TY - CONF A1 - Eberwein, Robert A1 - Hajhariri, Aliasghar A1 - Camplese, Davide A1 - Scarponi, Giordano Emrys A1 - Cozzani, Valerio A1 - Otremba, Frank T1 - A comparative study on insulation materials in tanks for the storage of cryogenic fluids in fire incidents N2 - Liquefied Hydrogen (LH2) or Liquefied Natural Gas (LNG) establish themselves as important energy carriers in the transport sector. Its storage requires tanks with Thermal Super Insulations (TSI) to keep the transported fluid cold. TSI has proven itself in various applications over a long time, but not in the land transport sector, where accidents involving collisions, fires, and their combination are to be expected. The focus of this study is to investigate the behavior of different types of TSI when exposed to a heat source that represents a fire. Therefore, a High-Temperature Thermal Vacuum Chamber (HTTVC) was used that allows the thermal loading of thermal insulation material in a vacuum and measuring the heat flow through the TSI in parallel. Within this study, 5 samples were tested regarding 3 different types of MLI, rock wool, and perlites. The thermal exposure caused different effects on the samples. In practice, this can be connected to the rapid release of flammable gases as well as a Boiling Liquid Expanding Vapour Explosion (BLEVE). These results are relevant for the evaluation of accident scenarios, the improvement of TSI, and the development of emergency measures. T2 - IMECE 2023 CY - New Orleans, Louisiana, USA DA - 29.10.2023 KW - LH2 KW - LNG KW - Fire PY - 2023 SP - 1 EP - 7 AN - OPUS4-58768 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eberwein, Robert A1 - Scarponi, Giordano T1 - Performance of MLI systems for LH2 Tanks in fire scenarios N2 - In the course of decarbonizing the energy industry, cryogenic energy carriers are seen as having great potential. This is because they allow significantly higher volumetric energy densities to be achieved than when these energy carriers are stored at typical temperatures on Earth. This is important for numerous energy-intensive applications, such as those found in all transport sectors. Important cryogenic energy carriers include liquefied hydrogen (LH2) and liquefied natural gas (LNG). The challenge is to keep the energy carrier cold for a long time. This is achieved by the implementation of thermal super-insulations (TSI) systems based on multilayer insulations (MLI), microspheres, perlites, and vacuum for instance, and which have proven to be effective in several cryogenic applications. However, due to the short period of use, the low number of documented incidents, and the still few investigations carried out in the field, the exploitation of such systems in the transport sector still suffers from insufficient knowledge about the course and consequences of incidents. Accidents involving collisions, fires, and their combination are quite common in the transportation sector and may generate extraordinary loads on the tank and its insulation system, eventually leading to tank failure. The presentation summarizes the findings from the cooperation of the University of Bologna and BAM regarding the experiments on diverse types of super-insulations with the High Temperature Thermal Vacuum Chamber, as well as the model approaches that were developed to calculate the heat transfer and degradation of MLI’s during high thermal exposure. As an outlook the application of the models, the Cryogenic High Temperature Thermal Vacuum Chamber, and the fire test on HGV-components are presented. T2 - ELVHyS - International Stakeholder's Seminars CY - Bologna, Italy DA - 30.09.2024 KW - LH2 KW - LNG KW - Cryogenic storage tank KW - Fire KW - Safety PY - 2024 AN - OPUS4-61205 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Camplese, Davide T1 - Modelling Fire Response of Cryogenic Liquid Hydrogen Tanks Equipped with Multilayer Insulation (MLI) Systems N2 - In the context of the growing global interest in hydrogen-based green energy, cryogenic tanks equipped with multi-layer insulation (MLI) are emerging as a leading solution for storing hydrogen in vehicles. The integrity of these systems might be threatened during fire exposure. This can trigger the degradation of the MLI materials and induce rapid pressurization of the tank with a high risk of catastrophic failure. In this work, a novel lumped model to simulate the thermal response of MLI-equipped cryogenic liquid hydrogen tanks is presented. The model integrates the accurate database “Coolprop” for hydrogen thermodynamic properties and sub-models for detailed simulation of MLI degradation, providing a realistic simulation of the experimental data obtained under normal operating conditions. The application of the model to several case studies considering different numbers of MLI layers and tank geometries demonstrates that aluminum-based MLI offers scarce protection in case of exposure to a hydrocarbon poolfire. T2 - CISAP 11 CY - Neapel, Italy DA - 15.09.2024 KW - Liquefied hydrogen KW - LNG KW - Fire KW - Insulation KW - MLI PY - 2024 AN - OPUS4-61389 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eberwein, Robert T1 - Storages For Cryogenic Gases And Their Safety Part 1 N2 - To accelerate the hydrogen uptake in Europe the project KICstartH2 funded by the European Union arranged the Joint European Summer School (JESS) that deals with several topics around hydrogen. A topic in this framework is the transport and storage of energy by hydrogen. Here cryogenic energy carriers are seen as having great potential. This is because they allow significantly higher volumetric energy densities to be achieved than when these energy carriers are stored at typical temperatures on Earth. This is important for numerous energy-intensive applications, such as those found in all transport sectors. Important cryogenic energy carriers include liquefied hydrogen (LH2) and liquefied natural gas (LNG). This presentation focuses on the physical parameters and methods relevant to the storage of cryogenic fluids. T2 - Joint European Summer School (JESS) CY - Athens, Greece DA - 15.09.2024 KW - Liquefied hydrogen KW - Liquefied natural gas KW - Cryogenic storage tank PY - 2024 AN - OPUS4-61083 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hajhariri, Aliasghar T1 - Investigation of Super Insulation degradation of a tank for cryogenic goods. Effect of fire on the storage of Cryogenic fluids N2 - Cryogenic liquefied gases, such as liquid hydrogen (LH2) and liquefied natural gas (LNG), are becoming more popular as eco-friendly energy sources. However, using these gases more often increases the risk of accidents, making it important to conduct thorough risk assessments. The storage systems for these gases rely on thermal superinsulation (TSI), which can fail under extreme heat, especially during fires. Therefore, it is essential to study how and why TSI fails. This research (part of PhD topic) aims to examine insulation performance, thereby improving the overall safety of cryogenic storage systems. T2 - Colloquium of Departement 3 CY - Berlin, Germany DA - 27.05.2024 KW - Investigation KW - Insulation degradation KW - Tank for cryogenic goods PY - 2024 AN - OPUS4-60462 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eberwein, Robert T1 - Novel Insulation Concepts for Large Scale Liquefied Hydrogen Storages N2 - The NICOLHy project aims to develop a novel insulation concept based on Vacuum Insulation Panels (VIP) that enables the safe, cost- and energy efficient storage of large quantities of LH2. Such large scale LH2 storage technology is necessary for establishing a hydrogen economy with dimensions between 40.000 m³ and more than 200.000 m³ of LH2. However, new design concepts are needed because the currently available technologies used in small and medium storages today are not suitable for up-scaling. The main problems prohibiting the up-scaling are the long production time due to the process chain, the low failure tolerance and the spherical shape, which reduces the payload in technical applications by up to 50% compared to other shapes. The novel concept will change these conditions by a system which is modular, open-form, time-and cost efficient while production, operation and service, multi-failure tolerant and applicable for onshore and offshore applications. The presentations shows details to the concept and presents several safety concerns the project has to deal with. T2 - ELVHyS - International Stakeholder's Seminars CY - Bologna, Italy DA - 30.09.2024 KW - LH2 KW - Insulation KW - Safety PY - 2024 AN - OPUS4-61208 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Harwege, Finn T1 - Characterisation of vacuum insulation panel based cryogenic insulation N2 - Current medium to large scale hydrogen storage tanks utilize a double walled tank with vacuum and a low thermal conductivity powder as bulk fill between the two tank walls. This approach offers poor failure resistance and is not economic to build at a large scale. In NICOLHy an alternative cryogenic insulation concept using vacuum insulation panels (VIP) targeted for tanks with capacities from 40 000 m³ to 100 000 m³ is in research. VIPs consist of a gas tight envelope that surrounds a low conductivity core material. Within the envelope, a vacuum is created, which supresses convective heat transfer. Since the core material is typically very low thermal conductivity, while the envelope material has a relatively high thermal conductivity, thermal bridges where two adjoining panels meet cannot be avoided. Modeling of the thermal behaviour of VIPs exists for the building industry, but not for cryogenic temperatures or applications with multiple layers of VIPs, both of which present a new challenge. Here, these challenges and goals for the thermal modeling within the project are presented, alongside an overview over the project itself. T2 - Themenvorstellung beim BTU Arbeitsgebiet Technische Akustik CY - Cottbus, Germany DA - 23.09.2024 KW - Liquefied Hydrogen PY - 2024 AN - OPUS4-61122 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Grotelüschen, Frank A1 - Eberwein, Robert A1 - Berhorst, Ralf T1 - Supertanker für H2: EU-Projekt konstruiert günstigen Riesenspeicher N2 - Wasserstoff stellt einen potenziellen Energieträger für den großskaligen Import von Energie nach Europa dar. Von seinen verschiedenen Speicherformen eignet sich hierfür insbesondere verflüssigter Wasserstoff, mit dem sich auf gleichem Volumen deutlich mehr Energie speichern lässt als bei der druckbasierten Speicherung. Verflüssigter Wasserstoff wird bei minus 253°C gespeichert und muss für dessen Transport lange bei dieser niedrigen Temperatur gehalten werden. Dies stellt besondere Herausforderungen an die thermische Isolation von Tanks. Der Erforschung nachhaltiger, kosten- und energieeffizienter sowie sicherer thermischen Isolationen wird im NICOLHy Projekt, unter Leitung der BAM, nachgegangen. KW - Verflüssigter Wasserstoff KW - Thermische Isolation PY - 2024 UR - https://www.deutschlandfunk.de/supertanker-fuer-h2-eu-projekt-konstruiert-guenstigen-riesenspeicher-dlf-d50ff14a-100.html PB - Deutschlandradio CY - Hamburg AN - OPUS4-60538 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Detjens, Marc A1 - Hübert, Thomas A1 - Tiebe, Carlo A1 - Banach, Ulrich T1 - Coulometric trace humidity measurement in technical gases N2 - Trace humidity was measured by using miniaturized planar coulometric sensors in technical gases such as hydrogen, nitrogen, helium, nitrous oxide, and synthetic air. Frost point temperatures tf in the gases ranged from −60 °C to −30 °C, which is equivalent to a vapour mole fraction xv from 10 μmol mol−1 to 376 μmol mol−1. In addition, the generated humidity was determined by using a precision dew point hygrometer as reference. Nonlinear calibration functions were calculated that correlated electric current (sensor signal) and reference humidity. Parameters of functions were tested with one-way analysis of variances (ANOVA) to prove if all used sensors had a similar behavior in the same gas during experiments. Results of ANOVA confirmed that averaged functions can be applied for trace humidity measurement in nitrogen, helium, nitrous oxide, and synthetic air. The calculated functions were negligibly different for nitrogen, helium, and synthetic air. In humidified nitrous oxide, a minor change of parameters was observed due to lower electrical currents. In total contrast to that, the measured sensor signals were significantly higher in humidified hydrogen and each sensor required its own calibration function. The reason was a recombination effect that favoured multiple measurements of water molecules. Nevertheless, it was possible to measure continuously trace humidity in all tested gases by using coulometric sensors with an expanded uncertainty below 2 K (k = 2). KW - ANOVA KW - Trace humdity measurement KW - Coulometric sensors KW - Chemical sensors KW - Measurement uncertainty PY - 2018 DO - https://doi.org/10.1063/1.5008463 SN - 0034-6748 SN - 1089-7623 VL - 89 IS - 8 SP - 085004, 1 EP - 8 PB - American Institute of Physics (AIP) CY - Maryland (USA) AN - OPUS4-45956 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Holtappels, Kai T1 - Renewable energies in Germany – Safety aspects with respect to pipelines N2 - BAM was asked to present German strategies and Projects with respect to Pipelines. Beside an introduction to BAM three Major Topics were presented: Power-to-Gas strategy in Germany, an application of distributed acoustic and fiber optic sensors for the continuous monitoring of pipes and so-called West-Jefferson Tests. T2 - 1st International Cold Regions Oil & Gas Seminar CY - Seoul, Korea DA - 07.12.2016 KW - Pipelines KW - Power-to-gas KW - Distributed acoustic sensors KW - Fiber optics PY - 2016 AN - OPUS4-38708 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tiebe, Carlo T1 - Explosive trace detection by ion mobility spectrometry for air cargo screening N2 - This article describes the application of the ion mobility spectrometry (IMS) as a technical link in the screening within the airfreight transport chain. Air freight is of very important also for German foreign trade. Every year around 4.3 Mt of freight are loaded at German airports and transported by air planes. The average value of a transported metric ton freight was approximately 81,000 € in 2015. Nearly 50 percent of the total air freight is transported in passenger planes as belly freight. Measures are necessary to detect illegal, dangerous items such as weapons, ammunition or improvised explosive devices (IED) to protect against attacks on air traffic security. The aim is to increase security in air traffic and at the same time contemporary increasing or at least unchanged efficiency in the airfreight transport chain. IMS is a suitable instrumental technology for the trace detection of explosives (ETD) and their precursors orthogonal to radiological x-ray measurements on suspicious freight within 30 seconds and per EU regulation 2015/1998, section 6.2. The ECAC* certified ETD system QS-B220 was used. The IMS performance is demonstrated on three target compounds, TNT, RDX and PETN. The results’ evaluation of this semi-quantitative screening is carried out by using statistical methods for reliability assessment, such as probability of detection (POD) and receiver operating characteristic (ROC). Their detection limits with a POD = 0.90 are determined after swab sampling on various surfaces. These screening results provide an objective decision-making aid to responsible control personnel in addition to x-ray measurements, whether there are or are no dangerous substances or objects in the cargo. *) ECAC = European Civil Aviation Conference T2 - 26th International Conference on Ion Mobility Spectrometry CY - Ozarow Mazowiecki (Warsaw), Poland DA - 23.07.2017 KW - Air traffic security KW - Ion mobility spectrometry KW - Explosive trace detection KW - Airfreight transport chain PY - 2017 AN - OPUS4-41188 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Prewitz, Marc T1 - Glaskapillaren für die Wasserstoffhochdruckspeicherung N2 - Wasserstoff spielt eine wichtige Rolle im Bereich der erneuerbaren Energien. Um die hohe gravimetrische Energiedichte auszunutzen, bietet sich die die Hochdruckspeicherung an. Um die theoretische Festigkeit, die geringe Wasserstoffpermeabilität vom Werkstoff „Glas“ und das Wissen von Griffith auszunutzen, sollten Glaskapillaren zum Einsatz kommen. Glas bietet diverse Möglichkeiten solche Kapillaren anzuordnen. Es beginnt bei der Bündelung von Einzelkapillaren und geht bis hin zu ganzen Strukturen. Allerdings stellt sich auch die Frage wie die Berstdruckfestigkeit optimal ausgenutzt und dabei noch die Permeation und das mechanische Langzeitverhalten beachtet werden kann. Ziel dieser Arbeit ist es, die wichtigen Einzelkomponenten diesbezüglich zu untersuchen und einen Langzeitspeicher mithilfe von Simulationen auszulegen. T2 - Fachausschuss I der DGG CY - Würzburg, Germany DA - 09.03.2016 KW - Wasserstoff KW - Hochdruckspeicherung KW - Glaskapillaren PY - 2016 AN - OPUS4-38389 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Holtappels, Kai T1 - Real-scale experiments in the field of fire and explosion safety - The test site for technical safety of BAM N2 - Die BAM hält mit dem TTS umfangreiche Möglichkeiten für Großversuche im Bereich Brand- und Explosionsschutz. Neben dem Themenfeld-Projekt CoFi-ABV werden andere Projekte des Fachbereichs 2.4 kurz vorgestellt. Außerdem werden die Möglichkeiten der BAM dargestellt, Behörden und Organisationen mit Sicherheitsaufgaben mit wissenschaftlich-technischer Expertise zu unterstützen. T2 - 13. Europäischer Katastrophenschutzkongress in Berlin CY - Berlin, Germany DA - 19.09.2017 KW - Großversuche KW - Explosionsschutz KW - Explosion KW - Behälterversagen KW - Alternative Kraftstoffe PY - 2017 AN - OPUS4-42181 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ried, Peter T1 - H2-permeability and burst pressure of glass capillaries N2 - This publication deals with the topics: pressure loading, permeability and burst pressure T2 - Intern. Con. on Glass ICG 2010 CY - Bahia, Brazil DA - 20.09.2010 KW - Pressure loading KW - Permeability KW - Burst pressure PY - 2010 N1 - Geburtsname von Kluge, Martin: Beckmann-Kluge, M. - Birth name of Kluge, Martin: Beckmann-Kluge, M. AN - OPUS4-22296 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schmidt, Anita T1 - UN-Kisten aus aller Welt N2 - Die BAM ist zuständige Behörde für die Zulassung von Gefahrgutverpackungen. Jetzt wurden die in der BAM eingegangenen Gefahrgutverpackungen aus Wellpappe des vergangenen Jahres auf ihre Zulassungskonformität überprüft. Dabei wurden 176 aus 16 Ländern auf Berstfestigkeit und Wasseraufnahme geprüft. KW - Gefahrgut KW - Transport KW - Logistik KW - Verpackung KW - Zulassung PY - 2017 SN - 0016-5808 VL - 2017 IS - 4 SP - 14 EP - 16 PB - Storck-Verlag Hamburg CY - Hamburg AN - OPUS4-40967 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Thöns, Sebastian A1 - Faber, M.H. A1 - Rücker, Werner T1 - Life cycle cost optimized monitoring systems for offshore wind turbine structures N2 - Monitoring information should be utilized to support optimal decisions. In this sense monitoring systems should be designed such as to optimize expected Life Cycle Costs. PY - 2013 SN - 978-3-200-03179-1 IS - Chapter 4 SP - 75 EP - 90 CY - Vienna, Austria AN - OPUS4-29103 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Holtappels, Kai T1 - Trust in Hydrogen Technologies - Safety Issues in the Hydrogen Value Chain N2 - In June 2020, updated in July 2023, the German government presented the National Hydrogen Strategy (NHS), its first strategy for achieving the goals of its hydrogen policy. The NHS sets out a coherent framework for action for the future production, transportation and use of hydrogen and its derivatives, including the corresponding research, innovations and investments. Various measures have been defined to achieve goals such as the decarbonization of various sectors and the market introduction of hydrogen technologies. This will ultimately lead to the introduction of many “new” technologies in many areas of our daily lives, which will only be successful if decision-makers and the public are convinced that these technologies are safe. Therefore, the safety of hydrogen technologies is an important pillar in gaining and maintaining confidence in these new technologies. Safety must keep pace with, or better still, anticipate trends in technological development in order to avoid overly conservative and expensive safety solutions, and at the same time demonstrate the usability and safety of hydrogen. Otherwise, single incidents – not necessarily explosions – can easily lead to uncertainties and therefore to a decrease in trust and acceptance. The presentation will give an overview of how safety issues are addressed in Germany. T2 - Department Seminar - Public Lecture CY - Windhoek, Namibia DA - 12.09.2025 KW - Trustworthiness KW - Hydrogen value chain KW - Safety KW - Public lecture PY - 2025 AN - OPUS4-64438 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tiebe, Carlo A1 - Hübert, Thomas A1 - Lorek, A. A1 - Wernecke, R. T1 - New planar trace humidity sensor N2 - A new planar sensor element for continuous coulometric trace humidity measurements in industrial gases has been developed. In order to ensure precise measurements a calibration facility including a precision dew point hygrometer as a reference device was developed. The sensor can measure the humidity in the frost point temperature range of -20 °C to -80 °C and has an expanded uncertainty of 2 K, a fast reaction time and a settling time of the entire system from 15 to 30 min. T2 - IMCS 2012 - 14th International meeting on chemical sensors CY - Nuremberg, Germany DA - 20.05.2012 KW - Trace humidity KW - Coulometric principle KW - HUMITRACE sensor KW - Humidity measurement PY - 2012 SN - 978-3-9813484-2-2 DO - https://doi.org/10.5162/IMCS2012/3.4.2 SP - 294 EP - 297 PB - AMA Service GmbH CY - Wunstorf AN - OPUS4-27570 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Holtappels, Kai T1 - Understanding the science and technology of hydrogen and clean energy projects N2 - As part of the Global African Hydrogen Summit, participating young people and students in Namibia and Africa learned how science and technological developments are interrelated and influence the development of a hydrogen infrastructure in Namibia. There is a global shortage of skilled workers, particularly in Namibia, who are needed now to build pilot plants and in the future to operate large-scale plants in Namibia. The presentation was intended to motivate the audience to pursue a relevant course of study and thus create prospects for the future. T2 - Global African Hydrogen Summit - Youth Programme CY - Windhoek, Namibia DA - 09.09.2025 KW - Science and technology KW - Open research topics KW - Skilled workers PY - 2025 AN - OPUS4-64437 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Gradt, Thomas T1 - Tribological properties of polymer composites for applications in LNG environment N2 - In a first test series, the friction and wear properties of 6 polymeric candidate materials for application in LNG tribosystems were tested. The most favorable properties showed PTFE composite, filled with carbon fibers and PEEK, which showed low and stable friction and a wear coefficient in the order of 10-7 mm3N-1m-1. PTFE containing PEEK composites seem to be also appropriate for LNG applications. Admixtures of graphite as solid lubricant result in lower wear. Contrary, a lubricating mechanism of MoS2 was not observed. The PI-materials showed comparatively high friction and medium wear. T2 - 21th International Colloquium Tribology CY - Stuttgart/Ostfildern, Germany DA - 09.01.2018 KW - Tribology KW - PEEK KW - PTFE composite KW - Friction PY - 2018 AN - OPUS4-43899 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Prewitz, Marc A1 - Müller, Ralf A1 - Marotzke, Christian A1 - Holtappels, Kai T1 - Characterization of glass capillary storage modules considering permeability and mechanical stress via finite elements N2 - Glass capillaries are potential candidates for long term hydrogen storage under high pressure. Burst pressure strongly drops with surface damaging, a polymer coating is needed. The aim is to study stress distribution within single coated glass capillaries sealed to metal fittings T2 - 88. Glastechnische Tagung DGG – ACerS GOMD 2014 CY - Aachen, Germany DA - 25.05.2014 KW - Burst test KW - Hydrogen storage KW - Polymer coating PY - 2014 AN - OPUS4-35784 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Theiler, Geraldine A1 - Gradt, Thomas T1 - Friction and wear behaviour of graphite filled polymer composites in hydrogen environment N2 - High performance polymer composites have been intensively investigated for tribological applications in air, but rarely in hydrogen environment. Author's previous benchmark of composites in liquid hydrogen (LH2) showed that graphite filled polymers have beneficial friction behaviour in this extreme condition. Therefore, further investigations have been undertaken in hydrogen environment. This paper presents first results obtained with polyimide composites filled with different types (natural, synthetic) and amounts of graphite in air, vacuum and hydrogen environments. A particular attention is taken to the influence of hydrogen on graphite as well as on the polymer matrix. KW - Polymer composites KW - Polyimide KW - Graphite KW - Friction KW - Wear KW - Hydrogen environment KW - Vacuum PY - 2015 DO - https://doi.org/10.2474/trol.10.207 SN - 1881-2198 VL - 10 IS - 2 SP - 207 EP - 212 CY - Tokyo, Japan AN - OPUS4-33554 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Liebig, F. A1 - Sarhan, R. M. A1 - Prietzel, C. A1 - Thünemann, Andreas A1 - Bargheer, M. A1 - Koetz, J. T1 - Undulated Gold Nanoplatelet Superstructures: In Situ Growth of Hemispherical Gold Nanoparticles onto the Surface of Gold Nanotriangles N2 - Negatively charged flat gold nanotriangles, formed in a vesicular template phase and separated by an AOT-micelle-based depletion flocculation, were reloaded by adding a cationic polyelectrolyte, that is, a hyperbranched polyethylenimine (PEI). Heating the system to 100 °C in the presence of a gold chloride solution, the reduction process leads to the formation of gold nanoparticles inside the polymer shell surrounding the nanoplatelets. The gold nanoparticle formation is investigated by UV−vis spectroscopy, small-angle X-ray scattering, and dynamic light scattering measurements in combination with transmission electron microscopy. Spontaneously formed gold clusters in the hyperbranched PEI shell with an absorption maximum at 350 nm grow on the surface of the nanotriangles as hemispherical particles with diameters of ∼6 nm. High-resolution micrographs show that the hemispherical gold particles are crystallized onto the {111} facets on the bottom and top of the platelet as well as on the edges without a grain boundary. Undulated gold nanoplatelet superstructures with special properties become available, which show a significantly modified performance in SERS-detected photocatalysis regarding both reactivity and enhancement factor. KW - Small-angle X-ray scattering KW - SAXS KW - gold KW - nanoparticle PY - 2018 DO - https://doi.org/10.1021/acs.langmuir.7b02898 SN - 0743-7463 VL - 34 IS - 15 SP - 4584 EP - 4594 PB - American Chemical Society AN - OPUS4-44704 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Holst, N. A1 - Khakpour, Thomas A1 - Holtappels, Kai A1 - Steinbach, J. T1 - Ignition behavior of methane-oxygen mixtures at elevated conditions N2 - Self-ignition behavior of mixtures of methane and oxygen was investigated in a temperature range from 600 to 800°C. Variations of mixture composition, inert gas content, temperature and filling rate of the ignition autoclave were carried out in order to establish process boundaries for high temperature partial oxidation processes. The tests show that considerably high methane contents are needed to avoid an ignition. Heating-up tests show that ignition is possible at surprisingly low temperatures. This can be attributed to pre-ignition reactions that produce more instable intermediates. T2 - 2011 AIChE Spring meeting & 7th global congress on process safety CY - Chicago, IL, USA DA - 13.03.2011 KW - Safety KW - Explosion KW - Self-ignition KW - Methane KW - Partial oxidation PY - 2011 SN - 978-0-8169-1067-10 IS - Topical 1 / #13 / 13h SP - 1 EP - 10 CY - New York, NY, USA AN - OPUS4-23626 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kröll, Mirco T1 - Tribological performance of polymer compounds in gaseous hydrogen N2 - In this study, friction and wear of conventional and alternative high performance polymer compounds, typically used for components of compressors, were investigated in gaseous hydrogen and nitrogen up to 80 bar of gas pressure. The compounds used were a commercial PEEK matrix with 10 wt.% each of PTFE, graphite, and short carbon fibres, a PPS matrix with 10 wt.% each of PTFE and graphite, and an experimental PA12 matrix with PTFE chemically coupled with an oleyl alcohol. Due to the cylindrical shape of the polymer samples, the contact area and pressure change if wear occurs. Therefore, experimental results of pre-screening tests have been used as input for FEM and an analytical model to determine the decreasing contact pressure over time. Afterwards, the outcome of the models was used to determine the duration of the experiments to reach typical contact pressures of seals in hydrogen compressors. T2 - ASMET TriboCorrosion International Conference 2025 CY - Vienna, Austria DA - 23.10.2025 KW - Hydrogen KW - Polymer KW - Tribometer KW - Comparability KW - Harmonisation KW - Oil-coupled compounds KW - Coefficient of Friction KW - Wear KW - FAIR data KW - Standardisation KW - Tribology KW - Database KW - i-TRIBOMAT PY - 2025 AN - OPUS4-64473 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Theiler, Geraldine A1 - Gradt, Thomas T1 - Gleitverhalten von PEEK-Kompositwerkstoffen in Wasserstoffumgebung N2 - Die Reibeigenschaften von PEEK Materialien gegen Stahlscheiben wurden in Luft, Vakuum und Wasserstoffumgebung untersucht. KW - PEEK-Komposite KW - Wasserstoff KW - Vakuum KW - Graphit PY - 2017 SN - 0724-3472 VL - 64 IS - 6 SP - 52 EP - 59 AN - OPUS4-42919 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Harwege, Finn A1 - Eberwein, Robert T1 - Testing of vacuum insulation panels for liquefied hydrogen storage tanks N2 - For the future use of liquefied hydrogen (LH2) as a green energy carrier, new concepts for storage tanks and in particular their insulation are necessary. The methodology applied in current LH2 tanks has some disadvantages while manufacturing and operation of large tanks that may be required in the future. While liquefied natural gas tanks exist in the necessary capacities, they are incompatible with LH2 due to its significantly lower storage temperature. In this paper, the possibility of using vacuum insulation panels (VIPs) as an alternative to the conventional double walled, powder filled vacuum insulation is presented. The two systems are introduced and compared on a conceptual level with a focus on the loss of vacuum failure mode. Furthermore, a test rig that enables the testing and quantification of thermal properties of VIP based insulations in ordinary and loss of vacuum conditions is presented. The test rig is a boil-off calorimeter using liquefied nitrogen and features a square cold surface with a side length of 3 m. An overview over the planned testing and its goals is given. KW - Liquefied Hydrogen KW - Insulation KW - Vacuum Insulation Panel KW - LH2 KW - Cryogenics PY - 2025 DO - https://doi.org/10.3303/CET2511612 SN - 2283-9216 VL - 2025 IS - 116 SP - 769 EP - 774 PB - AIDIC CY - Milano, Italy AN - OPUS4-63716 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bartelmeß, Jürgen T1 - Developments Towards a BODIPY-based fluorometric sensing device for multiple hazardous gases N2 - Fluorometric sensing is a versatile approach for trace analysis outside of the laboratory, requiring suitable sensor materials and their integration into sensing devices. The versatility of fluorophores as probes, especially in terms of the possibility to tailor their optical as well as their recognition properties by synthetic modifications in a wide range, renders them as superior active component for the preparation of optical sensing devices. Recent works at BAM in this field include, for example, the detection of nerve gas agents, illustrating impressively the aforementioned benefits of fluorophores in optical sensing applications. In the interdisciplinary project presented here, we target hazardous gases such as ammonia, benzene, and hydrogen sulfide, next to others, which pose a major threat to human health and environmental safety and for which the availability of a sensitive and reliable detection method is highly desirable. The dyes presented follow a “turn-on” fluorescence schematic, which allows for the selective and sensitive detection of the respective gaseous analyte. The immobilization of the probe in polymeric matrices is then the next step toward the fabrication of a prototype device for molecular sensing. Further steps in the project include the assembly of instruments for test-atmosphere generation, the referencing of the sensor system, development and implementation of an optical setup, and the testing of the prototype device under laboratory conditions and in the field. In this presentation, we give an overview over the recent developments on this topic in our groups. Highlights are hydrogen sulfide sensitive, BODIPY based transition metal complexes, which allow for a sensitive as well as selective detection of the toxic gas. In addition, we present a novel class of highly substituted BODIPY derivatives – pocket-BODIPYs – which are of a synthetically high versatility and can readily be modified to create pockets in the periphery of the molecule of defined geometries. This is illustrated on the successful encapsulation of benzene by a pocket-BODIPY derivative, confirmed by X-ray crystallographic analysis as well as by further spectroscopic and analytical methods. T2 - International Conference on Porphyrins and Phthalocyanins (ICPP-10) CY - Munich, Germany DA - 01.07.2018 KW - BODIPY dye KW - Fluorometric sensing KW - Gas sensing PY - 2018 AN - OPUS4-45646 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Thünemann, Andreas T1 - Structure Analysis of Functional Hydrogels with Small-Angle X-ray Scattering (SAXS) N2 - Hydrogel properties are largely determined by their network structure. Here, we report on the capabilities of SAXS methods for characterizing polymer-network gels. SAXS provides rich insight into different types and levels of nanostructural inhomogeneities in these soft matter materials. The structure analysis of alginate hydrogels, typically utilized in tissue engineering applications, will be discussed in detail. T2 - Polydays 2024 CY - Berlin, Germany DA - 30.09.2024 KW - SAXS KW - Small-angle X-ray scattering KW - Polymer KW - Gel PY - 2024 AN - OPUS4-61184 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schlichting, Joachim A1 - Ziegler, Mathias A1 - Maierhofer, Christiane A1 - Kreutzbruck, Marc T1 - Flying laser spot thermography for the fast detection of surface breaking cracks N2 - We report on recent developments in the detection of surface breaking cracks using flying laser spot thermography. Application of an infrared camera for mapping the thermal radiation after excitation with a diode laser equipped with an optical scanner allows us to examine a surface containing cracks in an entirely non-destructive, contactless and fast way, without even moving the camera. We developed an efficient and robust algorithm that can be applied directly to the recorded thermal sequences, and that derives a single image containing all crack signatures. For this crack detection technique, no specific synchronisation between laser and camera is required. Hence, our approach is suitable for an upgrade of existing thermographic systems. The feasibility of the proposed procedure is proven by testing an artificial test sample and a piece of rail that comprises roll contact fatigue cracks and by comparing the results with magnetic particle testing. T2 - 18th WCNDT - World conference on nondestructive testing CY - Durban, South Africa DA - 16.04.2012 KW - Thermography KW - Cracks KW - Laser KW - Flying spot PY - 2012 SN - 978-0-620-52872-6 IS - (Paper 499) SP - 1 EP - 7 AN - OPUS4-26352 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schilder, Constanze A1 - Kohlhoff, Harald A1 - Hofmann, Detlef A1 - Habel, Wolfgang ED - Boller, C. T1 - Structure-integrated fibre-optic strain wave sensor for pile testing and monitoring of reinforced concrete piles N2 - Reinforced concrete piles are used when structures are constructed on soft ground, because it is necessary to transfer the loads into deeper strata with a sufficient bearing capacity. Usually, static and dynamic pile tests are carried out in order to determine the pile’s behaviour and possible damages. The dynamic measurements can show the bearing behaviour and the structural integrity by using the theory of one-dimensional wave propagation. Commonly, the sensors are installed on the top of the pile head or embedded near the pile head. With the purpose of receiving more precise information about the pile features, now, a string of sensors is embedded at different levels of the pile. A fibre optic strain wave sensor has already been developed by Schallert. The sensor is based on the principle of the extrinsic Fabry-Perot interferometer and was already tested in laboratory and full-scale field tests with precast driven piles. It was possible to detect the introduced deformation caused by the static loading and the dilatational wave during dynamic low-strain as well as high-strain loading. Although the full-scale tests were successful, the high demands on the economy of the sensor required the optimisation of the sensor design. After laboratory tests with the optimised sensor, a cast-in-situ bored pile has been built at the BAM Test Site Technical Safety in Horstwalde, South of Berlin. In order to enable the comparison of the signals, additional fibre Bragg grating sensors, temperature sensors and resistance strain gauge sensors are embedded into the pile. In this paper, the optimised sensor and the setup of the cast-in-situ bored pile along with results of the conducted pile tests are shown together with an outlook on further field-tests in progress. T2 - EWSHM'12 - 6th European workshop on structural health monitoring 2012 CY - Dresden, Germany DA - 03.07.2012 PY - 2012 SN - 978-3-940283-41-2 VL - 1 SP - 523 EP - 530 CY - Berlin AN - OPUS4-26279 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Holtappels, Kai T1 - Nationale Allianz für Wasserstoff-Sicherheit N2 - Im Rahmen des jährlich stattfindenden BAM-UBA-Behörden-Erfahrungsaustauschs wurde vorrangig Mitarbeitenden aus örtlich zuständigen Vollzugs- und Genehmigungsbehörden die in Planung befindliche Nationale Allianz für Wasserstoff-Sicherheit vorgestellt. Die Allianz besteht aus insgesamt acht Institutionen mit einer breit aufgestellten Expertise zur Sicherheit von Wasserstoff und verfolgt das Ziel, die Entwicklung fehlender Methoden und Kriterien zur technischen Sicherheit von Wasserstoff voranzutreiben, Wissenslücken zu identifizieren und diese durch gemeinsame Forschung zu schließen sowie unabhängige und wissenschaftlich fundierte Bewertungen technischer Risiken bei Wasserstoffanwendungen vorzunehmen. T2 - BAM-UBA-Behördenerfahrungsaustausch CY - Berlin, Germany DA - 02.06.2025 KW - Wasserstoff KW - Sicherheit KW - nationale Allianz PY - 2025 AN - OPUS4-63429 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Detjens, Marc T1 - Influence of Gas Pressure on Coulometric Trace Humidity Measurement N2 - Planar coulometric sensors were investigated in humidified synthetic air at various absolute gas pressures, i. e. 2 bar, 5, bar, 10 bar, and 15 bar. Humidified gas flow at adjusted gas pressure was split into two flows, one passed a coulometric sensor and the other one passed a reference hygrometer after decompression. Both signals were recorded and then compared after calculation of resulting frost point temperature. Calculation is based on a calibration function obtained at ambient pressure. Comparison showed that an increasing pressure resulted in a higher derivation between sensor signal (calculated frost point temperature) and reference frost point temperature. At an absolute pressure of 2 bar the differences were minor in consideration of the uncertainty, however at 15 bar the differences were 6.77 K. Nevertheless, it was possible to measure the gas humidity at higher pressure with coulometric trace humidity sensors. T2 - 17th International Meeting of Chemical Sensors, IMCS 2018 CY - Vienna, Austria DA - 15.07.2018 KW - Gas pressure influence KW - Coulometric sensors KW - Trace humidity measurement PY - 2018 AN - OPUS4-45535 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Rübner, Katrin T1 - Aufbaukörnungen - Steigerung der Ressourceneffizienz im Bauwesen durch die Entwicklung innovativer Technologien für die Herstellung hochwertiger Aufbaukörnungen aus sekundären Rohstoffen auf der Basis von heterogenen Bau- und Abbruchabfällen, TP: Materialcharakterisierung KW - Bauabfall KW - Mineralischer Baustoff KW - Recycling KW - Granulieren PY - 2012 SP - 1 EP - 36 CY - Berlin AN - OPUS4-30066 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Schnell, A. A1 - Müller, A. A1 - Rübner, Katrin A1 - Ludwig, H.-M. ED - Thomé-Kozmiensky, K.J. ED - Goldmann, D. T1 - Mineralische Bauabfälle als Rohstoff für die Herstellung leichter Gesteinskörnungen N2 - enden Mengen und die erreichten Recyclingquoten sind in den seit 1996 erscheinenden Monitoringberichten der Arbeitsgemeinschaft Kreislaufwirtschaftsträger Bau dargestellt. In dem 2011 erschienen Bericht wird ausgewiesen, dass im Jahr 2008 58,2 Millionen Tonnen Bauschutt bestehend aus Beton- und Mauerwerkabbruch anfielen. Die Recyclingquoten bewegen sich um die 70 Prozent. Das in stationären oder mobilen Anlagen aufbereitete Material wird hauptsächlich im Tief- und Landschaftsbau eingesetzt. Ein Einsatz im Hochbau erfolgt nur durch einzelne Unternehmen. Hierbei werden hauptsächlich rezyklierte grobe Gesteinskörnungen für Normalbeton aus Betonbruch gewonnen. Heterogener Mauerwerkbruch, der Wandbaustoffe, Mörtel, Putz, Fliesen und weitere Bestandteile enthält, oder die bei der Aufbereitung zwangsläufig entstehenden Feinfraktionen finden bisher keine Verwendung. KW - Bauschutt KW - Bauabfälle KW - Leichte Gesteinskörnung KW - Stoffliches Recycling KW - Granulate PY - 2012 SN - 978-3-935317-81-8 VL - 5 SP - 469 EP - 494 PB - TK-Verl. CY - Neuruppin AN - OPUS4-25709 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Müller, A. A1 - Schnell, A. A1 - Rübner, Katrin T1 - Aufbaukörnungen aus Mauerwerkbruch N2 - Heterogene und feinkörnige Bauabfälle aus Mauerwerkbruch lassen sich heute nur auf einem sehr geringen Qualitätsniveau verwerten. Um diese Situation zu überwinden, wurde das Material als Rohstoff für die Herstellung von leichten Gesteinskörnungen verwendet, die ähnlich wie Blähtone und Blähschiefer in einem thermischen Prozess erzeugt werden. Auf der Grundlage einer Literaturübersicht wurde zunächst die grundsätzliche Eignung von Mauerwerkbruch bewertet. Es folgten experimentelle Untersuchungen, in welchen nachgewiesen werden konnte, dass Leichtgranulate mit definierten, einstellbaren Eigenschaften aus Mauerwerkbruch herstellbar sind. Sie sind in ihren Eigenschaften den leichten Gesteinskörnungen aus natürlichen Rohstoffen mindestens ebenbürtig. N2 - At present heterogeneous and fine-grained masonry rubble is recycled at a very low level. To overcome this situation the material is used as feedstock for the generation of lightweight aggregates, produced by a thermal process similar to the manufacturing of expanded clays and shales. On the basis of a literature review the suitability of masonry rubble as raw material is evaluated generally. Then materials from different recycling plants were experimentally tested. The results show, that expanded granules with defined, adjustable properties can be produced from masonry rubble. The properties of these secondary lightweight aggregates are at least equivalent to the properties of the known expanded clay aggregates. T2 - Lightweight Aggregates from Masonry Rubble KW - Blähgranulate KW - Leichte Gesteinskörnungen KW - Mauerwerkbruch KW - Rohstoffliches Recycling KW - Expanded aggregates KW - Feedstock recycling KW - Lightweight aggregates KW - Masonry rubble PY - 2012 DO - https://doi.org/10.1002/cite.201200089 SN - 0009-286X SN - 1522-2640 VL - 84 IS - 10 SP - 1780 EP - 1791 PB - Wiley-VCH Verl. CY - Weinheim AN - OPUS4-26643 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Gotor, Raúl A1 - Tiebe, Carlo A1 - Schlischka, Jörg A1 - Bell, Jérémy A1 - Rurack, Knut T1 - Detection of adulterated diesel using fluorescent test strips and smartphone readout N2 - The fluorescence properties of three molecular rotors, related to 4-dimethylamino-4-nitrostilbene (4-DNS), are studied versus different diesel/kerosene blends. In nonviscous solvents, these compounds can populate a twisted intramolecular charge transfer state which deactivates nonradiatively, successfully suppressing fluorescence emission. Solution experiments with diesel/kerosene blends showed a good linear correlation between the fluorescence intensity of the probe molecules and the diesel fraction of the blend. The dyes have been immobilized on paper, retaining their fluorescence behavior, i.e., negligible emission in the presence of nonviscous organic solvents and increasing fluorescence when the environment is increasingly viscous. When the impregnated paper is devised as a test strip, the latter is compatible with a newly designed smartphone reader system, which allows in-the-field measurements. The method can safely detect the presence of kerosene in diesel at ≥7%, which competes favorably with current standard methods for the detection of diesel adulteration. KW - Fuel adulteration KW - Diesel KW - Fluorescence KW - Test strip KW - Molecular rotor KW - Smartphone PY - 2017 DO - https://doi.org/10.1021/acs.energyfuels.7b01538 SN - 0887-0624 VL - 31 IS - 11 SP - 11594 EP - 11600 PB - American Chemical Society CY - Washington, D.C. AN - OPUS4-43103 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schmidt, Dirk T1 - Explosive cutting of pipelines for the determination of materials properties N2 - Incidents in the past already showed that pipelines transporting compressible fluids are in risk of suffering propagating ductile fractures in case of damages to the pipes. Therefore, the knowledge of the fracture properties of pipeline steels is of high importance. Commonly the properties are determined in laboratory scale, but these do not fully correspond with full-scale fracture behaviour especially at dynamic conditions when highly pressurized gases are released during the crack propagation. This paper describes so-called West Jefferson Tests and Midscale-Tests in which pipelines under pressure were cut with an explosive charge to initiate the crack propagation. T2 - 9th World Conference on Explosive and Blasting CY - Stockholm, Sweden DA - 10.09.2017 KW - Explosive cutting KW - Pipelines KW - Determination of materials PY - 2017 AN - OPUS4-41996 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Holtappels, Kai T1 - Sicherheit von Wasserstoff und Wasserstofftechnologien N2 - Der Nationale Wasserstoffrat (NWR) hat in einem Online-Seminar das Thema Sicherheit von Wasserstofftechnologien und aktueller Sachstand bzw. Herausforderungen in Deutschland aufgearbeitet. Dazu wurde ein Behördenvertreter (BAM), zwei Forschungsinstitutionen (FzJ und FhG IWM) sowie eine benannte Stelle (TÜV) eingeladen und die vorgestellten Themen in einem offenen Plenum diskutiert. T2 - Online-Seminar des Nationalen Wasserstoffrats CY - Online meeting DA - 07.06.2024 KW - Wasserstoff KW - Sicherheit KW - Herausforderungen KW - Elektrolyse KW - Dichtungswerkstoffe KW - Sicherheitsabstände KW - Reallabor BAM TTS KW - Nationale Allianz Wasserstoff-Sicherheit PY - 2024 AN - OPUS4-61483 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Theiler, Geraldine A1 - Gradt, Thomas T1 - Comparison of the sliding behaviour of several polymers in hydrogen N2 - The work presented here deals with the friction and wear behaviour of polymer materials in hydrogen. Commercially available grades of PEEK, PA, PPA, PAI, PI and PBI were investigated at room temperature in air and hydrogen gas (H2) as well as in liquid hydrogen at -253°C (LH2). T2 - 7th World Tribology Congress, WTC 2022 CY - Lyon, France DA - 10.07.2022 KW - Friction KW - Wear KW - Polymers KW - Hydrogen KW - Cryogenic PY - 2021 SP - 1 AN - OPUS4-62089 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Eberwein, Robert A1 - Rogge, Andreas A1 - Behrendt, F. A1 - Knaust, Christian T1 - Dispersion Modeling of LNG-Vapor on Land – A CFD-Model Evaluation Study N2 - Based on methane from renewable resources, LNG is an alternative fuel for heavy and long-distance traffic in land transport. Contrary to its positive properties, the fuel contains risks from an explosion and extremely low temperatures for personal and infrastructure safety. CFD-models are suitable for doing risk analyses for arbitrary scenarios. For examining how to model for risk research the dispersion of LNG-vapor, this paper contains a model variant study, with an evaluation by experiments. This paper describes the use of the CFD-code ANSYS Fluent for simulating experiments of the ‘LNG Safety Program Phase II‘. The content of the well-documented experiments was the research of the vaporization rate of LNG on land and the dispersion of LNG-vapor in the air. Based on the comparison to two experiments, overall 12 CFD-model variants with varying thermal and turbulence parameters were examined how they affect the transient LNG-vapor dispersion in air. The definition of turbulence-boundary-condition at the domain borders had the biggest impact on modeling, followed by the turbulence model. The most accurate model variant had been applied for observing the spreading behavior of LNG-vapor in the air after evaporation on land and analyzing the influence of the LNG-composition to the dispersion. The results show that the mixture of LNG-vapor and the air in the free field is cooler than the ambient air and spreads like a heavy gas on the ground. KW - LNG KW - CFD KW - Heavy gas KW - Model evaluation PY - 2020 DO - https://doi.org/10.1016/j.jlp.2020.104116 VL - 65 SP - 104116 PB - Elsevier Ltd. AN - OPUS4-50697 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schmidt, Anita T1 - Irrungen, Wirrungen und Lichtblicke - Überarbeitung des Gefahrguttransportrechts für Lithium- und Natrium-Ionen-Batterien N2 - Die Überarbeitung des Gefahrgutrechts hinsichtlich der Einstufung von Lithium- und Natrium - Ionen Batterien nach Gefährlichkeit trägt so einige Stilblüten - wie zuletzt den Vorschlag von 135 neuen UN Nummern für Lithiumbatterien. Die BAM trägt mit ihrer Kompetenz aus eigenen Untersuchungen und Forschung dazu bei, dass die deutsche Delegation bei den Vereinten Nationen, wo die Regelwerke weiterentwickelt werden, gezielte Vorschläge einbringen kann. Der Artikel beschreibt die aktuellen Entwicklungen. KW - Lithiumbatterien KW - Gefahrguttransport KW - Regelwerksentwicklung PY - 2024 VL - 2024 IS - 6 SP - 29 EP - 32 PB - Verkehrs-Verlag J. Fischer GmbH & Co. KG CY - Düsseldorf AN - OPUS4-62334 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schmidt, Anita T1 - Transport von Lithium-Batterien N2 - Im Bereich des Transports von Lithium-Batterien erfüllt die BAM gesetzliche Aufgaben. Diese betreffen insbesondere den Transport von Lithium-Batterien und die entsprechenden zulässigen (und von de BAM zugelassenen) Gefahrgutverpackungen. T2 - Erfa Verpackungen 2018 CY - Berlin, Germany DA - 27.09.2018 KW - Gefahrguttransport KW - Gefahrgutverpackungen KW - Lithium-Batterien PY - 2018 AN - OPUS4-47121 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tiebe, Carlo A1 - Banach, Ulrich A1 - Hübert, Thomas T1 - VDI/VDE-Richtlinie für Multigassensoren N2 - Technische Richtlinien enthalten Empfehlungen sowie Anforderungen zum Stand der Technik zur Aufstellung von Bewertungskriterien und Behandlung wissenschaftlich-technischer Fragen. Sie fördern den Erfahrungsaustausch und Technologietransfer zwischen Entwicklern und Anwendern. In unserem Beitrag stellen wir die Richtlinie VDI/VDE 3518 vor. Diese Richtlinienreihe definiert Begriffe, beschreibt den Aufbau und klassifiziert Multigassensoren (Blatt 1), befasst sich mit den Anforderungen für das Unterscheiden, Erkennen und mengenmäßige Bestimmen von Gemischen gasförmiger Stoffe und die Prüfung von Multigassensoren (Blatt 2) und gibt Anleitung für geruchsbezogene Messungen mit „Elektronischen Nasen“ (Blatt 3). Multigassensoren können als elektronische Nasen in Anlehnung an den biologischen Geruchssinn zur Wahrnehmung und Charakterisierung von Gerüchen eingesetzt werden. Die Spezifik von Multigassensoren besteht darin, dass durch die Wahl und Betriebsweise der Sensoren eine Vielzahl von geeigneten Messsignalen erzeugt werden, aus denen mit mathematischen Verfahren die für die Anwendung gewünschten Informationen extrahiert werden. Dazu ist ein Training der Messeinrichtung mit Proben bekannter Eigenschaften notwendig. Diese Richtlinie soll Herstellern, Anbietern und Nutzern als ein Leitfaden Informationen und Erläuterungen für die korrekte und sichere Arbeit mit Multigassensoren liefern. Sie soll Prüflaboratorien und Anwendern helfen, bei der Beurteilung von Qualitätsmerkmalen einheitlich vorzugehen und dafür gemeinsame Randbedingungen anzugeben T2 - 7. Anwendertreffen Ionenmobilitätsspektrometrie CY - Reutlingen, Germany DA - 06.03.2018 KW - Elektronische Nase KW - Multigassensorik KW - Richtlinie PY - 2018 AN - OPUS4-44452 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Theiler, Geraldine T1 - Influence of the counterface on the sliding behavior of polymer materials in hydrogen N2 - This presentation deals with the influence of the counterface materials on the sliding behaviour of some polymer materials in hydrogen. Polyimide (PI), polyetheretherketone (PEEK) and Polytetrafluoroethylene (PTFE) materials were investigated against hardened 52100 martensitic bearing steel and 304 austenitic stainless steel with similar roughness (Ra = 0.2 μm). Results indicate that the friction and wear of PI and PEEK materials depend on the counterface material. This effect wasn’t observed for PTFE composites. While the tribological performance of polyimide is better against 52100 in hydrogen, improved sliding behaviour of PEEK materials is observed with 304 counterface, particularly at higher sliding speed. Surface analyses of the transfer film reveal that the influence of the counterface is primarily related to the chemical nature of the steel for PI and to the thermal conductivity of the disc for PEEK materials. T2 - Hydrogenius & I2CNER Tribology Symposium CY - Online meeting DA - 29.01.2021 KW - Polymers KW - Hydrogen KW - Counterface KW - Friction KW - Wear PY - 2021 AN - OPUS4-52093 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Mair, Georg W. A1 - Günzel, Stephan A1 - Saul, Herbert A1 - Bock, Robert T1 - Die volumenabhängige Druckbegrenzung als Maßnahme zur Konsequenzsteuerung im Wasserstofftransport N2 - Mit der technologischen Entwicklung werden auch die Transporteinheiten für Druckgase größer und die zu transportierenden Gase wie Wasserstoff deutlich über die lange als Standard geltenden 200 bar hinaus komprimiert. Damit steigt das Konsequenzpotenzial eines Zwischenfalls, das nun begrenzt werden soll, um die bisherige Praxis mit wenigen Zwischenfällen von den Maßnahmen für die neuen Entwicklungen extrem großer Transportdruckbehälter abgrenzen zu können. Hierzu wurde – ausgehend von einer technologisch und sicherheitstechnisch störenden Begrenzung des Volumens von Bergungsdruckgefäßen – das sogenannte Druck-Volumen-Produkt als Kenngröße und Konsequenzmaß vorgeschlagen. Um eine breit akzeptierte Abgrenzung der heute etablierten Druckgefäße gegenüber den zukünftigen Einheiten mit noch mehr Gasinhalt erarbeiten zu können, wurde eine Arbeitsgruppe bei den Vereinten Nationen eingerichtet, deren Weg zu ihrem Ergebnis „Einführung einer Obergrenze von 1.5 Mio. bar-Liter für das Druck-Volumen-Produkt von Druckgefäßen“ mit den Wasserstoff- spezifischen Einzelschritten „Grenze zwischen Großunfall und Katastrophe“, „Die Wirkung von Druckwellen auf den menschlichen Körper“, „Die Ausbreitung von Druckwellen“, „Der Referenzwert für die Bevölkerungsdichte“ und „Die Druckwellenberechnung“ hier dargestellt ist. Dieses Ergebnis der UN-Arbeitsgruppe wird bis 2027 zu einer verbindlichen Begrenzung des Druckvolumenproduktes in Druckgefäßen führen. KW - Risikosteuerung KW - Druck-Volumen-Produkt KW - Katastrophe KW - Bevölkerungsdichte KW - Druckwelle PY - 2024 SN - 2191-0073 VL - 14 IS - 05-06 SP - 8 EP - 17 PB - VDI Fachmedien GmbH & Co. KG CY - Düsseldorf AN - OPUS4-64309 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tiebe, Carlo A1 - Neumann, Patrick P. A1 - Hüllmann, Dino A1 - Bartholmai, Matthias T1 - VDI/VDE 3518 Technische Richtlinie für Multigassensoren N2 - Der Beitrag präsentiert die erarbeiteten technischen Richtlinien zur Anwendung und Prüfung von Multigassensoren innerhalb der Richtlinienreihe VDI/VDE 3518 sowie in diesem Zusammenhang die Möglichkeiten der Sensorprüfung im akkreditierten Prüflabor des Fachbereichs 8.1 der BAM. Im Speziellen wird das in Kürze veröffentlichte Blatt 3 der Richtlinienreihe vorgestellt, das Bezug auf Multigassensoren für geruchsbezogene Messungen mit elektronischen Nasen nimmt. T2 - NetMon International training course - Low-cost Environmental Monitoring CY - BAM, Berlin, Germany DA - 09.04.2019 KW - Multigassensoren KW - Prüfung KW - Richtlinie PY - 2018 AN - OPUS4-47885 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Theiler, Geraldine A1 - Gradt, Thomas T1 - Environmental effects on the sliding behaviour of PEEK composites N2 - The sliding performance of PEEK materials against steel discs was investigated in air, vacuum and hydrogen environment. KW - Sliding friction KW - PEEK KW - Graphite KW - TiO2 KW - CNTs KW - Vacuum KW - Hydrogen PY - 2016 DO - https://doi.org/10.1016/j.wear.2016.09.019 SN - 0043-1648 SN - 1873-2577 VL - 368 SP - 278 EP - 286 PB - Elsevier B.V. AN - OPUS4-37927 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Theiler, Geraldine T1 - Polymer materials in hydrogen N2 - This presentation provides an overview of the applications and challenges related to polymer materials in hydrogen. The effects of hydrogen on polymers are described and test methods to evaluate the interactions between polymers and hydrogen are presented along with case studies. T2 - Masterstudiengang Wasserstofftechnologien DIU CY - Online meeting DA - 25.08.2023 KW - Hydrogen KW - Polymers PY - 2023 AN - OPUS4-61964 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Holtappels, Kai A1 - Theil, Benjamin A1 - Erdelen-Peppler, M. A1 - Meiwes, K.C. T1 - Explosive cutting of pipelines for the determination of materials properties N2 - Incidents in the past already showed that pipelines transporting compressible fluids are in risk of suffering propagating ductile fractures in case of damages to the pipes. Therefore, the knowledge of the fracture properties of pipeline steels is of high importance. Commonly the properties are determined in laboratory scale, but these do not fully correspond with full-scale fracture behaviour especially at dynamic conditions when highly pressurized gases are released during the crack propagation. This paper describes so-called West Jefferson Tests and Midscale-Tests in which pipelines under pressure were cut with an explosive charge to initiate the crack propagation. T2 - 9th World conference on Explosives and Blasting CY - Stockholm, Sweden DA - 10.09.2017 KW - Pipelines KW - Explosive cutting KW - Determination of materials PY - 2017 SN - 978-0-9550290-5-9 SP - 385 EP - 390 PB - European Federation of Explosives Engineers CY - UK AN - OPUS4-41994 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Holtappels, Kai T1 - Materialuntersuchung an Pipelinerohren unter Einsatz von Schneidladungen N2 - Extremprüfung an Pipelinerohren zur dauerhaften Gewährleistung der Sicherheit an Gasfernleitungen: An mehreren Pipelinerohren mit unterschiedlichen Dimensionen (Länge zwischen 8 und 36 m, Außendurchmesser von 400 bis 920 mm) und Wandstärken von 21 bis 38 mm wurden Versuche durchgeführt, bei denen unter Druck Risse in der Wandung durch geeignete Schneidladungen initiiert wurden. Diese Risse breiten sich aufgrund der in den Rohren in Form von Gasdruck gespeicherten Energie aus. In Abhängigkeit von den Materialeigenschaften der Pipelinerohre sowie den Prüfbedingungen von Druck (175 bis 300 bar) und Pipelinetemperatur (Umgebungstemperatur bis -30 °C) wurden die Rissgeschwindigkeiten und –längen bestimmt. Im Anschluss an die Versuche wurden die Rissstücke herausgetrennt, damit weitergehende Materialuntersuchungen (Scherfläche, Gefügestruktur etc.) durchgeführt werden können. Verschiedene Prüfmethoden wie z. B. Battelle Drop Weight Tear Test (BDTWW) oder Charpy Vee-Notched (CVN) liefern zum Teil stark voneinander abweichende Ergebnisse, so dass diese Untersuchungen in Anlehnung an einen West-Jefferson-Tests (WJT) durchgeführt wurden. T2 - 11. Infoveranstaltung Sprengstoffe und Pyrotechnik CY - BAM, Berlin, Germany DA - 19.05.2016 KW - Ferngasleitung KW - Materialeigenschaften KW - Rissgeschwindigkeit KW - Schneidladung PY - 2016 AN - OPUS4-36280 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Theiler, Geraldine T1 - Tribology of polymeric materials in gaseous and liquid hydrogen N2 - This presentation gives an overview of the tribological behaviour of polymeric materials in gaseous and luquid hydrogen. T2 - HYDROGENIUS-BAM Joint Hydrogen Symposium CY - Online meeting DA - 06.07.2021 KW - Polymers KW - Hydrogen KW - Friction KW - Wear PY - 2021 AN - OPUS4-53701 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Farhan, Muhammad A1 - Schneider, Ronald A1 - Thöns, Sebastian T1 - Corrigendum to Predictive information and maintenance optimization based on decision theory: a case study considering a welded joint in an offshore wind turbine support structure N2 - This article has been revised and republished due to substantial changes to the text of the original article, as published Online First on January 31, 2021. Most of the change were minor grammatical changes. The following changes are more significant and will be highlighted below. PY - 2022 DO - https://doi.org/10.1177/14759217211040385 SN - 1475-9217 VL - 21 IS - 4 SP - 1956 EP - 1956 PB - Sage Publications CY - London AN - OPUS4-55165 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Sauer, Hannah A1 - Okpeke, Bright Ebikemefa A1 - Dzielendziak, Agnieszka Sylwia A1 - Batcke, Lars A1 - Eberwein, Robert A1 - Ehlers, Sören T1 - Comparative life cycle assessment of different vacuum insulation panel core materials for cryogenic storage tanks – with a focus on glass bubbles as a novel core material N2 - Developing a sustainable hydrogen supply chain is important in facilitating the energy transition towards climate neutrality. Hydrogen in its free form can be stored and transported either as a gas or a liquid. Due to gaseous hydrogen's comparatively low energy density, liquefied hydrogen (LH 2) is often preferred, especially with regard to long-distance transportation and storage in bulk. A notable challenge associated with LH2 is the inherent requirement to preserve it at a low temperature of -253°C. Consequently, the utilisation of thermally insulated tanks is necessary to minimise LH 2 evaporation. There is a lack of literature on the environmental impacts of insulation materials and concepts for cryogenic storage tank applications in the hydrogen supply chain. Hence, this study investigates a novel concept, namely vacuum insulation panels (VIPs), focusing on their core materials, with a view to assessing their environmental sustainability and circularity. A cradle-to-grave life cycle assessment (LCA) model is employed to investigate six distinct VIP core materials, namely, silica aerogel, rigid polyurethane foam, expanded perlite, glass fibre, fumed silica, and glass bubbles (hollow glass microspheres), with a special focus on the latter. The LCA results show that polyurethane foam and silica aerogel rank low in environmental performance, making them less suitable as primary choice. Expanded perlite is the most environmentally friendly material option, followed by glass fibre, glass bubbles, and fumed silica. Improvements to the environmental impact of glass bubbles can be achieved via the implementation of closed-loop recycling in their life cycle. T2 - The World Hydrogen Technologies Convention 2025 CY - Dublin, Ireland DA - 21.10.2025 KW - LH2 KW - Insulation KW - Life cycle assessment PY - 2025 UR - https://www.whtc2025.com/conference-proceedings SP - 65 EP - 67 AN - OPUS4-64668 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Holtappels, Kai A1 - Kluge, Martin A1 - Ferrero, Fabio A1 - Schmidtchen, Ulrich T1 - Acetylenflaschen im Feuer N2 - Acetylen ist eines der wichtigsten technischen Gase und findet insbesondere Anwendung beim Schweißen und Schneiden verschiedener Werkstoffe. Damit Acetylen in entsprechenden Mengen vor Ort zur Verfügung gestellt werden kann, wird es in Druckgasbehälter abgefüllt. Im Falle eines Brandes stehen Acetylenflaschen im Verdacht, jederzeit – auch nach Löschen des Feuers – aufgrund einer möglicherweise initiierten Zerfallsreaktion zu bersten. Um insbesondere Personenschäden zu vermeiden, evakuieren und sperren die Rettungskräfte einen Sicherheitsbereich mit einem Radius von mindestens 200 m um die verdächtige Flasche ab. Gleichzeitig wird umgehend mit der Kühlung der Flasche begonnen. Wie lange muss aber eine Acetylenflasche gekühlt werden, bis sie sicher abtransportiert werden kann, und wie lange muss der Sicherheitsbereich mit dem großen Radius aufrecht erhalten werden? Diesen Fragen ist die BAM in den vergangenen Jahren im Rahmen verschiedener Untersuchungen und Projekte nachgegangen. KW - Acetylen KW - Druckbehälter KW - Poröses Material KW - Lösungsmittel PY - 2012 SN - 2191-0073 N1 - Geburtsname von Kluge, Martin: Beckmann-Kluge, M. - Birth name of Kluge, Martin: Beckmann-Kluge, M. VL - 2 IS - 4 SP - 19 EP - 25 PB - Springer-VDI-Verl. CY - Düsseldorf AN - OPUS4-25902 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Tiebe, Carlo A1 - Detjens, Marc A1 - Banach, Ulrich A1 - Hübert, Thomas T1 - Measurement uncertainty of coulometric trace humidity sensors N2 - Especially trace amounts of water vapour in gases can be reliably determined by coulometric trace humidity sensors. The principle of these sensors is based on water vapour absorption in a hygroscopic layer and its subsequent electrolytic decomposition. The calibration of sensors was performed in the humidity range, expressed as frost point temperature, from −30°C to −80°C . This range is equivalent to volume fractions smaller than 376 µL·L−1. Generated humidity was measured with coulometric sensors and a chilled dew point hygrometer that was used as reference. An empirical non-linear function was found between sensor signal and measured reference humidity. This function consists of two parameters with a measurement uncertainty. Both calibration parameters were checked by means of one-way analysis of variance. It showed that gas specific function can be used for humidity measurement in nitrogen, hydrogen, dinitrogen monoxide, compressed and synthetic air. It is possible to determine trace humidity in all tested gases with an expanded uncertainty less than 2.1 K (coverage factor k=2 ) regarding frost point temperature. KW - Trace humidity KW - Coulometric sensor KW - Measurement uncertainty KW - ANOVA PY - 2018 DO - https://doi.org/10.1515/teme-2018-0031 SN - 0171-8096 VL - 85 IS - 12 SP - 746 EP - 753 PB - De Gruyter CY - Oldenbourg AN - OPUS4-45959 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Theiler, Geraldine T1 - Benchmarking of polymer materials for tribological applications in hydrogen N2 - The focus of this study is to evaluate of hydrogen on the friction and wear behavior of a wide range of polymer materials. Thereby, the tribological performance of filled and unfilled polymers from different suppliers were compared at room temperature in air and hydrogen gas (H2) as well as in liquid hydrogen at -253°C (LH2). T2 - 62. Tribologie-Fachtagung der Gesellschaft für Tribologie e. V. CY - Online meeting DA - 27.09.2021 KW - Polymers KW - Hydrogen KW - Friction KW - Wear PY - 2021 AN - OPUS4-53700 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Theiler, Geraldine T1 - Friction and wear characteristics of polymers in gaseous and liquid hydrogen N2 - The tribological characteristics of pure and graphite filled polymers were investigated in gaseous hydrogen at ambient temperatures and in LH2 at -253°C. It could be shown that the tribological properties of PI and PEEK materials is related to the formation of a transfer film. The influence of both hydrogen and cryogenic temperatures will be discussed in the presentation. T2 - 21th International Colloquium Tribology CY - Stuttgart/Ostfildern, Germany DA - 09.01.2018 KW - Friction KW - Wear KW - Hydrogen KW - PEEK PY - 2018 AN - OPUS4-43902 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hildebrandt, Jana T1 - Aqueous Dispersions of polypropylene as possible reference material for nanoplastics N2 - Plastic debris in micron and nanometer scale pollutes the nature all over the world. The potential dangers of these pollutants remain unpredictable. While risk assessment studies on microplastics are already popular, nanoplastic has not yet reached the same focus of investigation. The reason for this difference is simple: There is a "methodological gap" in the analytics of plastic particles with a diameter smaller than 1 µm. Submicron and nanoplastic particles are currently not detectable in environmental matrices. Therefore, it is important for researchers to have a well-characterized nanoplastic material, that serves as a reference for nanoplastics found in nature. Our aim was to synthesize nanoplastics made from the most common used plastics such as polypropylene (PP). We found an easy way to form nanoparticles consisting of PP (nano-PP), adapting and improving the method presented for polystyrene (PS). Nano-PP was formed via a top-down method where the polymer was dispersed to acetone and then transferred to water. No additional surfactant is needed to obtain a dispersion which is stable for more than 35 weeks. The success of forming nanoplastics and their size was detected via scattering methods, predominantly dynamic light scattering (DLS). The chemical analysis of the nanoplastics was performed via Fourier Transform Infrared spectroscopy. To examine the good stability of the nanoparticles, zeta potential measurements were performed, which revealed zeta potentials of -30 to -40 mV. T2 - European Polymer Congress 2022 CY - Prag, Czechia DA - 26.06.2022 KW - Nanoplastic PY - 2022 AN - OPUS4-55960 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schneider, Ronald A1 - Thöns, Sebastian A1 - Straub, Daniel T1 - Reliability analysis and updating of deteriorating systems with subset simulation N2 - An efficient approach to reliability analysis of deteriorating structural systems is presented, which considers stochastic dependence among element deterioration. Information on a deteriorating structure obtained through inspection or monitoring is included in the reliability assessment through Bayesian updating of the system deterioration model. The updated system reliability is then obtained through coupling the updated deterioration model with a probabilistic structural model. The underlying high-dimensional structural reliability problems are solved using subset simulation, which is an efficient and robust sampling-based algorithm suitable for such analyses. The approach is demonstrated in two case studies considering a steel frame structure and a Daniels system subjected to high-cycle fatigue. KW - Structural reliability KW - Deterioration KW - Bayesian analysis KW - Inspection KW - Monitoring KW - Subset simulation PY - 2017 DO - https://doi.org/10.1016/j.strusafe.2016.09.002 SN - 0167-4730 SN - 1879-3355 VL - 64 SP - 20 EP - 36 PB - Elsevier AN - OPUS4-38218 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Liebig, Ferenc A1 - Moreno, Silvia A1 - Thünemann, Andreas A1 - Temme, Achim A1 - Appelhans, Dietmar A1 - Koetz, Joachim T1 - Toxicological investigations of “naked” and polymer-entrapped AOT-based gold nanotriangles N2 - tNegatively charged ultrathin gold nanotriangles (AuNTs) were synthesized in a vesicular dioctyl sodiumsulfosuccinate (AOT)/phospholipid-based template phase. These “naked” AuNTs with localized surfaceplasmon resonances in the NIR region at about 1300 nm and special photothermal properties are ofparticular interest for imaging and hyperthermia of cancerous tissues. For these kinds of applicationsthe toxicity and the cellular uptake of the AuNTs is of outstanding importance. Therefore, this studyfocuses on the toxicity of “naked” AOT-stabilized AuNTs compared to polymer-coated AuNTs. Poly-meric coating consisted of non-modified hyperbranched poly(ethyleneimine) (PEI), maltose-modifiedpoly(ethyleneimine) (PEI-Mal) and heparin. The toxicological experiments were carried out with twodifferent cell lines (embryonic kidney carcinoma cell line HEK293T and NK-cell leukemia cell line YTS).This study revealed that the heparin-coating of AuNTs improved biocompatibility by a factor of 50 whencompared to naked AuNTs. Of note, the highest nontoxic concentration of the AuNTs coated with PEI andPEI-Mal is drastically decreased. Overall, this is mainly triggered by the different surface charges of poly-meric coatings. Therefore, AuNTs coated with heparin were selected to carry out uptake studies. Theirpromising high biocompatibility and cellular uptake may open future studies in the field of biomedicalapplications. KW - Small-angle X-ray scattering KW - SAXS KW - Nanoparticle PY - 2018 DO - https://doi.org/10.1016/j.colsurfb.2018.04.059 SN - 0927-7765 VL - 167 SP - 560 EP - 567 PB - Elsevier AN - OPUS4-44844 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Holtappels, Kai T1 - Kompetenzzentrum H2Safety@BAM - Wir schaffen Vertrauen in Wasserstofftechnologien N2 - Im Rahmen des 4. Netzwerktreffens der Wasserstoffakteure im Landkreis TF und Region kamen auf Einladung der Bürgermeister der Gemeinden Baruth/Mark, Am Mellensee, Ludwigsfelde Akteure und Vertreter aus der Region zusammen, um den Aufbau einer Wasserstoffinfrastruktur zur wirtschaftlichen Förderung der Region zu diskutieren bzw. auch laufende Projekte vorzustellen. Die BAM hat ihre Wasserstoffaktivitäten auf dem BAM Testgelände Technische Sicherheit vorgestellt. T2 - 4. Netzwerktreffen der Wasserstoff-Akteure im Landkreis TF und Region CY - Glashütte, Germany DA - 26.05.2025 KW - Brandenburg KW - Netzwerk KW - Wasserstoffinfrastruktur PY - 2025 AN - OPUS4-63430 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Sieg, H. A1 - Klusmann, L. A1 - Ellermann, A. L. A1 - Böhmert, L. A1 - Thünemann, Andreas A1 - Braeuning, A. T1 - Counterions determine uptake and effects of aluminum in human intestinal and liver cells N2 - Aluminum (Al) is highly abundant in the biosphere and can occur in different physico-chemical states. It is present in human food and undergoes transitions between dissolved and particulate species during the passage of the gastrointestinal tract. Moreover, in a complex matrix such as food different inorganic and organic counterions can affect the chemical behavior of Al following oral uptake. In this work, the effects of different counterions, namely chloride, citrate, sulfate, lactate and acetylacetonate, on Al uptake and toxicity in the human intestine are studied. The respective Al salts showed different dissolution behavior in biological media and formed nanoscaled particles correlating in reverse with the amount of their dissolved fraction. The passage through the intestinal barrier was studied using a Caco-2 Transwell® system, showing counterion-dependent variance in cellular uptake and transport. In addition, Al toxicity was investigated using Al species (Al3+, metallic Al0 and oxidic γAl2O3 nanoparticles) and counterions individually or in mixtures on Caco-2 and HepG2 cells. The strongest toxicity was observed using a combination of Al species, depending on solubility, and the lipophilic counterion acetylacetonate. Notably, only the combination of both led to toxicity, while both substances individually did not show toxic effects. A toxification of previously non-toxic Al-species by the presence of acetylacetonate is shown here for the first time. The dependency on the concentration of free Al ions was demonstrated using sodium hydrogen phosphate, which was able to counteract the toxic effects by complexing free Al ions. These findings, using Al salts as an example for a common food contaminant, underline the importance of a consideration of the chemical properties of human nutrition, especially dissolution and hydrophobicity, which can significantly influence the cellular uptake and effects of xenobiotic substances. KW - SAXS KW - Small-angle X-ray scattering KW - Nanoparticle PY - 2022 DO - https://doi.org/10.1016/j.tiv.2021.105295 VL - 79 SP - 1 EP - 7 PB - Elsevier AN - OPUS4-54110 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Böhmert, L. A1 - Niemann, B. A1 - Thünemann, Andreas A1 - Lampen, A. T1 - Cytotoxicity of peptide-coated silver nanoparticles on the human intestinal cell line Caco-2 N2 - Silver nanoparticles are used in a wide range of consumer products such as clothing, cosmetics, household goods, articles of daily use and pesticides. Moreover, the use of a nanoscaled silver hydrosol has been requested in the European Union for even nutritional purposes. However, despite the wide applications of silver nanoparticles, there is a lack of information concerning their impact on human health. In order to investigate the eVects of silver nanoparticles on human intestinal cells, we used the Caco-2 cell line and peptide-coated silver nanoparticles with deWned colloidal, structural and interfacial properties. The particles display core diameter of 20 and 40 nm and were coated with the small peptide L-cysteine L-lysine L-lysine. Cell viability and proliferation were measured using Promegas CellTiter-Blue® Cell Viability assay, DAPI staining and impedance measurements. Apoptosis was determined by Annexin-V/7AAD staining and FACS analysis, membrane damage with Promegas LDH assay and reactive oxygen species by dichloroXuorescein assay. Exposure of proliferating Caco-2 cells to silver nanoparticle induced decreasing adherence capacity and cytotoxicity, whereby the formation of reactive oxygen species could be the mode of action. The eVects were dependent on particle size (20, 40 nm), doses (5–100 μg/mL) and time of incubation (4–48 h). Apoptosis or membrane damage was not detected. KW - Oral uptake KW - Intestinal cells KW - Peptide-coated silver nanoparticles KW - Cytotoxicity KW - Nanotechnology KW - Small-angle X-ray scattering KW - SAXS PY - 2012 DO - https://doi.org/10.1007/s00204-012-0840-4 SN - 0340-5761 SN - 1432-0738 VL - 86 IS - 7 SP - 1107 EP - 1115 PB - Springer CY - Berlin ; Heidelberg [u.a.] AN - OPUS4-26267 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Girod, Matthias A1 - Vogel, Stefanie A1 - Szczerba, Wojciech A1 - Thünemann, Andreas T1 - How temperature determines formation of maghemite nanoparticles N2 - We report on the formation of polymer-stabilized superparamagnetic single-core and multi-core maghemite nanoparticles. The particle formation was carried out by coprecipitation of Fe(II) and Fe(III) sulfate in a continuous aqueous process using a micromixer system. Aggregates containing 50 primary particles with sizes of 2 nm were formed at a reaction temperature of 30 °C. These particles aggregated further with time and were not stable. In contrast, stable single-core particles with a diameter of 7 nm were formed at 80 °C as revealed by small-angle X-ray scattering (SAXS) coupled in-line with the micromixer for particle characterization. X-ray diffraction and TEM confirmed the SAXS results. X-ray absorption near-edge structure spectroscopy (XANES) identified the iron oxide phase as maghemite. KW - Iron Oxide Nanoparticles KW - Micromixer KW - SAXS KW - XANES KW - Carboxydextran KW - Nanotechnology PY - 2015 DO - https://doi.org/10.1016/j.jmmm.2014.09.057 SN - 0304-8853 VL - 380 SP - 163 EP - 167 PB - Elsevier B.V. CY - Amsterdam AN - OPUS4-32564 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Hajhariri, Aliasghar A1 - Eberwein, Robert A1 - Camplese, Davide A1 - Emrys Scarponi, Giordano A1 - Otremba, Frank A1 - Cozzani, Valerio A1 - Seidlitz, Holger T1 - A Comprehensive Numerical Study of the Behaviour of an LH2 Storage Tank in the Event of a Fire N2 - As the world moves towards green energy production, effective storage and transportation solutions become essential. To support this transition, energy carriers with minimal or zero environmental impact are required. Liquified hydrogen represents a promising candidate due to its emissions-neutral properties. However, its highly flammable nature necessitates adherence to strict safety codes and standards. Storing hydrogen often requires advanced super-insulation materials. To enhance the safety of cryogenic hydrogen storage tanks under extreme conditions, such as those encountered during fire accidents, it is crucial to understand the thermal behaviour of the tank. Predicting pressurization and potential failure in advance demands a robust and comprehensive model. However, still such models suffer lack of detailed heat transfer models which account for various sub-processes during an accident scenario. Hence, this study introduces a comprehensive model for the pressurization of cryogenic tanks equipped with multi-layer insulation (MLI) systemsin the event of fire, which comprises several sub-models. These sub-models account for heat transfer phenomena through the thermal insulation at nominal conditions and its thermal degradation during fire exposure, the fluid, the internal pressurization, and the performance of the pressure relief valve. This study provides valuable insights into the safety and the behaviour of hydrogen storage tanks under thermal loads. KW - Heat transfer KW - Multi-Layer Insulation KW - Cryogenic KW - Liquid Hydrogen PY - 2025 DO - https://doi.org/10.3303/CET25116114 VL - 116 SP - 679 EP - 684 PB - AIDIC AN - OPUS4-63813 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Cano Murillo, Natalia T1 - Effect of high-pressure hydrogen environment on the physical and mechanical properties of different kinds of carbon black filled elastomers. N2 - As the transition towards the usage of renewable energy is getting urgent, the fluctuations of clean energy production require efficient storage alternatives. Hydrogen offers not only the possibility of energy storage but also, acts as an energy carrier. It is then important to study the effect of highly pressurized hydrogen atmosphere on the materials destinated for its storage and transport, in order to assure the reliable performance of the sealing materials containing hydrogen. In this study, a set of carbon black (CB) filled rubbers comprising hydrogenated acrylonitrile butadiene rubber (HNBR), acrylonitrile butadiene rubber (NBR) and ethylene propylene diene monomer rubber (EPDM) was tested under high pressure hydrogen atmosphere (1000 bar) and at different temperature conditions: 120°C for HNBR, room temperature and 85°C for NBR and EPDM. The influence of hydrogen on the materials properties was measured after 7 days of exposure under hydrogen and evaluated again after 48h. Density and volume change, as well as hardness, tensile tests, compression set, dynamic mechanical measurements and infrared spectroscopy evaluations were conducted to estimate the impact of high-pressure hydrogen on the rubber grades. Our study reveals, an effect on the physical and mechanical properties, possibly related to small changes in the matrix-filler interaction after the hydrogen exposure. All materials, however, show a trend to recover most of their properties 48h after hydrogen exposure. T2 - RubberCon 2023 CY - Edinburgh, Scotland DA - 09.05.2023 KW - Elastomers KW - Hydrogen exposure KW - Mechanical properties PY - 2023 AN - OPUS4-62007 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Saloga, Patrick E. J. T1 - Do non-thermal effects exist? - Microwave-assisted acceleration of silver nanoparticle synthesis and particle growth N2 - Ever since increasing a reaction’s yield while shortening the reaction time is the main objective in synthesis optimization. Microwave reactors meet these demands. In literature however their usage is under discussion due to claims of the existence of non-thermal effects resulting from the microwave radiation. Especially for nano-material syntheses it is of crucial importance to be aware of influences on the reaction pathway. Therefore, we compare ultra-small silver nanoparticles with mean radii of 3 nm, synthesized via conventional and microwave heating. We employed a versatile one-pot polyol synthesis of poly(acrylic acid) (PAA) stabilized silver nanoparticles, which display superior catalytic properties. No microwave specific effects in terms of particle size distribution characteristics, as derived by small-angle X-ray scattering (SAXS) and dynamic light scattering (DLS), are revealed. Due to the microwave reactor’s characteristics of a closed system, syntheses can be carried out at temperatures beyond the solvent’s boiling point. Particle formation was accelerated by a factor of 30 by increasing the reaction temperature from 200 °C to 250 °C. The particle growth process follows a cluster coalescence mechanism. A post-synthetic incubation step at 250 °C induces a further growth of the particles while the size distribution broadens. Thus, utilization of microwave reactors enables an enormous decrease of the reaction time as well as the opportunity of tuning the particles’ size. Possibly, decomposition of the stabilizing ligand at elevated temperatures results in reduced yields. A temperature of 250 °C and a corresponding reaction time of 30 s represent a compromise between short reaction times and high yields. T2 - 5th Nano Today Conference CY - Waikoloa Village, HI, USA DA - 06.12.2017 KW - Microwave synthesis KW - Small-angle scattering KW - Silver nanoparticles PY - 2017 AN - OPUS4-43497 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Holtappels, Kai T1 - Eine Frage der Technik? Verfahren und Kriterien für den sicheren Betrieb von Wasserstoffanlagen N2 - Das Webinar wird im Rahmen von TransHyDE Systemanalyse (AP5.3 Akzeptanzbewertungen) durchgeführt und adressiert aus einer interdisziplinären Perspektive relevante Aspekte der Sicherheit und öffentlichen Risikowahrnehmung von Wasserstoffprojekten. Dabei erfolgt ein Überblick über Standards der sicherheitstechnischen Forschung, Einblicke aus der Projektkommunikation mit Akteuren und Bürger*innen sowie die Vorstellung aktueller Forschungsergebnisse zur öffentlichen Wahrnehmung der Risiken von Wasserstofftechnologien. Die Diskussion geht den u.a. Fragen nach, welche Rolle das Thema Sicherheit in der aktuellen Planungspraxis spielt, wie transparent über Risiken kommuniziert werden kann, ohne Vertrauen zu gefährden und welche Kommunikationsansätze sich als zielführend zeigen, um gesellschaftlichen Unsicherheiten zu begegnen. Der Vortrag zeigt auf, dass der sichere Betrieb von Anlagen nicht nur mit der Technologie alleine gewährleistet werden kann. T2 - Lunch Talk: Wasserstoff im Fokus: Sicherheit, Risikowahrnehmung und Kommunikation CY - Online meeting DA - 08.12.2025 KW - Gefahrenanalyse KW - Methoden KW - Kriterien PY - 2025 AN - OPUS4-65040 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Theiler, Geraldine T1 - Comparison of the sliding behaviour of several polymers in hydrogen N2 - The work presented here deals with the friction and wear behaviour of polymer materials in hydrogen. Commercially available grades of PEEK, PA, PPA, PAI, PI and PBI were investigated at room temperature in air and hydrogen gas (H2) as well as in liquid hydrogen at - 253°C (LH2). T2 - 7th World Tribology Congress, WTC 2022 CY - Lyon, France DA - 10.07.2022 KW - Friction KW - Wear KW - Polymers KW - Hydrogen KW - Cryogenic PY - 2022 AN - OPUS4-62087 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Schönbucher, A. A1 - Schälike, Stefan T1 - Pool fires and spill fires N2 - Risk is the possibility of suffering damage. In engineering it may be quantified and is assessed as a combination of the expected frequency of an undesired event, e.g., in case of process plants a fire, an explosion, or a toxic release, and the damage associated with this event. Every possibility to suffer damage is a risk if it is uncertain whether it will become reality. Damage and uncertainty therefore are the two elements which determine a risk. If the Magnitude of damage and the uncertainty of its occurrence can be quantified, then a number may be assigned to the corresponding risk, the risk number. Frequently, this number refers to a which is based on a Gaussian model, Guideline part 2 with its physical modeling backbone will probably remain the Standard German Screening model for a couple of years to come. KW - Pool fires KW - Spill fires KW - Soot KW - Heat transfer KW - Modeling PY - 2012 SN - 978-3527306732 DO - https://doi.org/10.1002/14356007.q20_q05 IS - Chapter 2.3 SP - 47 EP - 60 PB - Wiley-VCH Verlag GmbH & Co. KGaA CY - Weinheim ET - 8th Ed. AN - OPUS4-27635 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bernardy, Christopher A1 - Habib, Abdel Karim A1 - Kluge, Martin A1 - Schalau, Bernd A1 - Schulze, Marcel A1 - Kant, Hanjo A1 - Orchini, Alessandro ED - Ruggiero, Eric J. T1 - Experimental investigation of large-scale hydrogen diffusion jet flames N2 - Hydrogen is a promising alternative to natural gas in industrial energy applications which would serve the goal of limiting global warming. However, wide application of hydrogen requires specific safety considerations taking into account that hydrogen is stored and transported under much higher pressure than natural gas. Thus, one scenario to be considered for hazard assessment is a sudden release of hydrogen from a leakage or safety valve and its subsequent ignition. For hydrocarbon flames, various jet flame models are available. However, hydrogen flames significantly differ from hydrocarbon flames in their combustion behavior, so that the applicability of these models to hydrogen has to be investigated. For that purpose, reals scale tests were carried out at the BAM Test Site Technical Safety. In addition, hydrocarbon jet flames (methane) were investigated. In these tests, the flame geometry and the thermal heat radiation were investigated for a release angle of 90°, for different release pressures (up to 220 bar) and mass flows (up to 0.175 kg/s). While existing heat radiation data from the literature are mostly based on unsteady outflow conditions and/or releases in still air, the experiments presented here are focused on ensuring a constant mass flow over the release duration under realistic free field conditions (with wind influence). This allows a better comparability with the stationary jet flame models and assessment of wind influence on model predictions. A number of parameters such as the surface emissive power of the jet flame and the radiant heat fraction were determined. A detailed comparison of the obtained experimental results with literature radiation models was performed. Good agreement between experimental and literature data was found for hydrogen whereas significant differences were identified for methane. Based on the investigations, empirical equations for modelling jet flames could be derived. T2 - American Society of Mechanical Engineers - Turbomachinery Technical Conference & Exposition GT2025 CY - Memphis, TN, USA DA - 16.06.2025 KW - Hydrogen release KW - Jet flame KW - Radiant heat fraction KW - Thermal radiation PY - 2025 SN - 978-0-7918-8877-3 DO - https://doi.org/10.1115/GT2025-FM2 SP - 1 EP - 11 PB - The American Society of Mechanical Engineers CY - Livingston AN - OPUS4-64098 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Beyer, M. A1 - Bothe, H. A1 - Schendler, Thomas T1 - Physikalisch-chemische Sicherheitstechnik und Explosionsschutz in PTB und BAM N2 - Unter diesem Motto arbeiten die BAM Bundesanstalt für Materialforschung und -prüfung und die PTB abgestimmt, aber mit eigenen Schwerpunkten, eng auf dem Gebiet des Brand- und Explosionsschutzes zusammen. Das Ziel dieser Zusammenarbeit ist die Gewährleistung sicherer Prozesse und Technik in einem sich ständig verändernden technischen und industriellen Umfeld. Das vorliegende Themenheft der PTB-Mitteilungen zeigt einen Ausschnitt aus dem gemeinsamen Aufgabengebiet mit dem Schwerpunkt des klassischen Explosionsschutzes. KW - Explosionsschutz KW - Politikberatung KW - Wissenstransfer PY - 2012 SN - 0176-2419 VL - 2012 SP - 18 EP - 22 PB - Stahl CY - Künzelsau AN - OPUS4-26293 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Schmidt, Birgit A1 - Koch, W. A1 - Pentzien, Simone A1 - Krüger, Jörg ED - Gabsch, T. T1 - Der Einsatz von Lasertechnik an Modellsystemen zentralasiatischer Wandmalereifragmente N2 - Eine Diplomarbeit im Studiengang Restaurierung an der Fachhochschule Potsdam bot den Rahmen. laserinduzierte Reinigung von ruß- und kunststoffbeschichteten Malschichten zu erproben. Dabei bildeten Untersuchungen zur Materialerfassung an originalen Wandmalereifragmenten der »Ritterhöhle« (Kirish. 6. bis 7.Jh. n. Chr.), heute im Besitz des Museums für Asiatische Kunst. Berlin, die Voraussetzung zum Bau adäquater Modellsysteme sowie der Auswahl geeigneter Laserparameter. In Zusammenarbeit mit der Arbeitsgruppe »Impulslaser-Technologien. Lasersicherheit« (Fachgruppe 6.4) an der Bundesanstalt für Materialforschung und -prüfung (BAM) konnten Möglichkeiten und Grenzen der Laserreinigung ermittelt werden, hu Zuge dessen sollten die Erkenntnisse dieser modellhaften Versuche eine Diskussion zur Anwendbarkeit der Lasertechnologie an originalen Objekten bereichern. KW - Laserreinigung KW - Wandmalerei KW - Verrußung KW - Kunststoffschicht KW - Probekörper PY - 2012 SN - 978-3-7338-0385-8 IS - Kap. 10 SP - 152 EP - 157 PB - Koehler & Amelang GmbH AN - OPUS4-26178 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schilder, Constanze A1 - Kusche, Nadine A1 - Schukar, Vivien A1 - Habel, Wolfgang ED - Liao, Y. ED - Jin, W. ED - Sampson, D.D. ED - Yamauchi, R. ED - Chung, Y. ED - Nakamura, K. ED - Rao, Y. T1 - Experimental qualification and validation of fibre optic strain sensors N2 - Strain sensors used in practical applications must provide reliable measurement data. To achieve this, sensor systems must be validated by using experimental facilities that enable physically independent statements about the performance of the sensor components. The paper describes qualification and validation procedures using a special facility to qualify surface-applied strain sensors and to achieve reliable sensor results. Based on examples concerning fibre optic strain sensor patches with and without FBG sensors, the determination of the strain gauge factor also under combined thermal and mechanical loading will be presented. These results are the basis for development of guidelines and standards. T2 - OFS2012 - 22nd International conference on optical fiber sensors CY - Beijing, China DA - 15.10.2012 KW - Fiber Bragg gratings KW - Sensors PY - 2012 DO - https://doi.org/10.1117/12.968801 SN - 0277-786X SN - 1996-756X N1 - Serientitel: Proceedings of SPIE – Series title: Proceedings of SPIE IS - 8421 SP - 1 EP - 4 PB - SPIE, the International Society for Optical Engineering CY - Bellingham, Wash. AN - OPUS4-27321 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Theiler, Geraldine T1 - On the sliding behavior of PAEK composites in vacuum environment N2 - The tribological behavior of PAEK composites were investigated in air and vacuum environment. Results indicate that the tribological performance of these compounds depends on material compositions, fiber orientation as well as test conditions. In vacuum, very low friction and wear coefficient were obtained at low sliding speed while severe wear occurred at high speed. T2 - The 6th World Tribology Congress - WTC 2017 CY - Beijing, China DA - 17.09.2017 KW - PAEK KW - Sliding performances KW - Vacuum PY - 2017 AN - OPUS4-42447 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Schönbucher, A. A1 - Schälike, Stefan A1 - Vela-Wallenschus, Iris A1 - Wehrstedt, Klaus-Dieter ED - Schmidt, J. T1 - CFD simulation of large hydrocarbon and peroxide pool fires N2 - Accidental fires in process Industries often occur as pool fires, which are hazardous to people and adjacent objects because of thermal radiation, largely sooting plumes and formation of other combustion products [1-3]. In addition to experimental pool fire tests, numerical investigation of these fires using Computational Fluid Dynamics (CFD) codes is becoming more important. In regard to safety, thermal radiation is one ofthe main interests in pool fire research. The Surface Emissive Power (SEP) is a key parameter to characterize thermal radiation emitted by a fire. The derived quantity SEP is usually defined as the heat flux due to thermal radiation in relation to flame surface AF. As well as the SEP, the temperatures Tandirradiances E of pool fires are ofparticular interest. CFD Simulation oflarge pool fires is helpful for abetter understanding of fire dynamics and to reduce the number oflarge-scale experiments. To predict the thermal radiation from the jet engine fuel JP-4 (d = 2, 8,16 and 25 m) and DTBP (di-tert-butyl peroxide, d= 1.12 and 3.4m) pool fires CFD methods are used, and the CFD results are compared with experiments. KW - Pool fire KW - JP 4 KW - Organic peroxide KW - DTBP KW - CFD KW - Surface emissive power KW - Irradiation KW - Safety distances PY - 2012 SN - 978-3-527-33027-0 N1 - Geburtsname von Vela-Wallenschus, Iris: Vela, I. - Birth name of Vela-Wallenschus, Iris: Vela, I. IS - Chapter 9 SP - 139 EP - 157 PB - Wiley-VCH Verlag GmbH & Co. KGaA AN - OPUS4-25897 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schalau, Bernd A1 - Rauchegger, Christian A1 - Schmidt, Dirk A1 - Thévenin, D. T1 - Einfluss der Quellhöhe auf die Ausbreitung schwerer Gase N2 - Im Rahmen von Störfallauswirkungsbetrachtungen werden oft Szenarien betrachtet, in denen Gase freigesetzt werden, die schwerer als Luft sind. Für die Berechnung der Gefährdungsbereiche wird in Deutschland oft die Richtlinie VDI 3783 eingesetzt. Die Methodik zur Bestimmung der Konzentrationsverteilung bei der Freisetzung eines Schwergases ist im Blatt 2 der Richtlinie dargestellt und basiert auf Windkanaluntersuchungen mit verschiedenen Ausbreitungsgebieten. Unter der Zielsetzung, eine möglichst konservative Abschätzung des Gefährdungsbereichs zu erhalten, erfolgte die Gasfreisetzung am Boden. In der Praxis sind aber immer wieder Szenarien zu untersuchen, bei denen die Gasfreisetzung aus Anlagenteilen über Bodenniveau erfolgt. Durch Freilandversuche sollen Anhaltswerte für die Bestimmung einer kritischen Quellhöhe, ab der eine Schwergasausbreitung nicht mehr zu betrachten ist, ermittelt werden. KW - Schwergas KW - VDI-Richtlinie 3783 KW - Gasausbreitung KW - Ausbreitungsmodelle KW - Störfallauswirkungsbetrachtungen PY - 2012 SN - 2191-0073 VL - 2 IS - 10 SP - 35 EP - 37 PB - Springer-VDI-Verl. CY - Düsseldorf AN - OPUS4-26736 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rolle, Annette A1 - Probst, Ulrich A1 - Ballheimer, Viktor A1 - Müller, Karsten A1 - Winkler, H. P. T1 - Transport condition effects on the sealing system and activity release within spent fuel transport casks N2 - Transport casks for spent fuel have to meet the International Atomic Energy Agency requirements for routine, normal and accident conditions of transport (RCT, NCT, and ACT). In regard to Containment capability a transport cask has to be designed to restrict the release of radioactive content to the required limits of 10'6 A2 per hour under NCT and A2 per week for ACT. Two barriers, which should avoid the release of fuel particles and fission products to the environment, are discussed in this paper: fuel rod claddings and the cask sealing System composed of cask body as well as of bolted lids and metallic seals. Both barriers can be affected by transport conditions. Vibrations and impact forces can increase the fraction of rods undergoing cladding breaches and can also lead to deformations or displacements of cask components involving an unloading or a movement of the lids or the seals. The above mentioned effects have to be properly considered in the safety analysis carried out by the applicant. The assumptions and results of the activity release calculations are verified by BAM Federal Institute for Materials Research and Testing. BAM is the German competent authority responsible, in particular, for Containment safety assessment within the licensing procedure of casks for spent fuel. T2 - RAMTRANSPORT 2012 - 9th International Conference on the Radioactive Materials Transport and Storage CY - London, UK DA - 22.05.2012 KW - Radioactive material KW - Safety assessment KW - Spent fuel KW - Leak tightness PY - 2012 SP - 1 EP - 9 AN - OPUS4-26498 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schartel, Bernhard T1 - Towards evidence-based development of flame retarded polymers N2 - Competence in polymer research and development is founded not only on technical/methodical components such as know-how, knowledge and communication, but also on scientific components. According to many sources the latter can be identified as a) identifying topics, tasks, opportunities, challenges, etc. b) describing /understanding phenomena and c) using evidence. Accepting this Basic background, this contribution demonstrates how a, b and c can be fulfilled in the development of flame retarded polymeric materials. Based on different examples of our work over the last 10 years, it is shown that innovation and co-operation are used to tackle actualtasks and opportunities, and that multi-methodical approaches and key experiments are sufficient to generate a deep understanding of phenomena as well as systematic investigations and comprehensive assessments. What is more, the examples shown demonstrate how guidelines are deduced for future material developments, which is, of course, the ultimate benefit of using evidence in applied polymer Science and engineering. T2 - 243rd National ACS meeting - Spring 2012 CY - San Diego, CA, USA DA - 25.03.2012 KW - Flame retardancy KW - Halogen-free KW - Flame retardancy mechanism KW - Fire property assessment PY - 2012 SN - 978-0-8412-2727-9 SN - 1550-6703 N1 - Serientitel: PMSE Preprints – Series title: PMSE Preprints VL - 243 SP - 38-PMSE PB - Amer Chemical SOC CY - Washington, USA AN - OPUS4-26381 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eberwein, Robert T1 - Systeme mit tiefkalt verflüssigten Gasen in Brandereignissen N2 - Die volumetrische Energiedichte eines Gases kann durch Verflüssigung erhöht wer-den. Diese findet statt, wenn das Gas unter den Siedepunkt abgekühlt wird. Verflüs-sigte Gase mit großer Bedeutung für die Energiewende sind verflüssigter Wasser-stoff (LH2) und verflüssigtes Erdgas (LNG), dessen Verflüssigung Temperaturen von unter -160 °C bedarf. Systeme zur Speicherung dieser verflüssigten Gase müssen in der Regel für Überdrücke ausgelegt sein und benötigen thermische Superisolierun-gen (TSI), um die tiefkalten Bedingungen über längere Zeit halten zu können und Verluste durch Boil-Off gering zu halten. TSI mit Vakuum und MLI oder Perlit sind für viele Anwendungen mit LNG und LH2 geeignet. Bei solchen Systemen handelt es sich in der Regel um doppelwandige Strukturen, bei denen die Innenwand mit dem tiefkalten Fluid in Kontakt steht. Die Lücke, zwischen der Innen- und der Außen-wand befindet sich unter Vakuumbedingungen und enthält zudem MLI oder Perlite. Diese Kombination von Isolationsmethoden ermöglicht es auf kleinstem Raum sehr gute thermische Isolationswirkung zu erreichen. Aus wirtschaftlicher Sicht sind die Systeme gut durchdacht. Das Wissen über das Verhalten dieser Systeme bei einem typischen Ereignis wie einem Brand ist jedoch begrenzt. Dieses Wissen ist aber not-wendig, um die Sicherheit der wachsenden Zahl von Anwendungen auf dem Markt bewerten zu können. T2 - H2-Kolloquium des Kompetenzzentrum „H2Safety@BAM” CY - Online meeting DA - 04.07.2022 KW - Tiefkalt KW - Verflüssigt KW - Isolation KW - Auslegungsüberschreitend PY - 2022 AN - OPUS4-55178 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Schartel, Bernhard A1 - Richter, K. H. A1 - Böhning, Martin ED - Morgan, A. B. ED - Wilkie, C. A. ED - Nelson, G. L. T1 - Synergistic use of talc in halogen-free flame retarded polycarbonate/Acrylonitrile-butadiene-styrene blends N2 - Pyrolysis, flammability, fire behavior, melt viscosity, and gas diffusion of bisphenol A polycarbonate/acrylonitrile-butadiene-styrene (PC/ABS) were investigated, with bisphenol A bis(diphenyl phosphate) (BDP), with 10 wt.% talc and with BDP in combination with 5, 10 and 20 wt.% talc, respectively. Compared to PC/ABS, PC/ABS + BDP results in an increased decomposition temperature of PC, a higher char yield, a significantly increased LOI, a V-0 classification in UL 94, a reduced peak heat release rate (pHRR), and a reduced total heat release (THR) in the cone calorimeter. This efficient flame retardancy is due to mechanisms in both the gas and condensed phases. PC/ABS + 10 wt.% talc shows a decrease in the PC decomposition temperature. The fire behavior is improved in part compared to PC/ABS, with an increased LOI and reduced pHRR. PC/ABS + BDP + 10 wt.% talc shows a strong synergism in LOI, a V-0 classification, and a decrease in pHRR, whereas THR is slightly increased compared to PC/ABS + BDP. Talc decreases the gas diffusion and enhances the flow limit for low shear rates, both of which influence the pyrolysis and flammability results. Further, talc improves the protection properties of the fire residues. Nevertheless it also partly suppresses flame inhibition and the charring effect of BDP. The synergism between BDP and talc in LOI is obtained even for low talc loadings in PC/ABS + BDP + talc, whereas for higher loadings saturation is observed. KW - Flame retardancy KW - PC/ABS KW - Aryl phosphate KW - Talc PY - 2012 SN - 978-0-8412-2780-4 DO - https://doi.org/10.1021/bk-2012-1118.ch002 N1 - Serientitel: ACS Symposium Series – Series title: ACS Symposium Series VL - 1118 IS - Chapter 2 SP - 15 EP - 36 PB - Oxford University Press AN - OPUS4-27563 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rücker, Werner A1 - Karabeliov, Krassimire A1 - Cuéllar, Pablo A1 - Baeßler, Matthias A1 - Georgi, Steven ED - Savidis, S.A. T1 - Ermittlung der Tragfähigkeit von Offshore Rammpfählen unter zyklischer Belastung - Modellversuche, Großversuche, numerische Verfahren N2 - Im Rahmen mehrerer vom BMU geförderter Forschungsvorhaben untersucht die BAM zusammen mit Partnern aus Industrie und Wissenschaft das Tragverhalten von zyklisch lateral und axial belasteten Rammpfählen für Offshore Windkraftanlagen. Neben Modellversuchen im Labor werden hierbei auch Großversuche im Maßstab 1: 2 und im Originalmaßstab durchgeführt. In diesen Großversuchen werden Parameter wie Tragfähigkeitsminderung infolge zyklischer Lasten im Druck- und Schwellbereich, sowie die Zunahme von Tragfähigkeiten durch sogenannte Anwachseffekte untersucht. Durch die zyklischen Belastungen werden insbesondere als unsicher anzunehmende Wertepaare in den derzeit verwendeten Interaktionsdiagrammen untersucht, wobei ein Hauptaugenmerk aber nicht nur auf dem Versagen des Pfahls, sondern auch auf der Ermittlung der Resttragfähigkeit nach definierten Zyklenzahlen liegt. Ein weiteres Ziel ist, die sich am Pfahlmantel in Abhängigkeit der oben genannten Parameter ergebenden Tragfähigkeiten durch numerische Berechnungen und durch Laborversuche zu erklären und ein existierendes Modell zur Ermittlung der Tragfähigkeit unter zyklischer Belastung auf der Grundlage aktueller Messdaten am Pfahl zu validieren und zu kalibrieren. Weiterhin finden durch den Projektpartner BARD Untersuchungen zur Abhängigkeit der Pfahltragfähigkeit von der Standzeit bei der Errichtung des Windparks BARD Offshore 1 statt. T2 - 8. Hans Lorenz Symposium CY - Berlin, Germany DA - 11.10.2012 PY - 2012 SN - 978-3-8440-1377-1 SN - 0342-3905 N1 - Serientitel: Veröffentlichungen des Grundbauinstitutes der Technischen Universität Berlin – Series title: Veröffentlichungen des Grundbauinstitutes der Technischen Universität Berlin IS - 60 SP - 311 EP - 329 PB - Shaker AN - OPUS4-27178 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Scheid, Marc A1 - Snoeys, J. A1 - Bunse, R. T1 - Neues aus den Normenausschüssen zum Staubexplosionsschutz N2 - Im Rahmen der Umsetzung der beiden ATEX-Richtlinien, insbesondere der Richtlinie 94/9/EG, entstanden im Normungsgremium CEN TC 305 bzw. in den einzelnen Arbeitsgruppen eine Vielzahl von europäischen Normen und technischen Regeln zum Staubexplosionsschutz. Zwischenzeitlich wurden mehrere der zuerst erstellten Regelwerke überarbeitet oder befinden sich derzeit in der Überarbeitung. Gleichzeitig werden weitere Regelwerke erstellt. Außerdem werden derzeit auf internationaler Ebene Normen im neu gegründeten Gremium SC 31 M „Non-electrical equipment and protective Systems for explosive atmospheres" erarbeitet. Dieser Beitrag gibt einen Überblick über kürzlich erstellte bzw. überarbeitete Regelwerke und derzeitige Projekte in CEN/TC 305 und IEC/SC 31 M mit Schwerpunkt auf Arbeiten in den Arbeitsgruppen WG 1 und WG 3 von CEN TC 305 bzw. in der Gruppe MT 80079-20-2 von IEC/SC 31 M. T2 - VDI-Fachtagung - Sichere Handhabung brennbarer Stäube CY - Nürnberg, Germany DA - 06.11.2012 KW - ATEX KW - Normung Staubexplosionsschutz KW - Sicherheitstechnische Kenngrößen KW - Konstruktiver Explosionsschutz PY - 2012 SN - 978-3-18-092182-2 SN - 0083-5560 N1 - Serientitel: VDI-Berichte – Series title: VDI-Berichte VL - 2182 SP - 17 EP - 29 PB - VDI-Verl. CY - Düsseldorf AN - OPUS4-27131 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Pretsch, Thorsten A1 - Ecker, Melanie A1 - Schildhauer, Markus A1 - Maskos, Michael T1 - Switchable information carriers based on shape memory polymer N2 - Herein we demonstrate the realization of a new technological concept, which enables the use of shape memory polymers (SMPs) as switchable information carriers. At first, we applied a surface-specific dyeing process based on 'guest-diffusion' on two sophisticated polymeric host materials, including a thermoplastic poly(ester urethane) SMP and a thermoset epoxy-based SMP. Upon drying, self-assembly of the dye molecules inside the polymer surfaces occurred, resulting in homogeneous color penetration depths of about 100 µm. Subsequently, the colored surfaces were patterned with quick response (QR) codes. For this purpose, laser ablation was used. The resulting cavity depth was exceeding the color penetration depth. This assured sufficient surface contrast and rendered the QR codes machine-readable. In a progressive approach, two thermo-mechanical functionalization protocols were designed in accordance with the thermal properties of the polymers. As a result of programming, the tag prototypes were converted into stable, temporary shapes with non-decodable QR code information. When thermally triggering the shape memory effect on the functionalized tags, we verified the mostly complete recovery of the polymer surface and the associated restoration into the almost original shape. As such, the QR code could again precisely be read out. We anticipate that tagging products with these information carriers is helpful for the purpose of secure one-time identification. KW - Shape memory polymer KW - Epoxy-based polymer KW - Poly(ester urethane) KW - Thermo-responsive polymer KW - Laser ablation KW - Laser marking KW - QR code KW - Functionalized tags KW - Tag technology KW - Smart tagging KW - Switchable information carrier KW - Authentification KW - Identification KW - Surface-specific dyeing KW - Guest diffusion PY - 2012 DO - https://doi.org/10.1039/c2jm16204k SN - 0959-9428 SN - 1364-5501 VL - 22 IS - 16 SP - 7757 EP - 7766 PB - Royal Society of Chemistry CY - Cambridge AN - OPUS4-25737 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Quiroz Penaranda, Vanessa A1 - Gumenyuk, Andrey A1 - Rethmeier, Michael T1 - Laser beam weldability of high-manganese austenitic and duplex stainless steel sheets N2 - Manganese alloyed stainless steels represent a cost-effective alternative to conventional CrNi- stainless steels due to strong fluctuations of the market prices for nickel seen during the last years. In CrMnNi steels, nickel is partially replaced by lower-cost manganese and small amounts of nitrogen for stabilization of the austenitic phase. This also brings benefits regarding the mechanical properties, as it results in an increased material strength. Laser beam welding of such materials was investigated for direct comparison with standard CrNi steels. Main emphasis was laid on finding adequate process parameters to achieve a stable welding process and obtain a good weld quality. Two different laser sources, a 4.4 kW Nd:YAG and a 5 kW CO2 laser, were used to weld 1.5 mm stainless steel sheets in continuous wave mode. A high-Mn austenitic (1.4376) and a lean duplex (1.4162) steel, as well as the standard austenitic (1.4301) and duplex (1.4362) grades were selected as test materials. Both butt and lap joint configurations were studied. Experiments were carried out systematically, varying the welding speed, laser power and focal point position in order to determine adequate process windows. The influence of the shielding gas type and flow rate on the process stability and the weld quality were investigated. The effects of weld edge preparation on the weld appearance and quality levels attained were also examined. The obtained welded joints were subjected to radiographic tests for detection of internal imperfections. Also a metallurgical characterization of the samples regarding the resulting phase composition or balance and hardness depending on the welding process parameters was conducted. Furthermore, tensile and potentiodynamic tests were performed to evaluate the mechanical and corrosion properties, respectively. The results provide an insight into the advantages and limitations of the laser beam welding process for joining high-manganese alloyed stainless steels. Conditions for the production of defect-free and corrosion-resistant welds having good mechanical properties could be determined. KW - Austenitic stainless steels KW - Corrosion KW - CO2 lasers KW - Duplex stainless steels KW - Laser welding KW - Manganese KW - Mechanical properties KW - Shielding gases KW - YAG lasers KW - Weldability PY - 2012 SN - 0043-2288 SN - 1878-6669 VL - 56 IS - 1/2 SP - 9 EP - 20 PB - Springer CY - Oxford AN - OPUS4-25404 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Weimann, Karin A1 - Hoffmann, C. T1 - Ressourceneffizienz im Betonrecycling - Rahmen und Möglichkeiten in Deutschland und der Schweiz N2 - Aufgrund der großen anfallenden Massenströme ist die Wiederverwertung von Baurestmassen in Industrienationen von besonderer Bedeutung. Auch vor dem Hintergrund der Ressourceneffizienz wird beispielsweise die Nutzung des in Bauschutt vorhandenen Wertstoffpotentials zunehmend wichtiger. Eine besondere Rolle spielt dabei die Wiederverwertung von Altbeton. Ein Grund hierfür ist der deutliche Anstieg des seit Mitte des letzten Jahrhunderts im Bauwesen verbrauchten Betons und die damit verbundene – zeitlich versetzte – Zunahme des Altbetonanteils im Bauschutt. Darüber hinaus ist das Wertstoffpotential von Altbeton im Vergleich zu anderen Abbruchmaterialien besonders groß, denn Altbeton kann unter bestimmten Bedingungen sehr hochwertig auch als rezyklierte Gesteinskörnung wieder in der Betonherstellung eingesetzt werden. Damit kann ein Kreislauf im Sinne eines Closed-loop-Recycling verwirklicht und Altbeton damit hochwertig wiederverwertet werden. T2 - R’13 - Fachtagung Recycling CY - Weimar, Germany DA - 19.09.2013 KW - Ressourceneffizienz KW - Beton KW - Recycling KW - Ökobilanzielle Betrachtung PY - 2013 IS - Paper 14 SP - 1 EP - 11 PB - Bauhaus-Univ. CY - Weimar AN - OPUS4-30061 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Grzeszkowski, Mateusz A1 - Prager, Jens ED - Linde, B. B. J. ED - Paczkowski, J. ED - Ponikwicki, N. T1 - Determination and visualization of the wave propagation on solid surfaces using a single head laser vibrometer N2 - This paper presents an automated system for the evaluation and visualization of structural vibrations on the surface of solid materials in an ultrasonic frequency range using a single head laser Doppler vibrometer. For this method, the vibrometer performs a continuous scan of the surface driven by a two-axes robotic system. Scan and measurement parameters can be adapted to the requirements of geometry, frequency and resolution. Data processing techniques are employed to improve the signal-to-noise ratio and minimize the effect of inconvenient laser beam reflections caused by speckles. T2 - International congress on ultrasonics CY - Gdansk, Poland DA - 05.09.2011 KW - Acoustic signal processing KW - Data visualisation KW - Doppler measurement KW - Measurement by laser beam KW - Robots KW - Structural acoustics KW - Structural engineering KW - Structural engineering computing KW - Vibration measurement PY - 2012 SN - 978-0-7354-1019-0 DO - https://doi.org/10.1063/1.3703184 SN - 0094-243X N1 - Serientitel: AIP conference proceedings – Series title: AIP conference proceedings IS - 1433 SP - 259 EP - 262 PB - American Institute of Physics CY - Melville, NY AN - OPUS4-27791 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Prager, Jens A1 - Gravenkamp, Hauke A1 - Rahman, Mehbub-Ur A1 - Köppe, Enrico T1 - Einsatz geführter Wellen für die Ultraschallprüfung N2 - Der Einsatz geführter Wellen für die zerstörungsfreie Prüfung mit Ultraschall eröffnet neue Möglichkeiten, räumlich ausgedehnte Bauteile mit begrenzter Zugänglichkeit auf ihre Integrität zu prüfen und gewinnt daher zunehmend an Bedeutung. Dieser Artikel behandelt die physikalischen Grundlagen der Schallausbreitung. Deren Verständnis bildet die Grundlage für die Entwicklung geeigneter Prüfsysteme. An Beispielen werden verschiedene Möglichkeiten zur Simulation der Schallausbereitung vorgestellt. Aktuelle Lösungsansätze zur Prüfung von plattenförmigen Strukturen und von Rohrleitungen werden beschrieben, wobei besonders auf die Sensortechnik und die speziellen Anforderungen an die Prüfhardware eingegangen wird. N2 - Guided waves are widely used for non-destructive testing using ultrasound. Recently, the method has become increasingly important for integrity tests of spatially extended components with limited accessibility. This article discusses the basic physics of the sound propagation of guided waves. Their understanding forms the basis for the successful development of adapted inspection systems. Examples for simulating the wave propagation using different methods are presented. Current approaches for the inspection of plate-like structures and pipelines are described with focus on sensor technology and the specific requirement on the test hardware. KW - Zerstörungsfreie Prüfung KW - Geführte Wellen KW - Ultraschallprüfung KW - Non-destructive evaluation KW - Guided waves KW - Ultrasound PY - 2012 DO - https://doi.org/10.1524/teme.2012.0168 SN - 0340-837X SN - 0178-2312 SN - 0171-8096 VL - 79 IS - 5 SP - 251 EP - 261 PB - Oldenbourg CY - München AN - OPUS4-26206 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Fittschen, U. A1 - de Oliveira Guilherme Buzanich, Ana A1 - Böttger, S. A1 - Rosenberg, D. A1 - Menzel, M. A1 - Jensen, W. A1 - Busker, M. A1 - Gotlib, Z. A1 - Radtke, Martin A1 - Riesemeier, Heinrich A1 - Wobrauschek, P. A1 - Streli, C. ED - de Oliveira Guilherme Buzanich, Ana T1 - A setup for synchrotron-radiation-induced total reflection X-ray fluorescence and X-ray absorption near-edge structure recently commissioned at BESSY II BAMline N2 - An automatic sample changer chamber for total reflection X-ray fluorescence (TXRF) and X-ray absorption near-edge structure (XANES) analysis in TXRF geometry was successfully set up at the BAMline at BESSY II. TXRF and TXRF-XANES are valuable tools for elemental determination and speciation, especially where sample amounts are limited (<1 mg) and concentrations are low (ng ml⁻¹ to μg ml⁻¹). TXRF requires a well defined geometry regarding the reflecting surface of a sample carrier and the synchrotron beam. The newly installed chamber allows for reliable sample positioning, remote sample changing and evacuation of the fluorescence beam path. The chamber was successfully used showing accurate determination of elemental amounts in the certified reference material NISTwater 1640. Low limits of detection of less than 100 fg absolute (10 pg ml⁻¹) for Ni were found. TXRF-XANES on different Re species was applied. An unknown species of Re was found to be Re in the +7 oxidation state. KW - TXRF KW - TXRF-XANES KW - Sample changer KW - BAMline KW - Re-XANES PY - 2016 DO - https://doi.org/10.1107/S1600577516001995 SN - 1600-5775 VL - 23 IS - 3 SP - 820 EP - 824 PB - International Union of Crystallography AN - OPUS4-38656 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kühn, Andreas A1 - Scharf, Oliver A1 - Ordavo, I. A1 - Riesemeier, Heinrich A1 - Reinholz, Uwe A1 - Radtke, Martin A1 - Berger, Achim A1 - Ostermann, Markus A1 - Panne, Ulrich T1 - Pushing the limits for fast spatially resolved elemental distribution patterns N2 - A new setup for fast spatially resolved measurements of elemental trace amounts under total reflection conditions using a new colour X-ray camera is described. Samples prepared on conventional total reflection X-ray fluorescence (TXRF) reflectors were measured at BESSY II synchrotron. A spatial resolution of 50 × 50 µm² was obtained, while the required time for the investigation of a 10 × 10 mm² sample is 30 seconds. The set-up is up to 350 times faster than conventional X-ray fluorescence systems for elemental traces. The major components of the X-ray camera are polycapillary optics and a pn-CCD chip with an active area of 13 × 13 mm². This area is divided into 264 × 264 pixels of 48 × 48 µm². A full X-ray spectrum with a resolution of 152 eV @ 5.9 keV and a chip temperature of 246 K is recorded for each pixel. The chip has a read-out rate of 400 Hz. PY - 2011 DO - https://doi.org/10.1039/c1ja10069f SN - 0267-9477 SN - 1364-5544 VL - 26 SP - 1986 EP - 1989 PB - Royal Society of Chemistry CY - London AN - OPUS4-24386 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Förste, F. A1 - Bauer, L. A1 - Streeck, C. A1 - Radtke, Martin A1 - Reinholz, Uwe A1 - Kadow, D. A1 - Keil, C. A1 - Mantouvalou, I. T1 - Quantitative Analysis and 2D/3D Elemental Imaging of Cocoa Beans Using X‑ray Fluorescence Techniques N2 - As an important raw material for the confectionery industry, the cocoa bean (Theobroma cacao L.) has to meet certain legal requirements in terms of food safety and maximum contaminant levels in order to enter the cocoa market. Understanding the enrichment and distribution of essential minerals but also toxic metals is of utmost importance for improving the nutritional quality of this economically important raw food material. We present three X-ray fluorescence (XRF) techniques for elemental bio-imaging of intact cocoa beans and one additional XRF technique for quantitative analysis of cocoa pellets. The interrelation of all the methods presented gives a detailed picture of the content and 3D-resolved distribution of elements in complete cocoa beans for the first time. KW - BAMline KW - Synchrotron KW - XRF KW - CXC KW - Cocoa PY - 2023 DO - https://doi.org/10.1021/acs.analchem.2c05370 VL - 95 SP - 5627 EP - 5635 PB - ACS Publications AN - OPUS4-57832 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tiebe, Carlo A1 - Hübert, Thomas A1 - Lorek, A. A1 - Wernecke, R. T1 - HUMItrace-Sensorsystem mit neuartigen planaren Spurenfeuchtesensoren N2 - Es wird ein Sensorsystem (HUMItrace III) zur Spurenfeuchtebestimmung in der Prozessmesstechnik vorgestellt. Die Bestimmung der Spurenfeuchte erfolgt mit neuentwickelten planaren Sensoren (HUMItrace-Sensoren) nach dem coulometrischen Messprinzip im Frostpunkttemperaturbereich von -80 °C bis -30 °C mit der Kalibriereinrichtung THG11 durch Mischen von trockenen und befeuchteten Teilgasströmen kalibriert. Die Gasfeuchte von Luft kann in diesem Bereich mit den HUMItrace-Sensoren mit einer erweiterten Unsicherheit von 2 K bestimmt werden. Die Sensoren können aber auch zur Gasfeuchtemessung in Wasserstoff, Stickstoff und Distickstoffmonoxid eingesetzt werden. Eine weitere Kalibriereinrichtung, THG-P12, generiert Prüfgase nach der Permeationsmethode; sie kann in das HUMItrace III Sensorsystem implementiert und zur vor-Ort-Kalibrierung der HUMItrace-Sensoren nach dem Standardadditionsverfahren genutzt werden. T2 - Temperatur 2013 - Verfahren und Geräte in der Temperatur- und Feuchtemesstechnik CY - Berlin, Germany DA - 05.06.2013 PY - 2013 SN - 3-9810021-8-0 SP - 257 EP - 262 AN - OPUS4-28732 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. A1 - Hajhariri, Aliasghar T1 - A modular concept for protection against debris flight - Design, properties and usage N2 - With advances in technological development, stationary and mobile storage units for compressed hydrogen are becoming larger and larger. Their number is also increasing. At the same time, their design has evolved from steel and aluminium to pressure vessels made of composite materials. For safety reasons the design approval of those composite cylinders requires fire engulfment tests, which are mainly organised as open-air tests always needs dedicated protection measures. Under some conditions those protections measures even reduce the effort for organisational safety measures if e.g. the emission of splinters can get totally prevented. Another aspect is the improved reproducibility of fire tests by reducing the influence of wind, especially wind turbulence. Between 2017 and 2019, BAM developed a stackable protective frame made of steel to safely capture splinters for the safe execution of high-energy impact tests. However, this frame was not flexible enough for the follow up project, which led to a completely new protection concept for (potentially) destructive tests on gas-filled pressure vessels. This concept is based on very robust building blocks with knobs and holes of a dimension of 1m x 0.5m x 0.5m made from welded steel. Despite their considerable weight of around 500 kg, they can be combined and stacked very easily like ‘Lego bricks’. The presentation will show the flexibility of the concept, some results of tests on the robustness against pressure waves and the effectiveness in wind attenuation. Finally, the interaction with a new, also modular burner concept for localised fires and full engulfment fires will be presented. T2 - 11th International Conference on Hydrogen Safety ICHS 2025 CY - Seoul, South Korea DA - 24.09.2025 KW - Splinter protection KW - Pressure vessel testing KW - Fire engulfment KW - Destructive tests KW - Rupture KW - Gaseous tests KW - Pressure wave KW - Test equipment KW - Precaution measures PY - 2025 AN - OPUS4-65099 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg W. T1 - Safety challenges of the hydrogen market ramp-up N2 - The presentation will provide some thoughts on the key safety challenges for staying safe during the market ramp-up phase of the rapidly expanding hydrogen economy. The focus is on storage aspects, but other topics are also covered. Each brief description of an aspect is followed by a proposal for solving the problem. Key words are safety aspects of hydrogen transport (CGH2 and LH2), risk control, consequence limitation, structural reliability control, safety monitoring through destructive and non-destructive testing, improvement of RCS through impact simulation, new approaches to safety assessment, outlook on the potential of NDT and digital product passports. T2 - 6th Germany–Korea Hydrogen Conference 2025 CY - Seoul, South Korea DA - 03.12.2025 KW - Risk-control KW - Regulatory measures KW - Operational safety KW - Mass transport KW - Full scale tests PY - 2025 AN - OPUS4-65102 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bartholmai, Matthias A1 - Neumann, Patrick P. A1 - Johann, Sergej A1 - Tiebe, Carlo A1 - Gawlitza, Kornelia A1 - Bartelmeß, Jürgen T1 - KonSens - Kommunizierende Sensorsysteme für die Bauteil- und Umweltüberwachung N2 - In the KonSens Project, sensor systems are developed, validated, and operated in form of functional models for the application areas Structure Integrated Sensors and Mobile Multi-gas Sensors. Key aspects are the detection and evaluation of corrosion processes in reinforced concrete structures as well as the detection and quantification of very low concentrations of toxic gases in air. The adaption of sensor principles from the lab into real-life application including appropriate communication techniques is a major task. In recent years, Structural Health Monitoring have gained in importance, since growing age of buildings and infrastructure as well as increasing load requirements demand for reliable surveillance methods. In this regard, the project follows two strategies: First, the development and implementation of completely embedded sensor systems consisting of RFID-tag and in situ sensors, and their further application potential (e.g. for precast concrete elements, roadways, wind power plants, and maritime structures). Secondly, the development of a long-term stable, miniaturized, fiber optic sensor for a ratiometric and referenced measurement of the pH-value in concrete based on fluorescence detection as an indicator for carbonation and corrosion. Environmental pollution through emission of toxic gases becomes an increasing problem not only in agriculture (e.g. biogas plants) and industry but also in urban areas. This leads to increasing demand to monitor environmental emissions as well as ambient air and industrial air components in many scenarios and in even lower concentrations than nowadays. The selectivity of luminescence-based sensors is enabled by the combination of the sensing dye and the material, which is used as accumulation medium for concentration of the analyte. This principle allows for developing gas sensors with high selectivity and sensitivity of defined substances. Additional benefits, particularly of fluorescence-based sensors, are their capability for miniaturization and potential multiplex mode. Objective is the development and implementation of sensors based on fluorescence detection for defined toxic gases (ammonia, hydrogen sulfide, ozone, and benzene) with sensitivity in the low ppm or even ppb range. Additionally, the integration of such sensors in mobile sensor devices is addressed. T2 - Colloquium of Optical Spectrometry (COSP) 2017 CY - Berlin, Germany DA - 27.11.2017 KW - RFID sensors KW - Sensors in concrete KW - Gas sensors KW - Mobile sensors KW - Fluorescence sensors PY - 2017 AN - OPUS4-43183 LA - mul AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eberwein, Robert A1 - Tugnoli, Alessandro A1 - Okpeke, Bright A1 - Campoari, Alessandro A1 - Zervaki, Anna T1 - NICOLHy - 2nd Stakeholder Advisory Board meeting N2 - The NICOLHy project aims to develop a novel insulation concept based on Vacuum Insulation Panels (VIP) that enables the safe, cost- and energy efficient storage of large quantities of LH2. Such large scale LH2 storage technology is necessary for establishing a hydrogen economy with dimensions between 40.000 m³ and more than 200.000 m³ of LH2. However, new design concepts are needed because the currently available technologies used in small and medium storages today are not suitable for up-scaling. The main problems prohibiting the up-scaling are the long production time due to the process chain, the low failure tolerance and the spherical shape, which reduces the payload in technical applications by up to 50% compared to other shapes. The novel concept will change these conditions by a system which is modular, open-form, time-and cost efficient while production, operation and service, multi-failure tolerant and applicable for onshore and offshore applications. The presentations shows details to the concept and presents several safety concerns the project has to deal with. This document contains all presentations from NICOLHys second Stakeholder Meeting. T2 - NICOLHy 2nd Stakeholder Meeting CY - Athens, Greece DA - 22.01.2025 KW - Liquefied hydrogen KW - Insulation KW - Tanks PY - 2025 AN - OPUS4-62564 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eberwein, Robert A1 - Hajhariri, Aliasghar A1 - Camplese, D. A1 - Scarponi, G. E. A1 - Cozzani, V. A1 - Otremba, Frank T1 - Insulation Materials Used in Tanks for the Storage of Cryogenic Fluids in Fire Scenarios N2 - The importance of tanks for storing cryogenic fluids in the energy industry is increasing because of ongoing political conflicts and the implementation of more environmentally friendly energy sources. Key representatives for the application of cryogenic tanks are natural gas in the form of Liquefied Natural Gas (LNG) and hydrogen, e. g. in the form of Liquefied Hydrogen (LH2), for which significantly higher transport capacities can be achieved with the same transport volume using cryogenic storages than with storages based solely on overpressure. What applies to all cryogenic transported fluids in common is their condition that must be maintained. Hence heat flows into the preserved fluid must be minimized. Thermal super Insulations (TSI) based on e. g. multilayer insulations (MLI), perlites, and vacuum are utilized for this purpose and have already proven themselves in similar applications. However, for the use of tanks for cryogenic fluids in the transport sector, there is insufficient knowledge regarding the course and consequences of incidents, which is due to the still short period of use and the few documented incidents, hence few investigations carried out in this field. Typical scenarios in the transport sector represent car accidents with collisions, fires, and their combination, which are associated with extraordinary loads on the tank. The focus of this study is to investigate the behavior of TSI as a result of their thermal exposure to a heat source representing a fire. It is worth mentioning that this could lead to an increase of the heat flux into a tank by several orders of magnitude, and to permanent damage of the TSI, ultimately rapid release of flammable gas as well as a Boiling Liquide Expanding Vapour Explosion (BLEVE). For this purpose, a high temperature thermal vacuum chamber (HTTVC) has been developed that allows thermal loading of MLI or perlites in a vacuum and simultaneous measurement of heat flow through this TSI. The HTTVC is designed to represent realistic insulation conditions and to withstand thermal loads from typical design fires. The HTTVC was applied to investigate TSI based on MLI and vacuum. It is shown that the thermal stress caused permanent damage to the TSI, with shrinkage, phase change, pyrolysis, and condensation being significant damage mechanisms. The results are relevant for the evaluation of accident scenarios and can thus contribute to the improvement of TSI and the development of emergency measures for the protection of persons and infrastructures. T2 - ASME 2023 Pressure Vessels & Piping Conference (PVP2023) CY - Atlanta, Georgia, USA DA - 16.07.2023 KW - LH2 KW - LNG KW - MLI KW - Fire PY - 2023 SP - 1 EP - 8 PB - ASME AN - OPUS4-57973 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hajhariri, Aliasghar ED - Eberwein, Robert ED - Perrone, Luca pakj ED - Cozzani, Valerio ED - Otremba, Frank ED - Seidlitz, Holger T1 - Study the Impact of Spacer at Thermal Degradation Process of MLI-based Insulation in Fire Condition N2 - To reduce carbon dioxide emissions, energy carries such as hydrogen consider to be a solution. Consumption of hydrogen as a fuel meets several restrictions such as its low volumetric energy density in gas phase. To tackle this problem, storage as well as transportation in liquid phase is recommended. To be able to handle this component in liquid phase, an efficient thermal insulation e.g., MLI insulation is required. Some studies have been revealed vulnerability of this type of insulation against high heat flux, for instance a fire accident. Some investigations have been depicted the importance of consideration of the MLI thermal degradation in terms of its reflective layer. However, limited number of studies have been focused on the thermal degradation of spacer material and its effect on the overall heat flux. In this study, through systematic experimental measurements, the effect of thermal loads on glass fleece, glass paper as well as polyester spacers are investigated. The results are reported in various temperature and heat flux profiles. Interpreting the temperature profiles revealed as the number of spacers in the medium increases, the peak temperature detectable by the temperature sensor on the measurement plate decreases. Moreover, the contribution of each individual spacer in all cases regarding the experimental temperature range is assessed to be around 8%. This value may increase to around 50% for glass paper and polyester spacers, and to around 25% for glass fleece spacers as the number of spacer layers increases up to six layers. To utilize the outcomes of the experiment later and integrate the results into numerical and CFD simulations, a model is proposed for the mentioned experimental temperature range up to 300°C to predict a heat flux attenuation factor. The model proposes a fitting factor that can reproduce the least square fitted line to the experimental data. T2 - 15th International Symposium on Hazards, Prevention, and Mitigation of Industrial Explosions Naples (ISHPMIE) CY - Naples, Italy DA - 10.06.2024 KW - Multi-Layer Insulation KW - Cryogenics KW - Liquid Hydrogen KW - Heat Transfer KW - Hydrogen Storage PY - 2024 SP - 744 EP - 755 AN - OPUS4-60461 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eberwein, Robert A1 - Scarponi, Giordano Emrys A1 - Cozzani, Valerio A1 - Otremba, Frank T1 - Lh2 Tanks In Fire Incidents - The Cryogenic High Temperature Thermal Vacuum Chamber Enables In-Depth Insights N2 - Liquefied Hydrogen (LH2) and Liquefied Natural Gas (LNG) establish themselves as important energy carriers in the transport sector. Their storage requires tanks with thermal super-insulations to keep them at cryogenic conditions for a long time. These insulation systems have proven itself in various applications over a long time. However, these insulations are still new in land transportation, where accidents involving collisions, fires, and their combination are to be expected. This study summarizes the results of the ongoing research program in which insulations commonly used in industry were analysed through experimental and numerical studies under fire-like conditions. It was found that there are strong differences among the various insulation systems. Several safety concerns and research gaps exists for layered insulations, which are typically used in land transport. To further analyse these insulation systems, a new test concept called Cryogenic High Temperature Thermal Vacuum Chamber (CHTTVC) was developed and manufactured. This concept enables the testing of large insulation samples under industrial conditions and the consideration of cryogenic conditions relevant for the investigation of various phenomena. The results are important for the evaluation of accident scenarios, the improvement of thermal super-insulations, and the development of emergency measures. T2 - IMECE 2024 CY - Oregon, Portland, USA DA - 17.11.2024 KW - LH2 KW - LNG KW - Fire KW - Insulation KW - Safety PY - 2024 SN - 978-0-7918-8869-8 SP - 1 EP - 7 PB - ASME AN - OPUS4-61751 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Camplese, D. A1 - Chianese, C. A1 - Scarponi, G. A1 - Eberwein, Robert A1 - Otremba, Frank A1 - Cozzani, V. T1 - Analysis of high temperature degradation of multi-layer insulation (MLI) systems for liquid hydrogen storage tanks N2 - The interest in hydrogen-based green energy is increasing worldwide, and the same is true for hydrogen-powered vehicles. Among the possible solutions to store hydrogen in such vehicles, cryogenic tanks equipped with multi-layer insulation (MLI) are the most promising to increase the amount of energy stored per unit volume. However, MLI is affected by severe deterioration when exposed to an external source of heat such as a fire following a car accident, leaving the tank unprotected and leading to failure in a relatively short time. In this work, a one-dimensional model to evaluate MLI thermal degradation when a liquid hydrogen tank is exposed to fire is presented. The relevance of taking MLI degradation into account when simulating the pressure increase due to external fire exposure is here demonstrated through the analysis of several case studies. The results show that MLI systems performance depletes within a few minutes of exposure to hydrocarbon poolfire. T2 - ICheaP 16 CY - Naples, Italy DA - 21.05.2023 KW - LH2 KW - MLI KW - Tiefkalt KW - Fire KW - Tank PY - 2023 SN - 2283-9216 VL - 2023 SP - 1 EP - 6 PB - AIDIC Servizi S.r.l. AN - OPUS4-57584 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -