TY - JOUR A1 - Lengas, Nikolaos A1 - Schlick-Hasper, Eva A1 - Müller, Karsten A1 - Neitsch, Marcel A1 - Johann, Sergej A1 - Zehn, M. T1 - Development of an analysis and testing concept for the evaluation of impact targets in the mechanical safety testing of dangerous goods packagings N2 - The mechanical and geometrical properties of impact targets greatly influence the outcome of a drop test. The International Agreement concerning the International Carriage of Dangerous Goods by Road (ADR) as well as ISO 2248 describe the characteristics of impact targets for drop tests of dangerous goods packagings. According to these regulations, the impact target’s surface needs to be unyielding, under testing conditions non-deformable, flat, and integral with a mass at least 50 times that of the heaviest packaging to be tested. The problem is that many production facilities, especially manufacturers of corrugated fibreboard boxes, do not have their own testing device with the required 50 times mass ratio of the impact target for a regulation compliant drop test during series production. Furthermore, at UN level it is considered necessary to revise these requirements. In the present paper, the impact target requirements are examined in detail and compared with those in other technical areas (e.g., impact target for container for the transport of radioactive materials). A research method is being developed to investigate the dependency between the mass ratio of the packaging and the target as well as the damage resistance of a drop tested package in relation to specific design characteristics. The results are of high relevance for industry purposes and intended to ensure a uniform level of safety assessment for the mechanical testing of dangerous goods packagings. KW - Corrugated fibreboard boxes KW - Dangerous goods packagings KW - Drop test KW - Impact target KW - Structural dynamics PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-549660 DO - https://doi.org/10.1002/pts.2656 SN - 0894-3214 SN - 1099-1522 VL - 35 IS - 9 SP - 689 EP - 700 PB - Wiley CY - New York, NY AN - OPUS4-54966 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Savidis, S. A1 - Bergmann, M. A1 - Schepers, Winfried A1 - Fontara, I.-K. T1 - Wave propagation in inhomogeneous media via FE/PML method N2 - The Perfectly Matched Layer (PML) method is an efficient approach to imposing radiation conditions at the bounded region of interest in case of wave propagation in unbounded domains. This paper presents and validates 3D FE/PML numerical schemes based on two different PML formulations for homogeneous and inhomogeneous geological media exhibiting discrete or continuous inhomogeneity. In the equation of motion for the PML domain the applied stretching behavior is expressed either as complex material properties or as complex coordinates. Both PML formulations are implemented in the FEM and verified against analytical solutions. Three different types of material inhomogeneity are considered: layered half-space, continuously inhomogeneous half-space with linear velocity profile and continuously inhomogeneous half-space with nonlinear velocity profile. Sensitivity analyses are conducted, and the performance of the developed numerical schemes is investigated taking into account a broad variation of the PML parameters. Recommendations are given for the optimal values of the PML parameters for the case of homogeneous and inhomogeneous geological media. KW - Perfectly Matched Layer (PML) KW - Unbounded domain KW - Finite elements KW - Continuously inhomogeneous geological media PY - 2022 DO - https://doi.org/10.1002/gete.202100028 VL - 45 IS - 2 SP - 98 EP - 107 PB - Ernst & Sohn CY - Berlin AN - OPUS4-54969 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wu, Dejian A1 - Schmidt, Martin A1 - Huang, W. A1 - Wei, A. A1 - Krause, U. A1 - Wu, W. T1 - Inhibition effect of N2/CO2 blends on the minimum explosion concentration of agriculture and coal dusts N2 - Minimum explosion concentration (MEC) of three agriculture dusts and two coal dusts was studied via a 20-L explosion chamber to reveal the role of gaseous inhibitors. Both active method (CO2 diluting air) and passive method (CO2 replacing O2) were used. The TG and DTG thermal analysis tests were conducted to study the pyrolysis and combustion characteristics of dust samples. An alternative explosion criterion based on combustion duration time was used to determine MEC, and compared with the standardized overpressure method. Under 10-kJ ignition condition, as oxygen mole fraction (XO2) decreased from 21% to 10%, MEC of agriculture dusts and coal dusts respectively increased by around 5 times and 2 times. The active inerting method with a lower N2/CO2 ratio was found to have a better suppression effect on the explosion of the five carbonaceous dusts because the blend has a higher specific heat and a lower oxygen diffusion rate. KW - CO2/N2 ratio KW - Explosion criterion KW - Combustion kinetics KW - Inerting effect KW - Explosion characteristics PY - 2022 DO - https://doi.org/10.1016/j.powtec.2022.117195 SN - 0032-5910 VL - 399 SP - 1 EP - 12 PB - Elsevier B.V. AN - OPUS4-55013 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kruschwitz, Sabine A1 - Munsch, Sarah T1 - Potential automatisierter NMR-Messungen zur Ermittlung von Hydratationseigenschaften - ein Vergleich mit Vicat- und Wärmeflusskalorimetrie-Ergebnissen N2 - Es werden Ergebnisse von 1H-NMR-Relaxometrie-Messungen an Salzbeton und einem alkali-aktivierten Material, die im Rahmen des Themenfeldprojektes Seal Waste Safe durchgeführt werden, vorgestellt. Dabei wird die zeitliche Entwicklung von ausgewählten Merkmalen der ermittelten T2-Relaxationszeitenverteilungen während der Hydratation betrachtet. Als Referenz zur Identifikation von charakteristischen Hydratationsereignissen dienen der Vicat-Nadeleindringversuch und Wärmeflusskalorimetrie. T2 - Online-Workshop „Dauerhafte Verschlussbauwerke für Endlager“ CY - Online meeting DA - 14.02.2022 KW - NMR-Relaxometrie KW - Alkali-aktiviertes Material KW - Salzbeton KW - Seal Waste Safe PY - 2022 AN - OPUS4-54945 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Weise, Frank A1 - von Werder, Julia A1 - Manninger, Tanja A1 - Maier, Bärbel A1 - Fladt, Matthias A1 - Simon, Sebastian A1 - Gardei, Andre A1 - Höhnel, Desirée A1 - Pirskawetz, Stephan A1 - Meng, Birgit T1 - A multiscale and multimethod approach to assess and mitigate concrete damage due to alkali-silica reaction N2 - Alkali-silica reaction (ASR) is a chemical reaction within concrete which can lead over time to cracking and spalling. Due to the complexity of the problem, it still causes damage to concrete constructions worldwide. The publication aims to illustrate the interdisciplinary research of the German Federal Institute for Materials Research and Testing (BAM) within the last 20 years, considering all aspects of ASR topics from the macro to the micro level. First, methods for characterization and assessment of ASR risks and reaction products used at BAM are explained and classified in the international context. Subsequently the added value of the research approach by combining different, preferably nondestructive, methods across all scales is explained using specific examples from a variety of research projects. Aspects covered range from the development of new test-setups to assess aggregate reactivity, to analysis of microstructure and reaction products using microscopical, spectroscopical and X-ray methods, to the development of a testing methodology for existing concrete pavements including in-depth analysis of the visual damage indicator and the de-icing salt input using innovative testing techniques. Finally, research regarding a novel avoidance strategy that makes use of internal hydrophobization of the concrete mix is presented. KW - Mitigation strategies KW - Concrete KW - Damage analysis KW - Alkali silica reaction KW - Road pavement KW - Accelerated testing KW - Non-destructive testing KW - Microstructure PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:101:1-2022052515100075090235 DO - https://doi.org/10.1002/adem.202101346 SN - 1527-2648 VL - 24 IS - 6 SP - 1 EP - 36 PB - Wiley-VCH CY - Weinheim AN - OPUS4-54951 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Weise, Frank A1 - Hüsken, Götz T1 - Ringversuch zum statischen Spaltzugversuch nach AL Sp-Beton N2 - Für die rechnerische Dimensionierung der Betondecken im Oberbau von Verkehrsflächen für den Neubau sowie die Erneuerung nach RDO-Beton 09 ist die statische Spaltzugfestigkeit an der unteren und oberen Bohrkernscheibe entsprechend der Vorgaben der AL Sp-Beton zu bestimmen. Aufgrund der unzureichenden Kenntnis der Präzision dieses Prüfverfahrens wurden, basierend auf dem Entwurf des FGSV-Merkblatts zur statistischen Auswertung von Prüfergebnissen, mit einem breit aufgestellten Ringversuch die statistischen Kennwerte an Labor- und Bestandsbetonen unter Vergleich- und Wiederholbedingungen ermittelt. Zur möglichst guten statistischen Absicherung nahmen an dem Ringversuch dreizehn erfahrene Prüfstellen teil, die vorab einem Audit unterzogen wurden. Zur Abdeckung des vielschichtigen Einsatzes des Prüfverfahrens erfolgte der Ringversuch an acht Prüflosen, die sowohl die Erst-/ Eignungsprüfung und Übereinstimmungskontrolle bei Neubaumaßnahmen, als auch die Restsubstanzbewertung von Betonfahrbahnplatten berücksichtigen. Zur Bewertung des Materialeinflusses wurde zusätzlich ein Prüflos mit Labormörtel untersucht. Die Probenvorbereitung erfolgte zentral an der BAM. Zur Sicherstellung einheitlicher Prüfbedingungen bei den Prüfstellen wurde zusätzlich eine detaillierte Standardarbeitsanweisung erarbeitet, die partiell bereits Eingang in das Normenwerk gefunden hat. Bei der Plausibilitätsprüfung aller prüflosspezifischen Einzelwerte der Spaltzug- und Druckfestigkeit wurden vereinzelt sowohl Ausführungsfehler als auch Übertragungs- und Tippfehler festgestellt. Der sich anschließende Lilliefors-Test zeigt, dass die ermittelten Einzelwerte bis auf wenige Aus-nahmen normalverteilt sind und damit die Voraussetzungen für die statistische Auswertung gegeben sind. Mittels grafischer Darstellung der Mandel’s h- und k-Werte wurden die Auffälligkeiten hinsichtlich der Mittelwerte und Varianzen prüflosspezifisch für die einzelnen Prüfstellen visualisiert und anschließend einige von ihnen mittels Grubbs- und Cochran-Test als Ausreißer identifiziert. Nach Ausreißerelimination wurde mit dem klassischen Verfahren bei der Spaltzugfestigkeit der geringste Variationskoeffizient unter Vergleich- und Wiederholbedingungen bei der Erst-/Eignungsprüfung mit 6,2 und 6,4 Prozent ermittelt. Bei einer Verminderung des Materialeinflusses durch die Verwendung eines Labormörtels verbessern sich die statistischen Kennwerte auf 4,5 und 5,3 Prozent. Mit 8,2 und 9,5 Prozent beziehungsweise 8,6 und 9,5 Prozent werden bei der Restsubstanzbewertung von Wasch- und Unterbetonen die höchsten Werte bestimmt. Das robuste Auswerteverfahren (ohne Eliminierung der Ausreißer) nach dem Entwurf des FGSV-Merkblatts zur statistischen Auswertung von Prüfergebnissen erwies sich in der Form als ungeeignet und bedurfte einer Überarbeitung. Bezüglich der vergleichend mit klassischen und robusten Verfahren gewonnenen Kennwerte ist festzustellen, dass bei sehr homogenen Messergebnissen eines Prüfloses beide Verfahren nahezu die gleichen statistischen Kennwerte liefern. Bei der Eliminierung von Ausreißern sind die Ergebnisse des robusten Verfahrens in der Regel etwas größer als die des klassischen Verfahrens. Die begleitenden vertiefenden Untersuchungen bei der Spaltzugprüfung mit innovativen Prüftechniken lieferten wertvolle Erkenntnisse zur Bewertung der Prüfeinflüsse. N2 - The computational design of concrete pavements according to the requirements of the RDO-Beton 09 requires the splitting tensile strength to be determined according to specifications of the AL Sp-Beton. However, detailed information on the precision of the described test procedure is missing. Therefore, a round robin test was set up in order to determine the statistical parameters of the prescribed splitting tensile strength test on laboratory concrete and cores extracted from concrete pavements in terms of repeatability and reproducibility. 13 testing institutes have been involved in the round robin test to guarantee a representative coverage of the sector. The selected testing institutes have been audited prior the round robin test in order to ensure their capabilities. The round robin test was divided into 8 testing lots for covering the broad field of possible applications. Thereby, the testing lots cover both the initial testing of concrete and quality control of new construction. The latter case implies also the assessment of existing concrete pavements. Additionally, a cementitious mortar was designed in order to consider the influence of the material, such as maximum grain size, on the test procedure. The samples were prepared at BAM to guarantee a uniform sample preparation. Furthermore, a standard operating procedure was prepared to assure constant test conditions at the testing institutes. This standard operating procedure is already partly considered by the corresponding standard. A revision of the data reported by the testing institutes revealed that execution errors, transcription errors as well as typing errors occurred. However, a Lilliefors-Test was conducted to verify the Gaussian distribution of the reported test data and to allow the further statistical analysis. Only view data sets do not follow a Gaussian distribution, has no remarkable influence on the obtained statistical data. By means of the graphical illustration of Mandel’s h- and k-values, abnormalities of the arithmetic mean and variance are depicted. These apparent abnormalities can be identified as outliers using the Grubbs and Cochran test. After eliminating the identified outliers, the corresponding statistical parameters have been determined using the classical method for data analysis. The lowest coefficient of variation that was determined for the splitting tensile strength by using the classical method for assessment of the repeatability and reproducibility of the test procedure amounts to 6.2 and 6.4%, respectively, for the initial testing of concrete. Reducing the material influence by using a cementitious mortar, the corresponding statistical parameters were reduced to 4.5 and 5.3%. On the contrary, the highest statistical values were obtained for the assessment of existing concrete pavements. Here, values of 8.2 and 9.5% were obtained for the exposed aggregate concrete and 8.6 and 9.5% for the subconcrete, respectively. The robust method for data analysis (without elimination of outliers) according to the draft version of the technical bulletin of the FGSV turned out to be inappropriate and required, therefore, a revision. Comparing the statistical parameters obtained by the classical and robust method used for data analysis it can be stated that both methods result in nearly identical values for homogeneous data sets without outliers. Considering outliers in the existing data sets, the statistical parameters obtained by the robust method are slightly higher than the values obtained by the classical method with elimination of outliers. The additional investigations on the splitting tensile strength using innovative test procedures provided valuable findings for the assessment of test results. KW - Verfahrenspräzision KW - Betonfahrbahndecke KW - Prüfverfahren AL Sp-Beton KW - Spaltzugfestigkeit KW - Ringversuch PY - 2022 SN - 978-3-95606-688-7 SN - 0943-9323 VL - Straßenbau Heft S 178 SP - 1 EP - 90 PB - Fachverlag NW in der Carl Ed. Schünemann KG CY - Bremen AN - OPUS4-54957 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Auersch, Lutz T1 - The role of vehicle dynamics in train-induced ground vibrations and the detection of irregular axle-pulse responses due to a varying track support stiffness N2 - Train-induced ground vibrations are all generated by the vehicle, by static or dynamic vehicle loads. The most important and most accepted excitation are the dynamic wheel loads from the passage over track irregularities. Dynamic wheel loads will be compared from parallel axle-box and ground vibration measurements at more than seven sites. Some low-frequency excitation of ground vibrations, typically between 10 and 30 Hz, cannot be found in the axle-box measurements. Therefore, other vehicle modes, such as rigid bogie modes, flexible carriage modes, rigid and flexible wheelset modes, have been analysed for additional excitation forces. These vehicle dynamics analyses give an explanation for higher axle-box results at high frequencies, but not for the excitation of the higher low-frequency ground-vibration component. Finally, the effect of the moving static train loads will be analysed. For a regular track and soil, the moving static train loads yield the quasi-static response which exists only in the low-frequency nearfield of the track. If the support stiffness is randomly varying along the track, the pulses on the track generate an additional low-frequency component which is called the irregular pulse responses. This component will be demonstrated by numerical analysis where all axle pulses are superposed in frequency domain. KW - Wheelset KW - Vehicle-track interaction KW - Rail roughness KW - Random dynamics and vibrations KW - Modal analysis PY - 2022 DO - https://doi.org/10.1177/09544097221086064 SN - 0954-4097 VL - 236 IS - 10 SP - 1218 EP - 1233 PB - Sage CY - London AN - OPUS4-55000 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Spitzer, Stefan A1 - Jankuj, V. A1 - Krietsch, Arne T1 - Comparative Study on Standardized Ignition Sources Part 2: Exploration of the Initial Igniting Volume of Standardized Ignition Sources for the Determination of Explosion Characteristics N2 - There are several standardized ignition sources in use for the determination of explosion characteristics of gases, vapors and dusts. In the standards the ignition source is stated, but they vary in stating other characteristics like burning duration, energy or burning volume. Since heat is not visible under normal circumstances a Schlieren-Technique was used to make the full heating volume and not just the flames visible. While an earlier paper of the authors focused on the ignition energy and burning duration of four standardized ignition sources, this paper focuses on the initial igniting volume, the ratio between initial igniting volume and the test-vessel size and other phenomena that were observed with the Schlieren-Technique-. T2 - Loss Prevention CY - Prag, Czechia DA - 06.06.2022 KW - Ignition source KW - Hybrid Mixtures KW - 20L-sphere PY - 2022 DO - https://doi.org/10.3303/CET2290087 SN - 2283-9216 VL - 2022 IS - 90 SP - 517 EP - 522 PB - AIDIC CY - Milano AN - OPUS4-55028 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Spitzer, Stefan T1 - Comparative Study on Standardized Ignition Sources Part 2: Exploration of the Initial Igniting Volume of Standardized Ignition Sources for the Determination of Explosion Characteristics N2 - There are several standardized ignition sources in use for the determination of explosion characteristics of gases, vapors and dusts. In the standards the ignition source is stated, but they vary in stating other characteristics like burning duration, energy or burning volume. Since heat is not visible under normal circumstances a Schlieren-Technique was used to make the full heating volume and not just the flames visible. While an earlier paper of the authors focused on the ignition energy and burning duration of four standardized ignition sources, this paper focuses on the initial igniting volume, the ratio between initial igniting volume and the test-vessel size and other phenomena that were observed with the Schlieren-Technique. T2 - Loss Prevention CY - Prague, Czech Republic DA - 06.06.2022 KW - Ignition source KW - Hybrid Mixtures KW - 20L-sphere PY - 2022 AN - OPUS4-55029 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schepers, Winfried A1 - Kulke, D. T1 - Ermittlung dynamischer Bodensteifigkeit aus konventionellen geotechnischen Berichten N2 - Am Beispiel von mehreren Bauvorhaben wird untersucht, mit welchen Unsicherheiten bei der Anwendung von Korrelationen zwischen Sondierergebnissen und Scherwellengeschwindigkeit zur Beschreibung der dynamischen Bodeneigenschaften gerechnet werden muss. Die Auswertung von Korrelationen aus der Literatur zur Abschätzung der Scherwellengeschwindigkeit aus Drucksondierdaten zeigt, dass bei homogenen Sandböden die Verteilung der Scherwellengeschwindigkeit über die Tiefe sehr gut wiedergegeben werden kann. Die Korrelationen haben dabei die Tendenz, den tatsächlichen Wert zu überschätzen. In den vorliegenden Fällen haben sich Überschätzungen zwischen 20 % und 50 % ergeben. Mit zunehmendem Feinkornanteil werden die Unsicherheiten aus den Korrelationen jedoch größer. T2 - 7. VDI-Fachtagung Baudynamik CY - Würzburg, Germany DA - 27.04.2022 KW - Dynamische Bodensteifigkeit PY - 2022 SN - 978-3-18-092379-6 SN - 0083-5560 VL - 2379 SP - 347 EP - 359 PB - VDI-Verlag CY - Düsseldorf AN - OPUS4-54762 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Auersch, Lutz T1 - Wellenausbreitung und Pfähle im inhomogenen Boden – Gesetzmäßigkeiten für die Gründung von Windenergieanlagen und für die Prognose von Bahnerschütterungen aus Tunneln N2 - Es wird eine gekoppelte Finite-Element-Randelementmethode zur Berechnung von Pfahlgrün-dungen in inhomogenen (geschichteten) Böden vorgestellt. Sie beruht auf den Greenschen Funktionen (Punktlastlösungen) für inhomogene Böden. Diese Lösungen können auch für die Wellenausbreitung in der Tiefe, zum Beispiel von einem Bahntunnel zu einem eingebetteten Gebäude, dem Kellergeschoss benutzt werden. Die Punktlastlösungen in der Tiefe werden mit der Halbraumlösung an der Bodenoberfläche und mit der Vollraumlösung verglichen und Gesetzmäßigkeiten für geschichtete Böden abgeleitet. Zu den Pfahlgründungen werden die Horizontalnachgiebigkeiten von Pfählen in geschichteten Böden dargestellt. Für den homogenen und den kontinuierlich steifer werdenden Boden werden Potenzgesetze für den Boden- und Pfahleinfluss aufgestellt. Der Vergleich mit dem Winkler-Modell der rein lokalen Bodenreaktion zeigt, dass die Winkler-Bettung in allen Fällen einen zu kleinen Bodeneinfluss ergibt. T2 - 7. VDI-Fachtagung Baudynamik CY - Würzburg, Germany DA - 27.04.2022 KW - Wellenausbreitung in der Tiefe KW - Nachgiebigkeiten KW - Windenergieanlagen PY - 2022 SN - 978-1-18-092379-6 SN - 0083-5560 VL - 2379 SP - 697 EP - 706 PB - VDI-Verlag CY - Düsseldorf AN - OPUS4-54768 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Auersch, Lutz T1 - Wellenausbreitung und Pfähle im inhomogenen Boden – Gesetzmäßigkeiten für die Gründung von Windenergieanlagen und für die Prognose von Bahnerschütterungen aus Tunneln N2 - Es wird eine gekoppelte Finite-Element-Randelementmethode zur Berechnung von Pfahlgrün-dungen in inhomogenen (geschichteten) Böden vorgestellt. Sie beruht auf den Greenschen Funktionen (Punktlastlösungen) für inhomogene Böden. Diese Lösungen können auch für die Wellenausbreitung in der Tiefe, zum Beispiel von einem Bahntunnel zu einem eingebetteten Gebäude, dem Kellergeschoss benutzt werden. Die Punktlastlösungen in der Tiefe werden mit der Halbraumlösung an der Bodenoberfläche und mit der Vollraumlösung verglichen und Gesetzmäßigkeiten für geschichtete Böden abgeleitet. Zu den Pfahlgründungen werden die Horizontalnachgiebigkeiten von Pfählen in geschichteten Böden dargestellt. Für den homoge-nen und den kontinuierlich steifer werdenden Boden werden Potenzgesetze für den Boden- und Pfahleinfluss aufgestellt. Der Vergleich mit dem Winkler-Modell der rein lokalen Boden-reaktion zeigt, dass die Winkler-Bettung in allen Fällen einen zu kleinen Bodeneinfluss ergibt. T2 - 7. VDI-Fachtagung Baudynamik CY - Würzburg, Germany DA - 27.4.2022 KW - Wellenausbreitung in der Tiefe KW - Pfahlnachgiebigkeiten KW - Erschütterungen KW - Tunnel PY - 2022 AN - OPUS4-54769 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Lu, Xin A1 - Chruscicki, Sebastian A1 - Schukar, Marcus A1 - Münzenberger, Sven A1 - Krebber, Katerina T1 - Application of Intensity-Based Coherent Optical Time Domain Reflectometry to Bridge Monitoring N2 - Although distributed fiber sensing techniques have been widely used in structural health monitoring, the measurement results of bridge monitoring, particularly under destructive testing, have rarely been reported. To the best of our knowledge, this paper is the first report of distributed vibration measurement results, which we obtained during a three-day destructive test on an abolished bridge. A coherent optical time domain reflectometry (COTDR) was used to acquire the vibration information while the bridge was being sawed. The obtained signal was analyzed in time and frequency domain. Some characteristics of the sawing-induced vibration were retrieved by the short-time Fourier transform; the vibration exhibited several high frequency components within the measured range up to 20 kHz and all the components appeared in the same time slot. Some unexpected signals were also detected. Thorough analysis showed that they are quite different from the sawing-induced vibration and are believed to originate from internal damage to the bridge (probably the occurrence of cracks). KW - Destructive testing KW - Structural health monitoring KW - Distributed fiber sensing KW - Distributed acoustic sensing PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-547451 DO - https://doi.org/10.3390/s22093434 VL - 22 IS - 9 SP - 3434 PB - MDPI AN - OPUS4-54745 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Michalchuk, Adam A1 - Morrison, C. T1 - From lattice vibrations to molecular dissociation N2 - The ease with which an energetic material can be initiated by mechanical impact is a critical parameter directing material safety and application. While impact sensitivity metrics are traditionally derived experimentally, recent developments have highlighted that the phenomenon is amenable to first principles simulation. In this chapter, we will outline a fully ab initio approach to predict the relative impact sensitivities of energetic materials based on the mechanochemical principles that link the impact event to vibrational energy transfer. This mechanism is key to rationalizing how a mechanical impact—which deposits energy into the low-frequency lattice vibrations—results in a molecular response. By simulating the vibrational energy levels (the so-called phonon density of states, PDOS) using first-principles computational methods (typically dispersion-corrected plane-wave density functional theory, PW-DFT) we can calculate the relative rate of energy propagation from the delocalized low-energy lattice vibrations through to the localized molecular modes. The latter traps the energy, which eventually results in bond rupture through heightened vibrational excitation. This method, based on vibrational up-pumping, offers a route toward predicting the impact sensitivities of a broad range of energetic materials, provided the crystal structure of the compound (or salt or co-crystal) is known. While it does not offer insight into the sensitizing roles undoubtedly played by crystal defects or grain boundaries, it does provide a level of understanding at the molecular and crystal packing levels. Correspondingly, this approach offers a feedback mechanism to chemists and materials scientists to guide the design of new materials with desired impact sensitivity behavior. KW - Energetic materials KW - Density functional theory KW - Material design PY - 2022 DO - https://doi.org/10.1016/B978-0-12-822971-2.00010-3 VL - 22 SP - 215 EP - 232 PB - Elsevier B.V. AN - OPUS4-54717 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Weise, Frank A1 - Fladt, Matthias A1 - Meyer, I. T1 - Bewertung der Innenhydrophobierung von Fahrbahndeckenbetonen als neuartige AKR-Vermeidungsstrategie T1 - Evaluation of internal water-repellent treatment of concrete pavements as a novel AAR preventive measure N2 - Zur Nutzbarmachung grenzwertig alkaliempfindlicher Gesteinskörnungen für Betonfahrbahndecken wurde basierend auf einer Literaturrecherche die Eignung von je einem Innenhydrophobierungsmittel auf der Basis eines Kalziumstearats (HM-A), eines Silan-Siloxan-Gemisches (HM-B) sowie eines der Vertraulichkeit unterliegenden Wirkstoffs (HM-C) für die neuartige AKR-Vermeidungsstrategie untersucht. Die Basis für die Eignungsuntersuchungen bildeten die Rezepturen im ARS 04/2013 für den OB (D>8)/UB sowie für den OB 0/8. Zur Herausarbeitung des Einflusses des Hydrophobierungsmittels auf die schädigende AKR fand in der groben Kornfraktionen ein alkaliempfindlicher Grauwackesplitt Anwendung. Aufgrund der unterschiedlichen Wechselwirkung zwischen dem LP-Bildner und dem Hydrophobierungsmittel wurde seine Dosierung beim HM-A reduziert sowie beim HM-B geringfügig und beim HM-C um ein Vielfaches erhöht. Ausgehend von den ausgewählten Rezepturen mit den unterschiedlichen Hydrophobierungsmitteln wurden bei den Untersuchungen u.a. folgende Erkenntnisse gewonnen: • Nachweis der Funktionalität aller drei Hydrophobierungsmittel im Festbeton durch signifikant reduzierte kapillare Aufnahme der Prüflösung. • Verschlechterung der mechanischen Eigenschaften und des Frost-Tausalzwiderstands des OB (D>8)/UB bei Zugabe aller Hydrophobierungsmittel. • Verzicht auf den Einsatz des HM-A im OB (D>8)/UB aufgrund drastischer Verschlechterung der Verarbeitbarkeit des Frischbetons und hohem Festigkeitsverlust. • Verzicht auf den Einsatz des HM-B im OB (D>8)/UB aufgrund der Überschreitung des Dehnungsgrenzwerts nach dem 9. bzw. 10. Zyklus (mit bzw. ohne zyklischer Vorschädigung) und der einhergehenden starken Abwitterung bei der KWL mit NaCl-Lösung. • Nachweis nachhaltiger Verminderung schädigender AKR in beiden Betonarten mit HM-C in Klimawechsellagerung und 60°C-Betonversuch mit externer Alkalizufuhr, allerdings zu Lasten der mechanischen Eigenschaften und des Frost-Tausalz-Widerstands. Fazit: Bei geeigneter Wirkstoffauswahl hat die Innenhydrophobierung das Potenzial für die Nutzbarmachung grenzwertiger Gesteinskörnung. Ihre Überführung in die Praxis erfordert jedoch eine weitere ganzheitliche Optimierung der Baustoffperformance. Das schließt auch die Verifizierung gezielter betontechnologischer Maßnahmen zur Verminderung der Verschlechterung der mechanischen Eigenschaften und des Frost-Tausalz-Widerstandes ein. N2 - In order to enable utilization of borderline-acceptable alkali-sensitive aggregates for concrete road pavements, the applicability of an internal hydrophobic treatment for a novel alkali-aggregate reaction (AAR) preventive measure was investigated. On the basis of a literature review, a calcium stearate (HM-A), a silane-siloxane emulsion (HM-B) and an active agent (HM-C), which is subject to confidentiality, were investigated. The mix designs from ARS 04/2013 for OB (D>8)/UB as well as for OB 0/8 formed the basis for the qualification tests. In order to shed light on the influence of the hydrophobic agent on the damaging AAR, alkali-sensitive greywacke chippings were used as the coarse grain aggregates. Due to the varying interaction between the air-entraining agent and the hydrophobic agent, the hydro-phobic agent dosage was reduced for HM-A, increased slightly for HM-B and increased many times over for HM-C. Based on the selected concrete mixes with the different hydrophobic agents the following findings were obtained: • Proof of the functionality of all three hydrophobic agents in hardened concrete by significantly reduced capillary absorption of the test solution. • Deterioration of the mechanical properties and the resistance to freeze-thaw with de-icing salt of the OB (D>8)/UB through the addition of all hydropho-bic agents. • The use of HM-A in OB (D>8)/UB should be avoided because of drastic deterioration of the workability of the fresh concrete and significant loss of strength. • The use of HM-B in OB (D>8)/UB was abandoned due to the exceeding of the expansion limit value from the 9th or 10th cycle onwards (with or without cyclical pre-damage) and the accompanying severe scaling during the cyclic climate storage test (CCST) with NaCl solution. • Proof of sustainable reduction of harmful AAR in both types of concrete with HM-C in CCST and 60°C concrete prism tests with external alkali supply. The disadvantage is deterioration of the mechanical properties and the resistance to freeze-thaw with de-icing salt. Conclusion: With a suitable selection of hydrophobic agent, internal waterrepellent treatment has the potential to enable utilization of borderline-acceptable alkali-sensitive aggregates. However, its transfer into practice re-quires a further holistic optimization of the building material performance. This includes the verification of specific concretetechnological measures to improve both, the mechanical properties and the resistance to freeze-thaw with de-icing salt. KW - Tausalzeintrag KW - Betonfahrbahndecke KW - Alkali-Kieselsäure-Reaktion PY - 2022 SN - 978-3-95606-643-6 SN - 0344-0788 VL - 1141 SP - 1 EP - 281 PB - Fachverlag NW in der Carl Ed. Schünemann KG CY - Bremen AN - OPUS4-54757 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Hothan, Sascha A1 - Häßler, Dustin ED - Kuhlmann, U. T1 - Reaktive Brandschutzsysteme N2 - Die Erkenntnisse zu reaktiven Brandschutzsystemen (RBS) werden kontinuierlich erweitert, was sich in der Entwicklung neuer Produkte und der Ausweitung des durch technische Regelungen abgedeckten Anwendungsbereichs äußert. Der vorliegende Beitrag konzentriert sich auf die Verwendung von RBS auf Stahlkonstruktionen. Neben einer umfassenden Darstellung der aktuellen nationalen und europäischen Regelungen zu RBS, werden technologische Besonderheiten und deren Einfluss auf den Regelungsinhalt im Beitrag thematisiert. Dabei werden neben sich abzeichnenden Neuerungen auch die entsprechenden wissenschaftlich-technologischen Grundlagen dargelegt. Ferner wird die Frage nach der Bewertung der Dauerhaftigkeit von RBS für deutlich über 10 Jahre hinausgehende Zeiträume, und den sich damit einstellenden Feuerwiderstand der Konstruktion behandelt. Der Beitrag schließt mit einer Darstellung zur aktuellen Forschung. Daraus abgeleitet wird ein Ausblick auf zukünftige Forschungsthemen. KW - Reaktives Brandschutzsystem KW - Stahl KW - Brandschutz KW - Feuerwiderstand PY - 2022 SN - 978-3-433-03361-6 SP - 367 EP - 400 PB - Ernst & Sohn Verlag CY - Berlin AN - OPUS4-54735 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Aree, T. A1 - McMonagle, C. J. A1 - Michalchuk, Adam A1 - Chernyshov, D. T1 - Low-frequency lattice vibrations from atomic displacement parameters of a-FOX-7, a high energy density material N2 - Highly anharmonic thermal vibrations may serve as a source of structural instabilities resulting in phase transitions, chemical reactions and even the mechanical disintegration of a material. Ab initio calculations model thermal motion within a harmonic or sometimes quasi-harmonic approximation and must be complimented by experimental data on temperature-dependent vibrational frequencies. Here multi-temperature atomic displacement parameters (ADPs), derived from a single-crystal synchrotron diffraction experiment, are used to characterize low-frequency lattice vibrations in the alpha-FOX-7 layered structure. It is shown that despite the limited quality of the data, the extracted frequencies are reasonably close to those derived from inelastic scattering, Raman measurements and density functional theory (DFT) calculations. Vibrational anharmonicity is parameterized by the Grüneisen parameters, which are found to be very different for in-layer and out-of-layer vibrations. KW - Energetic Materials KW - DFT KW - Structural dynamics KW - X-ray diffraction PY - 2022 DO - https://doi.org/10.1107/S2052520622002700 SN - 2052-5206 VL - 78 SP - 376 EP - 384 PB - Wiley-Blackwell CY - Oxford AN - OPUS4-54832 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Johann, Sergej A1 - Baensch, Franziska A1 - Sturm, Patrick A1 - Tiebe, Carlo A1 - Pötschke, Samuel A1 - Lay, Vera ED - Holl, H. T1 - HF RFID-based measurement comparison for method optimization in M2 concrete and alkali-activated mortars N2 - Monitoring of repositories for radioactive waste requires techniques which can be applied long-term under harsh conditions. In this work, the reliability and suitability of materials and a capacitive sensor for measuring relative humidity are investigated, which are to be embedded in the special concrete components for the closure structures of underground repository. Preliminary tests with accelerated aging of the materials used, validation of the sensors under difficult conditions, investigations of the surfaces after aging by pH 14 solution, defined exposure of the sensors in a climatic chamber and the microscope images are discussed. The results will be used for further development and optimization of the RFID based sensor systems which can be applied to monitor the condition of different building structures without cabling. T2 - 37th Danubia - Adria Symposium on Advances in Experimental Mechanics CY - Linz, Austria DA - 21.09.2021 KW - Alkali-activated mortars KW - Passive sensor interface KW - RFID KW - Structural health monitoring KW - Smart structures PY - 2022 DO - https://doi.org/10.1016/j.matpr.2022.03.465 SN - 2214-7853 VL - 62 IS - 5 SP - 2571 EP - 2576 PB - Elsevier CY - Amsterdam AN - OPUS4-54697 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Grunert, Wiebke A1 - Walter, Astrid A1 - Schwarz, Silke A1 - Lohrer, Christian T1 - Odysseus - preventing, countering, and investigating terrorist attacks through prognostic, detection, and forensic mechanisms for explosive precursors N2 - Die Bekämpfung des Terrorismus erfordert ein ganzes Arsenal an Instrumenten. Unter anderem ist das Wissen über die Ausgangsstoffe für Explosivstoffe – chemische Substanzen, die für legale Zwecke verwendet, aber auch für die illegale Herstellung selbstgemachter Sprengstoffe missbraucht werden können – von entscheidender Bedeutung. In diesem Zusammenhang wird das EU-finanzierte Projekt ODYSSEUS effektive und effiziente prognostische, nachweisende und forensische Instrumente entwickeln, um die Prävention, Bekämpfung und Untersuchung von Terroranschlägen mit selbstgebauten Sprengstoffen zu verbessern. Die gewonnenen Erkenntnisse sollen zur Erarbeitung von Instrumenten zur Überwachung der chemischen Lieferkette und zur Erkennung von Ausgangsstoffen für Explosivstoffe in (nahezu) Echtzeit beitragen. Die Instrumente werden in drei Anwendungsfällen praktisch erprobt. T2 - 43. Informationstagung Sprengtechnik CY - Siegen, Germany DA - 22.04.2022 KW - Home made explosives KW - Explosiv- und Ausgangsstoffe KW - Sensor PY - 2022 AN - OPUS4-54687 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mair, Georg T1 - Sicherheitsforschung im Bereich Wasserstoff – Transport von CGH2 N2 - Ein Aspekt des Gefahrguttransportes, der an Bedeutung in den letzten Jahren zugenommen hat, ist die Versorgung von Wasserstofftankstellen und anderen H2-Großverbrauchern über die Schiene aber insbesondere über die Straße. Mit Blick auf die primäre Form der Speicherung wird der Begriff der Sicherheit über den Aspekt der Häufigkeit eines definierten Ereignisses erläutert und auf die Besonderheiten der Druckgefäße aus Verbundwerkstoffen hingewiesen, wie auch den regulatorischen Hintergrund der Lebensdauerüberprüfung nach 15 Jahren nach den Vorgaben der zuständigen Behörde. In Deutschland sind diese Vorgaben in der BAM-Gefahrgutregel 021 geregelt, die in der GGR 022 durch eine Regelung zur Wiederkehrenden Prüfung dieser Umschließungen ergänzt wird. Beide BAM-Gefahrgutregeln basieren auf einem probabilistischen Ansatz und einer Konsequenzabschätzung über das Druck-Volumen-Produkt der Druckgefäße. Die neu im Recht verankerte EN 17339 ist die erste Norm, die speziell fest montierte Compositespeicher für den Wasserstofftransport regelt. Sie ermöglicht eine erhebliche Gewichtreduktion und führt eine Obergrenze für das Druckvolumen ein. Es wird kurz erläutert, dass gerade mit Blick auf Wasserstofftransporte über eine Arbeitsgruppe der Vereinten Nationen eine Begrenzung des Konsequenzpotentials in das internationale Recht eingeführt werden soll und welche Kriterien bei der systematischen Ermittlung des akzeptierten Wertes von 1.5 Mio bar Liter Einfluss haben. Mit Blick auf die Energiewende sieht es die BAM als besonders wichtig an, die Transportkosten zu senken, indem der Prüfaufwand reduziert und gleichzeitig die Erkenntnistiefe aus der betrieblichen Überwachung verbessert wird. Hierzu muss die Datenbasis für die probabilistische Bewertung der Lebensdauer von zerstörenden Prüfungen auf zerstörungsfreie Prüfungen umgestellt werden und idealerweise die 100% Prüfung zumindest in der ersten Hälfte des sicheren Lebens auf Stichproben reduziert werden. Dies und andere Aufgaben, die wichtig für eine sichere und attraktive Wasserstoffwirtschaft sind werden von dem Kompetenzzentrum H2Safety@BAM bearbeitet, dass in seinen Grundzügen kurz vorgestellt wird. T2 - IAA Transportation 2022 CY - Hannover,Germany DA - 20.09.2022 KW - H2Safety@BAM KW - Markthochlauf KW - Lebensdauervorhersage KW - zerstörungsfreie Prüfung ZfP KW - Risikosteuerung PY - 2022 AN - OPUS4-56984 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Pittner, Andreas A1 - Schürmann, Karsten ED - Böhmer, Heike ED - Brinkmann-Wicke, Tanja ED - Sell, Sabine ED - Simon, Janet ED - Tebben, Cornelia T1 - Automatisierte Rohrknotenfertigung in der Offshore-Windenergie – Potenzial zum Leichtbau im schweren Stahlbau N2 - Um den Klimawandel wirksam zu bekämpfen, ist es entscheidend, fossile Brennstoffe durch erneuerbare Energiequellen wie Wind-, Solar- und Wasserkraft sowie alternative Energieträger, beispielsweise grünen Wasserstoff, zu ersetzen. Offshore-Windenergie spielt hierbei eine zentrale Rolle, da sie dank der Kombination aus globaler Verfügbarkeit, relativ geringen Betriebskosten und fortgeschrittenem technischen Entwicklungsstand besonders geeignet ist, zur regenerativen Stromerzeugung beizutragen. Sie ist zudem ein Schlüsselelement für die Umsetzung des Europäischen Green Deals, der das Ziel verfolgt, bis 2050 Klimaneutralität in der EU zu erreichen. Expertenschätzungen zufolge ist eine Steigerung der aktuellen Kapazität von 25 GW im Jahr 2020 auf etwa 450 GW notwendig, um diese ambitionierten Ziele zu erfüllen. Bei der Entwicklung zukünftiger Offshore-Windparks, insbesondere in tieferen Gewässern, gewinnen Jacket-Gründungsstrukturen an Bedeutung. Diese Strukturen, die eine höhere Steifigkeit bei geringerem Materialeinsatz im Vergleich zu den bisher vorherrschenden Monopile-Gründungen bieten, basieren auf komplexen, räumlich aufgelösten Konstruktionen, die ähnlich den Öl- und Gasplattformen entwickelt werden. Die Herstellung der Jacketknoten, die bislang überwiegend manuell geschweißt wurden, birgt erhebliches Optimierungspotential. Durch Automatisierung und Digitalisierung der Fertigungsprozesse könnten nicht nur die Effizienz gesteigert, sondern auch die Qualität der Endprodukte durch präzise Überwachung und Kontrolle der Produktionsparameter verbessert werden. Diese technologischen Fortschritte sind für die Skalierung der Offshore-Windenergie und die Erreichung der Klimaziele von entscheidender Bedeutung. KW - Automatisierte Fertigung KW - Offshore Windenergie KW - Jacket-Gründungsstrukturen KW - Aufgelöste Tragstrukturen KW - Leichtbau PY - 2022 SN - 978-3-7388-0719-6 SP - 260 EP - 266 PB - Fraunhofer IRB Verlag CY - Stuttgart AN - OPUS4-59502 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Guo, Yongzheng A1 - Ren, Kaiyue A1 - Huang, Weixing A1 - Wu, Dejian T1 - An alternative explosion criterion of combustible dusts based on combustion duration time: Applications for minimum explosion concentration and limiting oxygen concentration N2 - minimum explosion concentration (MEC) and limiting oxygen concentration (LOC) in our recent works. This work further studies the reasonability and reliability of the alternative method experimentally and theoretically. Six different dust samples were tested via a 20-L spherical explosion chamber. The experimental results showed that the data of MEC and LOC determined by using the alternative and the standardized methods are in good agreement. The minimum flame propagation velocity (Sf) and the corresponding maximum combustion duration time (tc) were found at its MEC and LOC, suggesting that the theoretical analysis can well explain all the experimental data. It is the first time to study the theoretical basis of the explosion criterion, thus helping to improve our understandings of dust explosion characteristics, and to amend the explosion criterion in future test standards. KW - General Chemical Engineering PY - 2022 DO - https://doi.org/10.1016/j.powtec.2022.117851 SN - 0032-5910 VL - 409 SP - 1 EP - 13 PB - Elsevier BV CY - Amsterdam AN - OPUS4-59323 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Neitsch, Marcel T1 - Gefahrgutverpackungen richtig verwenden N2 - Im Vortrag wird an Praxisbeispielen auf die richtige Nutzung von Gefahrgutverpackungen einschl. der Bewertung der UN-Kennzeichen und anderer vom Gefahrgutrecht vorgeschriebener Kennzeichen eingegangen. T2 - 09. Gefahrgut-Infomarkt CY - Online meeting DA - 16.05.2022 KW - Gefahrgutverpackungen KW - ADR KW - UN-Kennzeichen KW - Gefahrguttransport PY - 2022 AN - OPUS4-58895 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Recknagel, Christoph A1 - Eilers, M. A1 - Alte-Teigeler, R. A1 - Borchers, R. A1 - Commer, T. A1 - Gallai, G. A1 - Goldschmidt, M. A1 - Habiger, D. A1 - Karczewski, B. A1 - Koll, R.-J. A1 - Lorenz, S. A1 - Marossow, H. A1 - Rossi, M. A1 - Schneider, T. A1 - Seiffart, J. A1 - Staeck, M. A1 - Stark, S. A1 - Wehner, H. A1 - Willand, E. T1 - Hinweise für die Herstellung von Fahrbahnübergängen aus Poyurea oder Polyurethan für Ingenieurbauten - H FüPP N2 - Diese Hinweisbroschüre erläutert allgemeine Planungsvoraussetzungen und Dimensionierungsregelungen, Baugrundsätze und Zulassungsbedingungen zur Anwendung innovativer Belagsdehnfugensysteme (Fahrbahnübergangskonstruktionen) in hochbeanspruchten Verkehrsflächen des Bundesfernstraßenbereiches. Alle planungsrelevanten, baustoffrelevanten, versuchstechnische, qualitätssichernden und baupraktischen Aspekte werden zur Unterstützung der Straßenbauverwaltungen, der Lieferfirmen und Ausführungsbetriebe erläutert. Die Veröffentlichung stellt eine technische Analyse aus Erfahrungssammlungen und Auswertung praktischer Erkenntnisse dar. KW - Brückenbeläge KW - Fahrbahnübergänge KW - Dehnfugenkonstruktionen KW - technische und technologische Anforderungen PY - 2022 SN - 978-3-86446-355-6 VL - 778 SP - 1 EP - 47 PB - Forschungsgesellschaft für Straßen- und Verkehrswesen CY - Köln AN - OPUS4-59374 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zhang, K. A1 - Schmidt, Wolfram A1 - Mezhov, Alexander T1 - Influence of the hydroxypropylation of starch on its performance as viscosity modifying agent N2 - Synopsis: Starch is a commonly used viscosity modifying agent (VMA). The performance of starch as VMA depends on its origin (e.g. potato, corn, cassava, etc.) and corresponding molecular properties, such as molecular weight, ratio between amylose and amylopectin etc. Depending upon the application, the efficiency of starch can be enhanced by hydroxypropylation. The maximum degree of substitution (DoS) cannot be greater than 3.0, which is the number of hydroxy groups per glucose monomer in the polymer. In the current research three potato starches exhibiting the DoS of 0.4, 0.6 and 0.8 were utilised. The influence of the modified starch on the rheological properties and hydration of cement paste, as well as the viscosity of the pore solution were investigated. Our findings show that the starch with the highest DoS increases the dynamic yield stress the most, while the plastic viscosity is less dependent on the DoS. Additionally, starch with the highest DoS retards hydration to lower degree than other starches. T2 - 13th International Conference on Superplasticizers and Other Chemical Admixtures in Concrete CY - Milan, Italy DA - 10.07.2022 KW - Potato starch KW - Rheological KW - Cement hydration KW - Pore solutions PY - 2022 DO - https://doi.org/10.14359/51736074 VL - 354 SP - 209 EP - 218 PB - ACI Special Publications AN - OPUS4-58320 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mezhov, Alexander A1 - Schmidt, Wolfram A1 - Zhang, H. A1 - Diesendruck, Ch. E. T1 - The effect of the charge density of a comb polyphosphate superplasticizer on the structural build-up of cement paste N2 - Synopsis: Lately, there has been rising attention to superplasticizers (SP) based on polyphosphate esters. However, the influence of the molecular structure of the polyphosphate polymers on time-dependent properties such as structural build-up has not been examined yet intensively. To investigate this effect, three comb polyphosphate superplasticizers with different charge densities were synthesised by free radical polymerisation. Our findings indicate that SP with the lowest and medium charge densities extend the induction period more strongly than the SP with the highest charge density. The reduction of the structural build-up rate is linearly dependent on the dosage and concentration of the functional group of polyphosphate SP in the cementitious system. This study proposes a mathematical equation expressing the relationship between the structural build-up rate during the induction period and the molecular structure of the polyphosphate SP. T2 - 13th International Conference on Superplasticizers and Other Chemical Admixtures in Concrete CY - Milan, Italien DA - 10.07.2022 KW - Admixture KW - Superplasticizer KW - Polyphosphate KW - Structural build-up PY - 2022 DO - https://doi.org/10.14359/51736079 VL - 354 SP - 255 EP - 262 PB - ACI Special Publications AN - OPUS4-58321 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Long, Lijia A1 - Döhler, M. A1 - Thöns, Sebastian T1 - Determination of structural and damage detection system influencing parameters on the value of information N2 - A method to determine the influencing parameters of a structural and damage detection system is proposed based on the value of Information analysis. The value of information analysis utilizes the Bayesian pre-posterior decision theory to quantify the value of damage detection system for the structural integrity management during service life. First, the influencing parameters of the structural system, such as deterioration type and rate are introduced for the performance of the prior probabilistic system model. Then the influencing parameters on the damage detection system performance, including number of sensors, sensor locations, measurement noise, and the Type-I error are investigated. The preposterior probabilistic model is computed utilizing the Bayes’ theorem to update the prior system model with the damage indication information. Finally, the value of damage detection system is quantified as the difference between the maximum utility obtained in pre-posterior and prior analysis based on the decision tree analysis, comprising structural probabilistic models, consequences, as well as benefit and costs analysis associated with and without monitoring. With the developed approach, a case study on a statically determinate Pratt truss bridge girder is carried out to validate the method. The analysis shows that the deterioration rate is the most sensitive parameter on the effect of relative value of information over the whole service life. Furthermore, it shows that more sensors do not necessarily lead to a higher relative value of information; only specific sensor locations near the highest utilized components lead to a high relative value of information; measurement noise and the Type-I error should be controlled and be as small as possible. An optimal sensor employment with highest relative value of information is found. Moreover, it is found that the proposed method can be a powerful tool to develop optimal service life maintenance strategies—before implementation—for similar bridges and to optimize the damage detection system settings and sensor configuration for minimum expected Costs and risks. KW - Damage detection systems KW - Value of information KW - Deteriorating structures KW - Probability of damage indication KW - Decision theory PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-508083 DO - https://doi.org/10.1177/1475921719900918 SN - 1475-9217 SN - 1741-3168 VL - 21 IS - 1 SP - 19 EP - 36 PB - Sage Publications CY - Thousand Oaks, Calif. AN - OPUS4-50808 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schartel, Bernhard A1 - Battig, Alexander A1 - Garfias González, K. I. A1 - Gleuwitz, F. R. A1 - Sánchez Olivares, G. T1 - Non-vegan flame-retardant (adjuvants in) biocomposites N2 - Emanating from developing flame retarded biocomposites, we have proposed renewable natural fibers (including keratin) taken from industrial waste as an authentic sustainable approach. More recently, we have investigated non-vegan flame retardant approaches. This paper loves to give you an insight into our ongoing projects on biogenic industrial wastes like leather, bone meal, and insects. Materials were characterized multi-methodically, flame retardant modes of action quantified, decomposition mechanism proposed, and synergisms explained. Considering the large quantities of leather waste (LW) in industrial-scale production, we underline LW as multifunctional bio-adjuvants. LW enhances the flame retardancy of poly(ethylene-vinyl acetate) (EVA) containing phosphorus flame retardants (P-FR). Products/by-products of the invertebrate and vertebrate farming, respectively, are promising bio-based adjuvants in flame retarded bio-epoxy thermosets. While the addition of bone meal yields the formation of an inorganic shield, protein-based powders from insects provide an intumescent behavior. In combination with a P-FR superior charring and self-extinguishing are obtained. Acknowledgement: In part of this work was supported by the Volkswagen Foundation grant “Experiment!” No. 97437. T2 - Fire and Polymers, workshop, ACS Division of Polymer Chemistry CY - Napa, California, US DA - 05.06.2022 KW - Fire behaviour KW - Renewable KW - Circular economy KW - Biocomposite PY - 2022 AN - OPUS4-55025 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Maack, Stefan A1 - Küttenbaum, Stefan A1 - Bühling, Benjamin A1 - Niederleithinger, Ernst T1 - Low frequency ultrasonic dataset for pulse echo object detection in an isotropic homogeneous medium as reference for heterogeneous materials in civil engineering N2 - The dataset presented contains ultrasonic data recorded in pulse echo mode. The investigated specimen is made of the isotropic homogeneous material polyamide and has a drill hole of constant diameter running parallel to the surface, which was scanned in a point grid using an automatic scanner system. At each measuring position, a pitch-catch measurement was performed using a sampling rate of 2 MHz. The probes used are arrays consisting of a spatially separated receiving and in-phase transmitting unit. The transmitting and receiving sides each consist of 12 point-shaped single probes. These dry-point contact (DPC) probes operate according to the piezoelectric principle at nominal frequencies of 55 kHz (shear waves) and 100 kHz (longitudinal waves), respectively, and do not require a coupling medium. The measurements are performed with longitudinal (100 kHz) and transverse (55 kHz) waves with different geometric orientations of the probe on the measurement surface. The data presented in the article provide a valid source for evaluating reconstruction algorithms for imaging in the low-frequency ultrasound range. KW - Non-destructive testing KW - Ultrasound KW - Pulse-echo method KW - Reference material KW - Reconstruction algorithm KW - Validation PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-547326 DO - https://doi.org/10.1016/j.dib.2022.108235 VL - 42 SP - 1 EP - 11 PB - Elsevier Inc. AN - OPUS4-54732 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Algernon, D. A1 - Arndt, R. A1 - Ebsen, B. A1 - Feistkorn, S. A1 - Friese, M. A1 - Große, C. A1 - Kathage, S. A1 - Keßler, S. A1 - Kurz, J. A1 - Küttenbaum, Stefan A1 - Lohse, C. A1 - Maack, Stefan A1 - Niederleithinger, Ernst A1 - Schickert, M. A1 - Schröder, G. A1 - Taffe, A. A1 - Walther, A. A1 - Wilcke, M. A1 - Wolf, J. A1 - Wöstmann, Jens T1 - Richtlinie B-LF 01: Leitfaden zur Erstellung von Prüfanweisungen für die Zerstörungsfreie Prüfung im Bauwesen (ZfP Bau) N2 - Der vorliegende Leitfaden dient zur Unterstützung der Entwicklung und Umsetzung von Prüfanweisungen für ZfP-Verfahren im Bauwesen. Er gibt einen Überblick über Verwendungszweck, Erstellung und Inhalte von Prüfanweisungen unter Berücksichtigung einheitlicher Standardisierungsziele. KW - Prüfanweisung KW - Beton KW - Leitfaden PY - 2022 SN - 978-3-947971-23-7 SP - 1 EP - 9 PB - Deutsche Gesellschaft für Zerstörungsfreie Prüfung e.V. (DGZfP) CY - Berlin ET - 1. Aufl., April 2022 AN - OPUS4-54985 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Maack, Stefan T1 - Low-frequency ultrasound data (pulse-echo technique) with shear horizontal and longitudinal waves on a reference polyamide specimen “BAM-Pk218” N2 - This dataset contains raw data observed with ultrasound measurements on a polyamide reference specimen at Bundesanstalt für Materialforschung und -prüfung (BAM), Berlin. The internal specimen identifier is „Pk218“. The measurements were conducted using the pulse-echo method. KW - Nondestructive testing KW - Ultrasound KW - Pulse-echo technique KW - Validation KW - Reference material KW - Reconstruction algorithm PY - 2022 DO - https://doi.org/10.7910/DVN/KVN7CY PB - Harvard College CY - Cambridge, MA, USA AN - OPUS4-54959 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Gnutzmann, Tanja A1 - Vorwerk, P. A1 - von der Linde, M. A1 - Herbster, C. A1 - Festag, S. A1 - Oberhagemann, D. A1 - Pohle, R. A1 - von Sicard, O. A1 - Freudenberg, O. A1 - Müller, S. A1 - Kelleter, J. A1 - Hofmann-Böllinghaus, Anja A1 - Thielsch, M. A1 - Krause, U. T1 - Brandschutz für Kulturgut: Das Projekt BRAWA N2 - Brände zerstören immer wieder wichtige Kulturgüter und gefährden nationales Kulturerbe. Das Projekt BRAWA erarbeitet neue Strategien und innovative Technologien, um die Brandsicherheit historischer Gebäude zu erhöhen. Dabei basiert das Konzept auf der Vernetzung von Sensoren, die bereits beim Auftreten bestimmter Gase in der Frühphase der Brandentstehung Alarm auslösen. Durch ein neuartiges Helferkonzept soll eine frühe Branderkennung und -bekämpfung ermöglicht werden. T2 - BMBF Innovationsforum "Zivile Sicherheit" 2022 CY - Berlin, Germany DA - 03.05.2022 KW - Brandschutz KW - Kulturgut KW - Historische Gebäude KW - Branddetektion KW - Sensornetzwerk PY - 2022 AN - OPUS4-54828 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Viefhues, Eva A1 - Döhler, M. A1 - Hille, Falk A1 - Mevel, L. T1 - Statistical subspace-based damage detection with estimated reference N2 - The statistical subspace-based damage detection technique has shown promising theoretical and practical results for vibration-based structural health monitoring. It evaluates a subspacebased residual function with efficient hypothesis testing tools, and has the ability of detecting small changes in chosen system parameters. In the residual function, a Hankel matrix of Output covariances estimated from test data is confronted to its left null space associated to a reference model. The hypothesis test takes into account the covariance of the residual for decision making. Ideally, the reference model is assumed to be perfectly known without any uncertainty, which is not a realistic assumption. In practice, the left null space is usually estimated from a reference data set to avoid model errors in the residual computation. Then, the associated uncertainties may be non-negligible, in particular when the available reference data is of limited length. In this paper, it is investigated how the statistical distribution of the residual is affected when the reference null space is estimated. The asymptotic residual distribution is derived, where its refined covariance term considers also the uncertainty related to the reference null space estimate. The associated damage detection test closes a theoretical gap for real-world applications and leads to increased robustness of the method in practice. The importance of including the estimation uncertainty of the reference null space is shown in a numerical study and on experimental data of a progressively damaged steel frame. KW - Damage detection KW - Uncertainty quantification KW - Statistical tests KW - Ambient excitation KW - Vibration measurement PY - 2022 DO - https://doi.org/10.1016/j.ymssp.2021.108241 SN - 0888-3270 VL - 164 SP - 108241 PB - Elsevier Ltd. AN - OPUS4-52998 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Mezhov, Alexander A1 - Ben Shir, I. A1 - Schmidt, A. A1 - Kovler, K. A1 - Diesendruck, Ch. E. T1 - Retardation mechanism of cement hydration by a comb polyphosphate superplasticizer N2 - The retardation mechanism of cement hydration as imparted by the addition of polyphosphate comb superplasticizer to model cement containing C3S, C3A and calcium sulfate hemihydrate is studied using XRD, ss NMR and calorimetry. Our findings show the retardation effect caused by the direct addition of polyphosphate comb superplasticizer differs significantly to that of conventional polycarboxylate superplasticizers. Conversely to polycarboxylates, polyphosphates, at a low dosage, inhibits the silicate reaction without affecting the aluminate reaction and formation of ettringite. Yet, at high doses, both reactions are hampered, and the induction period extended, followed by accelerated aluminate and silicate reactions. KW - Superplasticizer KW - Polyphosphate KW - Retardation KW - Cement hydration PY - 2022 DO - https://doi.org/10.1016/j.conbuildmat.2022.128698 SN - 0950-0618 VL - 352 SP - 1 EP - 13 PB - Elsevier Ltd. AN - OPUS4-58246 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Lapiro, I. A1 - Mezhov, Alexander A1 - Kovler, K. T1 - Performance of corrosion inhibitors in reinforced concrete elements under electrical voltage N2 - The current paper develops a novel accelerated corrosion test method based on Faraday’s law to investigate the performance of different inhibitors in reinforced concrete elements under electrical voltage. Using the proposed method two commercially available and three lab-made inhibitors were tested. Lab-made inhibitors based on potassium fluorosilicate and amine carboxylate showed the best performance over others. Furthermore, it is found that under an electrical potential environment beyond 3.6 V, the higher the concrete strength, the more efficient is the corrosion inhibition. Based on experimental results, a novel model describing the corrosion evolution in reinforced concrete was proposed. KW - Steel corrosion KW - Reinforced concrete KW - Accelerated test KW - Corrosion inhibitor KW - Stray current PY - 2022 DO - https://doi.org/10.1016/j.conbuildmat.2022.127656 SN - 0950-0618 VL - 342 IS - 342 SP - 1 EP - 10 PB - Elsevier Ltd. AN - OPUS4-58249 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Zhang, K. A1 - Mezhov, Alexander A1 - Schmidt, Wolfram T1 - Chemical and thixotropic contribution to the structural build-up of cementitious materials N2 - The structural build-up of fresh cement paste is often considered as a purely thixotropic phenomenon in literature even though cementitious materials undergo a non-reversible hydration process that can have an influence on the structuration process. In the current paper a method is proposed to validate the impact of the non-reversible structural build-up. It is shown that fresh cement paste samples lose their structural gain almost completely due to thixotropy while the structural build-up due to hydration can be observed but occurs in a significantly lower order of magnitude over the course of the first hours of hydration. In addition, it is shown, that the chemical component of the structural build-up accelerates with the onset of the acceleration period of hydration, while its contribution in the entire structural build-up remains constant. KW - Thixotropy KW - Structural build-up KW - Penetration test KW - Rheological properties PY - 2022 DO - https://doi.org/10.1016/j.conbuildmat.2022.128307 SN - 0950-0618 VL - 345 IS - 128307 SP - 1 EP - 10 PB - Elsevier Ltd. AN - OPUS4-58248 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zhang, K. A1 - Mezhov, Alexander A1 - Schmidt, Wolfram T1 - Thixotropic and chemical structural build-up of cement pastes with superplasticizer under different storage conditions N2 - Synopsis: The paper presents the results of a study on the influence of agitation on the structural build-up of fresh cement pastes using a penetration test. It first presents results about the influence of the penetrating shape’s geometry on the influence on the cement paste specimen. Then, results are shown for the load-deflection curves depending upon time and agitation before testing. Based on the observation of the force required to penetrate the sample, conclusions on the structural build-up can be made. The observations were made over the course of time with samples that were left at rest and partly agitated before testing at different time steps. The setup allows to identify the contribution of the chemical reaction to the structural build-up process. The presence of superplasticizer obviously reduces the load that cement paste can withstand, while the loss of thixotropy is found notably lower than that of neat cement pates T2 - 13th International Conference on Superplasticizers and Other Chemical Admixtures in Concrete CY - Milan, Italy DA - 10.07.2022 KW - Thixotropy KW - Superplasticizer KW - Structural build-up KW - Texture analyzer KW - Penetration test PY - 2022 DO - https://doi.org/10.14359/51736058 VL - 354 SP - 13 EP - 24 PB - ACI Special Publications AN - OPUS4-58324 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Mezhov, Alexander A1 - Zhang, K. A1 - Schmidt, Wolfram T1 - Interactions of Biobased Rheology Modifying Agents with Superplasticizer in Cement Paste N2 - Organic admixtures are an indispensable component of modern concrete. Thus, their purposeful application is not only technically and economically viable but in addition an inevitable tool to make concrete more environmentally friendly. In this context, the use of polysaccharides has increasingly gained interest in the built environment as sustainable resource for performance enhancement. However, due to its origin, biopolymers possess a vast variety of molecular structures which can result in incompatibilities with other polymers present in concrete, such as superplasticizers. The present study highlights effects of the joint application of different types of starches and polycarboxylates with respect to their influence on cement hydration and structural build-up of cement pastes. KW - Polysaccharides KW - Superplasticizers KW - Hydration KW - Cement PY - 2022 DO - https://doi.org/10.4028/www.scientific.net/CTA.1.563 SN - 2674-1237 SP - 563 EP - 568 PB - Trans Tech Publications Ltd, Switzerland CY - Basel, Switzerland. AN - OPUS4-58325 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Diercks, Philipp A1 - Veroy, K. A1 - Robens-Radermacher, Annika A1 - Unger, Jörg F. T1 - Multiscale modeling of heterogeneous structures based on a localized model order reduction approach N2 - Many of today’s problems in engineering demand reliable and accurate prediction of failure mechanisms of mechanical structures. Thus, it is necessary to take into account the heterogeneous structure on the smaller scale, to capture the underlying physical phenomena. However, this poses a great challenge to the numerical solution since the computational cost is significantly increased by resolving the smaller scale in the model. Moreover, in applications where scale separation as the basis of classical homogenization schemes does not hold, the influence of the smaller scale on the larger scale has to be modelled directly. This work aims to develop an efficient concurrent methodology to model heterogeneous structures combining the variational multiscale method (VMM) and model order reduction techniques. First, the influence of the smaller scale on the larger scale can be taken into account following the additive split of the displacement field as in the VMM. Here, also a decomposition of the global domain into subdomains, each containing a fine grid discretization of the smaller scale, is introduced. Second, local reduced approximation spaces for the smaller scale solution are constructed by exploring possible solutions for each subdomain based on the concept of oversampling and the solution of the associated transfer operator problem. Herein, we propose to choose the training data based on the solution of a reduced global problem to incorporate the actual physical behaviour of the structure of interest and to extend it by random samples to ensure sufficient approximation capabilities in general. The local reduced spaces are designed such that local contributions of each subdomain can be coupled in a conforming way. Thus, the resulting global system is sparse and reduced in size compared to the direct numerical simulation, leading to a faster solution of the problem. The authors gratefully acknowledge financial support by the German Research Foundation (DFG), project number 394350870, and by the European Research Council (ERC) under the European Union’s Horizon 2020 research and innovation programme (ERC Grant agreement No. 818473). T2 - Model Reduction and Surrogate Modeling (MORE) CY - Berlin, Germany DA - 19.09.2022 KW - Domin decomposition KW - Model oder reduction KW - Multiscale methodes KW - Variational multiscale method PY - 2022 AN - OPUS4-57332 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Schaumann, P. A1 - Hothan, Sascha A1 - Mund, M. A1 - Häßler, Dustin A1 - Schartel, Bernhard A1 - Daus, Lars-Hendrik T1 - Bewertung des Feuerwiderstandes von Stahlkonstruktionen mit reaktiven Brandschutzsystemen unter Berücksichtigung des Alterungsverhaltens N2 - Im Rahmen des Forschungsprojektes IGF 20470N wurden Untersuchungen zum Alterungsverhalten von reaktiven Brandschutzsystemen (RBS) auf Stahlbauteilen durchgeführt. Mithilfe der Ergebnisse einer umfangreichen Literaturrecherche sowie experimentellen und numerischen Untersuchungen sollte ein Vorschlag für ein Prüfkonzept zum Nachweis einer Nutzungsdauer von RBS von mehr als 10 Jahren auf Basis von Kurzzeitversuchen abgeleitet werden. Dabei setzt die Bewertung des Alterungsverhaltens von RBS voraus, dass die Mechanismen der Alterung hinreichend bekannt sind. Dafür wurden zunächst systematisch Daten von Kurz- und Langzeitversuchen von nationalen Zulassungsprüfungen der letzten Jahrzehnte ausgewertet. Anschließend wurden umfangreiche experimentelle Untersuchungen an einer wasserbasierten sowie einer epoxidharzbasierten Richtrezeptur durchgeführt. Da aus der Literatur bekannt ist, dass die Einflüsse der Bewitterung zu einer Veränderung der Konzentration der Bestandteile innerhalb der Beschichtung führen können, wurden Untersuchungen mit Mangelrezepturen durchgeführt, wobei systematisch einzelne Bestandteile reduziert wurden. Neben optischen Untersuchungen wurden thermoanalytische Verfahren (DSC-TG-, ATR-FTIR-, Elementar-, Farbanalyse) angewandt sowie Brandversuche an beschichteten Stahlplatten durchgeführt. Des Weiteren wurden die Richtrezepturen den beschleunigten Kurzzeitversuchen gemäß EAD 350402-00-1106 (2017) unterzogen, welche die Zulassung von Produkten auf europäischer Ebene regelt. Für die wasserbasierte Richtrezeptur wurden die Bewitterung für den feuchten Innenraum (Typ Z1) mehrfach wiederholt (1x, 3x, 6x). Für die epoxidharzbasierte Richtrezeptur entsprach die Bewitterung dem Zyklus für die Außenanwendung (Typ X). In Brandversuchen sowie thermoanalytischen und optischen Untersuchungen wurde das Alterungsverhalten sowie die thermische Schutzwirkung analysiert. Anschließend wurden numerische Simulationen von Stahlbauteilen mit gealterten RBS durchgeführt und anhand der experimentellen Untersuchungen validiert. Mithilfe der numerischen Modelle kann eine Bewertung der thermischen Schutzwirkung von Stahlbauteilen mit gealterten RBS vorgenommen werden. Mithilfe der gesammelten Erkenntnisse wurde ein Vorschlag für ein Prüfkonzept für den Nachweis einer Nutzungsdauer von mehr als 10 Jahren abgeleitet. Das Prüfkonzept besteht dabei aus einem Katalog von Möglichkeiten, die aktuellen Zulassungsprüfungen auf europäischer Ebene für eine Nutzungsdauer von 10 Jahren auf einen längeren Zeitraum zu erweitern. N2 - Within the scope of the research project IGF 20470N, investigations were carried out on the assessment of the aging behavior of intumescent coatings (ICs) for the fire protection of steel members. With the help of the results of an extensive literature research as well as experimental and numerical investigations, a proposal for a test concept for the proof of a service life of ICs of more than 10 years was to be derived on the basis of short-term tests. The evaluation of the aging behavior of ICs presupposes that the aging mechanisms are sufficiently known. For this purpose, data from short- and long-term tests of national approval tests of the last decades were first systematically evaluated. Subsequently, extensive experimental investigations were carried out on a water-based and epoxy resin-based model formulation. Since it is known from the literature that the effects of weathering may lead to a change in the concentrations of the constituents within the coating, investigations were carried out with formulations of the ICs in which individual constituents were systematically reduced. In addition to optical investigations, thermoanalytical methods (DSC-TG-, ATR-FTIR-, elemental-, color analysis) were used and fire tests were carried out on coated steel plates. Furthermore, the model formulations were subjected to the accelerated short-term tests of EAD 350402-00-1106 (2017), which regulates the approval of products at the European level. For the water-based model formulation, the weathering for the interior application with a high moisture content (type Z1) was repeated several times (1x, 3x, 6x). For the epoxy resin-based model formulation, the weathering corresponded to the cycle for exterior application (type X). Fire tests as well as thermoanalytical and optical investigations were carried out to analyze the aging behavior and the thermal protection performance. Subsequently, numerical simulations of steel members with aged ICs were carried out and validated on the basis of the experimental investigations. With the help of the numerical models, an evaluation of the thermal protection performance of steel members with aged ICs can be carried out. Bases on the findings, a proposal for a test concept for the verification of a service life of more than 10 years was derived. The test concept consists of a catalogue of possibilities for extending the current approval tests at European level for a service life of 10 years to a longer period. KW - Brandschutz KW - Dauerhaftigkeit KW - Alterung KW - Reaktive Brandschutzsysteme KW - Brandversuche PY - 2022 UR - https://dast.deutscherstahlbau.de/veroeffentlichungen/forschungsberichte SP - 1 EP - 367 PB - Stahlbau Verlags- und Service GmbH CY - Düsseldorf AN - OPUS4-57257 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Vogler, Nico A1 - Lehmann, Jens A1 - Bohlmann, Tatjana A1 - Kronemann, Jens T1 - Gel-bound Colourants as a Substitute for the Sprayed Application of pH-Indicator Solution N2 - In general, pH-sensitive colorants such as phenolphthalein are applied on freshly split surfaces of building structures to determine the state of carbonation. For years, it has been known that the aerosols of phenolphthalein are suspected of being carcinogenic. Hence, more work has currently being done on alternative indicators for the use in research and the use on construction sites. Over the past years, mainly pH indicators from other research areas and natural dyes were investigated for their usability to cementitious systems. This paper presents the experimental results of using phenolphthalein solution bound in agar-agar gel. This gel-bound indicator allows the future use of the already known phenolphthalein dye without the health hazards for the user. To demonstrate the flexibility of the gel-bound colorant, different application forms of the indicator were carried out and assessed. In addition, the results obtained by the different methods were statistically evaluated to ensure validity. The accuracy of the results was confirmed by thermogravimetric analysis and IR spectroscopic studies as reference methods. It has also succeeded to demonstrate the comparability of the results achieved by the gel-bound colorant with the results of the common sprayed application method. As an additional gain in knowledge, comparative results of indicator tests, TGA analysis, and FTIR investigation are shown. KW - Concrete Carbonation KW - Gel-bound Colorants KW - pH Indicator KW - Thermal Gravimetric Analysis KW - FTIR-ATR Measurements PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-551493 UR - http://www.sciencepublishinggroup.com/j/ajce DO - https://doi.org/10.11648/j.ajce.20221003.16 SN - 2330-8729 SN - 2330-8737 VL - 10 IS - 3 SP - 135 EP - 144 PB - Science Publishing Group CY - New York, NY AN - OPUS4-55149 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Hurtado-Hurtado, G. A1 - Morales-Velazquez, L. A1 - Valtierra-Rodríguez, M. A1 - Otremba, Frank A1 - Jáuregui-Correa, J. C. T1 - Frequency Analysis of the Railway Track under Loads Caused by the Hunting Phenomenon N2 - Hunting is a potentially dangerous phenomenon related to the lateral oscillation of the wheels that impacts the rails and causes the wear of the infrastructure’s components. Therefore, the analysis and timely detection of hunting can lead to the application of corrective maintenance tasks, reducing damages, and costs and even derailments as a result. In this work, the vibration response of a finite element model of a rail with hunting-induced loads by a single wheel is analyzed in three directions: longitudinal, lateral, and vertical. The contact patch forces are calculated by means of Simpack® using the Kalker linear theory and the contact Hertz theory. The system is solved by using the Newmark-_ approach. The results of the deflection and vibration analysis, following the proposed methodology, show how the different characteristics of the loads impact the rail. KW - Continuous wavelet transform KW - Empirical mode decomposition KW - Finite element method KW - Frequency analysis KW - Hunting phenomenon KW - Mechanical modelling KW - Rail vibrations PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-551517 UR - https://www.mdpi.com/2227-7390/10/13/2286/htm# DO - https://doi.org/10.3390/math10132286 VL - 10 IS - 13 SP - 1 EP - 17 PB - MDPI AN - OPUS4-55151 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wilrich, Cordula T1 - Chemikalienrecht & Gefahrstoffrecht: Schnittstelle zu Seveso-Richtlinie & Störfallverordnung N2 - Der Vortrag beleuchtet die Schnittstelle zwischen Chemikalienrecht und Störfallrecht. Der Hintergrund, die Struktur und wichtige Eckpunkte der CLP-Verordnung werden vorgestellt. Instrumente und Beispiele zur Verifizierung von Einstufungen nach CLP im Hinblick auf die Anwendung unter der Seveso-Richtlinie bzw. der Störfallverordnung werden erläutert. Außerdem werden mögliche Konsequenzen für Änderungen im Anwendungsbereich der Seveso-Richtlinie besprochen. T2 - BAM/UBA-Behördenerfahrungsaustausch CY - Berlin, Germany DA - 27.06.2022 KW - Anlagensicherheitsrecht KW - Chemikalienrecht KW - CLP-Verordnung KW - Gefahrstoff KW - GHS KW - Seveso-Richtlinie KW - Störfallverordnung PY - 2022 AN - OPUS4-55171 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wosniok, Aleksander A1 - Karapanagiotis, Christos T1 - Brillouin optical frequency-domain analysis for structural health monitoring N2 - We present our achievements in the development of distributed fiber optic sensing systems based on Brillouin optical frequency-domain analysis for structural health monitoring. The focus of the applications is on the gapless monitoring of geotechnical structures, large area infrastructures and electrical grids. The work includes the latest use of machine learning algorithms to reduce measurement time by coexistent increasing the measurement accuracy. T2 - 4th Workshop on Optomechanics and Brillouin Scattering CY - Erlangen, Germany DA - 14.06.2022 KW - Distributed sensing KW - BOFDA KW - Optical fiber sensor KW - Brillouin distributed fiber sensor PY - 2022 AN - OPUS4-55173 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Fürst, Richard A1 - Hejtmanek, P. A1 - Vlach, T. A1 - Repka, J. A1 - Mozer, V. A1 - Hajek, P. T1 - Experimental Evaluation of Carbon Reinforced TRC with Cement Suspension Matrix at Elevated Temperature N2 - Textile-reinforced concrete (TRC) is a new composite material comprising high-performance concrete and textile reinforcement from textile yarns with a matrix, usually consisting of epoxy resins (ER). The most significant advantage of ER is the homogenization of all filaments in the yarn and full utilization of its tensile potential. Nevertheless, ER matrix is a critical part of TRC design from the perspective of the fire resistance due to its relatively low resistance at temperatures of approximately 120 C. This work expands the previously performed mechanical tests at normal temperatures with cement suspension (CS) as a non-combustible material for the yarn matrix. Here, the mechanical properties of CS matrix at elevated temperatures were verified. It was found that the addition of polypropylene fibers into HPC negatively affected the mechanical results of CS matrix specimens. Simultaneously, thermal insulation effect of the covering layers with different thicknesses did not significantly influence the residual bending strength of specimens with CS matrix and achieved similar results as reference specimens. Furthermore, all specimens with ER matrix progressively collapsed. Finally, CS as a textile reinforcement of yarn matrix appears to be a suitable solution for increasing the temperature resistance of TRC structures and for substituting synthetic resins. KW - Cement matrix KW - Cement suspension KW - Carbon fibers KW - Textile reinforced concrete KW - High-performance concrete KW - Elevated temperature KW - Fire safety KW - Fire resistance PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-550766 DO - https://doi.org/10.3390/polym14112174 SN - 2073-4360 VL - 14 IS - 11 SP - 1 EP - 16 PB - MDPI CY - Basel, Switzerland AN - OPUS4-55076 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schmidt, Martin A1 - Gödde, M. A1 - Salg, S. A1 - Erdt, René T1 - Self-ignition Behaviour of Bulk Materials: How Reliable is the Extrapolation of Laboratory Tests? N2 - The self-ignition behaviour of bulks is usually determined with the aid of isoperibolic or adiabatic hot storage tests; the sample volumes here are typically in the range of approx. 100 cm³ to several litres. The extrapolation to technically relevant volumes holds, however, considerable uncertainties. To reduce these uncertainties, a test stand was set up that allows to investigation sample sizes of up to 1000 dm³. These allow the study of selfignition behavior closer to the conditions that prevail in practice. The suitability (or unsuitability) of the established methods (including dangerous goods classification tests) were to be demonstrated and influencing variables that cannot be measured on a laboratory scale were to be determined. In addition, various analytical methods were used for the determination of reaction kinetic data of solid bulk materials and to predict the self-ignition behaviour of large storages. These are thermal analyses such as differential scanning calorimetry DSC, simultaneous thermal analysis STA as well as microcalorimetry for highprecision measurement of heat flows. Complete test series using all mentioned test methods will be presented for crosslinked polyvinyl-pyrrolidone (PVP) and conclusions regarding the applicability of the extrapolation methods will be discussed. Hot storage tests up to semi-industrial scale and their combination with various thermoanalytical methods allow a much more precise prediction of the self-ignition behaviour of large bulks. A further promising approach to estimate their heat release rates, and hence, the risk of self-ignition under technical conditions, is the use of microcalorimetric methods. T2 - Loss Prevention 2022 CY - Prag, Czechia DA - 05.06.2022 KW - Self-ignition KW - Kinetic data KW - Semi-technical tests KW - Thermoanalytical methods PY - 2022 SN - 978-88-95608-88-4 DO - https://doi.org/10.3303/CET2290049 SN - 2283-9216 VL - 90 SP - 289 EP - 294 PB - AIDIC AN - OPUS4-55079 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schmidt, Martin A1 - Erdt, René A1 - Gödde, M. A1 - Salg, S. T1 - Self-ignition Behaviour of Bulk Materials: How Reliable is the Extrapolation of Laboratory Tests? N2 - The self-ignition behaviour of bulks is usually determined with the aid of isoperibolic or adiabatic hot storage tests; the sample volumes here are typically in the range of approx. 100 cm³ to several litres. The extrapolation to technically relevant volumes holds, however, considerable uncertainties. To reduce these uncertainties, a test stand was set up that allows to investigation sample sizes of up to 1000 dm³. These allow the study of selfignition behavior closer to the conditions that prevail in practice. The suitability (or unsuitability) of the established methods (including dangerous goods classification tests) were to be demonstrated and influencing variables that cannot be measured on a laboratory scale were to be determined. In addition, various analytical methods were used for the determination of reaction kinetic data of solid bulk materials and to predict the self-ignition behaviour of large storages. These are thermal analyses such as differential scanning calorimetry DSC, simultaneous thermal analysis STA as well as microcalorimetry for highprecision measurement of heat flows. Complete test series using all mentioned test methods will be presented for crosslinked polyvinyl-pyrrolidone (PVP) and conclusions regarding the applicability of the extrapolation methods will be discussed. Hot storage tests up to semi-industrial scale and their combination with various thermoanalytical methods allow a much more precise prediction of the self-ignition behaviour of large bulks. A further promising approach to estimate their heat release rates, and hence, the risk of self-ignition under technical conditions, is the use of microcalorimetric methods. T2 - Loss Prevention 2022 CY - Prague, Czech Republic DA - 05.06.2022 KW - Self-ignition KW - Kinetic data KW - Semi-technical tests KW - Thermoanalytical methods PY - 2022 AN - OPUS4-55080 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Ebell, Gino T1 - Potentialfeldmessung in Theorie und Praxis N2 - Durch das alkalische Porenwassermilieu ist Stahl im Beton vor Korrosion geschützt. Unter ungünstigen Umgebungsbedingungen (Karbonatisierung, Chlorideintrag) kann die passive Deckschicht auf der Stahloberfläche zerstört werden. Im weiteren Verlauf können sich korrosionsbedingte Folgeschäden, wie Risse und Abplatzungen am Bauwerk ergeben. Um notwendige Sanierungsmaßnahmen sind frühzeitige und weitgehend zerstörungsfrei ermittelte Informationen über das aktuelle Korrosionsverhalten der Stahlbewehrung von großer Bedeutung. Die Potentialfeldmessung ist ein etabliertes und weit verbreitetes Verfahren zur Beurteilung des Korrosionszustandes der Bewehrung in Stahlbetonbauwerken. Mit Hilfe dieses Verfahrens können Bereiche aktiv korrodierender Bewehrung zerstörungsfrei lokalisiert werden. In der Regel kommt diese Messmethode bei der Detektion chloridinduzierter Korrosion zum Einsatz T2 - Vorlesung TU-Berlin CY - Berlin, Germany DA - 30.06.2022 KW - Korrosion KW - Potentialfeldmessung PY - 2022 AN - OPUS4-55156 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lengas, Nikolaos A1 - Müller, Karsten A1 - Schlick-Hasper, Eva A1 - Neitsch, Marcel A1 - Johann, Sergej A1 - Zehn, M. W. T1 - Development of an analysis and testing concept for the evaluation of impact targets in the mechanical safety testing of dangerous goods packagings N2 - The mechanical and geometrical properties of impact targets greatly influence the outcome of a drop test. The International Agreement concerning the International Carriage of Dangerous Goods by Road (ADR) as well as ISO 2248 describe the characteristics of impact targets for drop tests of dangerous goods packagings. According to these regulations, the impact target’s surface needs to be unyielding, under testing conditions non-deformable, flat, and integral with a mass at least 50 times that of the heaviest packaging to be tested. The problem is that many production facilities, especially manufacturers of corrugated fibreboard boxes, do not have their own testing device with the required 50 times mass ratio of the impact target for a regulation compliant drop test during series production. Furthermore, at UN level it is considered necessary to revise these requirements. In the present paper, the impact target requirements are examined in detail and compared with those in other technical areas (e.g., impact target for container for the transport of radioactive materials). A research method is being developed to investigate the dependency between the mass ratio of the packaging and the target as well as the damage resistance of a drop tested package in relation to specific design characteristics. The results are of high relevance for industry purposes and intended to ensure a uniform level of safety assessment for the mechanical testing of dangerous goods packagings. T2 - IAPRI Bangkok 2022, 23rd World Packaging Conference CY - Online meeting DA - 12.06.2022 KW - Corrugated fibreboard boxes KW - Dangerous goods packagings KW - Drop test KW - Impact target KW - Structural dynamics PY - 2022 AN - OPUS4-55121 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schmidt, Dirk A1 - Ruwe, L. A1 - Heidermann, T. A1 - Kreißig, M. A1 - Kant, Hanjo A1 - Gutte, F. A1 - Bartsch, D. A1 - Bosse, P. A1 - Lucassen, A. A1 - Schmidt, Dirk T1 - Experimental study on the performance of the standardized test method for detonation flame arresters N2 - Flame arresters are autonomous protection systems and are among the constructive explosion protection measures that limit the effects of an explosion. In this study, the performance of the standardized test method regulated in the DIN EN ISO 16852 standard for in-line flame arresters for stable and unstable detonations, which is mainly designed for atmospheric conditions, is examined. In an interlaboratory comparison, experiments are performed for different pressures before ignition and explosion groups according to the standardized test method. The experimental data is analyzed in detail to further optimize the test method and to thus achieve an improved reproducibility of detonation tests at high pressures, especially regarding the deflagration to detonation transition. Based on these results, an improved test method for detonation flame arresters will be developed, which will ensure better reproducibility as well as applicability under non-atmospheric conditions. T2 - 28th ICDERS 2022 CY - Naples, Italy DA - 19.06.2022 KW - Flame arrester KW - Explosion protection KW - Experimental tests PY - 2022 AN - OPUS4-55101 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -