TY - CONF A1 - Mielentz, Frank A1 - Milmann, Boris A1 - Krause, Martin A1 - Müller, W. A1 - Crail, S. T1 - Zerstörungsfreie Risscharakterisierung in Betonbauteilen mit Ultraschall T2 - DGZfP-Berichtsband N2 - Die Risstiefenbestimmung in Festen Fahrbahnen ist hinsichtlich der Dauerhaftigkeit der Konstruktion von wesentlichem Interesse. Im Rahmen eines gemeinsamen Forschungsvorhabens mit der DB AG wurden aus der Literatur bekannte Ansätze bewertet und darauf aufbauend ein Verfahren zur bildgebenden Rissdarstellung entwickelt. Rissüberbrückende Bewehrung sowie Kontaktstellen zwischen den Rissflanken wirken als Schallbrücken und erschweren die Risscharakterisierung, wie bei einem Einsatz an einer Betriebserprobungsstrecke festgestellt wurde. Ein aus der Literatur bekanntes Verfahren der einfachen Laufzeitmessung erwies sich für die Tiefenbestimmung von realen verunreinigten Rissen als ungeeignet. T2 - Fachtagung Bauwerksdiagnose - Praktische Anwendungen Zerstörungsfreier Prüfungen CY - Leipzig, Germany DA - 25.10.2001 PY - 2001 VL - 76-CD SP - 1 EP - 10 PB - Deutsche Gesellschaft für Zerstörungsfreie Prüfung (DGZfP) CY - Berlin AN - OPUS4-1188 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mittag, Kornelia A1 - Colla, Camilla A1 - Krause, Martin A1 - Maierhofer, Christiane A1 - Mielentz, Frank A1 - Milmann, Boris A1 - Schneider, Gerhard A1 - Wöstmann, Jens A1 - Wiggenhauser, Herbert T1 - Zerstörungsfreie Messungen zur Beurteilung des inneren Zustandes fester Fahrbahnen der Deutschen Bahn AG: Vergleichsmessungen an Probeaufbauten im Labor T2 - DGZfP-Berichtsband N2 - Im Rahmen eines FE-Projektes “Inspektion Fester Fahrbahnen“ der BAM und der Deutschen Bahn AG geht es um die Anwendung und weitere Entwicklung zerstörungsfreier Messverfahren zur Beurteilung des Zustandes Fester Fahrbahnen. Nach ersten Versuchsreihen direkt im Gleis wurden für verschiedene Bauarten die charakteristischen Herstellungsbedingungen simuliert und systematisch untersucht. Die kombinierte Anwendung der drei Messverfahren Ultraschall-Array-, Impakt-Echo- und Impuls-Radar-Verfahren wird hier an dem Beispiel “Betonschwelle in Betoneinbettung” dargestellt. T2 - Fachtagung Bauwerksdiagnose - Praktische Anwendungen Zerstörungsfreier Prüfungen CY - Leipzig, Germany DA - 25.10.2001 KW - Impakt-Echo-Messverfahren KW - Impuls-Radar-Messverfahren KW - Ultraschall-Array-Messverfahren PY - 2001 VL - 76-CD SP - 1 EP - 8 PB - Deutsche Gesellschaft für Zerstörungsfreie Prüfung (DGZfP) CY - Berlin AN - OPUS4-1201 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bishop, J. L. A1 - Pieters, C. M. A1 - Dyar, M. D. A1 - Hamilton, V. E. A1 - Harloff-Puhr, Jan T1 - A spectral, chemical and mineralogical study of Mars analogue rocks T2 - Lunar and planetary science XXXIII - papers presented to the Thirty-Third Lunar and Planetary Science Conference N2 - A consortium has recently been initiated to study the macroscopic and microscopic properties of basaltic and andesitic rocks as analogue materials for Mars. The goal of this project is the integration of diverse spectroscopic approaches to evaluate the composition and texture of Mars materials using both in situ and remote sensing techniques. Initial emphasis is placed on assessment of the mineral composition for low albedo areas (basalt vs andesite vs weathering) of the Martian surface through spectral analysis of a suite of samples that have been exceptionally well characterized in the laboratory. The initial results indicate that the visible/NIR reflectance spectra, mid-IR reflectance and emission spectra, and Mössbauer spectra contain consistent diagnostic features associated with the measured modal mineralogy and provide baseline data for the first group of well characterized basalts. The consortium study involves integrating multiple remote sensing techniques for recent and upcoming missions to Mars in order to compare the results obtained by these instruments and thereby strengthen interpretive results. T2 - 33rd Lunar and Planetary Science Conference CY - Houston, TX, USA DA - 2002-03-11 PY - 2002 UR - http://www.lpi.usra.edu/meetings/lpsc2002/pdf/1168.pdf SN - 0161-5297 N1 - Geburtsname von Harloff-Puhr, Jan: Harloff, J. - Birth name of Harloff-Puhr, Jan: Harloff, J. N1 - Serientitel: LPI contribution – Series title: LPI contribution IS - 1109 SP - 1 EP - 2, paper #1168 PB - Lunar and Planetary Institute CY - Houston, Tex. AN - OPUS4-1218 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Maultzsch, Matthias T1 - The utilization of processed building rubble - A contribution of sustainability in concrete technology T2 - Proceedings of the Polish concrete days conference 2002 T2 - Polish Concrete Days Conference CY - Szczyrk, Poland DA - 08.10.2002 PY - 2002 SP - 629 EP - 639 PB - Polski Cement CY - Kraków AN - OPUS4-1547 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Meinhold, Uwe A1 - Mellmann, Günter A1 - Maultzsch, Matthias ED - Malhotra, V. M. T1 - Performance of high-grade concrete with full substitution of aggregates by recycled concrete T2 - Proceedings of the third CANMET/ACI international symposium on sustainable development of cement and concrete N2 - On the background of the need for reuse of building rubble and the saving of natural resources, a European Union research project was performed covering concrete technology and durability aspects. A very special precondition was the use of large-scale processed building rubble with unknown origin and the total replacement of aggregates above 2 mm. Comprehensive tests were carried out on the properties of the starting material from different processing plants and fresh concrete, particularly the interdependence of water addition and wor ability. Investigations on hardened concrete properties included strength devel-opment, creep and shrinkage, modulus of elasticity, capillary absorption, freezing and thawing resistance, and carbonation behavior over a long period. The results demonstrate that the industrial production of a high-grade, durable concrete is possible. The project is a promising contribution for sustainable development. T2 - Third CANMET/ACI International Symposium on Sustainable Development of Cement and Concrete CY - San Francisco, CA, USA DA - 16.09.2001 KW - Aggregates KW - Compressive strength KW - Concrete KW - Creep KW - Modulus of elasticity KW - Recycled concrete KW - Shrinkage PY - 2001 SN - 0-87031-041-0 N1 - Serientitel: ACI SP – Series title: ACI SP IS - SP 202 SP - 85 EP - 96 PB - American Concrete Institute (ACI) CY - Farmington Hills, Mich. AN - OPUS4-1933 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Leuschke, Günter T1 - Selbstentzündung von staubförmigen Materialien T2 - 5. Internationales Brandschutz-Seminar PY - 1976 SP - 145 EP - 159 PB - Vereinigung zur Förderung des Deutschen Brandschutzes CY - Karlsruhe AN - OPUS4-8432 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Aurich, Dietmar A1 - Baer, Wolfram A1 - Häcker, Ralf A1 - Klingbeil, Dietmar A1 - Künecke, Georgia A1 - Ohm, Katrin ED - Richard, H. A. T1 - Untersuchungen zur Bewertung des Zähigkeitsverhaltens im Übergangsbereich vom Spaltbruch zum Gleitbruch T2 - 32. Tagung des DVM-Arbeitskreises Bruchvorgänge - Festigkeits- und Bruchverhalten von Fügeverbindungen N2 - Im Hinblick auf das Verhalten von Bauteilen aus ferritischen Stählen im Übergangsbereich vom Gleitbruch zum Spaltbruch wurden in einem vom BMBF geförderten Forschungsvorhaben, über das nachfolgend auszugsweise berichtet wird, u.a. folgende Ziele verfolgt: • Abgrenzung des Anwendungsbereichs der elastisch-plastischen Bruchmechanik zu tiefen Temperaturen hin, • Möglichkeiten und Grenzen der Nutzung von Zähigkeitspotentialen im Übergangsbereich, • Ermittlung des Einflusses des Spannungszustandes auf das Bruchverhalten im Übergangsbereich und • Übertragbarkeit auf Bauteile. T2 - 32. Tagung des DVM-Arbeitskreises Bruchvorgänge CY - Berlin, Germany DA - 22.02.2000 PY - 2000 SN - 0943-3473 SP - 109 EP - 119 PB - DVM CY - Berlin AN - OPUS4-7025 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Böllinghaus, Thomas A1 - Hoffmeister, H. T1 - Hydrogen permeation in supermartensitic stainless steels dependent on heat treatment and chemical composition T2 - Corrosion 2000 - Papers N2 - Hydrogen might cause severe degradation of supermartensitic stainless steels, if they are activated during exposure to sour environments. Consistent and comprehensive data for hydrogen transport in these materials are thus required to support, in particular, modelling of hydrogen assisted cracking as a part of life time assessment of welded steel components. In addition to previously published diffusion coefficients and subsurface concentrations of a supermartensitic stainless steel further data dependent on heat treatment are provided by this contribution. Furthermore, a higher alloyed material has been investigated in the state as received and also in the quenched condition, in order to approach the influences of chemical composition on hydrogen transport in supermartensitic stainless steels. With respect to welding it turned out that the diffusion coefficient and the subsurface concentration are markedly dependent on heat treatment of the materials. T2 - Corrosion 2000 CY - Orlando, FL, USA DA - 2000-03-26 PY - 2000 SP - Paper 00141, 1 EP - 19 PB - NACE International CY - Houston, Tex. AN - OPUS4-11844 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kasch, Thomas A1 - Binder, Christian A1 - Brock, Thomas A1 - Hesse, Olaf A1 - Treisch, Nico T1 - Sind Berstscheiben in Anlagen für hochverdichteten Sauerstoff ein Sicherheitsrisiko? T2 - 3. Magdeburger Brand- und Explosionsschutztag / vfdb-Workshop N2 - Armaturen und Anlagenteile für Hochdruck-Sauerstoff enthalten meistens nichtmetallische Materialen als Sitz- und Dichtungswerkstoffe. Die Gefahr eines Ausbrands dieser Armaturen; ist grundsätzlich vorhanden, jedoch relativ gering, wenn neben dem richtigen Design geeignete metallische und nichtmetallische Materialien für die vorgesehenen Betriebsbedingungen von Druck und Temperatur gewählt werden. Aus sicherheitstechnischer Sicht sollte daher für Armaturen und Anlagenteile, die komplett aus Metall gefertigt und metallisch abgedichtet werden, eine noch geringere Gefahr eines Ausbrands bestehen. Während einer Versuchsreihe auf dem BAM-TTS- Frei Versuchsgelände mit Hochdruck-Sauerstoff brannte jedoch unerwartet ein solches - rein metallisches Anlagenteil - komplett ab. Bei diesen Versuchen platzt eine metallische Membran wie eine Berstscheibe bei einem bestimmten Sauerstoffdruck auf. T2 - 3. Magdeburger Brand- und Explosionsschutztag / vfdb-Workshop CY - Magdeburg, Germany DA - 21.03.2013 KW - Sauerstoff KW - Aluminium KW - Berstscheibe KW - Brandgefahr KW - Zündursache KW - Unfallanalyse PY - 2013 SN - 978-3-00-041601-9 SP - 1 EP - 8 AN - OPUS4-27996 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ramge, Peter A1 - Kühne, Hans-Carsten A1 - Ünal, Murat ED - Raupach, M. T1 - Modulare Ersatzmassen zur Reprofilierung denkmalgeschützter Natursteinbauwerke T2 - 3. Kolloquium Erhaltung von Bauwerken N2 - Weltweit besteht einen hoher, stetig wachsender Bedarf an Natursteininstandsetzung im Bereich des denkmalgeschützten Kulturguts. Das Ausbessem beschädigter Elemente mit sogenannten Steinersatzmassen ist dabei eine etablierte Technik. Hierfür werden Mörtel unterschiedlichster Zusammensetzung verwendet. Die Schwierigkeit für den Restaurator liegt in der Wahl, bzw. der Verfügbarkeit des optimalen Produkts, um im individuellen Fall sowohl den mechanischen und bauphysikalischen Anforderungen als auch den gestalterischen und denkmalpflegerischen Belangen gerecht zu werden. Anhand der im Beitrag an Fallbeispielen erläuterten häufig auftretenden Probleme und der daraus abgeleiteten Anforderungen an Natursteininstandsetzung, lässt sich die Komplexität dieser Aufgabe erkennen. An der BAM wird derzeit im Rahmen eines Forschungsprojekts ein modulares Steinersatzsystem entwickelt. Ziel der Entwicklung ist es dem Restaurator die größtmögliche Freiheit in der Anpassung des Mörtels an die Originalsubstanz zu geben. Erste Ergebnisse aus Parameterstudien zur Bindemittel- und Sandvariation sowie zu Polymermodifikationen werden vorgestellt. T2 - 3. Kolloquium Erhaltung von Bauwerken CY - Ostfildern, Germany DA - 22.01.2013 PY - 2013 SN - 978-3-943563-03-0 SP - 333 EP - 349 CY - Ostfildern AN - OPUS4-28000 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hille, Falk A1 - Said, Samir A1 - Schmid, Wolfgang T1 - Lasteinwirkung- und Zustandsüberwachung von großen Spannbetonbrücken T2 - Messen im Bauwesen 2013 - Ingenieuraufgaben und messtechnische Lösungen N2 - Die dauerhafte messtechnische Überwachung von Brückenbauwerken ist nach wie vor eine neuartige Verfahrensweise zur Bestimmung des Ist-Zustandes von Tragwerken. Der Fachbereich 7.2 Ingenieurbau der BAM befasst sich seit mittlerweise mehr als 25 Jahren mit der Entwicklung von Methoden und Verfahren dieser Form der Bauwerksüberwachung. Die damit verbundene Tätigkeit umfasst die Beschreibung theoretischer Grundlagen, die Entwicklung von Algorithmen zur Erfassung, Bearbeitung und Auswertung von Messsignalen, die Bewertung der Ergebnisse bezüglich Tragsicherheit, Gebrauchstauglichkeit und Restnutzungsdauer und nicht zuletzt die Untersuchung und Verifizierung der praktischen Anwendbarkeit. Dabei standen insbesondere die sogenannten dynamischen Verfahren im Blickpunkt der Aktivitäten. Ursprünglich zur Überwachung von rotierenden Maschinenkomponenten entwickelt und dann auch erfolgreich zur Überwachung von Bauteilen der Flugzeug-, Raumfahrt- und Automobilindustrie weiterentwickelt, weckten diese Verfahren weltweit das Interesse der sich mit der Sicherheit bestehender Baukonstruktionen befassenden Wissenschaftler und Ingenieure. Ein beachtenswertes Projekt der BAM in diesem Zusammenhang ist die Dauerüberwachung der Westendbrücke in Berlin, das Mitte der 90er Jahre von der damaligen Senatsverwaltung für Stadtentwicklung von Berlin (ehemals Bauen, Wohnen und Verkehr) in Auftrag gegeben und über viele Jahre gefördert wurde. Im Rahmen dieses Aufsatzes werden am Beispiel dieses Projektes, das sich wie ein roter Faden durch die Entwicklungsgeschichte des Monitorings an der BAM zieht, die Motivationen und Zielstellungen dargelegt, das Überwachungssystem vorgestellt und die gemachten Erfahrungen anhand einiger Ergebnisse erläutert. In einem weiteren Kapitel wird ein Ausblick auf die Zukunft des Monitorings mit angepassten Zielvorstellungen, neuen Methodiken und Strategien geworfen. T2 - Messen im Bauwesen 2013 - Ingenieuraufgaben und messtechnische Lösungen CY - Berlin, Germany DA - 12.03.2013 KW - Structural health monitoring KW - Spannbetonbrücken KW - Westendbrücke PY - 2013 SN - 978-3-9815360-5-8 SP - 107 EP - 119 AN - OPUS4-28070 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rethmeier, Michael A1 - Gook, Sergej A1 - Gumenyuk, Andrey ED - Turichin, G. T1 - Prospects of application of laser-GMA hybrid welding for manufacturing of large diameter longitudinal welded high strength steel pipes T2 - VII. International scientific and technical conference 'Beam technologies & laser application' (Proceedings) T2 - VII. International scientific and technical conference 'Beam technologies & laser application' CY - Saint-Petersburg, Russia DA - 2012-09-18 KW - High strength steel KW - Laser hybrid welding KW - Modified spray arc KW - Longitudinal weld KW - Pipeline PY - 2013 SP - 130 EP - 140 PB - Publishing house SPbSPU AN - OPUS4-28040 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Pentzien, Simone A1 - Rabin, Ira A1 - Hahn, Oliver A1 - Krüger, Jörg A1 - Kleber, F. A1 - Hollaus, F. A1 - Diem, M. A1 - Sablatnig, R. ED - Park, J.-I. ED - Kim, J. T1 - Can Modern Technologies Defeat Nazi Censorship? T2 - ACCV 2012 Workshops, 11th Asian conference on computer vision N2 - Censorship of parts of written text was and is a common practice in totalitarian regimes. It is used to destroy information not approved by the political power. Recovering the censored text is of interest for historical studies of the text. This paper raises the question, whether a censored postcard from 1942 can be made legible by applying multispectral imaging in combination with laser cleaning. In the fields of art conservation (e.g. color measurements), investigation (e.g. Analysis of underdrawings in paintings), and historical document analysis, multispectral imaging techniques have been applied successfully to give visibility to information hidden to the human eye. The basic principle of laser cleaning is to transfer laser pulse energy to a contamination layer by an absorption process that leads to heating and evaporation of the layer. Partial laser cleaning of postcards is possible; dirt on the surface can be removed and the obscured pictures and writings made visible again. We applied both techniques to the postcard. The text could not be restored since the original ink seems to have suffered severe chemical damage. T2 - ACCV 2012 Workshops, 11th Asian conference on computer vision CY - Daejeon, Korea DA - 05.11.2012 KW - Laser cleaning KW - Multispectral imaging KW - Image restoration KW - Image enhancement PY - 2013 SN - 978-3-642-37483-8 SN - 0302-9743 VL - II IS - LNCS 7729 SP - 13 EP - 24 PB - Springer CY - Berlin Heidelberg AN - OPUS4-28160 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Scheid, Marc A1 - Kusche, Christian A1 - Schröder, Volkmar A1 - Barth, Uli ED - Pierucci, S. ED - Klemes, J.J. ED - De Rademaeker, E. ED - Fabiano, B. ED - Buratti, S.S. T1 - Tests on suitability of the ignition source 'exploding wire' for the determination of explosion characteristics of combustible dusts in the 20-L-sphere T2 - Proceedings of the 14th EFCE symposium on loss prevention and safety promotion in the process industries N2 - According to international standards several safety characteristics of dusts are determined in the 20-Lsphere (also known as SIWEK Chamber). Dust cloud ignition is carried out using pyrotechnical igniters. Due to various disadvantages of such igniters the need for alternative ignition sources arises again and again. An alternative ignition source could be the so called 'exploding wire' or 'fuse wire'. The paper presents test results of a comparative study between both ignition sources for the determination of the safety characteristics Maximum Explosion Pressure and Maximum Explosion Pressure Rise of five selected dusts in the 20-L-sphere. In addition to that the ignition mechanisms of both ignition sources were analysed by high speed camera recordings and the ignition energy was determined with electric and calorimetric recordings. T2 - 14th International symposium on loss prevention and safety promotion in the process industries CY - Florence, Italy DA - 12.05.2013 KW - Sicherheitstechnische Kenngrößen Staub KW - Staubexplosionsschutz KW - Explodierender Draht KW - Alternative Zündquelle PY - 2013 SN - 978-88-95608-22-8 DO - https://doi.org/10.3303/CET1331118 SN - 1974-9791 N1 - Serientitel: Chemical engineering transactions – Series title: Chemical engineering transactions IS - 31 SP - 703 EP - 708 PB - AIDIC, Associazione Italiana di Ingegneria Chimica CY - Milano AN - OPUS4-28554 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Krietsch, Arne A1 - Gothe, C. A1 - Scheid, Marc A1 - Krause, U. ED - Makhviladze, G. ED - Molkov, V. ED - Bradley, D. ED - Sunderland, P. ED - Tamanini, F. T1 - Determination of explosion behaviour of nano powders with modified 20-L-sphere test T2 - ISFEH7 - 7th International seminar on fire & explosion hazards (Proceedings) N2 - This paper describes a modified experimental setup for the test apparatus 20-L-Sphere (also known as 20-L Siwek Chamber), that enables the test samples to be kept under inert atmospheric conditions nearly until ignition. This setup was designed to allow the determination of safety characteristics of nano powders under most critical circumstances (e.g. minimisation of the influence of oxidation before the test itself). The aim of this modification was to determine, whether or not the current setup and procedures underestimate the explosion violence and ignitability of nano powders. For this purpose, two different methods, the so called inerting method and the modified method (using a special nozzle called mushroom nozzle) are used. Both methods are described in the paper. The work includes experimental results of micrometer dusts to validate the modified method. Moreover first results of nanometer iron and aluminium dusts are presented, which were kept at inert conditions until shortly before the ignition. The tested nano iron was found to react pyrophoric, as soon as it gets in contact with air, while the tested nano aluminium did not generally show such behaviour. Tests with nano aluminium using the inerting method revealed a higher pressure rise in comparison to the standard test procedure. This could suggest a different extent of passivation. To investigate this effect more closely, further testes with more nano powders are required. T2 - ISFEH7 - 7th International seminar on fire & explosion hazards CY - Providence, RI, USA DA - 05.05.2013 KW - Nano material KW - Dust explosion KW - Safety characteristics KW - Nanopowder PY - 2013 SN - 978-981-07-5936-0 SN - 978-981-07-5940-7 DO - https://doi.org/10.3850/978-981-07-5936-0_13-03 SP - 801 EP - 809 PB - Research publishing AN - OPUS4-28560 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Krietsch, Arne A1 - Romahn, T.-M. A1 - Scheid, Marc A1 - Krause, U. ED - Pierucci, S. ED - Klemes, J.J. ED - De Rademaeker, E. ED - Fabiano, B. ED - Buratti, S.S. T1 - Modified setup of 20-L-sphere for the determination of safety characteristics of nano powders T2 - Proceedings of the 14th EFCE symposium on loss prevention and safety promotion in the process industries N2 - This paper describes a modified experimental setup for the test apparatus 20-L-Sphere (also known as 20-L Siwek Chamber), that enables the test samples to be kept under inert atmospheric conditions nearly until ignition. This setup was designed to allow the determination of safety characteristics of nanopowders under most critical circumstances (e.g. minimisation of the influence of oxidation before the test itself). The aim of this modification was to determine, whether or not the current setup and procedures underestimate the explosion violence and ignitability of nanopowders. The work includes experimental results of micrometer dusts to validate the modified setup. Moreover first results of nanometer iron and Aluminium dusts are presented, which were kept at inert conditions until shortly before the ignition. The tested nano iron was found to react pyrophoric, as soon as it gets in contact with air, while the tested nano Aluminium did not generally show such behaviour. T2 - 14th International symposium on loss prevention and safety promotion in the process industries CY - Florence, Italy DA - 12.05.2013 KW - Dust explosion KW - Nanopowder PY - 2013 SN - 978-88-95608-22-8 DO - https://doi.org/10.3303/CET1331135 SN - 1974-9791 N1 - Serientitel: Chemical engineering transactions – Series title: Chemical engineering transactions IS - 31 SP - 805 EP - 810 PB - AIDIC, Associazione Italiana di Ingegneria Chimica CY - Milano AN - OPUS4-28561 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rohwetter, Philipp A1 - Habel, Wolfgang ED - Jaroszewicz, L.R. T1 - Fibre-optic sensors for partial discharge-generated ultrasound in elastomeric high-voltage insulation materials T2 - EWOFS 2013 - 5th European workshop on optical fibre sensors (Proceedings) N2 - Recent progress in the development of ultrasonic fibre-optic sensors for detecting acoustic emission from partial discharge in elastomeric insulations is presented. These sensors are an important part of a proposed comprehensive scheme for the fibre-optic monitoring of cable accessories. After specifying the underlying design goals the improved fibre-optic sensor design is outlined. It is experimentally shown that it offers about ten-fold improvement over a previously investigated resonant cantilever-type design in terms of detection limit, making it competitive with conventional piezoelectric transducers, however with the added compatibility with strong electrical fields and electromagnetically noisy environments. T2 - EWOFS 2013 - 5th European workshop on optical fibre sensors CY - Kraków, Poland DA - 2013-05-19 KW - Acoustic emission KW - Fiber optics sensors KW - Sensors KW - Transducers KW - Ultrasonics KW - Ultrasonography KW - Fiber-optic condition monitoring KW - Partial discharge KW - Silicone elastomer KW - Stress cone KW - High-voltage cable accessories KW - Sagnac interferometer KW - Acoustic waveguide PY - 2013 SN - 978-0-819-49634-8 DO - https://doi.org/10.1117/12.2025824 SN - 0277-786X N1 - Serientitel: Proceedings of SPIE – Series title: Proceedings of SPIE VL - 8794 IS - 181 SP - 879407-1 EP - 879407-4 AN - OPUS4-28563 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Weltschev, Margit A1 - Schwarzer, Stefanie A1 - Otremba, Frank ED - Pierucci, S. ED - Klemes, J.J. ED - De Rademaeker, E. ED - Fabiano, B. ED - Buratti, S.S. T1 - Comparison of the operating life of tank containers, tank vehicles and rail cars for the carriage of dangerous goods in practice, analysis of causes of damage T2 - Proceedings of the 14th EFCE symposium on loss prevention and safety promotion in the process industries N2 - More than 400 Mt of dangerous materials are transported in Germany every year, of which 150 Mt are by road. Tank containers, tank vehicles and rail tank cars are used for the carriage of dangerous goods in large quantities. Data on the operating life of tanks are only available, in practice, to a minor degree. They are only partly published, mainly after accidents. The BAM-List - Requirements for Tanks for the Carriage of Dangerous Goods, which has compatibility evaluations of metallic and polymeric materials, has been the basis for substance-related prototype approvals for tank containers and portable tanks designed for the carriage of dangerous goods by the BAM since publication of the first edition in 1989. These data are also used for the approval of rail tank cars and road tank cars and are used as a source of knowledge not only in Germany but also worldwide. Tank leakages caused by tanks or rail tank cars being made of tank and sealing materials which are not resistant to the fill goods are avoided by using the material resistance data of the BAM. Corrosion damage is among the main causes of damage. Uniform and non-uniform area corrosion without mechanical stress in aqueous substances is one of the most frequent types of corrosion during the transport of chemicals in tanks. Much damage by pitting corrosion occurs during the transport of substances containing chlorides or substances which separate chloride ions in the presence of moisture. Operational stresses are caused by the effects of both the road and the dangerous goods being transported. Mechanical damage often results from long-term overstressing and occurs after longer operating times. Operational failures cause damage which may appear during the service of tank containers, road tank cars or rail tank cars. The damage results from the inattention of employees when opening and closing the valves. Traffic accidents also cause damage to tanks and frames. Many cases of damage are due to weld area cracks resulting from four basic errors in construction, material, manufacturing and operation. Manufacturing errors can be undetected and the starting point of cracks which only grow under service conditions. Manufacturing errors result from variations in measurement and design, fittings, state of surface (hardness, abrasiveness) and mechanical surface damage (scratches, cracks). Incorrectly welded joints and errors during mechanical deformation are typical mistakes when installing the component parts. Variations in the wall thickness or combinations of different materials lead to manufacturing errors too. A lot of tanks are not used for the transport of dangerous goods before the end of their service life as they do not fulfil the revised technical safety requirements in the Dangerous Goods Regulations. Predictions in the BAM-List based on literature data and corrosion test results are reflected in the service (operating) life. Rail tank cars made of carbon steel, for example, which are mainly used for the transport of petroleum products, can achieve a service life of 40 – 50 y. Rail tank cars produced of austenitic CrNi- or CrNiMo-steel can reach an operating life of at least 30 y, whereby the corrosiveness of the transport substances plays an important role. T2 - 14th International symposium on loss prevention and safety promotion in the process industries CY - Florence, Italy DA - 12.05.2013 KW - Gefahrguttanks KW - Eisenbahnkesselwagen KW - Schadensursachen KW - Lebensdauer PY - 2013 SN - 978-88-95608-22-8 DO - https://doi.org/10.3303/CET1331094 SN - 1974-9791 N1 - Serientitel: Chemical engineering transactions – Series title: Chemical engineering transactions IS - 31 SP - 559 EP - 564 PB - AIDIC, Associazione Italiana di Ingegneria Chimica CY - Milano AN - OPUS4-28568 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Pfennig, A. A1 - Wolf, Marcus A1 - Wiegand, Reiner A1 - Bork, Claus-Peter T1 - New in-situ measurement technique to determine corrosion fatigue in components and pipes under cyclic load T2 - MWWD & IEMES 2012 (Proceedings) N2 - In the field of water pipelines, geothermal energy production as well as carbon capture and storage technology (CCS) materials have to provide a high resistance to corrosion and mechanical stress. The combination of cyclic load and corrosive aqueous environment leads to corrosion fatigue of pipes and components (e.g. pumps) and thus inevitably to the reduction of the lifetime of these components. To estimate the reliability of components from adjusted in-situ-laboratory experiments a corrosion chamber was designed and tested with CO2 saturated corrosive aqueous media flowing at a steady rate. Unique feature of this special chamber is its installation directly onto the sample and thus providing flexible usability in almost every testing machine. This allows simultaneous mechanical loading of the sample, operation at temperatures up to 100 °C and exposure to fluid flow of corrosive liquids and gases. The lifetime reduction of AISI 420C (X46Cr13, 1.4034) is demonstrated at T=60 °C, geothermal brine: Stuttgart Aquifer flow rate: 9 l/h, CO2. S-N plots, micrographic-, phase-, fractographic- and surface analysis were applied to obtain sustainable information on the corrosion fatigue behavior. Maximum number of cycles (here 12.5 x 106 cycles to failure) is reached at σa =173 MPa. No typical fatigue strength exists and passive corrosion fatigue may be identified as failure cause. T2 - MWWD & IEMES 2012 CY - Budva, Montenegro DA - 22.10.2012 KW - Corrosion fatigue KW - Corrosion chamber KW - S-N-plots KW - Steel KW - In-situ experiment PY - 2012 SN - 978-9944-5566-6-8 SP - 1 EP - 8 AN - OPUS4-28569 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kusche, Nadine A1 - Schukar, Vivien A1 - Hofmann, Detlef A1 - Basedau, Frank A1 - Habel, Wolfgang A1 - Woschitz, H. A1 - Lienhart, W. ED - Jaroszewicz, L.R. T1 - Field examples for optical fibre sensor condition diagnostics based on distributed fibre-optic strain sensing T2 - EWOFS 2013 - 5th European workshop on optical fibre sensors (Proceedings) N2 - Fibre optic sensors for monitoring in safety-relevant structures have to be validated in order to proof their reliability under typical structural load conditions. The reliable use of optical fibre sensors depends strongly on an appropriate and qualitative application. Diagnostics of the physical condition of embedded and surface-applied fibre optic strain sensors are demonstrated on field examples. Distributed strain measurement based on Rayleigh backscattering is used to determine breakage of the fibre, interface adhesion problems and to identify application related strain transfer mechanisms. T2 - EWOFS 2013 - 5th European workshop on optical fibre sensors CY - Kraków, Poland DA - 19.05.2013 KW - Fibre Bragg grating KW - Rayleigh backscattering KW - Condition diagnostics KW - Strain KW - Strain transfer PY - 2013 SN - 978-0-81949-634-8 DO - https://doi.org/10.1117/12.2025567 SN - 0277-786X N1 - Serientitel: Proceedings of SPIE – Series title: Proceedings of SPIE VL - 8794 IS - Paper 8794 - 181 SP - 879433-1 EP - 879433-4 AN - OPUS4-28570 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Komann, Steffen A1 - Gröke, Carsten A1 - Droste, Bernhard T1 - Assessment of quality assurance measures for radioactive material transport packages not requiring competent authority design approval T2 - WM2013 Conference (Proceedings) N2 - The majority of transports of radioactive materials are carried out in packages which don’t need a package design approval by a competent authority. Low-active radioactive materials are transported in such packages e.g. in the medical and pharmaceutical industry and in the nuclear industry as well. Decommissioning of NPP’s leads to a strong demand for packages to transport low and middle active radioactive waste. According to IAEA regulations the “non-competent authority approved package types” are the Excepted Packages and the Industrial Packages of Type IP-1, IP-2 and IP-3 and packages of Type A. For these types of packages an assessment by the competent authority is required for the quality assurance measures for the design, manufacture, testing, documentation, use, maintenance and inspection (IAEA SSR 6, § 306). In general a compliance audit of the manufacturer of the packaging is required during this assessment procedure. Their regulatory level in the IAEA regulations is not comparable with the “regulatory density” for packages requiring competent authority package design approval. Practices in different countries lead to different approaches within the assessment of the quality assurance measures in the management system as well as in the quality assurance program of a special package design. To use the package or packaging in a safe manner and in compliance with the regulations a management system for each phase of the life of the package or packaging is necessary. The relevant IAEA-SSR6 § 801 requires documentary verification by the consignor concerning package compliance with the requirements. T2 - WM2013 Conference CY - Phoenix, Arizona, USA DA - 24.02.2013 PY - 2013 SN - 978-0-9836186-2-1 SP - 1 EP - 8 CY - Phoenix, Arizona, USA AN - OPUS4-28504 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schälike, Stefan A1 - Mishra, Kirti Bhushan A1 - Malow, Marcus A1 - Berger, Anka A1 - Wehrstedt, Klaus-Dieter A1 - Schönbucher, A. ED - Pierucci, S. ED - Klemes, J.J. ED - De Rademaeker, E. ED - Fabiano, B. ED - Buratti, S.S. T1 - Mass burning rate of a large TBPB pool fire - experimental study and modeling T2 - Proceedings of the 14th EFCE symposium on loss prevention and safety promotion in the process industries N2 - Data and prediction for the mass burning rate of a tert-butyl-peroxy-benzoat (TBPB) pool fire (pool diameter = 3 m) is presented. The mass burning rates of TBPB fires are up to six times higher and less dependent on pool diameter compared to hydrocarbon pool fires caused by an additional heat release rate due to exothermic decomposition reaction in the liquid phase. This heat release rate is calculated using a 1st order reaction kinetic obtained from micro calorimetric measurements. A new model is derived considering the heat release rate due to the decomposition reaction which is shown to be 100 % of the heat release rate radiated to the pool surface. With the presented model, including also physical quantities, especially the limiting fuel concentration for upward flame propagation, it is possible to predict the mass burning rates of large TBPB pool fires. The predicted values are in very good agreement with the experiments. T2 - 14th International symposium on loss prevention and safety promotion in the process industries CY - Florence, Italy DA - 12.05.2013 KW - Mass burning rate KW - TBPB (tert-butyl-peroxy benzoat) KW - Pool fire KW - Experimental study KW - Modeling PY - 2013 SN - 978-88-95608-22-8 DO - https://doi.org/10.3303/CET1331143 SN - 1974-9791 N1 - Serientitel: Chemical engineering transactions – Series title: Chemical engineering transactions IS - 31 SP - 853 EP - 858 PB - AIDIC, Associazione Italiana di Ingegneria Chimica CY - Milano AN - OPUS4-28501 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Klippel, Alexander A1 - Scheid, Marc A1 - Krause, U. ED - Makhviladze, G. ED - Molkov, V. ED - Bradley, D. ED - Sunderland, P. ED - Tamanini, F. T1 - Progress on the research into the influence of dustiness on dust explosions T2 - ISFEH7 - 7th International seminar on fire & explosion hazards (Proceedings) N2 - In practice, occurring explosive dust/air mixtures are usually not homogeneous and in many cases do not spread over the whole enclosure. For the safety measure explosion venting, a smaller venting area might be sufficient as calculated according to venting standards (EN 14491 'Dust Explosion Venting Protective Systems'). The tendency of bulk materials to form dust clouds is not taken into account so far. To optimize the design of explosion protection measures, a new safety characteristic the so-called 'dustiness' (see VDI 2263 part 9 'Determination of Dustiness of Bulk Materials'.) could be useful. Dustiness means the tendency of dust to form dust clouds. There are six dustiness groups (DG) from one to six (one means little tendency to stay airborne, six the opposite). The paper describes first results on the reasons for different dustiness and on dust explosion venting for several dusts of different dustiness. A 75 L vertical tube apparatus for vented dust explosion experiments was created. Pressure, pressure rises and flame speeds were measured to evaluate the course of the dust explosions. In addition the paper includes CFD simulations (ANSYS CFX) about the possibilities to model the dust/air mixtures with the Euler/Lagrange approach. In order to simulate the settling of dust clouds more realistic the particle surface area was adjusted and the particle size distribution was taken into account. Results were compared to experimentally determined terminal velocities. T2 - ISFEH7 - 7th International seminar on fire & explosion hazards CY - Providence, RI, USA DA - 05.05.2013 KW - CFD KW - Dust explosions KW - Dustiness KW - Venting PY - 2013 SN - 978-981-07-5936-0 SN - 978-981-07-5940-7 DO - https://doi.org/10.3850/978-981-07-5936-0_13-01 SP - 781 EP - 790 PB - Research Publishing AN - OPUS4-28502 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zencker, Uwe A1 - Qiao, Linan A1 - Kasparek, Eva Maria A1 - Völzke, Holger T1 - Modeling of cylindrical casks under horizontal drop test conditions T2 - IHLRWM 2013 - 14th International high-level radioactive waste management conference (Proceedings) N2 - Cylindrical casks made of ductile cast iron are used for transport, interim storage and final disposal of radioactive waste in Germany. A basic design criterion is the ability to withstand a horizontal drop without impact Binders onto a foundation representative for the real ground of a storage facility. The increasing use of more cost-effective material compositions requires optimized cask geometries to reduce stresses and strains in the cask structure. For example, a non-uniform wall thickness was introduced to reduce maximum wall bending stresses. As a result, the load characteristics changed from line load to point load at bottom and lid side under horizontal drop fest conditions. Hereby, the position of highest stress inside the structure has shifted significantly. This was the reason for a systematic investigation of effects caused by small design changes or small variations of fest conditions. It led to a better understanding of the positions of high local stresses, their time history and maximum value for cylindrical casks under horizontal drop test conditions. Hence, the paper presents the lessons learnt from modeling and simulating such scenarios considering an impact without limiters onto a realistic target. T2 - 14th International high-level radioactive waste management conference CY - Albuquerque, New Mexico, USA DA - 28.04.2013 KW - Cylindrical cask KW - Ductile cast iron KW - Numerical simulation KW - Horizontal drop test KW - Storage facility KW - Concrete foundation PY - 2013 SN - 978-1-62748-644-6 SP - 1114 EP - 1119 (Paper # 6862) PB - Omnipress AN - OPUS4-28529 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wolff, Dietmar A1 - Jaunich, Matthias A1 - Stark, Wolfgang T1 - Investigating the performance of rubber seals at low temperatures T2 - IHLRWM 2013 - 14th International high-level radioactive waste management conference (Proceedings) N2 - Rubbers are widely used as main sealing materials for Containers for low and intermediate level radioactive waste and as additional component to metal seals in spent fuel and high active waste containers. The save enclosure of the radioactive container inventory has to be guaranteed according to legislation and appropriate guidelines for long term storage periods as well as down to temperatures of -40 °C for transportation. Therefore the understanding of failure mechanisms that lead to leakage at low temperatures is necessary to ensure a proper material choice which is certainly also influenced by additional factors as e.g. the aging behavior. T2 - 14th International high-level radioactive waste management conference CY - Albuquerque, New Mexico, USA DA - 28.04.2013 KW - Rubber seals KW - Elastomers KW - Compression set KW - Low temperature KW - Leakage rate PY - 2013 SN - 978-1-62748-644-6 SP - 1 EP - 7(Paper # 6888) PB - Omnipress AN - OPUS4-28530 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Pfeil, Norbert A1 - Jochum, C. A1 - Mitropetros, K. A1 - Schmelzer, P.G. ED - Pierucci, S. ED - Klemes, J.J. ED - De Rademaeker, E. ED - Fabiano, B. ED - Buratti, S.S. T1 - Keeping and improving process and plant safety competence - what is needed, what should be done? T2 - Proceedings of the 14th EFCE symposium on loss prevention and safety promotion in the process industries N2 - In March 2004 with the position paper “Maintaining and improving competence in safety engineering” of the DECHEMA/GVC Research Committee "Safety Engineering in Chemical Plants", an initiative came up against the tendency that more and more process and plant safety (PPS) orientated professorships turn to other more fashionable research topics. The Research Committee was concerned that PPS in both academic teaching and research could suffer a negative development - despite of its importance. In 2009 a corresponding Dutch initiative followed. To bring these both and other similar initiatives together, within the 8th European Congress of Chemical Engineering held in Berlin in September 2011 a two days Special session on PPS competence was jointly organized by EFCE, ProcessNet and EPSC. All presentations and conclusions drawn by the organizers (the authors of this paper) are electronically available. The paper addresses the before mentioned initiatives, highlights views and results from the ECCE 8’s special session on PPS competence, and indicates steps necessary to be taken and recent developments. T2 - 14th International symposium on loss prevention and safety promotion in the process industries CY - Florence, Italy DA - 12.05.2013 KW - Anlagensicherheit KW - Prozessindustrie KW - Lehre KW - Forschung PY - 2013 SN - 978-88-95608-22-8 DO - https://doi.org/10.3303/CET1331063 SN - 1974-9791 N1 - Serientitel: Chemical engineering transactions – Series title: Chemical engineering transactions IS - 31 SP - 373 EP - 378 PB - AIDIC, Associazione Italiana di Ingegneria Chimica CY - Milano AN - OPUS4-28540 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Liehr, Sascha A1 - Burgmeier, J. ED - Jaroszewicz, L.R. T1 - Quasi-distributed measurement on femtosecond laser-induced scattering voids using incoherent OFDR and OTDR T2 - EWOFS 2013 - 5th European workshop on optical fibre sensors (Proceedings) N2 - We propose to use focused femtosecond laser pulses to create scattering damage in standard singlemode optical fibres as reference points for quasi-distributed sensing applications. Such sensor fibres are interrogated with incoherent optical frequency domain reflectometry (I-OFDR) technique and optical time domain reflectometry (OTDR). A performance comparison of both techniques with the clear advantage of the I-OFDR is presented as well as a quasi-distributed length change measurement application. Also dynamic measurement based on the I-OFDR technique is demonstrated on a femtosecond laser-induced sensor chain. T2 - EWOFS 2013 - 5th European workshop on optical fibre sensors CY - Kraków, Poland DA - 19.05.2013 KW - Optical fiber sensors KW - Femtosecond laser KW - Strain sensor KW - OFDR KW - OTDR PY - 2013 SN - 978-0-81949-634-8 DO - https://doi.org/10.1117/12.2026780 SN - 0277-786X N1 - Serientitel: Proceedings of SPIE – Series title: Proceedings of SPIE VL - 8794 IS - Paper 8794 - 181 SP - 87943N-1 EP - 87943N-4 AN - OPUS4-28734 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tiebe, Carlo A1 - Hübert, Thomas A1 - Lorek, A. A1 - Wernecke, R. T1 - HUMItrace-Sensorsystem mit neuartigen planaren Spurenfeuchtesensoren T2 - Temperatur 2013 - Verfahren und Geräte in der Temperatur- und Feuchtemesstechnik N2 - Es wird ein Sensorsystem (HUMItrace III) zur Spurenfeuchtebestimmung in der Prozessmesstechnik vorgestellt. Die Bestimmung der Spurenfeuchte erfolgt mit neuentwickelten planaren Sensoren (HUMItrace-Sensoren) nach dem coulometrischen Messprinzip im Frostpunkttemperaturbereich von -80 °C bis -30 °C mit der Kalibriereinrichtung THG11 durch Mischen von trockenen und befeuchteten Teilgasströmen kalibriert. Die Gasfeuchte von Luft kann in diesem Bereich mit den HUMItrace-Sensoren mit einer erweiterten Unsicherheit von 2 K bestimmt werden. Die Sensoren können aber auch zur Gasfeuchtemessung in Wasserstoff, Stickstoff und Distickstoffmonoxid eingesetzt werden. Eine weitere Kalibriereinrichtung, THG-P12, generiert Prüfgase nach der Permeationsmethode; sie kann in das HUMItrace III Sensorsystem implementiert und zur vor-Ort-Kalibrierung der HUMItrace-Sensoren nach dem Standardadditionsverfahren genutzt werden. T2 - Temperatur 2013 - Verfahren und Geräte in der Temperatur- und Feuchtemesstechnik CY - Berlin, Germany DA - 05.06.2013 PY - 2013 SN - 3-9810021-8-0 SP - 257 EP - 262 AN - OPUS4-28732 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Prager, Jens A1 - Köppe, Enrico A1 - Bartholmai, Matthias T1 - Früherkennung von Strukturschäden mittels geführter Lamb-Wellen T2 - 16. ITG/GMA-Fachtagung - Sensoren und Messsysteme 2012 N2 - Eine Reihe von Prüfproblemen in der chemischen Industrie, in Kraftwerksanlagen und in Transportsystemen ist aufgrund schwieriger Zugangsmöglichkeiten nur begrenzt technisch bzw. wirtschaftlich effizient durchführbar. Das hier vorgestellte Projekt beinhaltet die Entwicklung eines Verfahrens der zerstörungsfreien Prüfung über weite Entfernungen (bis zu 100 m), das zum Einsatz in automatisierten Messsystemen bzw. zur Integration in Langzeitüberwachungssysteme geeignet ist. Grundlage des Verfahrens ist die gezielte Anregung und Auswertung von Lamb-Wellenmoden, wodurch eine effektive Unterscheidung von Fehler- und Formanzeigen sowie eine Klassifizierung unterschiedlicher Fehlertypen möglich werden. Der Vorteil der Nutzung geführter Wellen für die zerstörungsfreie Prüfung liegt in ihrer vergleichsweise guten Ausbreitungsfähigkeit über weite Entfernungen. Die sich daraus ergebenden Möglichkeiten der Untersuchung großer bzw. schwer zugänglicher Bereiche einer Struktur bieten innovative Ansätze für die Entwicklung robuster Structural-Health-Monitoring-Systeme (SHM). Erst durch die Verfügbarkeit leistungsfähiger Rechentechnik wird ein breiter Einsatz derartiger Verfahren möglich. Die Technik kann zur Materialcharakterisierung an ebenen bzw. zylindrischen, dünnwandigen Flächen aus Metall oder auch CFK genutzt werden. Adressierte Anwendungsfelder sind z.B. die Untersuchung von Flugzeugtragflächen oder Pipelines. Des Weiteren wird der Einsatz solcher Verfahren zur Überwachung sicherheitsrelevanter Bauteile z.B. aus Laminaten angestrebt, wie sie verstärkt in der Luft- und Raumfahrt Anwendung finden. Im Rahmen des Projekts wurde auf Grundlage vorhandener Technik (Wellenanregung mittels Ultraschall-Gruppenstrahlprüfköpfen) ein umfassendes Verständnis für die Technologie und anwendungsrelevante Parameter (Probenmaterial und -dimensionen, Welleneigenschaften, Anregungs-, Transmissions-, Reflektionscharakteristika) gewonnen und Algorithmen zur Erkennung von Schädigungsbildern (z.B. Riss, Loch, Verdünnung) entwickelt. Neben der Algorithmusentwicklung zur Detektion und Analyse von Schadstellen, lag ein Projektschwerpunkt in der Entwicklung einer geeigneten Gerätetechnik. Als sensorisches Elemente wurde Ultraschall-Gruppenstrahlertechnik eingesetzt. Besondere Anforderungen werden an die Technik zur Anregung der Wellenmoden unter Verwendung geeigneter Piezoaktoren gestellt. In diesem Bereich existiert bislang keine kommerziell erhältliche Gerätelösung, weshalb eine Neuentwicklug der Anregetechnik realisiert wurde. Speziell für die hohe Anzahl an Aktorkanälen, die benötigt wird, um unterschiedliche Moden und Wellenformen anzuregen, wurde eine äußerst leistungsfähige Anregeeinheit entwickelt. T2 - 16. GMA/ITG-Fachtagung 'Sensoren und Messsysteme' CY - Nürnberg, Germany DA - 22.05.2012 KW - Lamb-waves KW - Ultrasound KW - Non-destructive evaluation KW - Early-damage-detection KW - Structural health monitoring PY - 2012 SN - 978-3-9813484-0-8 DO - https://doi.org/10.5162/sensoren2012/5.2.1 SP - 531 EP - 540 CY - Wunstorf AN - OPUS4-26008 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Neuschaefer-Rube, U. A1 - Bartscher, M. A1 - Neugebauer, M. A1 - Härtig, F. A1 - Goebbels, Jürgen A1 - Ehrig, Karsten A1 - Staude, Andreas T1 - Measurement of micro gears - comparison of optical, tactile-optical and CT-measurements T2 - Proceedings of SPIE 7864 N2 - Micro gears are applied in an increasing quantity in many applications. Therefore, precise measurements are of growing importance to ensure their quality. This contribution describes the measurement of gears of a micro planetary gear set with a tactile probe, a tactile-optical probe, an optical sensor, and computed tomography (CT). For the tactile measurements, a high precision piezoresistive microprobe was used. A so-called fiber probe was applied for tactile-optical measurements. This probe applies image processing to determine the position of the tactile probing element. For all tactile and tactile-optical measurements, single point probing was used. The optical measurements were carried out with an imaging sensor based on focus variation. Due to limited accessibility, on some gears not all regions could be measured by the optical sensor and the tactile-optical probe. In contrast to this, with CT the whole part could be measured with high point density. We used a micro-CT system and carried out measurements with Synchrotron-CT. All the sensors used deliver measurement data in Cartesian coordinates. It is a challenge to transfer these data into coordinates in which gear parameters are defined. For this, special attention must be paid to the determination of the gear axis and to the orientation of the teeth. The applied procedures are detailed for different micro gears. The comparison between data of different measurements was carried out successfully. The deviations between the CT data and the tactile or tactile-optical data lie in the range of only a few micrometers. KW - Micro gears KW - Coordinate metrology KW - Computed tomography KW - Optical sensors KW - Tactile probes PY - 2011 DO - https://doi.org/10.1117/12.872413 SN - 0277-786X SN - 0038-7355 SN - 0361-0748 N1 - Serientitel: Proceedings series – Series title: Proceedings series IS - 7864 SP - 78640H-1 EP - 78640H-9 PB - VDE-Verl. CY - Berlin ; Offenbach AN - OPUS4-25998 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bäßler, Ralph A1 - Weltschev, Margit T1 - UNS S44400 - A low cost and corrosion-resistant alternative to the austenite containing nickel for tank applications T2 - NACE International corrosion conference 2012 (Proceedings) N2 - In Germany the “BAM-List - Requirements for Tanks for the Transport of Dangerous Goods” is the basis for substance-related prototype approvals for tank Containers undertaken by the BAM1 - Federal Institute for Materials Research and Testing. Compatibility evaluations of selected metallic materials as well as of polymeric gasket and lining materials under the influence of approximately 7200 dangerous goods have been published in the BAM-List since 1989. The ferritic Steel UNS S44400 (X2CrMoTil8-10, 1.4521) was originally developed as alternative for the austenitic grade AISI316L (X2CrNiMo 17-12-2, 1.4404). Due to its characteristic profile this Steel was qualified for applications requiring high strength values at concomitant adequate corrosion resistance. Because of the lack of Nickel this Steel is a cost-efficient alternative to the Ni-containing austenites. No corrosion test results of UNS S44400 under the influence of dangerous goods were published in the BAM-List so far. Only data on the behavior of AISI 316L are listed. Therefore test specimens of this Steel were exposed to selected corrosive substances in order to compare both steels. Due to the reduced alloy content a reduced corrosion resistance of the Steel UNS S44400 in acidic substances, such as formic acid, acetic acid and sulfuric acid, in comparison to the austenitic CrNiMosteels was expected but not observed. Tests in an alkaline medium showed sufficient resistance. T2 - NACE International Corrosion Conference 2012 CY - Salt Lake City, USA DA - 01.03.2012 KW - Steel KW - Dangerous goods KW - Transport tanks KW - Duplex steel KW - Corrosion KW - 1.4362 KW - X2CrNiN23-4 PY - 2012 SP - 1-7 (C2012-0001290) AN - OPUS4-25979 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Böllinghaus, Thomas A1 - Mente, Tobias T1 - Schadensfälle geschweißter Rohrleitungen und Maßnahmen zur Vermeidung T2 - 14. Sommerkurs Werkstoffe und Fügen N2 - Aus wirtschaftlich-technischer Perspektive ergeben sich in den letzten zehn Jahren hinsichtlich der Werkstoffinnovation und -auswahl für geschweißte Rohrleitungen im Wesentlichen zwei Entwicklungsrichtungen: Im Bereich der niedriglegierten Stähle werden immer höher festere Feinkombaustähle mit Streckgrenzen von inzwischen über 900 MPa verwendet. Wirtschaftliches Ziel ist hierbei eine möglichst hohe Kosteneinsparung durch Reduktion der Wanddicke. Für korrosionsbeanspruchte Komponenten, unter anderem im Petrochemie- und Energieanlagenbau besteht das wirtschaftliche Ziel primär darin, eine höhere Kosteneinsparung durch neue Legierungskonzepte zu erzielen und zwar möglichst so, dass bei mindestens gleicher Festigkeit auf die Verwendung von teuren Elementen, wie beispielsweise Nickel, verzichtet werden kann. Beispiele hierfür sind insbesondere hochlegierte martensitische Cr-V-Stähle, supermartensitische Stähle, Lean-Duplexstähle, superaustenitische Stähle und austenitische Cr-Mn-Stähle. Für einige der neu eingeführten Grundwerkstoffe sind die Zusatzwerkstoffe noch in der Entwicklung. In jedem Fall stellen diese Werkstoffinnovationen besondere Ansprüche hinsichtlich einer Rissvermeidung während der schweißtechnischen Verarbeitung, um von vornherein riss- bzw. fehlerfreie Rohrleitungen herzustellen, die eine hohe Sicherheit gegen ein Versagen während der Inbetriebnahme und im Verlauf der vorgesehenen Lebensdauer aufweisen. Fast alle dieser neu eingeführten Rohrleitungswerkstoffe weisen eine reduzierte Heiß- oder Kaltrissresistenz vor allem während des Schweißens mit modernen Hochleistungsprozessen, bspw. Laserhybridschweißen, auf. Dabei besteht nach wie vor Forschungsbedarf hinsichtlich der jeweiligen Entstehungsmechanismen. Da es in den letzten zehn Jahren immer häufiger zu Produktionsausfällen und Schadensfällen mit teilweise katastrophalen Konsequenzen gekommen ist, werden die Ursachen und die Vermeidung fertigungsbedingter Heiß- und Kaltrisse im Folgenden zusammengefasst. T2 - 14. Sommerkurs Werkstoffe und Fügen CY - Magdeburg, Germany DA - 23.09.2011 PY - 2011 SN - 978-3-940961-56-3 SP - 45 EP - 54 CY - Magdeburg AN - OPUS4-26196 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Gerlitzke, A.-K. A1 - Nörthemann, K. A1 - Lang, M. A1 - Milstrey, M. A1 - Kaufer, R. A1 - Woratz, M. A1 - Banach, Ulrich A1 - Hübert, Thomas A1 - Moritz, W. T1 - Long-term stability of the low energy hydrogen sensor T2 - IMCS 2012 - 14th International meeting on chemical sensors N2 - A silicon MIS-structure prepared with thin layers of the super-ionic conductor LaF3 and Pd is used to detect hydrogen. The sensor is able to detect hydrogen in a concentration range from below one ppm to the lower flammable limit in air which is 4 vol.-%. The chip operates at room temperature which results in an extremely low energy consumption compared to other hydrogen sensors. Only once per day a short heating pulse is necessary to reactivate the sensor chip. In cooperation with the BAM, a long-term experiment was carried out. The duration of the measurement was about three months, with a hydrogen exposure every two weeks. The sensor signal remained stable over the measured period. T2 - IMCS 2012 - 14th International meeting on chemical sensors CY - Nuremberg, Germany DA - 20.05.2012 KW - Hydrogen detection KW - Long-term measurement KW - MIS-structure KW - Low energy sensor PY - 2012 SN - 978-3-9813484-2-2 DO - https://doi.org/10.5162/IMCS2012/P2.5.1 SP - 1571 EP - 1574 PB - AMA Service GmbH CY - Wunstorf AN - OPUS4-26177 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Gravenkamp, Hauke A1 - Saputra, A. A. A1 - Song, C. A1 - Prager, Jens ED - Linde, B. B. J. ED - Paczkowski, J. ED - Ponikwicki, N. T1 - Detection of defects in thin-walled structures by means of lamb waves T2 - International congress on ultrasonics N2 - In this paper the Scaled Boundary Finite Element Method (SBFEM) is applied for the simulation of Lamb waves in cracked plates. This method is highly advantageous to study the interaction of different Lamb wave modes with cracks as the crack is not discretized and no refinement is required around the crack tip. Numerical examples are presented for the reflection of the fundamental symmetric and antisymmetric modes from cracks of different depth. The spatial Fourier transformation is employed to calculate the amplitudes of reflected Lamb wave modes. The results reveal possibilities to obtain details of the crack geometry in non-destructive testing and structural health monitoring applications. T2 - International congress on ultrasonics CY - Gdansk, Poland DA - 05.09.2011 KW - Lamb waves KW - Scaled boundary finite element method KW - Simulation KW - Crack detection PY - 2012 SN - 978-0-7354-1019-0 DO - https://doi.org/10.1063/1.3703223 SN - 0094-243X N1 - Serientitel: AIP conference proceedings – Series title: AIP conference proceedings IS - 1433 SP - 443 EP - 446 PB - American Institute of Physics CY - Melville, NY AN - OPUS4-26203 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Grehn, M. A1 - Tsai, W.J. A1 - Höfner, M. A1 - Seuthe, T. A1 - Bonse, Jörn A1 - Mermillod-Blondin, A. A1 - Rosenfeld, A. A1 - Hennig, J. A1 - Achtstein, A. W. A1 - Theiss, C. A1 - Woggon, U. A1 - Eberstein, M. A1 - Eichler, H.J. T1 - Nonlinear optical properties of binary and ternary silicate glasses upon near-infrared femtosecond pulse laser irradiation T2 - International symposium on high power laser ablation 2012 N2 - Some nonlinear optical properties such as the nonlinear refractive index and the nonlinear effective absorption, as well as the laser-induced single-pulse ablation threshold are characterized for a series of binary and ternary silicate glasses upon irradiation with near-infrared femtosecond laser pulses (800 nm, 130 fs). The laser-induced ablation threshold varies from 2.3 J/cm² in case of potassium silicate glass up to 4.3 J/cm² in case of Fused Silica. Nonlinear refractive indices are qualitatively similar within the range 1.7-2.7×10-16 cm²/W. Complementary optical and physico-chemical properties like band gap energy and the glass transformation temperature have been measured for all the glasses. T2 - International symposium on high power laser ablation 2012 CY - Santa Fe, NM, USA DA - 30.04.2012 KW - Laser-induced damage threshold KW - Laser ablation KW - Nonlinear refractive index KW - Silicate glass systems KW - Glass transformation temperature KW - Coefficient of thermal expansion PY - 2012 SN - 978-0-7354-1068-8 DO - https://doi.org/10.1063/1.4739918 N1 - Serientitel: AIP conference proceedings – Series title: AIP conference proceedings VL - 1464 SP - 660 EP - 670 AN - OPUS4-26318 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ballheimer, Viktor A1 - Wille, Frank A1 - Rolle, Annette A1 - Droste, Bernhard T1 - Mechanical behaviour of high burn-up SNF under normal and accident transport conditions - present approaches and perspectives T2 - PVP2012 - Proceedings of the ASME 2012 Pressure vessels & piping division conference N2 - Transport packages for spent fuel have to meet the International Atomic Energy Agency requirements for different transport conditions. Physical state of spent fuel and fuel rod cladding as well as geometric configuration of fuel assemblies are important inputs for the evaluation of package capabilities under these conditions. In this paper, the mechanical behaviour of high burn-up spent fuel assemblies under transport conditions is analysed with regard to assumptions to be used in the activity release and criticality safety analysis. In particular the different failure modes of the fuel rods (fine cracks or complete breakage), which can cause release of gas, volatiles, fuel particles or fragments have to be properly considered in these assumptions. In view of the complexity of interactions between the fuel rods as well as between fuel assemblies, basket, and cask containment, the exact mechanical analysis of such phenomena is nearly impossible. The gaps in information concerning the material properties of cladding and pellets, especially for the high burn-up fuel, make the analysis more complicated additionally. In this context some practical approaches based on experiences of BAM Federal Institute for Material Research and Testing within safety assessment of packages for transport of spent fuel are discussed. T2 - ASME 2012 Pressure vessels & piping division conference CY - Toronto, Ontario, Canada DA - 15.07.2012 KW - Fuel rods KW - High burn-up KW - Mechanical behaviour KW - Transport conditions PY - 2012 SP - PVP2012-78302, 1-7 PB - American Society of Mechanical Engineers CY - New York AN - OPUS4-26320 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schempp, Philipp A1 - Pittner, Andreas A1 - Rethmeier, Michael A1 - Tang, Z. A1 - Seefeld, T. A1 - Cross, C.E. ED - Babu, S. S. ED - Bhadeshia, H.K. ED - Cross, C.E. ED - David, S.A. ED - DebRoy, T. ED - DuPont, J.N. ED - Koseki, T. ED - Liu, S. T1 - Influence of alloy and solidification parameters on grain refinement in aluminium weld metal due to inoculation T2 - Trends in welding research - Proceedings of the 9th international conference N2 - Refinement of the weld metal grain structure can improve the mechanical properties of the weld and decrease the susceptibility to solidification cracking of the weld metal. In this study, commercial Al Ti5B1 grain refiner was used to refine the microstructure of LB (laser beam) and GTA (gas tungsten arc) aluminum welds by inoculation. The grain refiner additions led to a significant decrease in the weld metal mean grain size whereby a transition from columnar to equiaxed grain structure (Columnar to Equiaxed Transition, CET) was observed. The development of both grain size and shape depended upon the base metal (Al alloys 1050A, 5083 and 6082) and upon the welding process. The GTA welding process allowed a more pronounced and a more efficient refinement than in LB welds. Furthermore, the influence of the solidification conditions on the CET was investigated through temperature measurements in the weld metal. The temperature profiles revealed a faster solidification of LB welds than in GTA welds. The results from the temperature measurements were also used to estimate (according to an existing model) the critical thermal gradient at which the CET occurs. T2 - 9th International conference on trends in welding research CY - Chicago, Illinois, USA DA - 04.06.2012 KW - Aluminium KW - LBW KW - GTAW KW - Grain refinement KW - Alloy 1050A KW - Alloy 5083 KW - Alloy 6082 KW - Al Ti5B1 PY - 2013 SN - 978-1-62708-998-2 SP - 98 EP - 107 PB - ASM international AN - OPUS4-27907 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wöhlecke, Andreas A1 - Müller, Werner ED - Kilchert, M. T1 - Aktueller Stand der Zulassung für Geokunststoffe durch die BAM und derzeitige Arbeitsthemen des Fachbeirats und seiner Arbeitsgruppen T2 - 9. Leipziger Deponiefachtagung - Planung, Bau, Betrieb, Stilllegung, Nachsorge, und Nachnutzung von Deponien N2 - Bereits vor der vergangenen Leipziger Deponiefachtagung waren eine Reihe von Zulassungsrichtlinien für Geokunststoffprodukte verabschiedet worden. Dokumente wurden nun überarbeitet und weitere sind hinzugekommen. Die Zulassungsscheine für bereits bestehende und auch neue Zulassungen werden auf dieser Basis für die Produkte erneuert oder erstellt. T2 - 9. Leipziger Deponiefachtagung CY - Leipzig, Germany DA - 26.02.2013 PY - 2013 SP - 29 EP - 43 AN - OPUS4-27901 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Teichmann, Bernd A1 - Krüger, Simone T1 - Systematische Untersuchung des Brandverhaltens und des Feuerwiderstands von Photovoltaik-Modulen einschließlich der Emissionen im Brandfall und Entwicklung eines Prüfverfahrens zum Einfluss von PV-Modulen auf die harte Bedachung T2 - Brand- und Explosionsschutztag 2013 N2 - In Deutschland sind z.Zt. über 1 Million PV-Anlagen am Netz [1], Immer häufiger kommen dabei Dünnschichtmodule mit toxikologisch bedenklichen Inhaltsstoffen zum Einsatz wie z.B. Cadmium, Indium oder Selen. Aber selbst die klassischen Silizium Dickschichtmodule enthalten als Kontaktmaterial signifikante Mengen an Blei. Besonders aus Sicht des Brandschutzes werfen sich vor diesem Hintergrund mehrere Fragen auf: Wie groß ist die toxikologische Gefährdung durch PV-Module im Brandfall und wie verhalten sich die Module bei einem Brand? Um hier Transparenz zu schaffen, wurden in diesem Forschungsvorhaben systematische Branduntersuchungen an verschiedenartigen Photovoltaik-Modulen durchgeführt. Als Ergebnis können Aussagen getroffen werden zu: - Brandverhalten, - Feuerwiderstand der Module einschließlich der tragenden Konstruktion, - mechanische Integrität, - Einflüsse auf die harte Bedachung sowie - Emissionen im Brandfall. T2 - Brand- und Explosionsschutztag 2013 CY - Magdeburg, Germany DA - 21.03.2013 PY - 2013 AN - OPUS4-27918 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael A1 - Kromm, Arne A1 - Kannengießer, Thomas ED - Babu, S. S. ED - Bhadeshia, H.K. ED - Cross, C.E. ED - David, S.A. ED - DebRoy, T. ED - DuPont, J.N. ED - Koseki, T. ED - Liu, S. T1 - Residual stresses in multi-layer component welds T2 - Trends in welding research - Proceedings of the 9th international conference T2 - 9th International conference on trends in welding research CY - Chicago, Illinois, USA DA - 2012-06-04 KW - Shrinkage restraint KW - Component welding KW - Submerged arc welding KW - Multi-run weld KW - Residual stresses KW - Reaction force KW - XRD KW - Large scale test PY - 2013 SN - 978-1-62708-998-2 SP - 48 EP - 54 PB - ASM international AN - OPUS4-27954 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kotsifaki, D.G. A1 - Zekou, L. A1 - Pentzien, Simone A1 - Krüger, Jörg A1 - Serafetinides, A.A. ED - Saunders, D. ED - Strlic, M. ED - Korenberg, C. ED - Luxford, N. ED - Birkhölzer, K. T1 - Cleaning of artificially soiled papers by infrared and mid-infrared lasers T2 - LACONA IX - Lasers in the conservation of artworks (Proceedings) N2 - One of the most important materials presenting and witnessing human culture is paper. The cleaning of paper is often necessary because contamination must be removed so that the fragile organic substrate can be preserved. The conventional cleaning methods are mechanical or involve the application of chemicals. These methods can damage drawings or print layers to some extent or make the original paper substrate brittle. More specifically, the use of a scalpel blade can cause damage to fibers. Chemical cleaning is difficult to perform locally, can dissolve foreign matter that then migrates into the paper substrate, or involves volatile organic compounds that can be harmful to the conservator. There is, therefore, a need for new conservation technologies aimed at the safe cleaning of paper. Lasers have proved to be an appropriate tool for cleaning as the energy dose and penetration depth at the specific point of contamination can be controlled. Additionally, if used properly, laser cleaning is not destructive to the paper. T2 - LACONA IX - Lasers in the conservation of artworks CY - London, UK DA - 07.09.2011 KW - Laser cleaning KW - Paper KW - Artificial soiling KW - Nanosecond laser KW - Microsecond laser PY - 2013 SN - 978-1-904982-87-6 SP - 219 EP - 221 PB - Archetype publications Ltd. AN - OPUS4-27956 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Pfennig, Anja A1 - Linke, B. A1 - Schulze, S. A1 - Kranzmann, Axel T1 - Corrosion in pipe steels exposed to supercritical CO2 during carbon capture and storage CCS T2 - EUROCORR 2011 - Developing solutions for the global challenge N2 - The CCS technique involves the compression of emission gasses in deep geological layers. To guarantee the safety of the site, CO2-corrosion of the injection pipe steels has to be given special attention when engineering CCS-sites. To get to know the corrosion behaviour samples of the heat treated steel 1.72252CrMo4, used for casing, and the stainless injection-pipe steel 1.4034 X46Cr13 were kept at T=60 °C and ambient pressure as well as p=100 bar for 700 h - 8000 h in a CC 2-saturated synthetic aquifer environment similar to possible geological on-shore CCS-sites in the northern German Basin. The isothermal corrosion behaviour obtained by mass gain of the steels in the gas phase, the liquid phase and the intermediate phase gives surface corrosion rates around 0.1 to 0.8 mm/year at ambient pressure and much lower about 0.02 to 0.2 mm/year at 100 bar where the CO 2 is in its supercritical state. Severe pit corrosion with pit heights around 4.5 mm are only located on the 42CrMo4 steel. Main phase of the continuous complicated multi-layered carbonate/oxide structure is siderite FeCO 3 in both types of steel. T2 - EUROCORR 2011 - Developing solutions for the global challenge CY - Stockholm, Sweden DA - 04.09.2011 KW - Steel KW - Pipeline KW - Corrosion KW - Carbonate layer KW - CCS KW - CO2-storage PY - 2011 SP - Paper 1044-1 EP - Paper 1044-8 AN - OPUS4-28008 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Pfennig, Anja A1 - Linke, B. A1 - Schulze, S. A1 - Kranzmann, Axel T1 - Static and dynamic long term corrosion experiments in CCS-conditions T2 - EUROCORR 2011 - Developing solutions for the global challenge N2 - Dealing with first corrosion screening experiments to predict the reliability and safety of Germanys first Carbon Capture and Storage site in the northern Bassin of Germany, northwest of the Capital Berlin, laboratory experiments have been established to simulate the particular conditions at T=60 °C, highly saline aquifer water similar to 'Stuttgart Aquifer', but only at ambient pressure. With mounting 2 independent full 2-grade titanium autoclave systems (running up to 250 bar and 300 °C) pressures up to p=100 bar are possible. In 2010 a specific corrosion chamber of 2-grade titanium working up to 100 °C, flowing aqui fer water with different gas mixtures was designed to fit to a high cycle fatigue testing machine. Long term fatigue experiments simulating fatigue crack growth under corrosive environments will soon start. These experiments may not only help engineering a CCS site, but results can be used to improve the maintenance of geothermal energy production sites, especially moved parts such as pumps and shafts. T2 - EUROCORR 2011 - Developing solutions for the global challenge CY - Stockholm, Sweden DA - 04.09.2011 KW - CO2 KW - Static corrosion KW - High cycle fatigue KW - Steel KW - CCS KW - CO2-storage KW - Corrosion PY - 2011 SP - 1 EP - 7 (Paper 1087) AN - OPUS4-28009 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schälike, Stefan A1 - Mishra, Kirti Bhushan A1 - Wehrstedt, Klaus-Dieter A1 - Schönbucher, A. T1 - Experimentelle Untersuchung der Massenabbrandraten multipler n-Heptan und Di-tert-butylperoxid Poolfeuer T2 - 3. Magdeburger Brand- und Explosionsschutztag / vfdb-Workshop N2 - Es werden Experimente zur Bestimmung der Massenabbrandraten von multiplen Poolfeuern präsentiert. Als Modellsubstanzen dienen n-Heptan und Di-tert-butylperoxid (DTBP). Es werden Versuche im Labormaßstab mit Durchmessern von d = 6 cm und relativen Abständen von 0.08 ≤ D/d ≤ 4 beschrieben und durch Feldversuche mit Pooldurchmessern d = 1.5 m und relativen Abständen zwischen den Pool von 0.17 ≤ D/d ≤ 1 ergänzt. Es kann gezeigt werden, dass die Massenabbrandraten multipler Feuer im Vergleich zu Einzelfeuern mit gleicher Brennstoffoberfläche bis zu einem Faktor 5.9 (n-Heptan) und 1.6 (DTBP) erhöht sind. Die Erhöhung ist abhängig vom relativen Abstand zwischen den Pools D, der Anzahl der Pools N und vom jeweiligen Brennstoff und zeigt ein lokales Maximum, welches mit dem Merging-Bereich der Flammenverschmelzung zusammenfällt. Die Massenabbrandrate als Funktion des relativen Abstandes zwischen den Pools kann durch eine Vergrößerung der Flammenbodenoberfläche infolge Flammenverschmelzung erklärt werden. T2 - 3. Magdeburger Brand- und Explosionsschutztag / vfdb-Workshop CY - Magdeburg, Germany DA - 22.03.2013 KW - Multiple Poolfeuer KW - Massenabbrandraten KW - n-Heptan KW - DTBP PY - 2013 SN - 978-3-00-041601-9 SP - 1 EP - 11 AN - OPUS4-27982 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mohamed, Zeinab A1 - Krüger, Simone A1 - Friedrich, Jörg Florian T1 - Deposition of thick polymer or inorganic layers with flame-retardant properties by combination of plasma and spray processes T2 - 3. Magdeburger Brand- und Explosionsschutztag / vfdb-Workshop N2 - Mixtures of hexamethyldisiloxane (HMDSO) and oxygen have been used for deposition of SiO2-like layers by plasma polymerization under low-pressure conditions onto polyethylene and polystyrene used as basecoat. Water glass was cast onto these 0.5 pm plasma thick siloxane-like layers with a thickness of 5 to 40 mu m. The adhesion of these bilayer systems and their flame resistance were tested. The effect of different plasma parameters such as monomer/gas ratio, pressure and power input into the discharge on the deposition rate and the composition of the formed layers was studied. Characterization and chemical composition of the formed films were performed using infrared, X-ray photoelectron and solid state nuclear magnetic resonance spectroscopy. Peel strengths of composites were measured and the locus of peel front propagation was detected. Thermal properties of composites were analyzed by thermo-gravimetric analysis. Finally, the fire-retardant properties of thick coated polymers were determined by exposure to flames and the behavior of coatings on the polymers during flaming was observed visually. T2 - 3. Magdeburger Brand- und Explosionsschutztag / vfdb-Workshop CY - Magdeburg, Germany DA - 21.03.2013 KW - Polymer KW - Plasmatechnologie KW - Analytik PY - 2013 SN - 978-3-00-041601-9 SP - 1 EP - 11 AN - OPUS4-27988 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Krüger, Simone A1 - Deubel, Jan A1 - Werrel, Martin A1 - Raspe, Tina A1 - Fettig, Ina A1 - Berger, Anka T1 - Brandtechnologische und chemisch-analytische Untersuchungen zum Einfluss von Brandbeschleunigern bei Zimmerbränden T2 - 3. Magdeburger Brand- und Explosionsschutztag / vfdb-Workshop N2 - Anhand von 5 verschiedenen Zimmerbrandversuchen wurde der Einfluss von Brandbeschleunigern auf den Brandverlauf experimentell untersucht. Es wurden verschiedene brandtechnologische Kennwerte, wie der Massenverlust des gesamten Brandraums, Brandraumtemperaturen, die Wärmefreisetzungen sowie die Rauchgasemissionen ermittelt und beurteilt. Die Rauchgasanalyse erfolgte im Schlot, im Brandraum sowie in der Brandraumöffnung mittels Fourier Transformierte Infrarot-FTIR-Spektroskopie. Neben diesen brandtechnologischen Untersuchungen erfolgten auch chemisch-analytische Untersuchungen nach dem Brand, mit dem Ziel, den eingesetzten Brandbeschleuniger nachzuweisen. Im Anschluss an die jeweiligen Zimmerbrandversuche wurden verschiedene Brandrückstandsproben aus dem Brandschutt, Wischproben von den Wänden und den übriggebliebenen Gegenständen sowie Proben in Form von Adsorbensmaterialien und Tenax-Röhrchen genommen und mit Hilfe der HSSPME-GC-MS-Methode (Headspace-Solid Phase Micro Extraction-Gas Chromatographie-Massenspekrometrie) in Hinblick eines möglichen Brandbeschleunigernachweis analysiert. T2 - 3. Magdeburger Brand- und Explosionsschutztag / vfdb-Workshop CY - Magdeburg, Germany DA - 21.03.2013 KW - Analytik KW - Brandbeschleuniger KW - Raumbrand PY - 2013 SN - 978-3-00-041601-9 SP - 1 EP - 10 AN - OPUS4-27991 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mishra, Kirti Bhushan A1 - Wehrstedt, Klaus-Dieter ED - Leipertz, A. T1 - Peroxy-fuels: potential applications in combustion engines T2 - 11th International congress on engine combustion processes - current problems and modern techniques N2 - Present work deals with the potential usage of peroxy-fuels (usually known as organic peroxides) in engine combustion processes. Although as additives (in small quantities < 5% to conventional fuels e.g. diesel, gasoline) peroxy-fuels are well known for many years their commercial applications as a main or primary fuel are not investigated in detail as such except a few. Since they are thermally unstable and energetic their safety demands great care during processing which restricts their commercial exploitation. However, once the issues with safety are resolved they can be much more advantageously employed than conventional fuels. Some of these advantages are: significant amount of fuel saving, reduction in amount of inducted air or even in the complete absence of air i.e. anaerobically, smaller volume of combustion (chamber), oxygenated fuel quality and low emissions. In this study we introduce an idea to develop the components of an engine operating solely on peroxy-fuels. The engine concept is based on single and multiple injectors in a cylinder with special material coating to ensure a temperature controlled processing. T2 - 11th International congress on engine combustion processes - current problems and modern techniques CY - Ludwigsburg, Germany DA - 14.03.2013 KW - Industrial fires KW - Storage units KW - Safety measures KW - Explosion KW - Overpressure KW - CFD simulation PY - 2013 SN - 3-931901-87-4 N1 - Serientitel: Berichte zur Energie- und Verfahrenstechnik (BEV) – Series title: Berichte zur Energie- und Verfahrenstechnik (BEV) IS - 13.1 SP - 157 EP - 164 AN - OPUS4-27951 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Weltschev, Margit A1 - Kohl, Anka A1 - Haufe, Manuela A1 - Werner, Jan T1 - Use of Fourier transform infrared spectroscopy to characterize nitric acid oxidation of polyethylene grades T2 - NACE International corrosion conference 2013 (Proceedings) N2 - Resistance to oxidative degradation by nitric acid has been selected for a comparison of polyethylene grades in a European standard on suitability proof for alternative plastic resins used for packagings and intermediate bulk containers (IBCs) for the transport of dangerous goods. Measurements of the infrared (IR) absorption spectra of microtome slices cut from the walls of jerricans, which were pre-stored with 55% nitric acid for 21 and 42 days at 40°C, showed changes in the structure of the polyethylene. The penetration depths of 55% nitric acid into the polyethylene grades are, in principle, suitable for evaluating the resistance to oxidative degradation of polyethylene grades after pre-storage of the packagings for 21 days. After this period the packaging wall is not fully penetrated. The intensities of the IR bands at 1565 cm-1 (-NO2), 1630 cm-1 (-C=C) and 1654 cm-1 (-O-NO2) increased with the treatment time with 55% nitric acid as a result of oxidative damage by the nitric acid. The high increase in absorbance of the -C=C band in the region 1630 - 1690 cm-1 is attributable to paraffinic chain cracks. The absorbance of the -O-NO2 band, formed as result of the nitration process was still low at a test temperature of 40°C. T2 - NACE International Corrosion Conference 2013 CY - Orlando, FL, USA DA - 17.03.2013 KW - Polyethylenformstoffe KW - Beständigkeit gegen oxidativen Abbau KW - Salpetersäure KW - Eindringtiefen KW - FTIR KW - Verpackungen zum Transport von Gefahrgütern PY - 2013 SN - 978-1-627-48145-8 SP - 1 EP - 11 (Paper No. 2070) PB - Curran CY - Red Hook, NY AN - OPUS4-27981 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rogge, Andreas T1 - Vorbeugender Brandschutz in Tunnelbauwerken T2 - Deutscher Bautechnik-Tag T2 - Deutscher Bautechnik-Tag CY - Hamburg, Germany DA - 2013-04-11 PY - 2013 N1 - Serientitel: DBV-Hefte – Series title: DBV-Hefte IS - 21 SP - 157 EP - 158 AN - OPUS4-28289 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Jaunich, Matthias A1 - Stark, Wolfgang A1 - Wolff, Dietmar T1 - Behaviour of rubber seals at low temperatures - results of component tests - T2 - Jahrestagung Kerntechnik 2013 (Proceedings) N2 - The investigation of low temperature properties of elastomeric sealing materials by means of thermo-analytical methods is a sound way to get information about the glass transition process. The breakdown temperature of the sealing function of O-ring seals was measured in a component test setup depending on material and degree of compression. An in depth explanation of the observed component tests behaviour is currently in preparation. It requires the results of thermo-analytical methods and measurements as the compression set (not shown here). With that, a model was developed to describe the correlation between physical material parameters and observed component behaviour. T2 - Jahrestagung Kerntechnik 2013 CY - Berlin, Germany DA - 14.05.2013 PY - 2013 SP - 1 EP - 6 AN - OPUS4-28574 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -