TY - CONF A1 - Rhode, Michael A1 - Kannengießer, Thomas T1 - Call for interested people to contribute to series of comprehensive papers on welding and joining of components for sustainable energy systems N2 - Joining and welding technologies are of high importance for the manufacturing of components and parts used in sustainable energy generation, conversion, and transport. In that connection, offshore and on-shore installed wind turbines are of high interest for the generation of electrical energy as well as photo-voltaic systems (solar cells). The electricity can be either directly transported or conversed via power-to-gas e.g., to hydrogen. In that scope, electrolyzer up to MW-range are of interest as well as the conver-sion back to electricity via fuel cells. In addition, hydrogen is a key element of the decarburization of in-dustries as well as the mobility sector encompassing sea, air and land transportation driven by hydrogen or its derivates. Well-known examples cover the direct reduction of iron ore to replace the conventional blast furnace process up to gas turbines or fuel cells for home-end use. All mentioned technologies re-quire reliable components, which are to a high extend dependent on joining and especially welding pro-cessing of materials. Especially, the (petro-) chemical industry has many years of experience with both materials used in hydrogen applications. The challenge is e.g., the transition to mass production of sys-tem components of electrolyzers/fuel cells and for distribution grids. At this point, the scalability of cur-rently applied joining processes often limits the economic efficiency, whereas especially laser welding or additive manufacturing will be of high interest. In that connection, it is very important to provide answers by joint research of universities, institutes, and industrial companies. Very often, solutions are already available and “just” have to be investigated and adapted for the new application, like repair welding of NG pipelines. For that reason, we want to set up a series of comprehensive papers with the aforementioned title. The idea is to get an in-depth but manageable overview of the importance of joining technologies in sustaina-ble energy generation, conversion, and transport encompassing current processes, limitations, and fur-ther perspectives. In that connection, the additive manufacturing is gaining more and more attention. If applicable, current challenges in the adaption or creation of new standards/regulations shall be addressed. T2 - IIW Intermediate Meeting, Com. II-A CY - Incheon, Republic of Korea DA - 12.03.2024 KW - Hydrogen KW - Welding KW - Comprehensive study KW - Component manufatcturing KW - Additive manufacturing PY - 2024 AN - OPUS4-59676 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Srinivasan, Krishnanand A1 - Gumenyuk, Andrey A1 - Rethmeier, Michael T1 - Laser Metal Deposition of Rene 80—Microstructure and Solidification Behavior Modelling N2 - New developments in nickel-based superalloys and production methods, such as the use of additive manufacturing (AM), can result in innovative designs for turbines. It is crucial to understand how the material behaves during the AM process to advance the industrial use of these techniques. An analytical model based on reaction–diffusion formalism is developed to better explain the solidification behavior of the material during laser metal deposition (LMD). The well-known Scheil–Gulliver theory has some drawbacks, such as the assumption of equilibrium at the solid–liquid interface, which is addressed by this method. The solidified fractions under the Scheil model and the pure equilibrium model are calculated using CALPHAD simulations. A differential scanning calorimeter is used to measure the heat flow during the solid–liquid phase transformation, the result of which is further converted to solidified fractions. The analytical model is compared with all the other models for validation. KW - Laser metal deposition KW - Solidification behavior KW - Additive manufacturing KW - Analytical model KW - Nickel‐based superalloy PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-612095 DO - https://doi.org/10.3390/mi15101234 SN - 2072-666X VL - 15 IS - 10 SP - 1 EP - 14 PB - MDPI AN - OPUS4-61209 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Scharf-Wildenhain, R. A1 - Hälsig, A. A1 - Hensel, J. A1 - Wandtke, Karsten A1 - Schröpfer, Dirk A1 - Kannengießer, Thomas T1 - Heat control and design‑related effects on the properties and welding stresses in WAAM components of high‑strength structural steels N2 - Commercial high-strength fller metals for wire arc additive manufacturing (WAAM) are already available. However, widespread industrial use is currently limited due to a lack of quantitative knowledge and guidelines regarding welding stresses and component safety during manufacture and operation for WAAM structures. In a joint research project, the process- and material-related as well as design infuences associated with residual stress formation and the risk of cold cracking are being investigated. For this purpose, reference specimens are welded fully automated with defned dimensions and systematic variation of heat control using a special, high-strength WAAM fller metal (yield strength>790 MPa). Heat control is varied by means of heat input (200–650 kJ/m) and interlayer temperature (100–300 °C). The ∆t8/5 cooling times correspond with the recommendations of fller metal producers (approx. 5–20 s). For this purpose, additional thermo-physical forming simulations using a dilatometer allowed the complex heat cycles to be reproduced and the resulting ultimate tensile strength of the weld metal to be determined. Welding parameters and AM geometry are correlated with the resulting microstructure, hardness, and residual stress state. High heat input leads to a lower tensile stress in the component and may cause unfavorable microstructure and mechanical properties. However, a sufciently low interlayer temperature is likely to be suitable for obtaining adequate properties at a reduced tensile stress level when welding with high heat input. The component design afects heat dissipation conditions and the intensity of restraint during welding and has a signifcant infuence on the residual stress. These complex interactions are analyzed within this investigation. The aim is to provide easily applicable processing recommendations and standard specifcations for an economical, appropriate, and crack-safe WAAM of high-strength steels. KW - GMA welding KW - Additive manufacturing KW - Residual stresses KW - High-strength steel KW - Cold cracking safety KW - Heat control KW - Wind energy PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-567397 DO - https://doi.org/10.1007/s40194-022-01450-x SN - 1878-6669 VL - 2022 SP - 1 EP - 11 PB - Springer CY - Berlin AN - OPUS4-56739 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Engelking, Lorenz A1 - Eissel, A. A1 - Schröpfer, Dirk A1 - Treutler, K. A1 - Kannengießer, Thomas A1 - Wesling, V. T1 - Optimisation of surface residual stresses using ultrasonic‑assisted milling for wire‑arc additive manufactured Ni alloy components N2 - Nickel alloys are cost intensive materials and generally classified as difficult-to-cut material. However, machining of these materials is needed especially in case of alloy 36 (1.3912), which is commonly used in mould construction for the production of fibre-reinforced composites. With regard to repair, modification and manufacturing of such components, additive manufacturing offers significant economic advantages. Nevertheless, subsequent machining steps are needed to achieve the final component contour and defined surface conditions. Dependent on the material and machining process conditions, detrimental tensile residual stresses may be the result on the machined surface, having negative impact on the component performance and safety. In this investigation, machining experiments were carried out on wire arc additive manufactured components made of alloy 36, varying the cutting speed and the feed rate. In addition, the conventional milling process (CM) was compared with a modern, hybrid machining process, the ultrasonic-assisted milling (US). The cutting forces and the surface-near residual stresses were analysed using X-ray diffraction. A significant improvement of the machinability as well as the surface integrity by using the ultrasonic assistance was observed, especially at low cutting speeds. The CM induced mainly tensile residual stresses, the US mainly compressive residual stresses. KW - Surface integrity KW - Ultrasonic-assisted milling KW - Additive manufacturing KW - Ni alloy KW - Alloy 36 PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-575246 DO - https://doi.org/10.1007/s00170-023-11326-z SN - 1433-3015 VL - 126 IS - 9 SP - 4191 EP - 4198 PB - Springer Nature AN - OPUS4-57524 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eissel, A. T1 - Modification of CoCr alloys to optimize of additively welded microstructures and subsequent surface finishing N2 - Due to increasing requirements relating to the efficiency of highly stressed components in turbine or plant construction, the use of cost-intensive, difficult to process materials is increasingly necessary today. In this context, cobalt-chromium alloys in particular are highly resistant to thermal and mechanical stress, as well as to corrosive and abrasive loads. Moreover, increasingly complex structures and the optimisation of resource efficiency also require additive manufacturing steps for the production or repair of components in many sectors. In order to realise a homogeneous and isotropic microstructure, alloy modifications are made to the alloy CoCr26Ni9Mo5W. For this purpose, hafnium and zirconium are added at 1 % and 0,33 % by mass each, as these elements are supposed to have a positive effect on the microstructure morphology. Plasma-Transferred-Arc is used for the welding tests. Wall structures are welded by multiple single-layer, overlapping welding beads on low-alloyed steel substrate (S355). The results show that the alloying elements hafnium and zirconium have a clear influence on the microstructure. Hardness measurements were also carried out. With each modification, the hardness is increased compared to the original material. The machining analyses show a reduction in cutting forces using ultrasonic assisted milling for high cutting speed and low feed rate. T2 - 2021 Intermediate meeting of C IX NF CY - Online meeting DA - 09.03.2021 KW - Alloy modification KW - Ultrasonic-assisted milling KW - Plasma-Transferred-Arc KW - Filler metal modification KW - Additive manufacturing PY - 2021 AN - OPUS4-52356 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eissel, A. T1 - Alloy modification for additive manufactured Ni alloy components Part I: Effect on microstructure and hardness N2 - Alloy 36 (1.3912), also known as “Invar”, is an alloy with 36% nickel. The alloy has a remarkably low thermal expansion coefficient in certain temperature ranges. Therefore, it is used in applications in which dimensional stability is critical, such as moulding tools for composite materials in aerospace and automotive applications. Moreover, increasingly complex structures and the optimisation of resource efficiency also require additive manufacturing steps for the production or repair of components. Additively manufactured components have a heterogeneous microstructure and anisotropic mechanical properties. In part I of this investigation, the initial alloy 36 is modified with the elements Ti, Zr and Hf up to a maximum of 0.33 wt.-%. The influence of the modification elements on the microstructure as well as on the hardness of the AM components is examined. Part II focusses on the effect of the alloy modifications on machinability as well as on the surface integrity of plasma-transferred-arc-welded (PTA) and finish milled invar components. The results show that PTA welding cause numerous finely distributed precipitates with high silicon content. T2 - 75th IIW Annual Assembly CY - Tokyo, Japan DA - 17.07.2022 KW - Alloy modification KW - Alloy 36 KW - Additive manufacturing PY - 2022 AN - OPUS4-55439 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eissel, A. T1 - Alloy modification for additive manufactured Ni alloy components Part I: Effect on microstructure and hardness N2 - Alloy 36 is an iron-based alloy with 36% nickel. It is used in applications in which dimensional stability is critical, such as molding tools for composite materials in aerospace and automotive applications. Moreover, increasingly complex structures and the optimisation of resource efficiency also require additive manufacturing steps for the production or repair of components. Additively manufactured components have a heterogeneous microstructure and anisotropic mechanical properties. In addition, the manufactured components require subsequent machining surface finishing due to the high requirements. Nickel iron alloys are difficult to machine. Additionally, inhomogeneous microstructure may lead to unstable cutting forces and conditions. Alloy modifications are made to the alloy 36. For this purpose, titanium, zirconium and niobium are added up to 1 % by mass each. Plasma-Transferred-Arc is used for the welding tests. The hardness profile is determined on the transverse section. The initial structure as well as the modifications have an austenitic structure. The microstructure of the modifications of Alloy 36 with 1% Ti and 1% Zr is not refined, instead the grain size increases. T2 - IIW C-II Intermediate meeting CY - Online meeting DA - 17.03.2022 KW - Alloy modification KW - Alloy 36 KW - Additive manufacturing PY - 2022 AN - OPUS4-56622 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Engelking, Lorenz T1 - Optimisation of surface residual stresses using hybrid milling processes for additive manufactured Nickel alloy components N2 - Ni alloys are cost intensive materials and generally classified as difficult-to-cut materials. However, machining of these materials is needed especially in case of alloy 36 (1.3912), which is commonly used in mould construction for the production of fibre-reinforced composites. With regard to repair, modification and manufacturing of such components, additive manufacturing offers significant economic advantages. Nevertheless, subsequent machining steps are needed to achieve the final component contour and defined surface conditions. Dependent on the material and machining process conditions, detrimental tensile residual stresses may be the result on the machined surface, having negative impact on the component performance and safety. Recent studies exhibited that hybrid machining processes, such as ultrasonic-assisted milling (USAM), are suitable for achieving favourable residual stress states at the surface of difficult-to-cut Ni-Cr alloys. In this investigation, wire arc additive manufactured (WAAM) specimens of alloy 36 were finish milled under different milling conditions. In addition to the machined surfaces condition and topology, the surface-near residual stresses were analysed using X-ray diffraction (XRD). Especially for low cutting speeds, significantly improved surface properties, roughness parameters and lower mechanical and microstructural degradations were found for the specimen machined with USAM compared to conventional milling. The improved surface integrity could furthermore be observed by a significant reduction of the tensile residual stresses in the surface boundary area. T2 - Bachelor-, Master-, Doktoranden-Kolloquium, Otto-von-Guericke-Universität Magdeburg CY - Magdeburg, Germany DA - 18.05.2022 KW - Surface integrity KW - Ultrasonic-assisted milling KW - Additive manufacturing KW - Ni alloy KW - Alloy 36 PY - 2022 AN - OPUS4-54908 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Engelking, Lorenz A1 - Eissel, A. A1 - Schröpfer, Dirk A1 - Treutler, K. A1 - Kannengießer, Thomas A1 - Wesling, V. T1 - Effect of alloy modification for additive manufactured Ni alloy components on microstructure and subsequent machining properties N2 - Ni alloys are generally classified as difficult-to-cut materials and cost intensive. Additive manufacturing (AM) offers economic advantages. However, machining of these AM components is mandatory to create the final contour or surface. The inhomogeneous and anisotropic microstructure and properties of AM components causes an unstable cutting process. Moreover, undesirable tensile residual stresses are generated due to subsequent machining. In this investigation, the initial alloy 36 is modified with Ti and Nb up to 1.6 wt.-% and build-up welded via gas metal arc welding (GMAW) and plasma-transferred-arc (PTA). Then, finish-milling tests are carried out to investigate the influence of the modification as well as the cutting parameters on the resulting cutting force and the surface integrity. In addition, the conventional milling process (CM) is compared with the ultrasonic-assisted milling process (US), which has a significant influence on the machinability as well as on the surface integrity. T2 - Additive Fertigung – Werkstoffe – Prozesse – Wärmebehandlung 2022 CY - Bremen, Germany DA - 29.06.2022 KW - Additive manufacturing KW - Alloy 36 KW - Alloy modification KW - Ultrasonic-assisted milling KW - Surface integrity PY - 2022 SP - 57 EP - 67 AN - OPUS4-55430 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Eissel, A. A1 - Engelking, Lorenz A1 - Treutler, K. A1 - Schröpfer, Dirk A1 - Wesling, V. A1 - Kannengießer, Thomas T1 - Investigations on influencing the microstructure of additively manufactured Co‑Cr alloys to improve subsequent machining conditions N2 - Co-Cr alloys are frequently used for highly stressed components, especially in turbine and plant construction, due to their high resistance to thermal and mechanical stress, as well as to corrosive and abrasive loads. Furthermore, they are classified as difficult-to-cut materials because of their high strength and toughness as well as their low thermal conductivity. However, for Co, an increased cost and supply risk can be observed in recent years. Therefore, additive manufacturing (AM) offers significant economic advantages due to higher material efficiency regarding repair, modification, and manufacturing of such components. Concerning inhomogeneity and anisotropy of the microstructure and properties as well as manufacturing-related stresses, a lot of knowledge is still necessary for the economic use of additive welding processes in SMEs. In addition, subsequent machining, particularly contour milling, is essential to generate the required complex contours and surfaces. Hence, additive and machining manufacturing processes need to be coordinated in a complementary way, especially due to additional challenges arising in milling of heterogeneous hard-to-cut microstructures. Recently, it has been shown that modern, hybrid cutting processes, such as ultrasonic-assisted milling (US), can improve the cutting situation. In this investigation, the Co-Cr initial alloy is additionally modified with Ti and Zr up to 1 wt% with the aim to enhance the homogeneity of the microstructure and, thus, the machinability. Hence the investigation includes finish milling tests of the AM components and the comparison of US and conventional machining. Both the modifications and the ultrasonic assistance exhibit a significant effect on the machining situation; for example US causes a higher surface integrity of the finish milled surfaces compared to conventional milling. T2 - International Congress on Welding, Additive Manufacturing and associated non-destructive testing CY - Online meeting DA - 08.06.2022 KW - Cobalt-chromium alloy KW - Additive manufacturing KW - Ultrasonic-assisted milling KW - Surface integrity PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-560917 DO - https://doi.org/10.1007/s40194-022-01397-z SP - 1 EP - 9 PB - Springer CY - Heidelberg AN - OPUS4-56091 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eissel, A. T1 - Investigations on influencing the microstructure of additively manufactured Co-Cr alloys to improve subsequent machining conditions N2 - Co-Cr alloys are frequently used for highly stressed components, especially in turbine and plant construction, due to their high resistance to thermal and mechanical stress, as well as to corrosive and abrasive loads. Furthermore, they are classified as difficult-to-cut materials because of their high strength and toughness as well as their low thermal conductivity. However, for Co, an increased cost and supply risk can be observed in recent years. Therefore, additive manufacturing (AM) offers significant economic advantages due to higher material efficiency regarding repair, modification, and manufacturing of such components. Concerning inhomogeneity and anisotropy of the microstructure and properties as well as manufacturing-related stresses, a lot of knowledge is still necessary for the economic use of additive welding processes in SMEs. In addition, subsequent machining, particularly contour milling, is essential to generate the required complex contours and surfaces. Hence, additive and machining manufacturing processes need to be coordinated in a complementary way, especially due to additional challenges arising in milling of heterogeneous hard-to-cut microstructures. Recently, it has been shown that modern, hybrid cutting processes, such as ultrasonic-assisted milling (US), can improve the cutting situation. In this investigation, the Co-Cr initial alloy is additionally modified with Ti and Zr up to 1 wt.-% with the aim to enhance the homogeneity of the microstructure and, thus, the machinability. Hence the investigation includes finish milling tests of the AM components and the comparison of US and conventional machining. Both the modifications and the ultrasonic assistance exhibit a significant effect on the machining situation, e.g., US causes a higher surface integrity of the finish milled surfaces compared to conventional milling. T2 - International Congress on Welding, Additive Manufacturing and associated non destructive testing CY - Online meeting DA - 08.06.2022 KW - Co-Cr-alloy KW - Additive manufacturing KW - Ultrasonic-assisted milling KW - Surface integrity PY - 2022 AN - OPUS4-55431 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Engelking, Lorenz T1 - Alloy modification for additive manufactured Ni alloy components Part II: Effect on subsequent machining properties N2 - Alloy 36 (1.3912), also known as “Invar”, is an alloy with 36% nickel. It was developed in 1897 by Guillaume and stands out for its very low thermal expansion coefficient. It is classified as a difficult-to-cut material and is commonly used for the production of fiber-reinforced composites in the field of mold construction. Additive manufacturing (AM) offers many economic advantages regarding the repair, modification and manufacture of entire components. Subsequent machining of the AM components is necessary to account for complex structures, final contours or defined surfaces. This is usually done using a tool with a geometrically defined cutting edge, i.e., milling processes. Surface integrity is determined by metallurgical (e.g., microstructure of the subsurface), topological (e.g., surface defects, roughness) and mechanical (e.g., residual stresses) factors, which is crucial in terms of component safety and performance. Modern, hybrid cutting processes, such as ultrasonic-assisted milling (US), provide potentially improvement of the cutting situation of these components. In part I of this investigation, the initial alloy 36 is modified with the elements Ti, Zr and Nb up to a maximum of 1 wt.-%. The influence of the modification elements on the microstructure as well as on the hardness of the AM components is examined. Part II focusses on the effect of the alloy modifications on machinability as well as on the surface integrity of plasma-transferred-arc-welded (PTA) and finish milled invar components. The results show a significant positive influence of ultrasonic assistance on the resulting cutting force of both materials. The modification with 1% Ti shows a positive influence on the surface integrity, as the roughness of the conventional machining processes is lower compared to the initial alloy, which has to be confirmed in further experiments. T2 - IIW C-II Intermediate meeting CY - Online meeting DA - 17.03.2022 KW - Alloy modification KW - Ultrasonic-assisted milling KW - Plasma-Transferred-Arc KW - Surface integrity KW - Alloy 36 KW - Additive manufacturing PY - 2022 AN - OPUS4-54910 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Engelking, Lorenz T1 - Alloy modification for additive manufactured Ni alloy components Part II: Effect on subsequent machining properties N2 - Alloy 36 (1.3912), also known as “Invar”, is an alloy with 36% nickel. It was developed in 1897 by Guillaume and stands out for its very low thermal expansion coefficient. It is classified as a difficult-to-cut material and is commonly used for the production of fiber-reinforced composites in the field of mold construction. Additive manufacturing (AM) offers many economic advantages regarding the repair, modification and manufacture of entire components. Subsequent machining of the AM components is necessary to account for complex structures, final contours or defined surfaces. In part I of this investigation, the initial alloy 36 is modified with the elements Ti, Zr and Hf up to a maximum of 0.33 wt.-%. The influence of the modification elements on the microstructure as well as on the hardness of the AM components is examined. Part II focusses on the effect of the alloy modifications on machinability as well as on the surface integrity of plasma-transferred-arc-welded (PTA) and finish milled invar components. Machining tests were carried out, to investigate the influence of ultrasonic assistance and the effects of modification elements Ti, Zr and Hf on the occurring cutting forces, temperatures and resulting surface integrity of the AM components made of alloy 36 and their modifications. The results show a significant positive influence of ultrasonic assistance on the resulting cutting force as well as on the roughness of all materials investigated. T2 - 75th IIW Annual Assembly CY - Tokyo, Japan DA - 17.07.2022 KW - Alloy modification KW - Alloy 36 KW - Additive manufacturing KW - Ultrasonic-assisted milling KW - Surface integrity PY - 2022 AN - OPUS4-55432 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Engelking, Lorenz T1 - Effect of alloy modification for additive manufactured Ni alloy components on microstructure and subsequent machining properties N2 - Ni alloys are generally classified as difficult-to-cut materials and cost intensive. Additive manufacturing (AM) offers economic advantages. However, machining of these AM components is mandatory to create the final contour or surface. The inhomogeneous and anisotropic microstructure and properties of AM components causes an unstable cutting process. Moreover, undesirable tensile residual stresses are generated due to subsequent machining. In this investigation, the initial alloy 36 is modified with Ti and Nb up to 1.6 wt.-% and build-up welded via gas metal arc welding (GMAW) and plasma-transferred-arc (PTA). Then, finish-milling tests are carried out to investigate the influence of the modification as well as the cutting parameters on the resulting cutting force and the surface integrity. In addition, the conventional milling process (CM) is compared with the ultrasonic-assisted milling process (US), which has a significant influence on the machinability as well as on the surface integrity. T2 - Additive Fertigung – Werkstoffe – Prozesse – Wärmebehandlung 2022 CY - Bremen, Germany DA - 29.06.2022 KW - Additive manufacturing KW - Alloy 36 KW - Alloy modification KW - Ultrasonic-assisted milling KW - Surface integrity PY - 2022 AN - OPUS4-55429 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Treutler, K. T1 - Nickel-iron-alloy modification to enhance additively welded microstructure for subsequent milling N2 - The aerospace industry uses nickel-iron-alloys to create moulding tools for composite materials because of the low coefficient of thermal expansion. These tools have a large-sized and complex structure, making them cost-intensive and difficult to manufacture. Therefore, the focus is set on additive manufacturing, which can additionally enable the repair of components in order to eliminate local defects. However, the process usually results in a heterogeneous microstructure and anisotropic mechanical properties. As there is a high demand for a precise and exact fit of the precision moulds and thus the surface quality, the welded components must be subsequently machined. Nickel-iron alloys are difficult to machine and an inhomogeneous microstructure also leads to unstable cutting forces. Consequently, a refinement and homogenisation of the microstructure morphology is achieved through specific alloy modifications in order to stabilise and improve the subsequent machining process. Studies on the refinement of FeNi 36 based on vacuum arc melting furnaces are used as a starting point. Therefore, titanium and niobium are chosen as modification elements with a maximum 1 % weight percent and are added to nickel-iron base alloy. The elements are alloyed and build-up welded by using plasma-transferred-arc welding. The resulting microstructure morphology of the welded wall structure and the machining properties are then determined. Furthermore, the influence on the coefficient of thermal expansion is investigated in connection with the modification and the welding process itself. It can be shown that even small amounts of niobium have a significant influence on the structural morphology of the welded layers during plasma-transferred-arc welding. T2 - 2nd international Conference on Advanced Joining Processes 2021 CY - Sintra, Portugal DA - 21.10.2021 KW - Alloy modification KW - Ultrasonic-assisted milling KW - Nickel-iron-alloy KW - Additive manufacturing KW - Plasma transferred arc welding PY - 2021 AN - OPUS4-53635 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael T1 - Joining processes for components in hydrogen technologies: Current need and future importance N2 - This presentation gives an overview on the importance of joining processes for component fabrication in hydrogen technologies. For that reason, the current need and future research and developement activites are highlighted for the three technological fields: hydrogen storage, transport and use (in terms of the emerging field of additive manufacturing). Finally, some remarks are given for necessary changes in the standardization. T2 - IIW Intermediate Meeting, Comm. II-A "Welding Metallurgy" CY - Online meeting DA - 17.03.2022 KW - Hydrogen KW - Welding KW - Research KW - Review KW - Additive manufacturing PY - 2022 AN - OPUS4-54488 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Engelking, Lorenz T1 - Optimisation of surface residual stresses using hybrid milling processes for additive manufactured Ni alloy components N2 - Ni alloys are cost intensive materials and generally classified as difficult-to-cut materials. However, machining of these materials is needed especially in case of alloy 36 (1.3912), which is commonly used in mould construction for the production of fibre-reinforced composites. With regard to repair, modification and manufacturing of such components, additive manufacturing offers significant economic advantages. Nevertheless, subsequent machining steps are needed to achieve the final component contour and defined surface conditions. Dependent on the material and machining process conditions, detrimental tensile residual stresses may be the result on the machined surface, having negative impact on the component performance and safety. Recent studies exhibited that hybrid machining processes, such as ultrasonic-assisted milling (USAM), are suitable for achieving favourable residual stress states at the surface of difficult-to-cut Ni-Cr alloys. In this investigation, wire arc additive manufactured (WAAM) specimens of alloy 36 were finish milled under different milling conditions. In addition to the machined surfaces condition and topology, the surface-near residual stresses were analysed using X-ray diffraction (XRD). Especially for low cutting speeds, significantly improved surface properties, roughness parameters and lower mechanical and microstructural degradations were found for the specimen machined with USAM compared to conventional milling. The improved surface integrity could furthermore be observed by a significant reduction of the tensile residual stresses in the surface boundary area. T2 - ICRS11, 11th International Conference on Residual Stresses CY - Nancy, France DA - 27.03.2022 KW - Surface integrity KW - Ultrasonic-assisted milling KW - Additive manufacturing KW - Ni alloy KW - Alloy 36 PY - 2022 AN - OPUS4-54904 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Barik, Birendra Kumar A1 - Chaurasia, Prashant Kumar A1 - De, Amitava T1 - Rapid estimation of temperature field and bead profile for wire arc directed energy deposition using an analytical heat conduction model N2 - A prior estimation of the temperature field and bead profile can help fabricate dimensionally consistent and structurally sound parts using wire arc directed energy deposition (DED-Arc). We present here a three-dimensional analytical heat transfer model with a volumetric heat source to compute the transient temperature field and melt pool dimensions for DED-Arc. The analytical model considers the thermal conductivity and volumetric heat capacity as a linear function of temperature. In contrast to assuming a pre-defined deposited track profile, the same is scaled from the analytically computed melt pool dimensions into the substrate. The computed deposit profiles of single and multiple tracks and layers are validated extensively with the corresponding experimentally measured results for a range of DED-Arc process conditions. KW - Additive manufacturing KW - Analytical model KW - Heat conduction analysis KW - Volumetric heat source KW - Deposit profile PY - 2025 DO - https://doi.org/10.1177/13621718251398070 SN - 1362-1718 SP - 1 EP - 14 PB - SAGE Publications AN - OPUS4-64836 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Zurcher, Theo A1 - Serrano-Munoz, Itziar A1 - Mishurova, Tatiana A1 - Abreu Faria, Guilherme A1 - Degener, Sebastian A1 - Fridrici, Vincent A1 - Charkaluk, Eric A1 - Bruno, Giovanni T1 - Sliding wear resistance and residual stresses of parts repaired by laser metal deposition N2 - Large temperature gradients inherent to additive manufacturing (AM) processes induce large residual stress (RS) in the final part. Because RS can influence the tribological properties, this study focuses on the relationship between wear sliding properties and RS in IN718 coatings. Such coatings were deposited with a Laser metal deposition (LMD) machine using two different scanning strategies. The wear resistance and RS state were investigated after surface milling. RS were measured before and after wear tests on a reciprocating sliding test apparatus. Two different X-ray diffraction techniques were employed to measure the surface and subsurface state RS: Laboratory Energy Dispersive X-ray Diffraction (LEDXD) and Synchrotron X-ray Energy Dispersive Diffraction (SXEDD). Due to the milling process, the coatings show similar depth distributions of RS from 22 to 92 μm depth, but exhibit different magnitudes depending on the scanning strategy used. Reciprocating sliding wear tests induced high compressive residual stresses that erased the initial RS state, and a similar wear behavior was observed in the two samples. These samples possess similar texture and grain morphology. This demonstrates that the influence of RS on wear resistance is a second-order effect. Nevertheless, it was observed that RS can still impact the wear performance at the early testing stages of the repaired parts. KW - Additive manufacturing KW - Wear resistance KW - Residual stress PY - 2023 DO - https://doi.org/10.1007/s10853-023-09129-4 SN - 0022-2461 SP - 1 EP - 18 PB - Springer AN - OPUS4-59084 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schröpfer, Dirk T1 - Influence of Ultrasonic-Assisted Milling on Surface Integrity of Additively Manufactured Components Using DED-Arc/GMAW N2 - Additive manufacturing (AM) is increasingly used for producing complex metallic com-ponents. Subsequent machining is essential to achieve final geometries and surface conditions. The resulting surface integrity, particularly the near-surface residual stress state, plays a crucial role in component performance and fatigue life. This study inves-tigates the potential of ultrasonic-assisted milling (USAM), a hybrid machining process, to improve surface integrity and machinability compared to conventional milling (CM). Three materials were investigated, two difficult-to-cut materials CoCr26Ni9Mo5W and FeNi36 and a low-alloy steel S355J2C. The CoCr26Ni9Mo5W and FeNi36 were addi-tively manufactured via DED-Arc and then machined with varying cutting speeds and feed rates within a Design of Experiments. USAM exhibited enhanced machinability and surface integrity, particularly at low cutting speeds, by reducing cutting forces up to 40% and shifting near-surface residual stresses from tensile to compressive. For S355J2C, USAM reduced cutting forces by approximately 45% and induced surface-near compressive residual stresses up to approximately -700 MPa, leading to a 11% higher fatigue strength compared to CM. These findings highlight the advantages of ultrasonic assistance in post-AM machining, offering enhanced fatigue performance and surface quality for various metallic materials. T2 - 4th International Conference on Advanced Joining Processes 2025 CY - Coimbra, Portugal DA - 16.10.2025 KW - Ultrasonic-assisted milling KW - Additive manufacturing KW - Surface integrity KW - Fatigue strength KW - Residual stress PY - 2025 AN - OPUS4-65051 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ávila Calderón, Luis T1 - Mechanical behaviour of AM metals: Creep of LPBF 316L and low-cycle-fatigue of LMD Ti-6Al-4V N2 - Additively manufactured metallic materials have already started to find application in safety-relevant components. However, this has only happened for certain materials and specific applications and loading conditions, since there is still an extensive lack of knowledge as well as of historical data regarding their mechanical behaviour. This contribution aims to address this lack of understanding and historical data concerning the creep behaviour of the austenitic stainless steel 316L manufactured by Laser-Powder-Bed-Fusion (L-PBF) and the low-cycle-fatigue behaviour of the titanium alloy Ti-6Al-4V manufactured by Laser-Metal-Deposition (LMD). Furthermore, it aims to assess their mechanical behaviour against their conventional counterparts. With that in mind, specimens from conventional and additive materials are tested and their mechanical behaviour analysed based on characteristic curves. To understand the damage behaviours the materials are characterized by destructive and non-destructive techniques before and after failure. T2 - 1st Workshop on In-situ Monitoring and Microstructure Development in Additive Manufacturing CY - Online Meeting DA - 10.12.2020 KW - Ti-6Al-4V KW - 316L KW - Additive manufacturing KW - Creep behaviour KW - Low-cycle-fatigue behaviour PY - 2020 AN - OPUS4-51879 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Dzugan, J. A1 - Lucon, E. A1 - Koukolikova, M. A1 - Li, Y. A1 - Rzepa, S. A1 - Yasin, M.S. A1 - Shao, S. A1 - Shamsaei, N. A1 - Seifi, M. A1 - Lodeiro, M. A1 - Lefebvre, F. A1 - Mayer, U. A1 - Olbricht, Jürgen A1 - Houska, M. A1 - Mentl, V. A1 - You, Z. T1 - ASTM interlaboratory study on tensile testing of AM deposited and wrought steel using miniature specimens N2 - An interlaboratory study, involving eigth international laboratories and coordinated by COMTES FHT (Czech Republic), was conducted to validate tensile measurements obtained using miniature specimens on additively manufactured (AM) components and artifacts. In addition to AM 316L stainless steel (316L SS), a wrought highstrength steel (34CrNiMo6V, equivalent to AISI 4340) was also used. Based on the results, a precision statement in accordance with ASTM E691 standard practice was developed, intended for inclusion in a proposed annex to the ASTM E8/E8M tension testing method. The primary outcomes of the study highlighted the agreement between yield and tensile strength measured from miniature and standard-sized tensile specimens. Furthermore, most tensile properties exhibited similar standard deviations, offering users insight into the efficacy of miniature specimen applications. KW - 316L stainless steel KW - Additive manufacturing KW - High-strength steel KW - Miniature specimens KW - Tensile tests PY - 2024 DO - https://doi.org/10.1016/j.tafmec.2024.104410 SN - 0167-8442 VL - 131 SP - 1 EP - 13 PB - Elsevier B.V. AN - OPUS4-60180 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rhode, Michael T1 - Additive manufacturing for components in hydrogen technologies N2 - With the introduction of a hydrogen-based energy and national economy, safety-relevant components for hydrogen technologies are becoming increasingly important. Characteristic of hydrogen technologies are, for example, harsh environmental conditions such as cryogenic or high-pressure storage, corrosion issues in fuel cells and electrolyzers, turbines, and many more. Additive manufacturing of components is becoming increasingly important and irreplaceable for the production of complex technical systems. Using the case studies of burners for gas turbines and electrodes and membranes for polymer (PEMFC) and solid oxide (SOFC) fuel cells, this article shows the potential of additive manufacturing of components. At the same time, however, the challenge of considering divergent mechanical properties depending on the direction of assembly in a "hydrogen-compatible" manner is also highlighted. Finally, the challenges posed by additive manufacturing and hydrogen for materials testing are highlighted under scenarios that are as realistic as possible. T2 - MPA-Workshop Hydrogen CY - Online meeting DA - 10.11.2022 KW - Additive manufacturing KW - Hydrogen KW - Technologies KW - Overview KW - Component PY - 2022 AN - OPUS4-56233 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Witte, Julien A1 - Treutler, Kai A1 - Schröpfer, Dirk A1 - Kannengießer, Thomas T1 - Influence of Microstructure on the Machinability and Surface Integrity of Additively Manufactured Iron Aluminides N2 - The increasing global focus on energy and resource efficiency has stimulated a growing interest in additive manufacturing. AM offers economic advantages and enables an efficient use of materials. However, AM components often require subsequent mechanical post-processing, such as machining (e.g. milling), to achieve the final contours or surfaces. This is a particular challenge due to the heterogeneous and anisotropic nature of AM structures, which affect machining and the resulting component properties. High-performance materials such as iron aluminide represent a promising alternative to conventional high-temperature materials with a significant economic advantage. However, the strength and hardness properties, which are advantageous for applications in highly stressed lightweight components, pose a challenge for economical machining in addition to the AM microstructure properties. The difficult-to-cut material causes accelerated tool wear and insufficient surface quality. This study shows that crack-free additive manufacturing of the three-component system of iron-nickel-aluminum is possible, and advantages in terms of machinability compared to FeAl-AM components are achieved. The more homogeneous microstructure leads to a reduction in cutting forces, with positive effects on the machinability and optimized surface integrity. Ultrasonic assisted milling (USAM) offers great potential to address the major challenges posed by difficult-to-cut materials and additively manufactured weld structures. Therefore, this study focuses on assessing the transferability of previous positive results by USAM to the selected iron aluminide alloys. The machinability of the aluminides is analyzed by varying significant influencing variables in finish milling experiments and evaluated in terms of the loads on the tool and the resulting surface integrity. T2 - AA Meeting of Commission IX ‘Behavior of Metals subject to Welding’ CY - Rhodes, Greece DA - 08.07.2024 KW - Iron aluminide KW - Additive manufacturing KW - Machinability KW - Surface integrity KW - Ultrasonic-assisted milling PY - 2026 SP - 1 EP - 16 AN - OPUS4-65530 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Surmeneva, M. A1 - Koptyug, A. A1 - Khrapov, D. A1 - Ivanov, Yuriy A1 - Mishurova, Tatiana A1 - Evsevleev, Sergei A1 - Prymak, O. A1 - Loza, K. A1 - Epple, M. A1 - Bruno, Giovanni A1 - Surmenev, R. T1 - In situ synthesis of a binary Ti–10at% Nb alloy by electron beam melting using a mixture of elemental niobium and titanium powders N2 - This study reports the results of the preliminary assessment to fabricate Ti-10at% Nb alloy by electron beam melting (EBM®) from a blend of elemental Nb and Ti powders. The microstructure of the EBM-manufactured Ti-10at% Nb alloys is sensitive to the following factors: different sintering properties of Nb and Ti powders, powder particle properties, material viscosities at varying melt pool temperatures, β-stabilizer element content and the EBM® process parameters. Three phases were observed in as-manufactured Ti-10at% Nb alloy: μm-size Nb phase, a Nb-rich β-solid solution surrounding Nb phase, lamellar structured α-phase and β-solid solution with different distribution and volume fraction. Thus, the combination of powder particle characteristics, very short time material spends in molten condition and sluggish kinetics of mixing and diffusional process in Ti-Nb alloy results in heterogeneous microstructures depending on the local Nb content in the powder blend and the EBM® process conditions. KW - Additive manufacturing KW - Electron beam melting KW - Ti-Nb alloy KW - In situ alloying PY - 2020 DO - https://doi.org/10.1016/j.jmatprotec.2020.116646 VL - 282 SP - 116646 PB - Elsevier B.V. AN - OPUS4-50457 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ulbricht, Alexander T1 - Separation of the Formation Mechanisms of Residual Stresses in LPBF 316L N2 - Rapid cooling rates and steep temperature gradients are characteristic of additively manufactured parts and important factors for the residual stress formation. This study examined the influence of heat accumulation on the distribution of residual stress in two prisms produced by Laser Powder Bed Fusion (LPBF) of austenitic stainless steel 316L. The layers of the prisms were exposed using two different border fill scan strategies: one scanned from the centre to the perimeter and the other from the perimeter to the centre. The goal was to reveal the effect of different heat inputs on samples featuring the same solidification shrinkage. Residual stress was characterised in one plane perpendicular to the building direction at the mid height using Neutron and Lab X-ray diffraction. Thermography data obtained during the build process were analysed in order to correlate the cooling rates and apparent surface temperatures with the residual stress results. Optical microscopy and micro computed tomography were used to correlate defect populations with the residual stress distribution. The two scanning strategies led to residual stress distributions that were typical for additively manufactured components: compressive stresses in the bulk and tensile stresses at the surface. However, due to the different heat accumulation, the maximum residual stress levels differed. We concluded that solidification shrinkage plays a major role in determining the shape of the residual stress distribution, while the temperature gradient mechanism appears to determine the magnitude of peak residual stresses. T2 - MLZ User Meeting 2020 CY - Online meeting DA - 08.12.2020 KW - Computed tomography KW - Neutron diffraction KW - X-ray diffraction KW - Additive manufacturing KW - Residual stress KW - Thermography KW - LPBF KW - Laser Powder Bed Fusion PY - 2020 AN - OPUS4-51793 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Khrapov, D A1 - Koptyug, A. A1 - Manabaev, K. A1 - Léonard, Fabien A1 - Mishurova, Tatiana A1 - Bruno, Giovanni A1 - Cheneler, D. A1 - Loza, K. A1 - Epple, M. A1 - Surmenev, R. A1 - Surmeneva, M. T1 - The impact of post manufacturing treatment of functionally graded Ti6Al4V scaffolds on their surface morphology and mechanical strength N2 - An ultrasonic vibration post-treatment procedure was suggested for additively manufac-tured lattices. The aim of the present research was to investigate mechanical properties andthe differences in mechanical behavior and fracture modes of Ti6Al4V scaffolds treated withtraditional powder recovery system (PRS) and ultrasound vibration (USV). Scanning electronmicroscopy (SEM) was used to investigate the strut surface and the fracture surface mor-phology. X-ray computed tomography (CT) was employed to evaluate the inner structure,strut dimensions, pore size, as well as the surface morphology of additively manufacturedporous scaffolds. Uniaxial compression tests were conducted to obtain elastic modulus,compressive ultimate strength and yield stress. Finite element analysis was performedfor a body-centered cubic (BCC) element-based model and for CT-based reconstructiondata, as well as for a two-zone scaffold model to evaluate stress distribution during elasticdeformation. The scaffold with PRS post treatment displayed ductile behavior, while USVtreated scaffold displayed fragile behavior. Double barrel formation of PRS treated scaffoldwas observed during deformation. Finite element analysis for the CT-based reconstructionrevealed the strong impact of surface morphology on the stress distribution in comparisonwith BCC cell model because of partially molten metal particles on the surface of struts,which usually remain unstressed. KW - Additive manufacturing KW - Electron beam melting KW - Computed tomography KW - FEM KW - Lattice structures PY - 2020 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-505960 DO - https://doi.org/10.1016/j.jmrt.2019.12.019 SN - 2238-7854 VL - 9 IS - 2 SP - 1866 EP - 1881 PB - Elsevier B.V. AN - OPUS4-50596 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Mishurova, Tatiana A1 - Sydow, B. A1 - Thiede, Tobias A1 - Sizova, I. A1 - Ulbricht, Alexander A1 - Bambach, M. A1 - Bruno, Giovanni T1 - Residual Stress and Microstructure of a Ti-6Al-4V Wire Arc Additive Manufacturing Hybrid Demonstrator N2 - Wire Arc Additive Manufacturing (WAAM) features high deposition rates and, thus, allows production of large components that are relevant for aerospace applications. However, a lot of aerospace parts are currently produced by forging or machining alone to ensure fast production and to obtain good mechanical properties; the use of these conventional process routes causes high tooling and material costs. A hybrid approach (a combination of forging and WAAM) allows making production more efficient. In this fashion, further structural or functional features can be built in any direction without using additional tools for every part. By using a combination of forging basic geometries with one tool set and adding the functional features by means of WAAM, the tool costs and material waste can be reduced compared to either completely forged or machined parts. One of the factors influencing the structural integrity of additively manufactured parts are (high) residual stresses, generated during the build process. In this study, the triaxial residual stress profiles in a hybrid WAAM part are reported, as determined by neutron diffraction. The analysis is complemented by microstructural investigations, showing a gradient of microstructure (shape and size of grains) along the part height. The highest residual stresses were found in the transition Zone (between WAAM and forged part). The total stress range showed to be lower than expected for WAAM components. This could be explained by the thermal history of the component. KW - Additive manufacturing KW - Neutron diffraction KW - Residual stress KW - Hybrid manufacturing KW - WAAM KW - Ti-6Al-4V PY - 2020 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-508245 DO - https://doi.org/10.3390/met10060701 VL - 10 IS - 6 SP - 701 PB - MDPI AN - OPUS4-50824 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mishurova, Tatiana T1 - Influence of residual stress and microstructure on mechanical performance of LPBF TI-6AL-4V N2 - Ti-6Al-4V alloy is intensively used in the aerospace industry because of its high specific strength. However, the application of Laser Powder Bed Fusion (LPBF) Ti-6Al-4V alloy for structurally critical load-bearing components is limited. One of the main limiting factors affecting the structural integrity, are manufacturing defects. Additionally, the high cooling rates associated with LPBF process result in the formation of large residual stress (RS) with complex fields. Such RS can cause cracking and geometrical distortions of the part even right after production. Also, the microstructure of LPBF Ti-6Al-4V in the as-built condition is significantly different from that of the conventionally produced alloy. All these factors affect the mechanical behavior of the material. Therefore, to improve the material performance it is important to evaluate the individual effect of RS, defects, and microstructure on fatigue life. To this aim Ti-6Al-4V LPBF material in as-built condition and subjected to different post-processing, including two heat treatments (for stress relief and microstructural modification) and Hot Isostatic Pressing (HIP, for densification), were investigated. Prior to Low Cycle Fatigue (LCF) tests at operating temperature (300°C), the microstructure (phases, crystallographic texture, and grain morphology), the mesostructure (defect shape and distribution), and subsurface RS on the LCF samples were investigated. It was found that the fatigue performance of HIPped samples is similar to that of conventionally produced Ti-6Al-4V. The tensile RS found at the surface of as-built samples decreased the fatigue life compared to heat-treated samples. Additionally, the modification of the microstructure (by heat treatment) did not affect the fatigue performance in the regime of mostly elastic strain. This shows that in the absence of tensile RS the manufacturing defects solely control the failure of LPBF components and densification has the strongest effect on the improvement of the mechanical performance. T2 - ASTM ICAM 2020 CY - Online meeting DA - 16.11.2020 KW - Additive manufacturing KW - Ti-6Al-4V KW - Computed tomography KW - Residual stress PY - 2020 AN - OPUS4-51695 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Sprengel, Maximilian A1 - Ulbricht, Alexander A1 - Evans, Alexander A1 - Kromm, Arne A1 - Sommer, Konstantin A1 - Werner, Tiago A1 - Kelleher, J. A1 - Bruno, Giovanni A1 - Kannengießer, Thomas T1 - Towards the optimization of post-laser powder bed fusion stress-relieve treatments of stainless steel 316L N2 - This study reports on the stress relaxation potential of stress-relieving heat treatments for laser powder bed fused 316L. The residual stress is monitored non-destructively using neutron diffraction before and after the heat treatment. Moreover, the evolution of the microstructure is analysed using scanning electron microscopy. The results show, that a strong relaxation of the residual stress is obtained when applying a heat treatment temperature at 900°C. However, the loss of the cellular substructure needs to be considered when applying this heat treatment strategy. KW - Residual stress KW - Additive manufacturing KW - Neutron diffraction KW - Projekt AGIL - Alterung additiv gefertigter metallischer Materialien und Komponenten PY - 2021 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-536045 DO - https://doi.org/10.1007/s11661-021-06472-6 SN - 1543-1940 VL - 52 IS - 12 SP - 5342 EP - 5356 PB - Springer CY - Boston AN - OPUS4-53604 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Nadammal, Naresh A1 - Mishurova, Tatiana A1 - Fritsch, Tobias A1 - Serrano-Munoz, Itziar A1 - Kromm, Arne A1 - Haberland, C. A1 - Portella, Pedro Dolabella A1 - Bruno, Giovanni T1 - Critical role of scan strategies on the development of microstructure, texture, and residual stresses during laser powder bed fusion additive manufacturing N2 - Laser based powder bed fusion additive manufacturing offers the flexibility to incorporate standard and userdefined scan strategies in a layer or in between the layers for the customized fabrication of metallic components. In the present study, four different scan strategies and their impact on the development of microstructure, texture, and residual stresses in laser powder bed fusion additive manufacturing of a nickel-based superalloy Inconel 718 was investigated. Light microscopy, scanning electron microscopy combined with electron backscatter diffraction, and neutron diffraction were used as the characterization tools. Strong textures with epitaxially grown columnar grains were observed along the build direction for the two individual scan strategies. Patterns depicting the respective scan strategies were visible in the build plane, which dictated the microstructure development in the other planes. An alternating strategy combining the individual strategies in the successive layers and a 67◦ rotational strategy weakened the texture by forming finer microstructural features. Von Mises equivalent stress plots revealed lower stress values and gradients, which translates as lower distortions for the alternating and rotational strategies. Overall results confirmed the scope for manipulating the microstructure, texture, and residual stresses during laser powder bed fusion additive manufacturing by effectively controlling the scan strategies. KW - Additive manufacturing KW - Laser powder bed fusion KW - Nickel-based superalloys KW - Scan strategies KW - Residual stresses KW - Microstructure and texture PY - 2021 DO - https://doi.org/10.1016/j.addma.2020.101792 VL - 38 SP - 1792 PB - Elsevier B.V. AN - OPUS4-51944 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Gunnerek, R. A1 - Soundarapandiyan, G. A1 - Mishurova, T. A1 - Schröder, J. A1 - Bruno, Giovanni A1 - Boykin, J. A1 - Diaz, A. A1 - Klement, U. A1 - Hryha, E.ON T1 - Chemical mechanical polishing of powder bed fusion – laser beam processed 316 L stainless steel N2 - Additive manufacturing via powder bed fusion – laser beam (PBF-LB) enables the fabrication of complex geometries but suffers from inherently rough surfaces and surface tensile residual stresses, both of which can compromise structural integrity, particularly under fatigue loading. To address these limitations, this study investigates chemical mechanical polishing (CMP) as a surface finishing method for improving surface quality and modifying the residual stress state in PBF-LB 316 L stainless steel. The work uniquely examines how scan rotation (0◦ vs. 67◦ rotation) and contour parameters influence CMP effectiveness in material removal, surface smoothing, and subsurface stress redistribution. With a targeted material removal of 110 μm, CMP reduced surface roughness (Sa) by up to 94 %, achieving values as low as 0.7 μm. Microstructural analysis revealed no grain refinement but identified a thin, plastically deformed surface layer. This plastic deformation resulted in the transformation of tensile surface stresses (340 MPa) into beneficial compressive stresses (􀀀 400 MPa), as confirmed by synchrotron X-ray diffraction, which also showed a shift toward isotropic strain distribution. Further, these findings demonstrate that the initial scan strategy influences CMP performance and that CMP can enhance both surface integrity and mechanical reliability without altering the underlying microstructure. This study advances the understanding of how process induced microstructure and surface features affect CMP outcomes, enabling more informed design of post-processing strategies for improved surface integrity and mechanical performance in additively manufactured metals. KW - Residual stress KW - Additive manufacturing KW - Chemical mechanical polishing KW - As-built microstructure KW - Surface roughness KW - Surface finishing KW - Material removal PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-640522 DO - https://doi.org/10.1016/j.jmatprotec.2025.119055 SN - 0924-0136/ VL - 345 SP - 1 EP - 12 PB - Elsevier B.V. AN - OPUS4-64052 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ávila Calderón, Luis T1 - Creep and fracture behavior of conventionally and additively manufactured stainless steel 316L N2 - A critical task within the frame of establishing process-structure-property-performance relationships in additive manufacturing (AM) of metals is producing reliable and well-documented material behavior’s data and knowledge regarding the structure-property correlation, including the role of defects. After all, it represents the basis for developing more targeted process optimizations and more reliable predictions of performance in the future. Within this context, this contribution aims to close the actual gap of limited historical data and knowledge concerning the creep behavior of the widely used austenitic stainless steel 316L, manufactured by Laser-Powder-Bed-Fusion (L-PBF). To address this objective, specimens from conventional hot-rolled and AM material were tested under application-relevant conditions according to existing standards for conventional material, and microstructurally characterized before and after failure. The test specimens were machined from single blocks from the AM material. The blocks were manufactured using a standard scan and build-up strategy and were subsequently heat-treated. The creep behavior is described and comparatively assessed based on the creep lifetime and selected creep curves and characteristic values. The effect of defects and microstructure on the material’s behavior is analyzed based on destructive and non-destructive evaluations on selected specimens. The AM material shows shorter creep lives, reaches the secondary creep stage much faster and at a lower strain, and features lower creep ductility compared to its conventional counterpart. The creep damage behavior of the AM material is more microstructure than defect controlled and is characterized by the formation and accumulation of single intergranular damage along the whole volume. Critical features identified are the grain morphology and the grain-boundary as well as the dislocation’s density. Micro-computed tomography (µCT) proves to be an alternative to metallography to analyze the creep damage. T2 - ASTM International Conference on Additive Manufacturing 2020 CY - Online meeting DA - 16.11.2020 KW - 316L KW - Creep behavior KW - Laser powder bed fusion KW - Additive manufacturing KW - Microstructure PY - 2020 AN - OPUS4-51823 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ávila Calderón, Luis T1 - Assessing the low cycle fatigue behaviour of additively manufactured Ti-6Al-4V: Challenges and first results N2 - The understanding of process-microstructure-property-performance (PMPP) relationships in additive manufacturing (AM) of metals is highly necessary to achieve wide-spread industrial application and replace conventionally manufactured parts, especially regarding safety-relevant applications. To achieve this understanding, reliable data and knowledge regarding material’s microstructure-property relationships (e.g. the role of defects) is needed, since it represents the base for future more targeted process optimizations and more reliable calculations of performance. However, producing reliable material data and assessing the AM material behaviour is not an easy task: big challenges are e.g. the actual lack of standard testing methods for AM materials and the occasional difficulties in finding one-to-one comparable material data for the conventional counterpart. This work aims to contribute to end this lack of reliable material data and knowledge for the low cycle fatigue behaviour of the most used titanium alloy in aerospace applications (Ti-6Al-4V). For this purpose, two sets of test specimens were investigated. The first set was manufactured from cylindrical rods produced by an optimized DED-L process and the second was manufactured from a hot formed round bar. The test specimens were cyclically loaded until failure in the low-cycle-fatigue (LCF) regime. The tests were carried out according to ISO 12106 between 0.3 to 1.0 % axial strain amplitude from room temperature up to 400°C. The LCF behaviour is described and compared between materials and with literature values based on cyclic deformation curves and strain-based fatigue life curves. Besides, the parameters of Manson-Coffin-Basquin relationship were calculated. The microstructures (initial and after failure) and fracture surfaces were comparative characterized. Thereby, the focus lied on understanding the role of grain morphology and defects on the failure mechanisms and fatigue lifetimes. For this latter characterization, optical microscopy (OM), scanning electron microscopy (SEM) and micro computed tomography (µCT) were used. T2 - 4th International Symposium on Fatigue Design and Material Defects CY - Online meeting DA - 26.05.2020 KW - Ti-6Al-4V KW - Additive manufacturing KW - Low cycle fatigue KW - Micro computed tomography KW - Microstructure PY - 2020 AN - OPUS4-50893 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Voloskov, Boris A1 - Mishurova, Tatiana A1 - Evlashin, Stanislav A1 - Bruno, Giovanni A1 - Sergeichev, Ivan T1 - Influence of artificial and process-induced defects on very high cycle fatigue characteristics of 316L stainless steel produced by laser powder bed fusion N2 - This study investigates the impact of artificially embedded defects on the very high cycle fatigue (VHCF) of 316L stainless steel produced by laser powder bed fusion (PBF-LB) technology. Each specimen contains a single embedded artificial defect of 180 μm or 350 μm in diameter, positioned at specific distances from the surface (ranging from 350 μm to 1200 μm). The defect position and size are quantified by X-ray computed tomography. Following VHCF testing, the fracture surfaces of the specimens are examined using scanning electron microscopy (SEM) and transmission electron microscopy (TEM) with electron diffraction analysis. The results demonstrate that the fracture surfaces predominantly display a fish-eye fracture type, with a fine granular area (FGA) surrounding the internal defects, typical for VHCF. The FGAs dimensions including thickness are estimated by means of microscopy analysis. However, despite the presence of relatively large artificial defects, cracks sometimes initiate from much smaller process-induced defects closer to the surface than the artificial ones. In conclusion, our study quantifies the relationship between the probability of crack initiation from artificial defects and the distance of the artificial defect from the specimen’s surface. KW - Additive manufacturing KW - X-ray CT KW - Porosity PY - 2025 DO - https://doi.org/10.1016/j.msea.2024.147571 VL - 920 SP - 1 EP - 13 PB - Elsevier B.V. AN - OPUS4-62117 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Dudziak, Mateusz A1 - Topolniak, Ievgeniia A1 - Silbernagl, Dorothee A1 - Altmann, Korinna A1 - Sturm, Heinz T1 - Long-time behavior of surface properties of microstructures fabricated by multiphoton lithography N2 - The multiphoton lithography (MPL) technique represents the future of 3D microprinting, enabling the production of complex microscale objects with high precision. Although the MPL fabrication parameters are widely evaluated and discussed, not much attention has been given to the microscopic properties of 3D objects with respect to their surface properties and time-dependent stability. These properties are of crucial importance when it comes to the safe and durable use of these structures in biomedical applications. In this work, we investigate the surface properties of the MPL-produced SZ2080 polymeric microstructures with regard to the physical aging processes during the post-production stage. The influence of aging on the polymeric microstructures was investigated by means of Atomic Force Microscopy (AFM) and X-ray Photoelectron Spectroscopy (XPS). As a result, a time-dependent change in Young’s Modulus, plastic deformation, and adhesion and their correlation to the development in chemical composition of the surface of MPL-microstructures are evaluated. The results presented here are valuable for the application of MPL-fabricated 3D objects in general, but especially in medical technology as they give detailed information of the physical and chemical time-dependent dynamic behavior of MPL-printed surfaces and thus their suitability and performance in biological systems. KW - Multiphoton lithography KW - Additive manufacturing KW - Microfabrication KW - SZ2080 negative photo-resist KW - Young´s modulus KW - Aging KW - Surface properties KW - X-ray photoelectron spectroscopy KW - Atomic force microscopy KW - Force-distance-curve PY - 2021 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-542166 DO - https://doi.org/10.3390/nano11123285 SN - 2079-4991 VL - 11 IS - 12 SP - 1 EP - 12 PB - MDPI CY - Basel AN - OPUS4-54216 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Agudo Jácome, Leonardo T1 - Low-Cycle Fatigue Behavior of Laser Powder Bed Fused Inconel 718 at Room and High Temperature N2 - The nickel-base superalloy Inconel 718 (IN718) is one of the most commonly used Ni-based superalloys for high temperature structural applications for its remarkable strength, as well as creep, fatigue, and corrosion resistance up to 650 °C. While IN718 has traditionally been employed as cast or wrought material, it is difficult to machine because of its high strength and toughness. The additive manufacturing of IN718 components made by metal AM has thus gained extensive attention to produce expensive near-net shaped components of high-temperature alloys such as IN718, for it saves material and costs in processing and machining steps. Among all metal additive manufacturing (AM) technologies, laser powder bed fusion (PBF-LB/M) is the most widespread, IN718 being one of the most common alloys produced with it. However, high cooling rates associated to the PBF-LB/M process, hinders the primary strengthening phases γ’’ and γ’ to form, as these cooling rates induce a dislocation cellular substructure, at which walls primary Laves phases bind segregating Nb, Ti and Mo. Many of the therefore needed heat-treatment strategies can then promote Laves-phase transformation into the stable δ phase along the cell and grain boundaries. Laves and δ phases, as well as grain-boundary primary carbides may have adverse effects on mechanical properties. The mostly needle-shaped δ phase was namely found to have a detrimental effect on creep rupture life while no direct effect on LCF fatigue life was evident. In this work room- and high-temperature (650 °C) low-cycle fatigue behavior of PBF-LB/M IN718 is investigated in the four-step heat-treated state and compared to wrought IN718. The microstructure of both materials is characterized across length scales via microscopy methods. The fatigue life at room temperature of the PBF-LB/M IN718 material is slightly lower than that for the wrought material, which is reversed at 650 °C. The cyclic stress response for both materials is marked by cyclic softening that is more pronounced at higher test temperatures. Multiple secondary cracks form at high strain amplitudes, at both room and high temperatures. High testing temperatures enhance specially crack formation at the transitions of regions between elongated grains and columns of stacked grains with ripple patterns in the PBF-LB/M material. Additional to this behavior, pronounced crack branching and deflection indicate that the cracks are controlled by sharp micromechanical gradients. T2 - EUROMAT 2025 CY - Granada, Spain DA - 14.09.2025 KW - Additive manufacturing KW - Low-cycle fatigue KW - Microstructural characterization KW - Ni-base superalloy PY - 2025 AN - OPUS4-64354 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Witte, Julien A1 - Treutler, Kai A1 - Schroepfer, Dirk A1 - Kannengiesser, Thomas A1 - Wesling, Volker T1 - Influence of microstructure on the machinability and surface integrity of additively manufactured iron aluminides N2 - The increasing global focus on energy and resource efficiency has stimulated a growing interest in additive manufacturing. AM offers economic advantages and enables an efficient use of materials. However, AM components often require subsequent mechanical post-processing, such as machining (e.g., milling), to achieve the final contours or surfaces. This is a particular challenge due to the heterogeneous and anisotropic nature of AM structures, which affect machining and the resulting component properties. High-performance materials such as iron aluminide represent a promising alternative to conventional high-temperature materials with a significant economic advantage. However, the strength and hardness properties, which are advantageous for applications in highly stressed lightweight components, pose a challenge for economical machining in addition to the AM microstructure properties. The difficult-to-cut material causes accelerated tool wear and insufficient surface quality. This study shows that crack-free additive manufacturing of the three-component system of iron-nickel-aluminum is possible, and advantages in terms of machinability compared to FeAl-AM components are achieved. The more homogeneous microstructure leads to a reduction in cutting forces, with positive effects on the machinability and optimized surface integrity. Ultrasonic assisted milling (USAM) offers great potential to address the major challenges posed by difficult-to-cut materials and additively manufactured weld structures. Therefore, this study focuses on assessing the transferability of previous positive results by USAM to the selected iron aluminide alloys. The machinability of the aluminides is analyzed by varying significant influencing variables in finish milling experiments and evaluated in terms of the loads on the tool and the resulting surface integrity. KW - Iron aluminide KW - Additive manufacturing KW - Machinability KW - Surface integrity KW - Ultrasonic-assisted milling process PY - 2026 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-656993 DO - https://doi.org/10.1007/s40194-026-02382-6 SN - 0043-2288 SP - 1 EP - 13 PB - Springer Science and Business Media LLC AN - OPUS4-65699 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -