technologie (HPLC) für Beschichtungs- sowie Instandsetzungszwecke vorgestellt. Gezeigt werden Ergebnisse mit Prozessgeschwindigkeiten von 10 m/min bei Laserleistungen von 2 kW, dabei können Flächenraten von mehr als 1 m2/h erreicht werden. Effiziente Beschichtungen von großen Flächen, beispielsweise auf rotationssymmetrischen Bauteilen stellen ein relevantes Anwendungsfeld für diesen Technologieansatz dar. Die Nickelbasislegierung Inconel 625 wird als Korrosionsschutzwerkstoff eingesetzt. Im Rahmen der Verfahrensprüfung werden die hergestellten Beschichtungen einer EDX Messung unterzogen. Prozesscharakteristische Kenngrößen wie z.B. die Auftragrate werden vorgestellt und vor dem Hintergrund wirtschaftlicher Kennzahlen diskutiert. Zusätzlich werden die Aufmischung, Spurgeometrie und Wärmeeinflusszone der Spuren und Schichten ausgewertet. Im Vergleich zum Laser-Pulver-Auftragschweißen werden Spuren bei hohen Prozessgeschwindigkeiten mit einer hohen Auftragrate erzeugt. T2 - DVS Congress 2019 CY - Rostock, Germany DA - 16.09.2019 KW - Highspeed-plasma-laser-cladding KW - Korrosionsschutz KW - Laser KW - Plasma KW - Auftragschweißen PY - 2019 SP - n.b. AN - OPUS4-49364 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Straße, Anne A1 - Gumenyuk, Andrey A1 - Scheuschner, Nils A1 - Altenburg, Simon A1 - Pignatelli, Giuseppe A1 - Gornushkin, Igor B. A1 - Baensch, Franziska A1 - Rethmeier, Michael T1 - In-situ Prozessüberwachung beim Laser-Pulver-Auftragschweißen (LPA) mittels Thermografie, optischer Emissionsspektroskopie (OES) und Schallemissionsanalyse (SEA) N2 - Vor allem in den letzten Jahren ist das Interesse der Industrie an der additiven Fertigung deutlich gestiegen. Die Vorteile dieser Verfahren sind zahlreich und ermöglichen eine ressourcenschonende, kundenorientierte Fertigung von Bauteilen, welche zur stetigen Entwicklung neue Anwendungsbereiche und Werkstoffe führen. Aufgrund der steigenden Anwendungsfälle, nimmt auch der Wunsch nach Betriebssicherheit unabhängig von anschließenden kostenintensiven zerstörenden und zerstörungsfreien Prüfverfahren zu. Zu diesem Zweck werden im Rahmen des von der BAM durchgeführten Themenfeldprojektes „Prozessmonitoring in Additive Manufacturing“ verschiedenste Verfahren auf ihre Tauglichkeit für den in-situ Einsatz bei der Prozessüberwachung in der additiven Fertigung untersucht. Hier werden drei dieser in-situ Verfahren, die Thermografie, die optische Emissionsspektroskopie und die Schallmissionsanalyse für den Einsatz beim Laser-Pulver-Auftragschweißen betrachtet. T2 - 41. Assistentenseminar der Füge- und Schweißtechnik CY - Magdeburg, Germany DA - 02.09.2020 KW - Laser-Pulver-Auftragschweißen (LPA) KW - Thermographie KW - Optische Emissionsspektroskopie (OES) KW - Schallemissionsanalyse (SEA) PY - 2021 SN - 978-3-96144-141-9 VL - 370 SP - 132 EP - 140 PB - DVS MEdia CY - Düsseldorf AN - OPUS4-53967 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Maierhofer, Christiane A1 - Krankenhagen, Rainer A1 - Röllig, Mathias A1 - Unnikrishnakurup, Sreedhar A1 - Monte, C. A1 - Adibekyan, A. A1 - Gutschwager, B. A1 - Knazowicka, L. A1 - Blahut, A. A1 - Gower, M. A1 - Lodeiro, M. A1 - Baker, G. A1 - Aktas, A. T1 - Einfluss thermischer und optischer Materialeigenschaften auf die Charakterisierung von Fehlstellen in Faserverbundwerkstoffen mit aktiven Thermografieverfahren N2 - In diesem Beitrag werden zerstörungsfreie Untersuchungen mittels aktiver Thermografie an Probekörpern aus CFK und GFK mit unterschiedlichen künstlichen Fehlstellen vorgestellt. Dabei wird die zeitliche und örtliche Temperaturverteilung nach Erwärmung mit Blitzlampen oder mit einem Infrarot-Strahler mit einer Infrarot-Kamera erfasst. Zur Rekonstruktion der Messdaten wurde ein numerisches Modell entwickelt. Dazu war die Bestimmung der thermischen und optischen Materialeigenschaften erforderlich. N2 - This paper presents results of the non-destructive evaluation of CFRP and GFRP test specimens with various artificial defects using active thermography. After heating the samples with flash lamps or with an infrared radiator, the temporal and spatial resolved temperature distribution is recorded with an infrared camera. For the reconstruction of the experimental data, a numerical model was developed. For the numerical simulations, the thermal and optical material parameters had to be determined. T2 - Temperatur 2017 CY - Berlin, Germany DA - 17.05.2017 KW - CFK KW - GFK KW - aktive Thermografie KW - numerische Simulation KW - Emissivität PY - 2017 SN - 978-3-944659-04-6 SP - 15 EP - 20 AN - OPUS4-41088 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Stankevich, S. A1 - Gumenyuk, Andrey A1 - Straße, Anne A1 - Rethmeier, Michael ED - Reisgen, U. ED - Schmidt, M. ED - Zaeh, M. ED - Rethmeier, Michael T1 - Measurement of thermal cycle at multi-pass layer build-up with different travel path strategies during DLMD process N2 - The shape of the parts, created by the technology of direct laser metal deposition (DLMD), is influenced by various parameters, for example, the power and diameter of the laser source spot. The contribution of energy from the laser affects the temperature distribution in the formed layers. The changing temperature in the working area entails a Change in the geometry of the layers and affects the stability of the process. In this paper, experiments on the measurement of temperature cycles in the DLMD process with different directions of the filling track are carried out. An infrared camera was used to measure thermal cycles. The calibration of the acquired data (i.e. correspondence table between the intensity of thermal radiation of the material and the absolute temperature) was done with help of two-color pyrometer ex situ and in situ measurements. The experiments are carried out on two materials 316L and Inconel 718. The effect of the maximum temperature on the layer height is shown, and thermal cycles in the formation of layers for different filling strategies are presented. T2 - Laser in Manufacturing Conference 2019 CY - Munich, Germany DA - 24.06.2019 KW - Thermography KW - Direct Laser Metal Deposition PY - 2019 SP - 1 EP - 9 AN - OPUS4-48716 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Altenburg, Simon A1 - Scheuschner, Nils A1 - Straße, Anne A1 - Gumenyuk, Andrey A1 - Maierhofer, Christiane T1 - Towards the determination of real process temperatures in the LMD process by multispectral thermography N2 - Due to the rapid thermal cycles involved in additive manufacturing of metals, high internal stresses and peculiar microstructures occur, which influence the parts mechanical properties. To systematically examine their formation, in-process measurements of the temperature are needed. Since the part emissivity is strongly inhomogeneous and rapidly changing in the process, the applicability of thermography for the determination of thermodynamic temperatures is limited. Measuring the thermal radiation in different wavelengths simultaneously, temperature and emissivity can be separated. Here, we present results of a preliminary study using multispectral thermography to obtain real temperatures and emissivities in directed energy deposition (DED) processes. T2 - Thermosense: Thermal Infrared Applications XLIII CY - Online meeting DA - 12.04.2021 KW - Additive Manufacturing KW - Process monitoring KW - Multispectral thermography KW - Laser metal deposition KW - TES KW - LMD KW - Temperature emissivity separation PY - 2021 DO - https://doi.org/10.1117/12.2587881 VL - 2021 SP - 77 EP - 83 PB - SPIE AN - OPUS4-52516 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Straße, Anne A1 - Gumenyuk, Andrey A1 - Rethmeier, Michael T1 - Quality improvement of laser welds on thick duplex plates by laser cladded buttering N2 - Because of its excellent corrosion resistance, high tensile strength and high ductility, duplex stainless steel 2205 offers many areas of application. Though laser beam welding accompanied by high cooling rates, duplex steels tend to perform higher ferrite contents in weld metal as the base metal, which leads to a reduction of ductility and corrosion resistance of the weld joint. To overcome this problem, a solution, based on buttering the plate edges by laser metal deposition (LMD) with material containing higher Ni concentrations prior to laser welding was suggested. In this context different process parameters for LMD process were investigated. In a second step the possibility of welding those edges defect free while achieving balanced austenite-ferrite ratio was verified with metallographic analysis, Electron Backscatter Diffraction (EBSD) and impact testing according to Charpy. T2 - Lasers in Manufacturing (LiM) 2019 CY - Munich, Germany DA - 24.06.2019 KW - Laser Metal Deposition; Laser Beam Welding; Duplex; Stainless Steel PY - 2020 SP - We_A31_4_4-1 EP - We_A31_4_4-6 PB - WLT (Wissenschaftliche Gesellschaft für Lasertechnik) AN - OPUS4-50143 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lüth, Peter A1 - Frost, K. A1 - Kurth, Lutz A1 - Malow, Marcus A1 - Schmidt, Martin A1 - Michael-Schulz, Heike A1 - Uhlig, S. A1 - Zakel, S. T1 - CEQAT-DGHS Ringversuchsprogramm für die Chemikaliensicherheit - Schlussfolgerungen N2 - Die Ursachen für Chemikalienunfälle können vielfältig sein. Prävention beginnt bereits im Prüflabor, wenn Chemikalien auf ihre gefährlichen Eigenschaften getestet werden. Dazu sind Prüfmethoden entwickelt und veröffentlicht worden, die heute weltweit Anwendung finden. Auf die Validität der Prüfmethode und richtige Durchführung der Prüfung im Laboratorium müssen sich Sicherheitsfachkräfte, Transporteure oder Händler verlassen können. Anhand der in den letzten 10 Jahren im Rahmen des CEQAT-DGHS von BAM und PTB durchgeführten Ringversuche (RV) wird gezeigt, dass bei allen bisher untersuchten Prüfmethoden ein Verbesserungsbedarf besteht. Die RV müssen daher zunächst auf die Methodenverbesserung und -validierung abzielen und nicht auf Leistungstests. Das Labormanagement und die praktische Durchführung der Prüfung sind in vielen Laboratorien verbesserungsbedürftig. Der Begriff „Erfahrung der Prüfer“ ist kritisch zu sehen: Eine „lange Erfahrung mit vielen Prüfungen“ ist nicht unbedingt ein Garant für richtige Ergebnisse. T2 - 15. BAM-PTB-Kolloquium zur chemischen und physikalischen Sicherheitstechnik CY - Braunschweig, Germany DA - 21.05.2019 KW - Gefahrgut KW - Gefahrstoff KW - Ringversuch KW - Prüfmethode KW - Validierung KW - Qualitätssicherung PY - 2019 UR - https://www.ptb.de/cms/index.php?id=18763 DO - https://doi.org/10.7795/210.20190521M SP - 1 EP - 8 PB - Physikalisch-Technische Bundesanstalt (PTB) CY - Braunschweig AN - OPUS4-49489 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ernst, A. A1 - Klein, S. A1 - Hall, T. A1 - Avila, Luis A1 - Bähre, D. T1 - Electrochemical dressing of hard tools for abrasive precision machining N2 - In this study an approach for dressing metallic bonded honing stones with hard cutting grains on the basis of electrolysis is investigated. By a combination of concepts from electrochemical machining (ECM) and electropolishing a test rig was designed and put into operation. In general, it can be stated that the Approach investigated in this paper has proved to be a suitable dressing method for honing stones. However, the dressing result is highly dependent on bond components, cutting grain size and concentration which lead to local differences in the material removal and irregular topographies. This could be overcome, for example, by setting the dressing parameters more precisely based on the best results presented in this paper. T2 - International Symposium on ElectroChemical Machining Technology CY - Saarbrücken, Germany DA - 14.11.2019 KW - Irregular topography KW - Honing KW - Electrochemical dressing KW - Honing Stone KW - Laser Scanning Microscopy KW - Electropolishing PY - 2019 SN - 978-3-00-064086-5 SP - 96 EP - 108 PB - Fertigungstechnik Saarbrücken CY - Saarbrücken AN - OPUS4-49490 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lüth, Peter A1 - Frost, K. A1 - Kurth, Lutz A1 - Malow, Marcus A1 - Schmidt, Martin A1 - Michael-Schulz, Heike A1 - Uhlig, S. A1 - Zakel, S. T1 - CEQAT-DGHS Ringversuchsprogramm für die Chemikaliensicherheit – Entwicklung von Verfahren zur Verifizierung der Prüfapparatur am Beispiel der Prüfmethode UN Test N.5 N2 - Prävention beginnt im Prüflabor, wenn Chemikalien auf ihre gefährlichen Eigenschaften getestet werden. Dazu sind Prüfmethoden entwickelt und veröffentlicht worden, die heute weltweit Anwendung finden. Auf die Validität der Prüfmethode und richtige Durchführung der Prüfung im Laboratorium müssen sich Sicherheitsfachkräfte, Transporteure oder Händler verlassen können. Anhand der in den letzten 10 Jahren im Rahmen des CEQAT-DGHS von BAM und PTB durchgeführten Ringversuche (RV) wird gezeigt, dass bei allen bisher untersuchten Prüfmethoden ein Verbesserungsbedarf besteht. Die RV müssen daher zunächst auf die Methodenverbesserung und -validierung abzielen und nicht auf Leistungstests. Das Labormanagement und die praktische Durchführung der Prüfung sind in vielen Laboratorien verbesserungsbedürftig. Der Begriff „Erfahrung der Prüfer“ ist kritisch zu sehen: Eine „lange Erfahrung mit vielen Prüfungen“ ist nicht unbedingt ein Garant für richtige Ergebnisse. Bei der Prüfung der gefährlichen Eigenschaften von Chemikalien sind Referenzmaterialen auf Grund der Instabilität in der Regel nicht verfügbar. Für Prüflaboratorien sind RV daher eine Alternative bei der Qualitätssicherung. RV sind jedoch aufwendig und können nur in relativ großen Zeitabständen durchgeführt werden. Es sind deshalb Verfahren zur Verifizierung z. B. der in den Laboratorien verwendeten Prüfapparaturen zu entwickeln. Die Entwicklung von Verifizierungsverfahren wird am Bespiel der Prüfmethode UN Test N.5 demonstriert. T2 - 15. BAM-PTB-Kolloquium zur chemischen und physikalischen Sicherheitstechnik CY - Braunschweig, Germany DA - 21.05.2019 KW - Gefahrgut KW - Gefahrstoff KW - Ringversuch KW - Prüfmethode KW - Validierung KW - Qualitätssicherung KW - Verifizierung PY - 2019 UR - https://www.ptb.de/cms/index.php?id=18763 DO - https://doi.org/10.7795/210.20190521E SP - 1 EP - 10 CY - Braunschweig AN - OPUS4-49495 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rahammer, M. A1 - Myrach, Philipp A1 - Maierhofer, Christiane A1 - Busse, G. A1 - Kreutzbruck, M. T1 - Auflösungsgrenzen der Lockin-Thermografie zur Prüfung von Faserkunststoffverbunden N2 - Aktive Thermografie mit Lockin-Anregung ist ein zerstörungsfreies Prüfverfahren, das insbesondere auch die Prüfung von kohlenstofffaserverstärkten Kunststoffen ermöglicht. Um eine Standardisierung dieses Verfahrens voranzubringen, wurden im Rahmen eines Forschungsprojektes umfangreiche Untersuchungen zur Validierung des Verfahrens durchgeführt. Für die Anregungsmethoden optisch und Ultraschall wurden die wichtigsten Parameter systematisch untersucht. Auf der Auswertungsseite ist dies z.B. der Einfluss der spektralen Empfindlichkeit verschiedener Kamerasysteme. Für die Anregungen sind unter anderem die Einflüsse von Anregungsenergie und Ultraschallfrequenz untersucht worden. Auch Materialparameter, wie der Lagenaufbau bei CFK-Probekörpern, beeinflussen die Ergebnisse stark. T2 - 24. Stuttgarter Kunststoffkolloquium CY - Stuttgart, Germany DA - 25.02.2015 KW - Zerstörungsfreie Prüfung KW - Lockin-Thermografie KW - Faserkunststoffverbunde KW - Non-destructive testing KW - Lockin-Thermography KW - Fibre-reinforced plastics PY - 2015 SP - 1 EP - 7 AN - OPUS4-32876 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Holzweber, Markus A1 - Hodoroaba, Vasile-Dan A1 - Unger, Wolfgang T1 - What about ionic liquids as a 'hot' certified reference material candidate to check your EDS below 1 keV? N2 - Energy-dispersive X-ray spectrometry (EDX) is one of the most applied methods used for the analysis of the chemical composition of solids and thin films. Recent progress in EDS (Energy Dispersive X-ray Spectrometer) technology has increased the general performance also in the energy range < 1 keV addressing low Z elements. Suitable test materials to be employed especially to check the low-energy EDS performance – also in line with ISO 15632 - are rather limited and mainly based on C K and F K lines. In order to obtain valid results in laboratories accredited in compliance with ISO/IEC 17025 it is necessary to periodically check the instrument performance. T2 - M&M 2015 - Microscopy & Microanalysis CY - Portland, Oregon, USA DA - 02.08.2015 KW - Reference material KW - EDX KW - Ionic liquids PY - 2015 DO - https://doi.org/10.1017/S1431927615009356 VL - 21 SP - Suppl. 3, Paper 0856 AN - OPUS4-34211 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Röhsler, Andreas A1 - Sobol, Oded A1 - Nolze, Gert A1 - Unger, Wolfgang A1 - Böllinghaus, Thomas T1 - Use of time-of-flight secondary ion mass spectrometry for the investigation of hydrogen-induced effects in austenitic steel AISI 304L N2 - During the energy transformation from fossil fuels to renewable energy sources, the use of hydrogen as fuel and energy storage can play a key role. This presents new challenges to industry and the scientific community alike. The storage and transport of hydrogen, which is nowadays mainly realized by austenitic stainless steels, remains problematic, which is due to the degradation of mechanical properties and the possibility of phase transformation by hydrogen diffusion and accumulation. The development of materials and technologies requires a fundamental understanding of these degradation processes. Therefore, studying the behavior of hydrogen in austenitic steel contributes to an understanding of the damage processes, which is crucial for both life assessment and safe use of components in industry and transportation. As one of the few tools that is capable of depicting the distribution of hydrogen in steels, time-of-flight secondary ion mass spectrometry was conducted after electrochemical charging. To obtain further information about the structural composition and cracking behavior, electron-backscattered diffraction and scanning electron microscopy were performed. Gathered data of chemical composition and topography were treated employing data fusion, thus creating a comprehensive portrait of hydrogen-induced effects in the austenite grade AISI 304L. Specimens were electrochemically charged with deuterium instead of hydrogen. This arises from the difficulties to distinguish between artificially charged hydrogen and traces existing in the material or the rest gas in the analysis chamber. Similar diffusion and permeation behavior, as well as solubility, allow nonetheless to draw conclusions from the experiments. T2 - 21st International Conference on Secondary Ion Mass Spectrometry CY - Kraków, Poland DA - 10.09.2017 KW - AISI 304L KW - Hydrogen KW - ToF-SIMS KW - Austenitic stainless steel PY - 2018 DO - https://doi.org/10.1116/1.5013931 SN - 1071-1023 VL - 36 IS - 3 SP - Article 03F103, 1 EP - 6 PB - American Vacuum Society (AVS) AN - OPUS4-44840 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Unger, Jörg F. A1 - Gründer, Klaus-Peter A1 - Hille, Falk A1 - Liehr, Sascha A1 - Maack, Stefan A1 - Niederleithinger, Ernst A1 - Pirskawetz, Stephan A1 - Rogge, Andreas A1 - Said, Samir A1 - Viefhues, Eva A1 - Zorn, Sebastian ED - Baeßler, Matthias ED - Möller, G. ED - Rogge, Andreas ED - Schiefelbein, N. T1 - Innovative Messsysteme zum Brückenmonitoring am Beispiel einer Versuchsbrücke – vom Sensor bis zur Zustandsprognose N2 - In der aktuellen Projektphase liegt der Fokus auf der Datenaufnahme, -bearbeitung und -speiche-rung mit dem Ziel, automatisierte Auswerteverfahren einsetzen zu können. Aktuell wurden primär punktuelle Messungen an ausgewählten Messtagen aufgenommen. Die Systeme sollen so weiter-entwickelt werden, dass sie sich auch für kontinuierliche Messungen im Rahmen von Monitoring-aufgaben eignen. Ein wichtiger Fokus bei der Auswertung ist die Kombination mit numerischen Modellen, die mithilfe von Bayesian Update Verfahren und den aufgenommenen Messdaten kalibriert und im Verlauf der Monitoringaufgabe angepasst werden sollen. Insbesondere sollen auch zeitabhängige Modelle, die eine zeitliche Entwicklung von Struktureigenschaften beinhalten (Kriechen, Schwinden, Ermüdung, Korrosion) dazu verwendet werden, die zukünftige Performance der Struktur bewerten zu können. Basierend darauf werden dann Konzepte zur Planung von Inspektion und Wartung erstellt. T2 - Messen im Bauwesen 2017 CY - Berlin, Germany DA - 14.11.2017 KW - Brückeninfrastruktur KW - Innovative Messverfahren KW - Stereofotogrammetrie PY - 2017 SN - 978-3-9818270-8-8 VL - 2017/1 SP - 7 EP - 19 PB - Bundesanstalt für Materialforschung und -prüfung (BAM) CY - Berlin AN - OPUS4-44306 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kindrachuk, Vitaliy A1 - Titscher, Thomas A1 - Hirthammer, Volker A1 - Unger, Jörg F. ED - Meschke, G. ED - Pichler, B. ED - Rots, J.G. T1 - A continuum damage model for the simulation of concrete under cyclic loading N2 - Lifetime aspects including fatigue failure of concrete structures were traditionally only of minor importance. Because of the growing interest in maxing out the capacities of concrete, its fatigue failure under compression has become an issue. A variety of interacting phenomena such as e.g. loss of prestress, degradation due to chemical reactions or creep and shrinkage influence the fatigue resistance. Failure due to cyclic loads is generally not instantaneous, but characterized by a steady damage accumulation. Therefore, a reliable numerical model to predict the performance of concrete over its lifetime is required, which accurately captures order effects and full three-dimensional stress states. Many constitutive models for concrete are currently available, which are applicable for specific loading regimes, different time scales and different resolution scales. However, a key limitation of those models is that they generally do not address issues related to fatigue on a structural level. Very few models can be found in the literature that reproduce deterioration of concrete under repeated loading-unloading cycles. This is due to the computational effort necessary to explicitly resolve every cycle which exceeds the currently available computational resources. The limitation can only be overcome by the application of multiscale methods in time. The objective of the paper is the development of numerical methods for the simulation of concrete under fatigue loading using temporal multiscale methods. First, a continuum damage model for concrete is developed with a focus on fatigue under compressive stresses [1]. This includes the possibility to model stress redistributions and capture size effects. In contrast to cycle based approaches, where damage is accumulated based on the number of full stress cycles, a strain based approach is developed that can capture cyclic degradation under variable loading cycles including different amplitudes and loading frequencies. The model is designed to represent failure under static loading as a particular case of fatigue failure after a single loading cycle. As a consequence, most of the material parameters can be deduced from static tests. Only a limit set of additional constitutive parameters is required to accurately describe the evolution under fatigue loading. Another advantage of the proposed model is the possibility to directly incorporate other multi-physics effects such as creep and shrinkage or thermal loading on the constitutive level. Second, a multiscale approach in time is presented to enable structural computations of fatigue failure with a reduced computational effort. The damage rate within the short time scale corresponding to a single cycle is computed based on a Fourier based approach [2]. This evolution equation is then solved on the long time scale using different implicit and explicit time integration schemes. Their performance and some limitations for specific loading regimes is discussed. Finally, the developed methods will be validated and compared to experimental data. [1] Vitaliy Kindrachuk, Marc Thiele, Jörg F. Unger. Constitutive modeling of creep-fatigue interaction for normal strength concrete under compression, International Journal of Fatigue, 78:81-94, 2015 [2] Vitaliy Kindrachuk, Jörg F. Unger. A Fourier transformation-based temporal integration scheme for viscoplastic solids subjected to fatigue deterioration, International Journal of Fatigue, 100:215-228, 2017 T2 - Conference on Computational Modelling of concrete and concrete structures (EURO_C 2018') CY - Bad Hofgastein, Austria DA - 26.02.2018 KW - Fatigue KW - Concrete KW - Damage PY - 2018 SN - 978-1-138-74117-1 DO - https://doi.org/10.1201/9781315182964-19 SP - 155 EP - 164 PB - CRC Press, Taylor & Francis Group CY - Boca Raton, Lodon, New York, Leiden AN - OPUS4-47999 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eberwein, Robert A1 - Hajhariri, Aliasghar A1 - Camplese, Davide A1 - Scarponi, Giordano Emrys A1 - Cozzani, Valerio A1 - Otremba, Frank ED - Di Benedetto, Almerinda T1 - Experimental Research Of A Tank For A Cryogenic Fluid With A Wall Rupture In A Fire Scenario N2 - In the course of decarbonizing the energy industry, cryogenic energy carriers as liquefied hydrogen (LH2) and liquefied natural gas (LNG) are seen as having great potential. In technical applications, the challenge is to keep these energy carriers cold for a long time. This is achieved in the road transport sector and also stationary applications by thermal super insulations (TSI) which based on double-walled tanks with vacuum and multilayer insulation (MLI) in the interspace. This study focuses on the behaviour of widely used combustible MLI in a fire scenario, at vacuum and atmospheric pressure conditions. The former corresponds to the typical design condition and the latter to the condition after an outer hull rapture of a tank. Furthermore, two fire scenarios were taken into account: a standard-oriented approach and a hydrocarbon fire-oriented approach. For the study, a test rig was applied that allows testing of TSI at industrial conditions and subsequent analysis of TSI samples. The test rig allows thermal loading and performance analysis of TSI samples at the same time. Comparing the tests, the samples degraded differently. However, no sudden failure of the entire MLI was observed in any test. These results are relevant for the evaluation of incidents with tanks for the storage of cryogenic fluids and can thus contribute to the improvement of TSI and the development of emergency measures for the protection of persons and infrastructures. T2 - 15th International Symposium on Hazards, Prevention and Mitigation of Industrial Explosions (ISHPMIE) CY - Neapel, Italy DA - 10.06.2024 KW - Liquefied hydrogen KW - Liquefied natural gas KW - Cryogenic storage tank KW - Fire KW - Thermal insulation KW - Multi-Layer Insulation PY - 2024 SP - 707 EP - 717 AN - OPUS4-60460 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hajhariri, Aliasghar ED - Eberwein, Robert ED - Perrone, Luca pakj ED - Cozzani, Valerio ED - Otremba, Frank ED - Seidlitz, Holger T1 - Study the Impact of Spacer at Thermal Degradation Process of MLI-based Insulation in Fire Condition N2 - To reduce carbon dioxide emissions, energy carries such as hydrogen consider to be a solution. Consumption of hydrogen as a fuel meets several restrictions such as its low volumetric energy density in gas phase. To tackle this problem, storage as well as transportation in liquid phase is recommended. To be able to handle this component in liquid phase, an efficient thermal insulation e.g., MLI insulation is required. Some studies have been revealed vulnerability of this type of insulation against high heat flux, for instance a fire accident. Some investigations have been depicted the importance of consideration of the MLI thermal degradation in terms of its reflective layer. However, limited number of studies have been focused on the thermal degradation of spacer material and its effect on the overall heat flux. In this study, through systematic experimental measurements, the effect of thermal loads on glass fleece, glass paper as well as polyester spacers are investigated. The results are reported in various temperature and heat flux profiles. Interpreting the temperature profiles revealed as the number of spacers in the medium increases, the peak temperature detectable by the temperature sensor on the measurement plate decreases. Moreover, the contribution of each individual spacer in all cases regarding the experimental temperature range is assessed to be around 8%. This value may increase to around 50% for glass paper and polyester spacers, and to around 25% for glass fleece spacers as the number of spacer layers increases up to six layers. To utilize the outcomes of the experiment later and integrate the results into numerical and CFD simulations, a model is proposed for the mentioned experimental temperature range up to 300°C to predict a heat flux attenuation factor. The model proposes a fitting factor that can reproduce the least square fitted line to the experimental data. T2 - 15th International Symposium on Hazards, Prevention, and Mitigation of Industrial Explosions Naples (ISHPMIE) CY - Naples, Italy DA - 10.06.2024 KW - Multi-Layer Insulation KW - Cryogenics KW - Liquid Hydrogen KW - Heat Transfer KW - Hydrogen Storage PY - 2024 SP - 744 EP - 755 AN - OPUS4-60461 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Auersch, Lutz A1 - Said, Samir T1 - Measurement of slab track behaviour at different sites N2 - Measured train passages and hammer impacts in combination with track-soil calculation have been successfully used for the detection of damaged slab tracks. This approach is now extended to intact slab and ballast tracks. The vibrations of many tracks have been measured at several levels from rail, sleeper, track plate, base plate, base layer to the subsoil by velocity or acceleration sensors. The time histories have to be integrated once or twice to get the displacements. The displacement signals include an arbitrary time-dependent shift which must be eliminated or respected in the interpretation. On the other hand, the calculation of slab and ballast tracks have been done in frequency-wavenumber domain. The displacements along the track and the frequency-dependent compliance transfer functions can be calculated. The latter can be compared with the results of the hammer impacts on the track. The deformation of the track can be transformed to time histories for a whole train and compared to the measured train passages. Many slab (and ballast) tracks have been measured at different sites. The displacements of the tracks are presented, and the following parameters have been analysed in the measurement results: slab track vs. ballast track, different types of slab tracks, damaged slab tracks, different trains, switches at different measuring points, an elastic layer, the mortar layer, different soils at different places. The soil should have the dominant influence on the track-plate displacements. Slab and ballast track yield also big differences in maximum displacement and width of deformation. Some of the preceding aspects will be analysed in comparison of measurement and theory. T2 - 26th International Congress on Sound and Vibration (ICSV26) CY - Montreal, Canada DA - 07.07.2019 KW - Displacements KW - Slab track KW - Train passage KW - Hammer impact KW - Vibration measurements PY - 2019 SN - 978-1-9991810-0-0 SN - 2329-3675 SP - T15RS01_316_1 EP - T15RS01_316_8 PB - Canadian Acoustical Association CY - Montreal, Kanad AN - OPUS4-48498 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Uhlmann, E. A1 - Düchting, J. A1 - Petrat, T. A1 - Graf, B. A1 - Rethmeier, Michael T1 - Heat treatment of SLM-LMD hybrid components N2 - Additive manufacturing is no longer just used for the production of prototypes but already found its way into the industrial production. However, the fabrication of massive metallic parts with high geometrical complexity is still too time-consuming to be economically viable. The combination of the powder bed-based selective laser melting process (SLM), known for its geometrical freedom and accuracy, and the nozzle-based laser metal deposition process (LMD), known for its high build-up rates, has great potential to reduce the process duration. For the industrial application of the SLM-LMD hybrid process chain it is necessary to investigate the interaction of the processes and its effect on the material properties to guarantee part quality and prevent component failure. Therefore, hybrid components are manufactured and examined before and after the heat treatment regarding the microstructure and the hardness in the SLM-LMD transition zone. The experiments are conducted using the nickel-based alloy Inconel 718. T2 - LiM 2019 CY - München, Germany DA - 23.06.2019 KW - Additive Manufacturing KW - Selective Laser Melting KW - Hybrid components KW - Inconel 718 KW - Laser Metal Deposition PY - 2019 SP - 1 EP - 9 AN - OPUS4-48410 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Vahlsing, Thorsten A1 - Raum, Hanne A1 - Casperson, Ralf A1 - Pohl, Rainer A1 - Heckel, Thomas A1 - Beilken, D. A1 - Dilz, K. A1 - Rühe, S. T1 - FE-simulation of eddy current signals produced from basic model cracks for running surface rail defects N2 - Non-destructive testing for surface crack detection and head check depth quantification at the gauge corner of railway tracks can be achieved using eddy current methods. With the extension of the tested zone to the running surface, rail defect signal types other than head checks can be measured. Due to their mostly irregular shape, a quantitation based on a calibration against regular test cracks of varying depth may not be linear. Estimates of the expected influence of more complex crack patterns may be obtained by a finite element simulation of sufficiently simple limiting cases, like two displaced or intersecting cracks or a simply branched or flexed crack. As a first step, a 3D finite element model of the HC10 eddy current probe distributed by Prüftechnik Linke und Rühe (PLR), Germany was built and verified against measured results from an (easily fabricated) reference block with isolated long cracks. T2 - 15th Railway Engineering Conference CY - Edinburgh, UK DA - 03.07.2019 KW - Finite element analysis KW - Eddy current testing KW - Rail inspection PY - 2019 SP - 1 EP - 11 AN - OPUS4-48529 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schlegel, Moritz-Caspar A1 - Akkerman, Floris T1 - One step back, two steps forward – Resource efficiency requirements within ecodesign N2 - Resource efficiency is a much discussed topic in terms of improving the sustainability of energy related and energy non-related products. Resource efficiency aspects such as the availability of spare parts, the ability to dismantle, etc. have been included in draft working documents in the revision of several already existing Ecodesign regulations as a first step. However, often these aspects are not consistent with the current technology and design of these products. A possible reason could be a lack of sufficient consultation or of a methodology which is sufficiently tailored for this topic. The established strategies and tools, used by policymakers, such as the Methodology for the Ecodesign of Energy-related Products (MEErP), do not seem to deal with these aspects appropriately. Draft requirements need to be very well developed before being discussed with member states and other related stakeholders, because including resource efficiency parameters could lead to additional, very wide-ranging effects on society. This topic cannot be covered well with legislative tools developed primarily for energy aspects. In this paper, a method is presented which can be used to combine products’ properties with crucial resource efficiency indicators. The method can be used to develop a set of draft legislative requirements and to pre-evaluate these requirements by target groups which would be affected by additional legal requirements. These include: market surveillance authorities, standardization organizations, manufacturers and their associations, environmental organizations and research facilities. The method incorporates stakeholders’ feedback to identify potential resource efficiency measures for materials and/or products, their impact on the European ecology, economy and society. Based on this it would help to develop legislative requirements which are feasible and desirable. The results can then be fed into the formal legislative process, probably speeding it up. T2 - ECEEE 2019 Summer Study on Energy Efficiency CY - Belambra Presqu'île de Giens, France DA - 03.06.2019 KW - Resources KW - Circular economy KW - Ecodesign KW - Energy policy PY - 2019 UR - https://www.eceee.org/library/conference_proceedings/eceee_Summer_Studies/2019/ SN - 978-91-983878-5-8 SN - 2001-7960 VL - 2019 SP - 1553 EP - 1562 AN - OPUS4-48341 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wosniok, Aleksander T1 - Messgenauigkeit und Reproduzierbarkeit bei der Messung der Brillouin-Frequenzverschiebung für die faseroptische Bestimmung der Temperaturverteilung N2 - Auf der Grundlage der in DIN EN 61757-2-2:2017 beschriebenen Standardisierungsmethoden wurden in dieser Arbeit wichtige Leistungsparameter von vier kommerziellen Messsystemen zur ortsaufgelösten faseroptischen Erfassung der temperatur- und dehnungsabhängigen Brillouin-Frequenzverschiebung untersucht. Gemäß der oben genannten Norm konzentrierte sich hier die Ermittlungsprüfung auf messtechnische Aspekte reiner Temperaturmessungen. Dabei diente die Ermittlung von einem festgelegten Satz dreier Betriebsverhaltenskenngrößen in Form von quantitativen Angaben des Messfehlers, der Wiederholgenauigkeit sowie der räumlichen Unsicherheit einem Vergleich der getesteten Messsysteme. Alle faseroptischen Messungen wurden mit einer Faserschleife ausgeführt, d. h. als Sensorkonfiguration der Messfaser wurde eine Schleifenanordnung gewählt. Die Messverfahren der getesteten Messysteme basierten somit auf der Brillouin-optischen Zeit- bzw. Frequenzbereichsanalyse. Die Betriebsverhaltenskenngrößen wurden ferner bei unterschiedlichen Werten zweier messtechnischer Parameter, des Frequenzschrittes und der Mittelungsrate, für Standardeinstellungen der Laserleistungswerte der in die Sensorfaser einzukoppelnden Laserlichtsignale ermittelt. Auf diesem Weg lassen sich relevante Aussagen zur Optimierung der Messgenauigkeiten in Bezug auf Messdauer treffen. T2 - 20. GMA/ITG-Fachtagung Sensoren und Messsysteme 2019 CY - Nuremberg, Germany DA - 25.06.2019 KW - Faseroptischer Sensor KW - Ortsaufgelöste Brillouin-Sensorik KW - Verteilte faseroptische Temperaturmessung KW - Brillouin-Frequenzverschiebung KW - Betriebsverhaltenskenngrößen PY - 2019 SN - 978-3-9819376-0-2 DO - https://doi.org/10.5162/sensoren2019/P2.1 SP - 656 EP - 662 PB - AMA Service GmbH CY - Wunstorf AN - OPUS4-48346 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Unger, Jörg F. A1 - Kindrachuk, Vitaliy A1 - Hirthammer, Volker A1 - Titscher, Thomas A1 - Pohl, Christoph T1 - The importance of multiphysics and multiscale modelling of concrete to understand its complex macroscopic properties N2 - Concrete is a complex material. Its properties evolve over time, especially at early age, and are dependent on environmental conditions, i.e. temperature and moisture conditions, as well as the composition of the material. This leads to a variety of macroscopic phenomena such as hydration/solidification/hardening, creep and shrinkage, thermal strains, damage and inelastic deformations. Most of these phenomena are characterized by specific set of model assumptions and often an additive decomposition of strains into elastic, plastic, shrinkage and creep components is performed. Each of these phenomena are investigated separately and a number of respective independent models have been designed. The interactions are then accounted for by adding appropriate correction factors or additional models for the particular interaction. This paper discusses the importance of reconsider even in the experimental phase the model assumptions required to generalize the experimental data into models used in design codes. It is especially underlined that the complex macroscopic behaviour of concrete is strongly influenced by its multiscale and multiphyscis nature and two examples (shrinkage and fatigue) of interacting phenomena are discussed. T2 - International RILEM Conference on Materials, Systems and Structures in Civil Engineering CY - Lyngby, Denmark DA - 22.08.2016 KW - Concrete KW - Multiscale KW - Multiphysics PY - 2016 VL - 1 SP - 115 EP - 124 PB - International RILEM Conference on Materials, Systems and Structures in Civil Engineering, Conference segment on COST TU1404 AN - OPUS4-38651 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lecompagnon, Julien A1 - Hirsch, Philipp Daniel A1 - Rupprecht, C. A1 - Ziegler, Mathias ED - Mendioroz, A. ED - Avdelidis, N. P. T1 - Thermographic testing using 2D pseudo-random illumination and photothermal super resolution reconstruction N2 - Due to the diffusive nature of heat propagation in solids, the detection and resolution of internal defects with active thermography based non-destructive testing is commonly limited to a defect-depth-to-defect-size ratio greater than or equal to one. In the more recent past, we have already demonstrated that this limitation can be overcome by using a spatially modulated illumination source and photothermal super resolution-based reconstruction. Furthermore, by relying on compressed sensing and computational imaging methods we were able to significantly reduce the experimental complexity to make the method viable for investigating larger regions of interest. In this work we share our progress on improving the defect/inhomogeneity characterization using fully 2D spatially structured illumination patterns instead of scanning with a single laser spot. The experimental approach is based on the repeated blind pseudo-random illumination using modern projector technology and a high-power laser. In the subsequent post-processing, several measurements are then combined by taking advantage of the joint sparsity of the defects within the sample applying 2D-photothermal super resolution reconstruction. Here, enhanced nonlinear convex optimization techniques are utilized for solving the underlying ill-determined inverse problem for typical simple defect geometries. As a result, a higher resolution defect/inhomogeneity map can be obtained at a fraction of the measurement time previously needed. T2 - Thermosense: Thermal Infrared Applications XLIV CY - Orlando, Florida, USA DA - 05.04.2022 KW - Thermography KW - Super resolution KW - NDT KW - Material testing KW - Internal defects KW - DMD KW - DLP PY - 2022 DO - https://doi.org/10.1117/12.2618562 SN - 0277-786X VL - 12109 SP - 1 EP - 10 PB - SPIE AN - OPUS4-54909 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Krankenhagen, Rainer A1 - Maierhofer, Christiane ED - Drachenberg, T. T1 - Thermische Kontraste - Der Blick hinter die Fassade N2 - Die Thermografie beruht auf der bildlichen Darstellung von Temperaturunterschieden oder auch thermischen Kontrasten an der Oberfläche eines Untersuchungsobjektes. Diese bilden sich nur her-aus, wenn sich das Untersuchungsobjekt gerade erwärmt oder abkühlt. Der Beitrag erklärt mittels eines stark vereinfachten Modells die Entstehung solcher Kontraste als dynamischen Effekt verschiedener Abkühlgeschwindigkeiten. Neben Laborergebnissen werden beispielhaft einige Ergeb-nisse von einem mittelalterlichen Baudenkmal präsentiert, um das Verständnis für die thermografische Inspektion von Fassaden zu vertiefen. T2 - 14. Konservierungswissenschaftliches Kolloquium Berlin Brandenburg CY - Berlin, Germany DA - 12.11.2021 KW - Ablösungen KW - Aktive Thermografie KW - Bauthermografie KW - Metallanker PY - 2021 SN - 978-3-945880-90-6 VL - 61 SP - 104 EP - 119 PB - Hendrik Bäßler CY - Berlin AN - OPUS4-55475 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Barretto, T. A1 - Gentes, S. A1 - Braun, J. A1 - Averin, Anton A1 - Lecompagnon, Julien A1 - Stroncik, N. T1 - Automated non-destructive internal corrosion detection on radioactive drums (ZIKA) N2 - The aim of the ZIKA research project, funded by the BMBF funding program FORKA (FKZ:15S9446 A-C), is the automated detection of internal corrosion of radioactive drums using non-destructive testing (NDT). The newly gained findings will be combined with research results from the previous project EMOS (FKZ:15S9420), which dealt with the external damage of drums. Using NDT, internal corrosion and possible internal sources of damage can be identified before they become a safety-relevant issue. However, if internally sourced damages can be seen externally, the integrity of the damaged drum is no longer guaranteed, which has significant consequences. Therefore, early detection before integrity failure is of particular importance for interim storage facilities with low- and medium-level radioactive waste drums. T2 - Kerntechnik 2024 CY - Leipzig, Germany DA - 11.06.2024 KW - Corrosion detection KW - Non-destructive testing KW - Automated inspection system PY - 2024 SP - 1 EP - 5 AN - OPUS4-60322 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Pech May, Nelson Wilbur A1 - Lecompagnon, Julien A1 - Hirsch, Philipp Daniel A1 - Ziegler, Mathias T1 - Robot-assisted infrared thermography for surface breaking crack detection on complex shaped components N2 - Infrared thermography using a focused (spot or line) beam has proved to be effective for detection of surface breaking cracks on planar samples. In this work, we use the same principle, but applied to complex shaped components, like a rail section, a gear, and a gas turbine blade. We use a six-axis robot arm to move the sample in front of our thermographic setup. Several scanning paths and thermographic parameters are explored: scanning speed, density of points in each scanning slice, laser power and camera frame-rate. Additionally, we explore semi-automatic evaluation algorithms for crack detection, as well as 2D-to-3D registration of the found indications. T2 - SPIE Future Sensing Technologies, 2023 CY - Yokohama, Japan DA - 18.04.2023 KW - Complex shaped component testing KW - Flying line thermography KW - Robot-assisted thermography KW - Crack detection KW - Robot path planning KW - 2D/3D thermographic registration PY - 2023 DO - https://doi.org/10.1117/12.2666757 VL - 12327 SP - 1 EP - 3 PB - SPIE Future Sensing Technologies AN - OPUS4-59867 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Koch, Claudia A1 - Blind, K. ED - Jakobs, K. ED - Morone, P. T1 - Testbeds for standardization in the IIoT N2 - In the paper, we discuss the role and impacts of testbeds in standardization for the industrial internet of things. Based on a multiple case study, four different approaches were identified followed in the testbeds with regard to their standardization activities. T2 - 24th EURAS Annual Standardisation Conference CY - Rom, Italy DA - 13.06.2019 KW - IIoT KW - Industrie 4.0 KW - Normen KW - Standards KW - Normung KW - Standardization KW - Agile KW - Testbed PY - 2019 SN - 978-3-95886-282-1 SP - 215 EP - 234 PB - Verlagshaus Mainz CY - Aachen AN - OPUS4-49121 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -