TY - CONF A1 - Ávila Calderón, Luis Alexander A1 - Hammerschmidt, T. A1 - Stotzka, R. A1 - Forti, M. A1 - Olbricht, Jürgen A1 - Skrotzki, Birgit A1 - Lenze, A. A1 - Gedsun, A. A1 - Hickel, Tilmann A1 - Tsybenko, H. A1 - Chmielowski, M. A1 - Hunke, S. A1 - Shakeel, Y. T1 - Demonstration of the Infrastructure Use Case 02: Framework for curation and distribution of reference datasets N2 - In our current view, reference datasets in the MSE domain represent specific material properties, e.g., structural, mechanical, … characteristics. A reference dataset must fulfill high-quality standards, not only in precision of measurement but also in a comprehensive documentation of material, processing, and testing history (metadata). This Infrastructure Use Case (IUC) aims to develop a framework for generating reference material datasets using creep data of a single crystal Ni-based superalloy as a best practice example. In a community-driven process, we aim to encourage the discussion and establish a framework for the creation and distribution of reference material datasets. In this poster presentation, we highlight our current vision and activities and intend to stimulate the discussion about the topic reference datasets and future collaborations and work. T2 - NFDI-MatWerk Conference CY - Siegburg, Germany DA - 27.06.2023 KW - Referenzdaten KW - Reference data KW - Creep KW - Metadata schema KW - Syngle Crystal alloy PY - 2023 AN - OPUS4-57924 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Trappe, Volker A1 - Ghafafian, Carineh T1 - Scarf-joint repairs under fatigue loading investigated for sandwich shell applications N2 - Wind turbine rotor blades are produced as aerodynamic, three-dimensionally formed sandwich shell structures using mainly glass fiber reinforced plastics (GFRP). The GFRP used today have the potential to withstand the harsh operating conditions of rotor blades over the projected service life of 20 years. Premature damages that occur can be traced primarily back to design and/or manufacturing imperfections, as well as unusually high load scenarios (for instance lightning strikes, or strong winds combined with system control errors). Therefore, rotor blades have to be repaired several times (on average 2-3 times) during their projected service life. Approximately 70% of these are repairs of small- to medium-sized sandwich shells, carried out by technicians directly accessing the blade by suspended roping at the wind turbine location. The goal is to execute repairs that will last over the remaining service life, i.e. be sustainable. Within the framework of a research project carried out at BAM, Division 5.3 Polymer Matrix Composites, Department 5 for Materials Engineering, not only was the geometric shape (round vs. square in relation to the top view) varied, but also the layup of the scarf repair structure, variables that have not been studied systematically to-date. Sub-component scale sandwich shell specimens with representative repairs were used in this work in addition to coupon-scale specimens that are more commonly seen in literature. These sub-component shell specimens were tested using a unique shell test bench under loading conditions representative of wind turbine blade shell operating conditions with respect to fatigue strength. Using non-destructive testing methods (field strain measurement and thermography), damage development and distribution was monitored and analyzed in-situ. As a result, a concept was developed in which the repaired areas showed at least equivalent if not higher fatigue strength than the reference shells that were not repaired. T2 - ICFC9 - The 9th International Conference on the Fatigue of Composites CY - Vicenza, Italy DA - 21.06.2023 KW - Repair of sandwich shell structures KW - Non-destructive testing KW - Wind turbine blades PY - 2023 AN - OPUS4-57929 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schilling, Markus A1 - Bayerlein, Bernd A1 - Birkholz, H. A1 - von Hartrott, P. A1 - Waitelonis, J. A1 - Sack, H. T1 - PMDco - Platform MaterialDigital Core Ontology: Achieving High-Quality & Reliable FAIR Data N2 - Knowledge representation in the materials science and engineering (MSE) domain is a vast and multi-faceted challenge: Overlap, ambiguity, and inconsistency in terminology are common. Invariant and variant knowledge are difficult to align cross-domain. Generic top-level semantic terminology often is too abstract, while MSE domain terminology often is too specific. In this poster presentation, an approach how to maintain a comprehensive and intuitive MSE-centric terminology composing a mid-level ontology–the PMD core ontology (PMDco)–via MSE community-based curation procedures is shown. The PMDco is designed in direct support of the FAIR principles to address immediate needs of the global experts community and their requirements. The illustrated findings show how the PMDco bridges semantic gaps between high-level, MSE-specific, and other science domain semantics, how the PMDco lowers development and integration thresholds, and how to fuel it from real-world data sources ranging from manually conducted experiments and simulations as well as continuously automated industrial applications. T2 - DVM Arbeitskreis Betriebsfestigkeit - Potenziale der Betriebsfestigkeit in Zeiten des technologischen und gesellschaftlichen Wandels CY - Munich, Germany DA - 11.10.2023 KW - Digitalization KW - Semantic Web Technologies KW - FAIR KW - Data Interoperability KW - PMD Core Ontology PY - 2023 AN - OPUS4-58602 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Radners, Jan A1 - Han, Ying A1 - von Hartrott, Philipp A1 - Skrotzki, Birgit T1 - Aluminum High Temperature Fatigue N2 - The high operating temperatures of radial compressor wheels in exhaust gas turbochargers lead to abchange in the original microstructure of the heat-resistant aluminum alloy EN AW-2618A (overaging). This is caused by thermal loads that are close to the age hardening temperature and can even exceed it for a short time. The aging mechanisms have been investigated together with low cycle fatigue (LCF), thermomechanical fatigue (TMF) and creep up to max. 190 °C in previous research projects. The behavior of the alloy under high cycle fatigue (HCF) and the influence of load spectra have hardly been investigated. Since the operating temperatures of centrifugal compressors are expected to increase in the future, this research project investigated the HCF behavior at 230 °C, a test temperature significantly higher than the age hardening temperature. The objectives of the project were to establish a suitable experimental database, to understand the relevant microstructural processes, and to further develop and adapt suitable models and evaluation methods. In addition to a basic characterization of the HCF behavior in the initial condition T61, the experimental investigation program included targeted mechanical tests to isolate the influencing factors of mean stress (𝑅 = −1, 𝑅 = 0.1), material overaging (T61, 10 h/230 °C, 1000 h/230 °C), test temperature (20 °C, 230 °C), test frequency (0.2 Hz, 20 Hz) as well as variable amplitudes. On this basis, the models and evaluation methods developed in the previous projects were adapted and further developed to reflect thermal and mechanical loads in the lifetime assessment. T2 - The FVV Transfer + Networking Event (Herbst 2023) CY - Würzburg, Germany DA - 04.10.2023 KW - Aluminum alloys KW - Fatigue KW - EN AW-2618A PY - 2023 AN - OPUS4-58537 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Radners, Jan A1 - Han, Ying A1 - von Hartrott, Philipp A1 - Skrotzki, Birgit T1 - Aluminum High Temperature Fatigue N2 - The high operating temperatures of radial compressor wheels in exhaust gas turbochargers lead to a change in the original microstructure of the heat-resistant aluminum alloy EN AW-2618A (overaging). This is caused by thermal loads that are close to the age hardening temperature and can even exceed it for a short time. The aging mechanisms have been investigated together with low cycle fatigue (LCF), thermomechanical fatigue (TMF) and creep up to max. 190 °C in previous research projects. The be-havior of the alloy under high cycle fatigue (HCF) and the influence of load spectra have hardly been investigated. Since the operating temperatures of centrifugal compressors are expected to increase in the future, this research project investigated the HCF behavior at 230 °C, a test temperature significantly higher than the age hardening temperature. The objectives of the project were to establish a suitable experimental database, to understand the relevant microstructural processes, and to further develop and adapt suitable models and evaluation methods. In addition to a basic characterization of the HCF behavior in the initial condition T61, the experimental investigation program included targeted mechanical tests to isolate the influencing factors of mean stress (𝑅=−1, 𝑅=0.1), material overaging (T61, 10 h/230 °C, 1000 h/230 °C), test temperature (20 °C, 230 °C), test frequency (0.2 Hz, 20 Hz) as well as variable amplitudes. On this basis, the models and evaluation methods developed in the previous projects were adapted and further developed to reflect thermal and mechanical loads in the lifetime assessment. T2 - The FVV Transfer + Networking Event (Herbst 2023) CY - Würzburg, Germany DA - 04.10.2023 KW - Aluminum alloys KW - Fatigue KW - EN AW-2618A PY - 2023 SP - 1 EP - 30 AN - OPUS4-58562 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kolsch, Nico A1 - Meyer, Lena A1 - Zocca, Andrea A1 - Wilbig, Janka A1 - Günster, Jens T1 - Enabling online quality control of powder deposition for 3d printing in microgravity N2 - 3D printing or additive manufacturing in space is of great value for long-term human spaceflight missions and space stations, conveniently offering access to a ‘virtual warehouse’ of tools and spare parts on the push of a button. The process only needs one type of feedstock such as powder or filament and only as much material as the final part requires, giving it a huge weight benefit over traditional subtractive methods. While 3D printers are already operational on the ISS since 2014, the utilized processes are only capable of manufacturing relatively low strength parts from polymers not suitable for many tools or critical components. To gain access to high quality metal prints, a modified Laser Powder Bed Fusion (LPBF) process was developed to stabilize the critical powder bed in microgravity through a gas flow [2]. This setup was able to generate a (miniature) steel wrench during parabolic flights, but a reliable layer deposition has raised challenges due to the combination of gas flow parameters with microgravity conditions. Furthermore, the quality and density of the powder bed, which is critical for the process, cannot be examined afterward on the ground. This is due to hyper gravity phases during the flight that are influencing the properties of the powder bed. In this paper, the challenges of the layer deposition are revised, and the subsequent evolution of the recoating system explained. Later, the challenges of an in-situ quality control, evaluation, and quantification of the properties of the powder bed are examined. As a solution, a high-resolution line-scanner is proposed and its implementation int the compact LPBF system demonstrated. Its ability to measure common defects such as ridges in the deposited layer is shown in experiments at normal gravity. As an illustration, Figure 1 shows an extreme case of the formation of ridges. T2 - European Conference on Spacecraft Structures Materials and Environmental Testing CY - Toulouse, France DA - 28.03.2023 KW - Additive manufacturing KW - In-space manufacturing KW - Online quality control KW - Microgravity KW - Powder deposition PY - 2023 AN - OPUS4-57249 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zocca, Andrea A1 - Günster, Jens T1 - A comparison of layerwise slurry deposition and (LSD-print) laser induced slip casting (LIS) for the additive manufacturing of advanced ceramics N2 - The presentation gives an overview of two slurry-based additive manufacturing (AM) technologies specifically developed for advanced ceramic materials. The “Layerwise Slurry Deposition” (LSD-print) is a modification of Binder Jetting making use of a ceramic slurry instead of a dry powder as a feedstock. In this process, a slurry is deposited layer-by-layer by means of a doctor blade and dried to achieve a highly packed powder layer, which is then printed by jetting a binder. The LSD-print technology combines the high-speed printing of binder jetting with the possibility of producing a variety of high-quality ceramics with properties comparable to those achieved by traditional processing. The Laser Induced Slip casting (LIS) technology follows a novel working principle by locally drying and selectively consolidating layer-by-layer a ceramic green body in a vat of slurry, using a laser as energy source. LIS combines elements of Vat Photopolymerization with the use of water-based feedstocks containing a minimal amount of organic additives. The resulting technology can be directly integrated into a traditional ceramic process chain by manufacturing green bodies that are sintered without the need of a dedicated debinding. Both technologies offer high flexibility in the ceramic feedstock used, especially concerning material and particle size. Advantages and disadvantages are briefly described to outline the specific features of LSD-print and LIS depending on the targeted application. T2 - AM Ceramics CY - Vienna, Austria DA - 27.09.2023 KW - Additive Manufacturing KW - Dental KW - Ceramics KW - Feldspar PY - 2023 AN - OPUS4-58468 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zocca, Andrea A1 - Schubert, Hendrik A1 - Günster, Jens A1 - Hoffman, Moritz A1 - Bogna Stawarczyk, Bogna T1 - Additive Manufacturing for dental restorations by layerwise slurry deposition (LSD-print) technology N2 - The growing market of custom-made dental restorations offers a major potential for an application of ceramic additive manufacturing (AM). The possibility to individualize patient specific design and to establish new efficient workflows, from model generation to manufacturing, can be fully exploited by AM technologies. However, for mass customization to be truly envisioned, ceramic AM needs to achieve a level of maturity, aesthetic quality, and productivity comparable to established manufacturing processes. In this presentation, the potential of the “layerwise slurry deposition” LSD-print technology for dental applications will be explored. It has been shown in the past years that the LSD-print can be applied to advanced ceramic materials such as alumina and silicon-infiltrated silicon carbide. For these materials, the LSD-print technology combines the high-speed printing of binder jetting with the possibility of producing a variety of high-quality ceramics. The current development deals with the challenges of applying this technology to a feldspar dental material, comparing the quality of AM restorations with the equivalent material for an established CAD/CAM workflow. Preliminary results not only indicate that the AM material produced by LSD-print can be competitive in terms of mechanical properties, but also that aesthetically satisfactory restorations can be manufactured for veneers, inlays and onlays as well as single unit fixed dental prostheses (FDPs). The presentation focuses on the material and technological challenges alongside the process chain, from the printing process, to debinding, firing and finishing the restorations. T2 - XVIIIth Conference of the European Ceramic Society CY - Lyon, France DA - 02.07.2023 KW - Additive Manufacturing KW - Layerwise slurry deposition KW - dental KW - ceramic PY - 2023 AN - OPUS4-58469 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bayerlein, Bernd T1 - News from the working area - Semantic Interoperability N2 - This presentation provides a comprehensive overview of recent developments and the current status within the Semantic Interoperability work area, with a particular emphasis on the advancements related to the Platform MaterialDigital Core Ontology (PMDco). The presentation will delve into the collaborative and community-supported curation process that has been instrumental in shaping PMDco. Additionally, we will introduce the innovative Ontology Playground, showcasing its role in fostering experimentation and exploration within the realm of ontology development. T2 - MaterialDigital Vollversammlung CY - Karlsruhe, Germany DA - 21.09.2023 KW - Semantic Representation KW - FAIR data management KW - Semantic Interoperability KW - Knowledge graph and ontologies KW - PMD Core Ontology KW - MaterialDigital PY - 2023 AN - OPUS4-58422 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - THES A1 - Charmi, Amir T1 - A multiscale numerical framework for the simulation of anistropic material response of additively manufactured stainless steel 316L undergoing large plastic deformation N2 - Additive manufacturing (AM) offers significantly greater freedom of design compared to conventional manufacturing processes since the final parts are built layer by layer. This enables metal AM, also known as metal 3D printing, to be utilized for improving efficiency and functionality, for the production of parts with very complex geometries, and rapid prototyping. However, despite many technological advancements made in recent years, several challenges hinder the mass adoption of metal AM. One of these challenges is mechanical anisotropy which describes the dependency of material properties on the material orientation. Therefore, in this work, stainless steel 316L parts produced by laser-based powder bed fusion are used to isolate and understand the root cause of anisotropy in AM parts. Furthermore, an efficient and accurate multiscale numerical framework is presented for predicting the deformation behavior of actual AM parts on the macroscale undergoing large plastic deformations. Finally, a novel constitutive model for the plastic spin is formulated to capture the influence of the microstructure evolution on the material behavior on the macroscale. KW - Additive Fertigung KW - Austenitischer Stahl KW - Finite-Elemente-Methode KW - Mehrskalenmodell KW - Simulation PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:gbv:wim2-20240207-173356-002 DO - https://doi.org/10.25643/dbt.59550 SP - 1 EP - 163 PB - Bauhaus-Universität Weimar CY - Weimar AN - OPUS4-59511 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Maaß, Robert T1 - Tracing structural dynamics in metallic glasses during cryogenic cycling N2 - Highly unrelaxed structural states of metallic glasses have often advantageous mechanical properties. Since metallic glasses continuously relax with time (age) or inherently are well relaxed after processing, methods to uniformly rejuvenate the material are needed. One approach that has received attention is the so-called cryogenic-cycling method, during which a metallic glass is repeatedly immersed into liquid nitrogen. In some cases, cryogenic cycling is truly efficient in increasing the stored excess enthalpy of metallic glasses, but it does not seem to be universally applicable to all alloys and structural states. The origins for these differences remain unclear due to our limited understanding of the underlying structural evolution. In order to shed more light onto the fundamental structural processes of cryogenic cycling, we pursue in-situ x-ray photon correlation spectroscopy (XPCS) to trace the atomic-scale structural dynamics of a Zr-based metallic glass in two different structural states (ribbon and bulk metallic glass). This method allows calculating the relaxation times as a function of time throughout the thermal cycling. It is found that the investigated glasses exhibit heterogeneous structural dynamics at 300 K, which changes to monotonic aging at 78 K. Cryogenic cycling homogenizes the relaxation time distribution for both structural states. This effect is much more pronounced in the ribbon, which is the only structural state that rejuvenates upon cycling. We furthermore reveal how fast atomic-scale dynamics is correlated with long-time average structural relaxation times irrespective of the state, and that the ribbon exhibits unexpected additional fast atomic-scale relaxation in comparison to the plate material. Overall, a picture emerges that points towards heterogeneities in fictive temperature as a requirement for cryogenic energy storage. T2 - MRS Fall 2020 - Invited Talk CY - Boston, MA, USA DA - 27.11.2020 KW - Relaxation metallic glasses PY - 2020 AN - OPUS4-59542 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kalinka, Gerhard T1 - Testing the fibre matrix interface of short glass fibre reinforced PMCs with using the push out technique N2 - With this presentation, the push-out technique is explained. The focus of the experimental work is on the characterization of the fiber-matrix interface of short fiber reinforced composites. The reinforcing component was glass fibers and the matrix polymer was PA6.6 and PPA. It is demonstrated for the first time that the push-out technique ca be applied on injection molded short fiber PMC and is sensitive to the mechanical interface properties. Further studies are planned on the influence of multiple processing, the temperature and humidity. T2 - Composirtes United Workshop „Fiber Matrix Interphases“ CY - Online meeting DA - 09.11.2023 KW - Polymer Matrix Composite KW - Glass Fibres KW - PA6.6 KW - PPA KW - Push-out Test KW - Interface Strength PY - 2023 AN - OPUS4-59053 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schilling, Markus A1 - Bayerlein, Bernd A1 - Birkholz, H. A1 - Hanke, T. A1 - Waitelonis, J. A1 - Sack, H. T1 - PMDco: Achieving High-Quality & Reliable FAIR Data N2 - Knowledge representation in the materials science and engineering (MSE) domain is a vast and multi-faceted challenge: Overlap, ambiguity, and inconsistency in terminology are common. Invariant and variant knowledge are difficult to align cross-domain. Generic top-level semantic terminology often is too abstract, while MSE domain terminology often is too specific. In this presentation, an approach how to maintain a comprehensive and intuitive MSE-centric terminology composing a mid-level ontology–the PMD core ontology (PMDco)–via MSE community-based curation procedures is shown. The PMDco is designed in direct support of the FAIR principles to address immediate needs of the global experts community and their requirements. The illustrated findings show how the PMDco bridges semantic gaps between high-level, MSE-specific, and other science domain semantics, how the PMDco lowers development and integration thresholds, and how to fuel it from real-world data sources ranging from manually conducted experiments and simulations as well as continuously automated industrial applications. T2 - Kupfer-Symposium CY - Jena, Germany DA - 29.11.2023 KW - Ontology KW - Semantic Web Technologies KW - Plattform MaterialDigital KW - PMDco PY - 2023 AN - OPUS4-59031 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Gomes Fernandes, Roger A1 - Al-Mukadam, Raschid A1 - Bornhöft, Hansjörg A1 - Reinsch, Stefan A1 - Müller, Ralf A1 - Selle, Susanne A1 - Deubener, Joachim T1 - Viscous Sintering of Acid Leached Glass Powders N2 - The process of viscous flow sintering is a phenomenon that is closely linked to the surface properties of the glass particles. In this work, we studied the extreme case of acid-leaching of soda-lime-silicate glass beads of two different particle size distributions and its effects on non-isothermal viscous sintering of powder compacts. Depth profiling of the chemical composition after leaching revealed a near-surface layer depleted in alkali and alkaline earth ions, associated with concurrent hydration as mass loss was detected by thermogravimetry. Heating microscopy showed that acid treatment of glasses shifted the sinter curves to higher temperatures with increasing leaching time. Modelling of the shrinkage with the cluster model predicted a higher viscosity of the altered surface layer, while analysis of the time scales of mass transport of mobile species (Na+, Ca2+ and H2O) during isochronous sintering revealed that diffusion of Na+ can compensate for concentration gradients before sintering begins. Also, exchanged water species can diffuse out of the altered layer, but the depletion of Ca2+ in the altered surface layer persists during the sinter interval, resulting in a glass with higher viscosity, which causes sintering to slow down. KW - Glass powder KW - Viscous sintering KW - Acid-leaching KW - Sinter retardation PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-589008 DO - https://doi.org/10.52825/glass-europe.v1i.681 VL - 1 SP - 37 EP - 53 AN - OPUS4-58900 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - von Hartrott, Philipp A1 - Skrotzki, Birgit T1 - Room temperature and elevated temperature tensile test and elastic properties data of Al-alloy EN AW-2618A after different aging times and temperatures N2 - The dataset contains two types of data: elastic properties (Young's and shear modulus, Poisson's ratio) between room temperature and 250 °C and a set of tensile tests at different aging times, aging temperatures, and test temperatures. KW - Aluminium alloy KW - Young's modulus KW - Shear modulus KW - Aging KW - Tensile test KW - Strength PY - 2023 UR - https://doi.org/10.5281/zenodo.10377164 DO - https://doi.org/10.5281/zenodo.10377163 PB - Zenodo CY - Geneva AN - OPUS4-59161 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Schilling, Markus A1 - Bayerlein, Bernd A1 - Birkholz, H. A1 - Fliegener, S. A1 - Grundmann, J. A1 - Hanke, T. A1 - von Hartrott, P. A1 - Waitelonis, J. T1 - PMD Core Ontology (PMDco) N2 - The PMD Core Ontology (PMDco) is a comprehensive framework for representing knowledge that encompasses fundamental concepts from the domains of materials science and engineering (MSE). The PMDco has been designed as a mid-level ontology to establish a connection between specific MSE application ontologies and the domain neutral concepts found in established top-level ontologies. The primary goal of the PMDco is to promote interoperability between diverse domains. PMDco's class structure is both understandable and extensible, making it an efficient tool for organizing MSE knowledge. It serves as a semantic intermediate layer that unifies MSE knowledge representations, enabling data and metadata to be systematically integrated on key terms within the MSE domain. With PMDco, it is possible to seamlessly trace data generation. The design of PMDco is based on the W3C Provenance Ontology (PROV-O), which provides a standard framework for capturing the generation, derivation, and attribution of resources. By building on this foundation, PMDco facilitates the integration of data from various sources and the creation of complex workflows. In summary, PMDco is a valuable tool for researchers and practitioners in the MSE domains. It provides a common language for representing and sharing knowledge, allowing for efficient collaboration and promoting interoperability between diverse domains. Its design allows for the systematic integration of data and metadata, enabling seamless traceability of data generation. Overall, PMDco is a crucial step towards a unified and comprehensive understanding of the MSE domain. PMDco at GitHub: https://github.com/materialdigital/core-ontology KW - Ontology KW - Semantic Web technologies KW - Digitalization KW - Data Interoperability KW - PMD Core Ontology PY - 2023 UR - https://github.com/materialdigital/core-ontology/blob/f2bd420348b276583fad6fa0fb4225f17b893c78/pmd_core.ttl PB - GitHub CY - San Francisco, CA, USA AN - OPUS4-59352 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Dmitriev, A. I. A1 - Nikonov, A. Y. A1 - Österle, Werner T1 - Molecular dynamics modeling of the sliding performance of an amorphous silica nano-layer - The impact of chosen interatomic potentials N2 - The sliding behavior of an amorphous silica sample between two rigid surfaces is in the focus of the present paper. Molecular Dynamics using a classical Tersoff’s potential and a recently developed ReaxFF potential was applied for simulating sliding within a thin film corresponding to a tribofilm formed from silica nanoparticles. The simulations were performed at different temperatures corresponding to moderate and severe tribological stressing conditions. Simulations with both potentials revealed the need of considering different temperatures in order to obtain a sound interpretation of experimental findings. The results show the striking differences between the two potentials not only in terms of magnitude of the resistance stress (about one order of magnitude) but also in terms of friction mechanisms. The expected smooth sliding regime under high temperature conditions was predicted by both simulations, although with Tersoff’s potential smooth sliding was obtained only at the highest temperature. On the other hand, at room temperature Tersoff-style calculations demonstrate stick-slip behavior, which corresponds qualitatively with our experimental findings. Nevertheless, comparison with a macroscopic coefficient of friction is not possible because simulated resistance stresses do not depend on the applied normal pressure. KW - Molecular dynamics KW - Thin tribofilm KW - Resistance stress KW - Sliding simulation KW - Amorphous silica PY - 2018 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-449366 DO - https://doi.org/10.3390/lubricants6020043 SN - 2075-4442 VL - 6 IS - 2 SP - 43, 1 EP - 11 PB - MDPI CY - Basel AN - OPUS4-44936 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Pfennig, A. A1 - Kranzmann, Axel T1 - Corrosion and Fatigue of Heat Treated Martensitic Stainless Steel 1.4542 used for Geothermal Applications N2 - During capture and storage technology (CCS) as well as in geothermal energy production Steels need to withstand the corrosive environment such as: heat, pressure, salinity of the aquifer and CO2-partial pressure. 1.4542 shows unusual corrosion phenomena, but is still sufficiently resistant in corrosive environments. To better understand its behaviour differently heat treated coupons of 1.4542 and for comparison X20Cr13 and X46Cr13 were kept in the artificial brine of the Northern German Basin at T=60 °C. Ambient pressure as well as p=100 bar for 700 h - 8000 h in water saturated supercritical CO2 and CO2-saturated synthetic aquifer Environment was applied. Fatigue tests were performed via push-pull tests with a series of 30 specimens from 150 MPa to 500 MPa (sinusoidal dynamic test loads, R=-1; resonant frequency ~ 30 Hz). FeCO3 and FeOOH are corrosion products also after dynamic corrosion tests. Martensitic microstructure offers good corrosion resistance in geothermal environment. The S-N-curve showing no typical fatigue strength and very steep slopes of possible fatigue strength for finite life. Possible influencing artefacts, such as Al-inclusions could not be correlated to early rupture despite specimens containing inclusions at the fracture surface and cross section reached lower number of cycles. Applied potential proofed to enhance fatigue life tremendously. KW - High Alloyed Steel KW - Pitting KW - Corrosion Fatigue KW - Corrosion KW - Endurance Limit PY - 2019 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-503765 DO - https://doi.org/10.20319/mijst.2019.51.138158 SN - 2454-5880 VL - 5 IS - 1 SP - 138 EP - 158 PB - Global Research and Development Services Publishing CY - Rajasthan, India AN - OPUS4-50376 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Pfennig, A. A1 - Wolf, M. A1 - Kranzmann, Axel T1 - The role of surface texture on the corrosion fatigue behavior of high alloyed stainless steel exposed to saline aquifer water environment N2 - Corrosion fatigue specimen with different surfaces (technical surfaces after machining and polished surfaces) of high alloyed martensitic stainless steel X46Cr13 (1.4043) and duplex stai nless steel X2CrNiMoN22 3 2 (1.4462) were compared at load amplitudes from 175 MPa to 325 MPa in the geothermal brine of the N orthern German Basin at 98 °C. Surface corrosion layers and pits reveal carbonate corrosion products on the surface such as FeCO 3 and FeOOH as the main precipitation phases with no dependence on the original surface roughness . At high stress amplitudes above 275 MPa technical surfaces (P50% at σa 300 MPa=5 × 10 5 ) resulted in more cycles to failure than polished (P50% at σa 300 MPa=1.5 × 10 5 ). The greater slope coefficient for technical surfaces k = 19.006 compared to polished surfaces k =8.78 demonstrate s earlier failure at given stress amplitude σa . KW - Corrosion KW - CCS KW - Carbon storage KW - Aquifer KW - Heat treatment PY - 2019 DO - https://doi.org/10.17706/ijmse SN - 2315-4527 VL - 7 IS - 2 SP - 26 EP - 33 PB - IAP - International Academy Publishing CY - San Bernardino, CA AN - OPUS4-50365 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Pfennig, A. A1 - Wolf, M. A1 - Kranzmann, Axel T1 - In-situ testing of corrosion and corrosion fatigue behavior of stainless steels in geothermal environment N2 - In CCS environment (carbon capture and storage) pipes are loaded statically and/or cyclically and at the same time exposed constantly to the highly corrosive hot thermal water. Experimental procedures such as ambient pressure immersions tests, in-situ corrosion fatigue experiments using a flexibly designed corrosion chamber at ambient pressure and a specially designed corrosion chamber at high pressure. Experimental set-ups for push/pull and rotation bending load are introduced. The corrosion behavior and lifetime reduction of high alloyed steels (X46Cr13, 1.4043), (X5CrNiCuNb16-4, 1.4542) and (X2CrNiMoN22-5-3, 1.4462) is demonstrated (T=60 °C, geothermal brine: Stuttgart Aquifer flow rate: 9 l/h, CO2 ). T2 - 10th International Conference on Chemical, Biological and Environmental Engineering ICBEE 2018 CY - Berlin, Germany DA - 27.09.2018 KW - Adiabatic calorimeter KW - Thermal energy storage KW - Phase change material KW - Salt eutectics PY - 2018 DO - https://doi.org/10.7763/IPCBEE.2018.V103.5 VL - 103 SP - 13 EP - 20 AN - OPUS4-50364 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -