TY - RPRT A1 - Göbel, Petra A1 - Meckel, Lothar A1 - Schiller, Wolfgang T1 - Untersuchung zur Erarbeitung von Kennwerten bei Einrichtungsmaterialien (Holzwerkstoffen, Möbeln und Textilien) hinsichtlich der Formaldehyd-Emission - Teil B: Textilien N2 - An Proben aus der Produktion wurde die Abhängigkeit der Emission vom Zeitpunkt der Probenahme, die Korrelation zu bestehenden Prüfverfahren durch Extraktion und der Einfluss des Klimas untersucht. Es zeigt sich, dass die Luftfeuchtigkeit einen großen Einfluss uf die Formaldelhyd-Emission hat. Ein Prüfverfahren zur Bestimmung der Ausgleichskonzentration von Formaldehyd wird vorgeschlagen. T3 - BAM Forschungsberichtreihe - 165 PY - 1989 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-2857 SN - 978-3-88314-935-7 SN - 0938-5533 VL - 165 SP - 1 EP - 79 PB - Wirtschaftsverlag NW CY - Bremerhaven AN - OPUS4-285 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Rabe, Torsten A1 - Schiller, Wolfgang Arno A1 - Roosen, A. A1 - Wagner, M. T1 - Charakterisierung keramischer Grünfolien und Laminate JF - Fortschrittsberichte der Deutschen Keramischen Gesellschaft T2 - Symposium Grünkörpercharakterisierung ; 8. Keramik-Tag der BAM CY - Berlin, Deutschland DA - 2001-05-28 PY - 2001 SN - 0177-6983 VL - 16 IS - 2 SP - 152 EP - 159 PB - Bauverlag CY - Bad Honnef AN - OPUS4-1836 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Rabe, Torsten A1 - Rudert, Rainer A1 - Harbich, Karl-Wolfram A1 - Schiller, Wolfgang Arno T1 - Microstructural Characterization of Green Ceramic Tapes and Laminates T2 - Proceedings of the Materials Week 2000 T2 - Materials Week 2000 ; International Congress on Advanced Materials, Their Processes and Applications 2000 CY - Munich, Germany DA - 2000-09-25 PY - 2000 SN - 3-88355-296-8 CY - München AN - OPUS4-1006 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eberstein, Markus A1 - Dernovsek, O. A1 - Nicolaides, Dagmar A1 - Schiller, Wolfgang Arno T1 - Modifikation von La2O3-B2O3-TiO2-Gläsern zur Einstellung von Mikrowelleneigenschaften niedrigsinternder Dielektrika T2 - Kurzreferate / 75. Glastechnische Tagung T2 - 75. Glastechnische Tagung CY - Wernigerode, Deutschland DA - 2001-05-21 PY - 2001 SP - 301 EP - 305 PB - DGG, Deutsche Glastechnische Gesellschaft e.V. CY - Frankfurt/M. AN - OPUS4-1651 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eberstein, Markus A1 - Schiller, Wolfgang Arno A1 - Drüe, K.-H. A1 - Thust, H. T1 - Design and characterization of microwave LTCC modified by high permittivity glasses T2 - Ceramic applications for microwave and photonic packaging T2 - IMAPS Advanced Technology Workshop on Ceramic Applications for Microwave and Photonic Packaging CY - Providence, RI, USA DA - 2002-05-02 PY - 2002 SP - 1 EP - 6 CY - Washington, DC AN - OPUS4-1652 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schiller, Wolfgang Arno A1 - Eberstein, Markus A1 - Müller, Ralf T1 - Glass Ceramic Composites for Microsystems JF - Glass science and technology PY - 2003 SN - 0927-4472 VL - 76 C1 SP - 54 EP - 59 PB - Elsevier CY - Amsterdam AN - OPUS4-2592 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schiller, Wolfgang Arno A1 - Eberstein, Markus A1 - Müller, Ralf T1 - Glas-Keramik-Komposite für Mikrosysteme und Sensoren JF - DGG-Journal PY - 2002 SN - 1618-8721 VL - 1 IS - 2 SP - 17 PB - Deutsche Glastechnische Gesellschaft CY - Offenbach AN - OPUS4-3115 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Peplinski, Burkhard A1 - Schiller, Wolfgang Arno A1 - Wenzel, Klaus-Jürgen A1 - Schultze, Dietrich A1 - Schiemann, Ingrid ED - Delhez, R. T1 - Phase selective chemical analysis of multi-component solids by X-ray powder diffratio - On the composition of a-cordierite-like solid solutions crystallizing from non-stoichiometric glasses T2 - Proceedings of the fifth European powder diffraction conference T2 - 5th European Powder Diffraction Conference CY - Parma, Italy DA - 1997-05-25 KW - Glass-ceramics KW - Cordierite KW - Solid solutions KW - Lattice parameter refinement KW - Whole-powder-pattern fitting KW - Rietveld analysis KW - Chemical analysis PY - 1998 SN - 0-87849-807-9 SN - 0255-5476 N1 - Serientitel: Materials science forum – Series title: Materials science forum IS - 278-281/2 SP - 578 EP - 583 PB - Trans Tech Publ. CY - Uetikon-Zürich AN - OPUS4-1196 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schiller, Wolfgang T1 - Kleben und Reinigen in der Textilrestaurierung JF - Restauro PY - 2002 SN - 0933-4017 IS - 5 SP - 344 EP - 348 PB - Callwey CY - München AN - OPUS4-1566 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Eberstein, Markus A1 - Schiller, Wolfgang Arno T1 - Neue niedrig sinternde Mikrowellenkeramik für Anwendungen in der mobilen Kommunikationstechnik JF - Keramische Zeitschrift PY - 2003 UR - http://www.keramische-zeitschrift.de/images/Keram_2003.pdf SN - 0023-0561 VL - 55 IS - 5 SP - 344 EP - 348 PB - DVS-Verl. CY - Düsseldorf AN - OPUS4-2754 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Eberstein, Markus A1 - Thiel, A. A1 - Reinsch, Stefan A1 - Müller, Ralf A1 - Deubener, J. A1 - Schiller, Wolfgang Arno T1 - Lösungs- und Kristallisationsvorgänge beim Sintern von Glasmatrix-Kompositen T2 - Programm und Referate / 79. Glastechnische Tagung T2 - 79. Glastechnische Tagung CY - Würzburg, Deutschland DA - 2005-05-23 KW - Glaspulver KW - Glasmatrix-Komposit KW - Sintern KW - Kristallisation PY - 2005 SN - 3-921089-43-3 SP - 7 Seiten PB - Deutsche Glastechnische Gesellschaft CY - Offenbach AN - OPUS4-10377 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schiller, Wolfgang Arno A1 - Gemeinert, Marion A1 - Güther, Wolfgang A1 - Schulz, Bärbel A1 - Brode, W. A1 - Müller, E. A1 - Modes, Ch. A1 - Gora, F. T1 - Zero Shrinkage LTCC für Mikrosensoren T2 - DKG Jahrestagung 2006 T2 - DKG Jahrestagung 2006 CY - Stuttgart, Germany DA - 2006-04-03 PY - 2006 AN - OPUS4-12424 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schiller, Wolfgang Arno A1 - Gemeinert, Marion T1 - Dünnfilmkompatible LTCC als Basis multifunktioneller Mehrlagengehäuse für Mikrosysteme T2 - Abschlusskolloquium zum BMBF-Projekt: Technologien für vertikale Mikrosystemaufbauten - Optobasis (16SV824/4) T2 - Abschlusskolloquium zum BMBF-Projekt: Technologien für vertikale Mikrosystemaufbauten - Optobasis (16SV824/4) CY - Berlin, Germany DA - 2002-03-05 PY - 2002 AN - OPUS4-6298 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schiller, Wolfgang Arno A1 - Rabe, Torsten T1 - Advanced LTCC Technologie: Neue werkstofftechnische konzepte für Kommunikations- und Sensoranwendungen T2 - DKG-Tagung "Technische Keramik in Funktion" T2 - DKG-Tagung "Technische Keramik in Funktion" CY - Hermsdorf (Thuringia), Germany DA - 2002-09-19 PY - 2002 AN - OPUS4-6300 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Zimmer, Hubertus A1 - Schiller, Wolfgang T1 - Quantitative Faseranalyse in Gegenwart von modifizierten Polyesterfasern JF - Melliand-Textilberichte PY - 1976 SN - 0025-8989 VL - 57 IS - 8 SP - 661 EP - 662 CY - Frankfurt, M. AN - OPUS4-8412 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schiller, Wolfgang T1 - Gesetzliche Textilkennzeichung in Deutschland T2 - DTV-Sachverständigenseminar; Forschungsinstitut Hohenstein T2 - DTV-Sachverständigenseminar; Forschungsinstitut Hohenstein CY - Bönnigheim, Germany DA - 2006-06-22 PY - 2006 AN - OPUS4-7701 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Rabe, Torsten A1 - Gemeinert, Marion A1 - Schiller, Wolfgang Arno T1 - Development of Advanced Low Temperature Co-fired Ceramics (LTCC) JF - Key engineering materials KW - LTCC KW - Zero shrinkage sintering KW - Multilayer KW - Material development PY - 2004 SN - 1013-9826 VL - 264-268 SP - 1181 EP - 1184 PB - Trans Tech Publ. CY - Aedermannsdorf AN - OPUS4-5843 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schiller, Wolfgang A1 - Zimmer, Hubertus T1 - Quantitative Bestimmung von Polypropylen-Fasern nach dem Heiß-Extraktionsverfahren JF - Melliand-Textilberichte PY - 1975 SN - 0025-8989 VL - 56 IS - 8 SP - 643 EP - 645 CY - Frankfurt, M. AN - OPUS4-8221 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schiller, Wolfgang T1 - Die neuen Pflegekennzeichen - Stets Priorität vor Fachwissen? T2 - Landesverbandstag des Textilreinigungs-Verbandes Nordrhein-Westfalen T2 - Landesverbandstag des Textilreinigungs-Verbandes Nordrhein-Westfalen CY - Rheine, Germany DA - 2005-03-18 PY - 2005 AN - OPUS4-7586 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schiller, Wolfgang A1 - Zimmer, Hubertus T1 - Analytisches Verhalten der nativen Fasern Wolle und Baumwolle bei Einwirkung von Hexafluorisopropanol JF - Melliand-Textilberichte PY - 1978 SN - 0025-8989 VL - 59 IS - 6 SP - 498 EP - 500 CY - Frankfurt, M. AN - OPUS4-8882 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Zimmer, Hubertus A1 - Schiller, Wolfgang T1 - Analysen von mit Bindern verfestigen Faservliesen JF - Schriftenreihe des Deutschen Wollforschungsinstituts PY - 1978 SN - 0170-6322 SN - 0930-3723 SP - 376 EP - 392 PB - TH CY - Aachen AN - OPUS4-8883 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Zimmer, Hubertus A1 - Schiller, Wolfgang T1 - Vergleich von zwei Methoden zur quantitativen Abtrennung von Elasthanfasern JF - Melliand-Textilberichte PY - 1979 SN - 0025-8989 VL - 60 IS - 3 SP - 18 EP - 22 CY - Frankfurt, M. AN - OPUS4-9119 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schiller, Wolfgang Arno A1 - Rabe, Torsten T1 - Neue werkstofftechnische Konzepte in der LTCC technologie T2 - 10. BAM Keramiktag / Symposium "Folie- und multilayertechnologie für funktionskeramische Anwendungen" T2 - 10. BAM Keramiktag / Symposium "Folie- und multilayertechnologie für funktionskeramische Anwendungen" CY - Berlin, Germany DA - 2003-04-10 PY - 2003 AN - OPUS4-5350 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schiller, Wolfgang Arno A1 - Rabe, Torsten T1 - LTCC-Keramik im Automobil T2 - MicroCar 2003 - Mikrowerkstoffe, Nanowerkstoffe für den Automobilbau T2 - MicroCar 2003 - Mikrowerkstoffe, Nanowerkstoffe für den Automobilbau CY - Leipzig, Germany DA - 2003-06-26 PY - 2003 AN - OPUS4-5351 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Zimmer, Hubertus A1 - Schiller, Wolfgang T1 - Analyse von mit Bindern verfestigten Nadelfilzfußbodenbelägen JF - Melliand-Textilberichte PY - 1977 SN - 0025-8989 VL - 58 IS - 11 SP - 931 EP - 934 CY - Frankfurt, M. AN - OPUS4-8673 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schiller, Wolfgang A1 - Zimmer, Hubertus T1 - Neue Wege in der quantitativen Faseranalyse JF - Melliand-Textilberichte PY - 1977 SN - 0025-8989 VL - 58 IS - 4 SP - 307 EP - 309 CY - Frankfurt, M. AN - OPUS4-8670 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schiller, Wolfgang T1 - Weltweite Trends bei Waschmitteln und der Haushaltswäsche T2 - Verbandstag der Ostdeutschen Textilreinigungs-Innung T2 - Verbandstag der Ostdeutschen Textilreinigungs-Innung CY - Schwerin, Germany DA - 2006-03-24 PY - 2006 AN - OPUS4-11993 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Tränkle, G. A1 - Fabich, F. A1 - Schiller, Wolfgang A1 - Reiners, Georg A1 - Hübert, Thomas A1 - Beck, Uwe T1 - Abschlussbericht zum Vorhaben Aufbau und Inbetriebnahme eines Zentrums für Mikrosystemtechnik (ZEMI) in Berlin-Adlershof PY - 2003 SP - 1 EP - 17 PB - Europäischer Fond für Regionale Entwicklung (EFRE) CY - Berlin AN - OPUS4-25603 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schiller, Wolfgang Arno A1 - Gemeinert, Marion A1 - Rabe, Torsten A1 - Modes, Ch. A1 - Brode, W. A1 - Bechtold, F. T1 - Neue Zero Shrinkage LTCC für Mikrosysteme hoher Präzision T2 - DKG/BAM-Symposium "Glasig-kristalline Funktionswerkstoffe - Vielfalt und Präzision" (12. Keramiktag der BAM) T2 - DKG/BAM-Symposium "Glasig-kristalline Funktionswerkstoffe - Vielfalt und Präzision" (12. Keramiktag der BAM) CY - Berlin, Germany DA - 2005-05-12 PY - 2005 AN - OPUS4-7810 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eberstein, Markus A1 - Müller, Ralf A1 - Reinsch, Stefan A1 - Rabe, Torsten A1 - Schiller, Wolfgang Arno A1 - Thiel, A. A1 - Deubener, J. T1 - Kinetic Modeling of LTCC-Shrinkage T2 - CICMT 2007 - 3rd International Conference and Exhibition on Ceramic Interconnect and Ceramic Microsystems Technologies (Proceedings) T2 - 3rd International Conference and Exhibition on Ceramic Interconnect and Ceramic Microsystems Technologies (CICMT 2007) CY - Denver, CO, USA DA - 2007-04-23 KW - LTCC KW - Glass matrix composites KW - Inclusions KW - Sintering kinetics KW - Modeling PY - 2007 SP - 1 EP - 8 PB - American Ceramic Soc. CY - Denver AN - OPUS4-14948 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schiller, Wolfgang Arno T1 - Hochleistungskeramik für die MIkrosystemtechnik und ihre Konsequenzen T2 - Symposium "Allgemeine Technologie", Leibnitz-Sozietät der Wissenschaften zu Berlin T2 - Symposium "Allgemeine Technologie", Leibnitz-Sozietät der Wissenschaften zu Berlin CY - Berlin, Germany DA - 2007-10-12 PY - 2007 AN - OPUS4-15868 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schiller, Wolfgang Arno A1 - Müller, Ralf A1 - Rabe, Torsten T1 - Über das Sintern von LTCC T2 - Symposium "Thermische Verfahrenstechnik" der DKG T2 - Symposium "Thermische Verfahrenstechnik" der DKG CY - Erlangen, Germany DA - 2007-11-27 PY - 2007 AN - OPUS4-15869 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schiller, Wolfgang Arno T1 - Keramische Multilayer für Mikrosysteme im Bereich Sensorik, Biomedizin und Energietechnik T2 - Symposium "Vision Keramik 2008++" T2 - Symposium "Vision Keramik 2008++" CY - Dresden, Germany DA - 2008-01-17 PY - 2008 AN - OPUS4-15870 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Weh, Lothar A1 - Venthur, Astrid A1 - Schiller, Wolfgang Arno T1 - Defekte und Oberflächenstrukturen in keramischen Folien auf Polyvinylbutyral-Basis JF - Keramische Zeitschrift N2 - Defekte und störende Oberflächenstrukturen keramischer Bauelemente, die aus keramischen Folien gefertigt werden, haben neben keramtechnologischen Prozessfehlern vielfach ihre Ursachen in dynamischen Prozessen bei der Trocknung der Nassschichten. Neben Einzeldefekten wie Poren oder Rissen können in Grünfolien während der Trocknung auch oberflächenspannungsinduzierte periodische Schichtdickenunterschiede auftreten. Grenzflächenendynamische Bewegungen wie auch die Bildung von Blasen oder Agglomeraten treten gleichermaßen in gegossenen keramischen Schichten und in keramikfreien Polyvinylbutyral/Weichmacher-Schichten auf. Das analoge Verhalten der untersuchten gegossenen keramischen Schichten und der entsprechenden keramikfreien Polymerschichten bezüglich der Entstehung dieser Oberflächenfehler sowie Möglichkeiten zur Fehlerreduzierung werden aufgezeigt. KW - Keramische Folien KW - Oberflächentopologie KW - Defekte KW - Marangoni-Instabilität KW - Schlicker KW - Oberfläche KW - Gefüge KW - Grenzflächenprozesse PY - 2004 UR - http://www.keramische-zeitschrift.de/index.cfm?objekt=Keram&jahr=2004&ausgabe=9&rubrik=Aus%20Forschung%20und%20Technik&lang=DE&artikel_id=202007&navi=2 SN - 0023-0561 VL - 9-10 SP - 562 EP - 572 PB - DVS-Verl. CY - Düsseldorf AN - OPUS4-4755 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schiller, Wolfgang Arno A1 - Gemeinert, Marion A1 - Güther, Wolfgang T1 - Werkstofftechnik der Hochleistungskeramik und Werbundwerkstoffe T2 - Materialica 2003 T2 - Materialica 2003 CY - Munich, Germany DA - 2003-09-15 PY - 2003 AN - OPUS4-4748 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Eberstein, Markus A1 - Müller, Ralf A1 - Reinsch, Stefan A1 - Rabe, Torsten A1 - Schiller, Wolfgang Arno A1 - Thiel, A. A1 - Deubener, J. T1 - Kinetic Modeling of LTCC Shrinkage: Effect of Alumina Content JF - Journal of microelectronics and electronic packaging N2 - We studied sintering of LTCC-type glass matrix composites (GMCs) consisting of small glass and alumina particles of equal size. Primarily, crystals act as rigid inclusions, decelerating the densification rate. In later stages, they also dissolve, partially increasing the viscosity. Release of alumina finally induces crystallization of alumosilicates, which enables post-firing stability. To study both effects, two model GMCs were prepared: an α-Al2O3 + barium alumoborosilicate glass (BABS)–GMC, which shows neither significant dissolution nor crystallization, and an α-Al2O3 + calcium alumoborosilicate glass (CABS)–GMC, which dissolves readily and promotes crystallization. The kinetics of shrinkage for both GMC were modeled by utilizing Frenkel theory for the early stage and Mackenzie–Shuttleworth theory for the late stage, assuming that sintering is superimposed by the weighted contributions of triparticle glass–crystal clusters, their random occurrence (ideal mixing), and a shrinkage rate controlled by the GMC effective viscosity. In agreement with modeling, the experimental results showed that the shrinkage rate of BABS–GMC decreases progressively for crystal volume fractions Φ > 0.15. The attainable shrinkage is reduced by up to 8% for Φ = 0.45. For the CABS–GMC with Φ = 0.25, a reduction of Φ to 0.20 was evident due to partial α-Al2O3 dissolution. This effect was found able to increase the sintering temperature by ~50–60 K. KW - LTCC KW - Glas Matrix Composites KW - Inclusions KW - Sintering Kinetics KW - Modeling PY - 2007 SN - 1551-4897 VL - 4 IS - 4 SP - 173 EP - 180 CY - Washington, DC AN - OPUS4-16506 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Reinsch, Stefan A1 - Müller, Ralf A1 - Eberstein, Markus A1 - Deubener, J. A1 - Thiel, A. A1 - Schiller, Wolfgang Arno ED - J.G. Heinrich, ED - C.G. Aneziris, T1 - Effect of dispersed Al2O3 particles on sintering of glass matrix composites T2 - Proceedings of the 10th International Conference of the European Ceramic Society T2 - 10th International Conference of the European Ceramic Society CY - Berlin DA - 2007-06-17 KW - LTCC KW - Glass matrix composites KW - Inclusions KW - Sintering kinetics KW - Modelling PY - 2007 SN - 3-87264-022-4 SP - 290 EP - 295 PB - Göller CY - Baden-Baden AN - OPUS4-17445 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eberstein, Markus A1 - Glitzky, Carsten A1 - Gemeinert, Marion A1 - Rabe, Torsten A1 - Schiller, Wolfgang Arno A1 - Modes, C. T1 - Design of LTCC with high thermal expansion T2 - Proceedings and exhibitor presentations - 4th International Conference and Exhibition on Ceramic Interconnect and Ceramic Microsystems Technologies T2 - IMAPS/ACERS 4th International Conference and Exhibition on Ceramic Interconnect and Ceramic Microsystems Technologies (CICMT 2008) CY - Munich, Germany DA - 2008-04-21 KW - LTCC KW - Glass ceramic composites KW - Coefficient of thermal expansion CTE KW - Design PY - 2008 SP - 000120 EP - 000126 PB - IMAPS, International Microelectronics and Packaging Society CY - Washington, DC AN - OPUS4-17436 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Müller, Ralf A1 - Reinsch, Stefan A1 - Eberstein, Markus A1 - Deubener, J. A1 - Thiel, A. A1 - Schiller, Wolfgang Arno T1 - Effects of dispersed Al2O3 particles on sintering of LTCC JF - Advanced materials research N2 - The sintering of Low Temperature Co-fired Ceramics prepared from alumoborosilicate glass- and Al2O3 powders of similar small particle size was studied by dilatometry, heating microscopy, microstructure analysis, glass- and effective viscosity measurements. The steric effect of Al3O3 inclusions was studied using a gnon-reactiveh model composite. With increasing Al3O3 volume fraction (Φ ≤ 0.45), sintering decelerates and its final stage shifts to higher temperature. The attainable shrinkage is reduced as Al2O3 particle clusters bearing residual pores become more frequent. The kinetics of sintering could be described formally superposing the weighed contributions of differentially sized and randomly composed glass-crystal particle clusters and assuming a sintering rate controlled by the effective matrix viscosity, which increases with Φ and with progressive wetting of Al2O3 particles during densification. The "reactive" model composite shows significant dissolution of Al2O3 into the glass, which has two opposed effects on sintering: reducing Φ and increasing glass viscosity. For the present case (Φ = 0.25), the latter effect dominates and sintering is retarded by Al2O3 dissolution. Crystallization of wollastonite starts after full densification. Dissolution of Al2O3 was found to promote the subsequent growth of anorthite. KW - LTCC KW - Glass matrix composites KW - Al2O3-inclusions KW - Sintering kinetics PY - 2005 SN - 1022-6680 SN - 1662-8985 VL - 39-40 SP - 375 EP - 380 PB - Trans Tech Publ. CY - Zurich AN - OPUS4-18441 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Müller, Ralf A1 - Eberstein, Markus A1 - Reinsch, Stefan A1 - Schiller, Wolfgang Arno A1 - Deubener, J. A1 - Thiel, A. T1 - Effect of rigid inclusions on sintering of low temperature co-fired ceramics JF - European journal of glass science and technology / B KW - Sintering KW - Glass Matrix Composites KW - Rigid Inclusion KW - Effective Viscosity KW - Kinetic Modelling KW - LTCC PY - 2007 SN - 1753-3562 SN - 0017-1050 SN - 0031-9090 SN - 1750-6697 VL - 48 IS - 4 SP - 259 EP - 266 PB - Society of Glass Technology CY - Sheffield AN - OPUS4-16211 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eberstein, Markus A1 - Rabe, Torsten A1 - Schiller, Wolfgang Arno T1 - Liquid Phases in LTCC - Key to Tailored Materials T2 - CICMT 2006 - 2nd International Conference and Exhibition on Ceramic Interconnect and Ceramic Microsystems Technologies (Proceedings) T2 - MAPS/ACerS 2nd International Conference and Exhibition on Ceramic Interconnect and Ceramic Microsystems Technologies (CICMT 2006) CY - Denver, CO, USA DA - 2006-04-24 KW - LTCC KW - Ceramic composites KW - Liquid phase sintering KW - Viscosity KW - Dielectric properties KW - Crystallization PY - 2006 SP - 1(?) EP - 8(?) PB - American Ceramic Society CY - Denver AN - OPUS4-14043 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Eberstein, Markus A1 - Rabe, Torsten A1 - Schiller, Wolfgang Arno T1 - Influences of the Glass Phase on Densification, Microstructure, and Properties of Low-Temperature Co-Fired Ceramics JF - International Journal of Applied Ceramic Technology N2 - Multilayer ceramic devices based on low-temperature co-fired ceramics (LTCC) materials provide a very promising technology. Most LTCC tapes available today contain considerable fractions of glass powders to lower the sintering temperature. However, the glassy phases offer more possibilities to set a proper sintering behavior, on the one hand, and to tailor the desired properties of the final LTCC substrate, on the other. The exploitation of demixing and subsequent crystallizing glass compositions was shown on an example of a low-permittivity (4.4)—low-loss (1.5 × 103) LTCC with a high quartz content. In another LTCC material, undesired demixing could be restricted and the crystal phase anorthite could be triggered by partial dissolution of alumina in the liquid phase during sintering. To estimate the effect of silver diffusion in the latter material, the surroundings of a pure silver via were studied. A silver-contaminated range of 50 µm was detected. Using model glasses containing silver oxide, a strong influence of dissolved silver on viscosity and crystallization behavior of the liquid phase was demonstrated. The dielectric properties of the sintered substrates were not degraded. KW - LTCC KW - Glass phases KW - Sintering KW - Dielectric properties PY - 2006 DO - https://doi.org/10.1111/j.1744-7402.2006.02108.x SN - 1546-542X SN - 1744-7402 VL - 27 IS - 6 SP - 428 EP - 436 PB - American Ceramic Soc. CY - Westerville, Ohio AN - OPUS4-14044 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Thiel, A. A1 - Eberstein, Markus A1 - Reinsch, Stefan A1 - Müller, Ralf A1 - Deubener, J. A1 - Schiller, Wolfgang Arno T1 - Viskosität von sinternden Glas/Kristallphasen-Kompositen T2 - Programm und Referate - 80. Glastechnische Tagung T2 - 80. Glastechnische Tagung CY - Dresden, Deutschland DA - 2006-06-12 PY - 2006 SN - 3-921089-46-8 SP - 1(?) EP - 3(?) PB - Verl. d. Dt. Glastechn. Ges. CY - Offenbach AN - OPUS4-14045 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Eberstein, Markus A1 - Thiel, A. A1 - Reinsch, Stefan A1 - Müller, Ralf A1 - Deubener, J. A1 - Schiller, Wolfgang Arno T1 - Sinterkinetik von Glasmatrix-Kompositen mit reaktiver Dispersphase T2 - Programm und Referate - 80. Glastechnische Tagung T2 - 80. Glastechnische Tagung CY - Dresden, Deutschland DA - 2006-06-12 PY - 2006 SN - 3-921089-46-8 SP - 4 Seiten PB - Verl. d. Dt. Glastechn. Ges. CY - Offenbach AN - OPUS4-14046 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Rabe, Torsten A1 - Eberstein, Markus A1 - Schiller, Wolfgang Arno ED - Kevin Ewsuk, ED - Kiyoshi Nogi, ED - Wäsche, Rolf ED - Yukichi Umakoshi, ED - Tom Hinklin, ED - Keizo Uematsu, ED - Tony Tomsia, ED - Hiroya Abe, ED - Hidehiro Kamiya, ED - Makio Naito, T1 - Low Temperature Co-Fired Ceramics (LTCC) - Design and Characterization of Interfaces T2 - Characterization and Control of Interfaces for High Quality Advanced Materials II / Ceramic Transactions T2 - 2nd International Conference on Characterization and Control of Interfaces for High Quality Advanced Materials, and Joining Technology for New Metallic Glasses and Inorganic Materials 2006 CY - Kurashiki, Japan DA - 2006-09-06 KW - Grenzflächenreaktionen KW - Keramische Multilayer KW - Sintern PY - 2007 SN - 978-0-470-18414-1 VL - 198 SP - 173 EP - 178 PB - John Wiley & Sons, Ltd. AN - OPUS4-16123 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schiller, Wolfgang Arno A1 - Müller, Ralf A1 - Rabe, Torsten ED - R. Clasen, ED - M. Herrmann, ED - Roosen, A. T1 - Über das Sintern von LTCC JF - Ceramic forum international / Beihefte / Fortschrittsberichte der Deutschen Keramischen Gesellschaft KW - LTCC KW - Komposite KW - Multilayer-Technik KW - Sintern KW - Simulation PY - 2007 SN - 0177-6983 VL - 21 IS - 1 SP - 41 EP - 46 PB - Göller CY - Baden-Baden AN - OPUS4-16428 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Reinsch, Stefan A1 - Gaber, Martin A1 - Müller, Ralf A1 - Schiller, Wolfgang Arno T1 - Rate controlled debindering of glass ceramic composites JF - Advanced materials research N2 - Green compacts of ceramics, glass ceramic composites and sinter glass ceramics contain different amounts of organic materials added as pressing aids or binders. Before sintering, these organics have to burn out completely. In oxidising atmospheres, the debindering process is mostly exothermic and therefore difficult to control. This uncontrolled heat production due to locally enhanced debindering and respective gas release may cause damages in the green compact microstructure. Therefore, debindering is usually operated with very low heating rates (< 3 K/min) which requires long processing times of many hours. In this paper, we will show that it is possible to reduce the processing time for debindering dramatically by using the decomposition rate of the organic binder, detected by the weight loss of the sample, as a control factor of the furnace. T2 - 9th ESG (European Society of Glass) Conference with the Annual Meeting of the ICG Glass - "The challenge for the 21st century" CY - Trencin, Slovakia DA - 2008-06-22 KW - Debindering KW - Thermo gravimetry KW - Glass ceramic composites PY - 2005 SN - 1022-6680 SN - 1662-8985 VL - 39-40 SP - 583 EP - 586 PB - Trans Tech Publ. CY - Zurich AN - OPUS4-17840 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schiller, Wolfgang Arno T1 - Zur Funktion der Gläser in der LTCC-Technologie T2 - DGG-Glasforum 2005, Schott AG T2 - DGG-Glasforum 2005, Schott AG CY - Mainz, Germany DA - 2005-10-18 PY - 2005 AN - OPUS4-11739 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schiller, Wolfgang Arno T1 - Hochleistungskeramik und Multilayer-Folien-Technik für Mikrosysteme T2 - Leibnitz-Sozietät, Klasse "Naturwissenschaften" T2 - Leibnitz-Sozietät, Klasse "Naturwissenschaften" CY - Berlin, Germany DA - 2005-12-08 PY - 2005 AN - OPUS4-11740 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Glitzky, Carsten A1 - Rabe, Torsten A1 - Eberstein, Markus A1 - Schiller, Wolfgang Arno A1 - Töpfer, J. A1 - Barth, S. A1 - Kipka, A. T1 - LTCC-Modules with integrated ferrite layers - Strategies for material development and co-sintering JF - Journal of microelectronics and electronic packaging N2 - The integration of passive components (resistors, capacitors, inductors) into LTCC modules is a challenging task in multilayer ceramics technology. We report on multilayer assemblies consisting of combined layers of ferrite and dielectric LTCC tapes. Ni-Cu-Zn ferrites with maximum shrinkage at 900°C were processed to green tapes and laminated with dielectric LTCC tapes. Cosintering at 900°C led to multilayers with different defects such as incomplete densification of the ferrite layers, cracks, and warpage. Since ferrite tapes do not really allow compositional changes without deterioration of magnetic properties, the dielectric tape was modified with the following objectives: (i) matching of the shrinkage curves of dielectric and ferrite materials, (ii) adjusting the coefficients of thermal expansion to avoid cracking during cooling, and (iii) controlling of interface reactions. Using this concept we fabricated dense and defect-free multilayers consisting of dielectric and ferrite layers. However, compositional changes of the individual ferrite tapes require the development of a specific dielectric tape material with tailored properties. KW - Coefficient of thermal expansion (CTE) KW - Cofiring KW - Ferrite KW - LTCC KW - Shrinkage PY - 2009 SN - 1551-4897 VL - 6 IS - 1 SP - 49 EP - 53 CY - Washington, DC AN - OPUS4-19708 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Müller, Ralf A1 - Meszaros, Robert A1 - Peplinski, Burkhard A1 - Reinsch, Stefan A1 - Eberstein, Markus A1 - Schiller, Wolfgang Arno A1 - Deubener, J. T1 - Dissolution of alumina, sintering, and crystallization in glass ceramic composites for LTCC JF - Journal of the American ceramic society KW - LTCC KW - Sintering KW - Crystallization KW - Alumina dissolution KW - Rietveld analysis PY - 2009 DO - https://doi.org/10.1111/j.1551-2916.2009.03089.x SN - 0002-7820 SN - 1551-2916 VL - 92 IS - 8 SP - 1703 EP - 1708 PB - Blackwell Publishing CY - Malden AN - OPUS4-20676 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Eberstein, Markus A1 - Reinsch, Stefan A1 - Müller, Ralf A1 - Deubener, J. A1 - Schiller, Wolfgang Arno T1 - Sintering of glass matrix composites with small rigid inclusions JF - Journal of the European Ceramic Society KW - Glass ceramics KW - Inclusions KW - Sintering KW - Mixing KW - Powders KW - Solid-state reaction PY - 2009 DO - https://doi.org/10.1016/j.jeurceramsoc.2009.02.007 SN - 0955-2219 SN - 1873-619X VL - 29 IS - 12 SP - 2469 EP - 2479 PB - Elsevier CY - Oxford AN - OPUS4-19570 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Eberstein, Markus A1 - Glitzky, Carsten A1 - Gemeinert, Marion A1 - Rabe, Torsten A1 - Schiller, Wolfgang Arno A1 - Modes, C. T1 - Design of LTCC with high thermal expansion JF - International Journal of Applied Ceramic Technology N2 - New applications of low-temperature co-fired ceramics (LTCC), such as pressure sensors or integrated functional layers, require materials that possess higher coefficients of thermal expansion (CTE). To fabricate LTCC with elevated CTE, two methods of material design are examined: firstly, glass ceramic composites (GCC), which consist of >50 vol% glass in the starting powder, and, secondly, glass-bonded ceramics (GBC), where glass is added as a sintering aid only. The CTE of GBC is mainly determined by the crystalline component. For GCC, the CTE can be well predicted, if CTE and elastic data of each phase in the microstructure are known. A nonlinear characteristic of the CTE versus phase composition was found with increasing Ecrystals/Eglass ratio and absolute CTE difference between the components. The glass composition and glass amount can be used to compensate the fixed properties of a crystalline material in a desired way. However, because the CTE and permittivity of a glass cannot be chosen independently, an optimum glass composition has to be found. For a given LTCC, it is possible to control the devitrification by shifting the glass composition. In this way, the resulting CTE values can be predicted more exactly and tailoring becomes possible. Different LTCC materials, based on the crystalline compounds Ba(La,Nd)2Ti4O12, ZrO2 (Y-TZP), SiO2 (quartz), and specially developed glasses, possessing an elevated CTE of around 10 × 10-6 K-1 while showing permittivity εr between 6 and 63, are introduced. KW - LTCC KW - Glass ceramic composites KW - Coefficient of thermal expansion CTE KW - Design PY - 2009 DO - https://doi.org/10.1111/j.1744-7402.2008.02316.x SN - 1546-542X SN - 1744-7402 VL - 6 IS - 1 SP - 1 EP - 8 PB - American Ceramic Soc. CY - Westerville, Ohio AN - OPUS4-18675 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Glitzky, Carsten A1 - Rabe, Torsten A1 - Eberstein, Markus A1 - Schiller, Wolfgang Arno A1 - Töpfer, J. A1 - Barth, S. A1 - Kipka, A. T1 - LTCC-modules with integrated ferrite layers - Strategies for material development and co-sintering T2 - CICMT 2008 - 4th International Conference and Exhibition on Ceramic Interconnect and Ceramic Microsystems Technologies, April 21-24, 2008, Munich, Germany (Proceedings) T2 - 2009 IMAPS/ACerS - 5th International Conference and Exhibition on Ceramic Interconnect and Ceramic Microsystems Technologies (CICMT) CY - Denver, Colorado, USA DA - 2009-04-21 KW - LTCC KW - Ferrite KW - Co-firing KW - Shrinkage KW - Coefficient of thermal expansion (CTE) PY - 2008 SN - 0-930815-83-1 SP - 000058 EP - 000063 AN - OPUS4-18926 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schiller, Wolfgang Arno A1 - Müller, Ralf A1 - Eberstein, Markus A1 - Reinsch, Stefan A1 - Rabe, Torsten T1 - Sintering of LTCC JF - Ceramic Forum International : cfi N2 - Low Temperature Co-fired Ceramic materials (LTCC) have attracted growing interest in recent years since they are promising candidates for highly integrated ceramic packaging. This paper surveys materials concepts of related glass ceramic composites (GCC) and discusses unsolved problems and challenges. The densification of GCC based on "viscous sintering" may be affected by steric effects and partial dissolution of dispersed crystal particles, crystallization and phase boundary reactions. KW - Sintering KW - Glass ceramic composites KW - Viscosity KW - Densification KW - Modelling PY - 2008 SN - 0173-9913 SN - 0196-6219 VL - 85 IS - 13 SP - 12 EP - 17 PB - Göller CY - Baden-Baden AN - OPUS4-19086 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Eberle, Arno A1 - Sievert, Rainer A1 - Schiller, Wolfgang Arno T1 - Flip-Chip-Lotbumps thermisch-zyklisch belastet - Einfluß des Substratmaterials auf das viskoplastische Verhalten von Flip-Chip-Lotbumps JF - Materialprüfung = Materials testing PY - 1998 SN - 0025-5300 VL - 40 IS - 9 SP - 350 EP - 352 PB - Carl Hanser Verlag CY - München AN - OPUS4-33715 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eberle, Arno A1 - Sievert, Rainer A1 - Schiller, Wolfgang Arno T1 - Numerical investigation on the influence of different substrate materials on the viscoplastic behaviour of flip chip solder bumps T2 - International symposium on advanced packaging materials 2000 (Proceedings) N2 - The finite element method was used to simulate the thermo-mechanical behaviour of a flip chip under thermocyclic loading between -55°C (-67°F) and 125°C (257°F). In order to simulate realistically the inelastic material response of the solder bump, Chaboche's viscoplastic material model instead of a classical ORNL-theory was implemented into the finite element code ABAQUS and applied to a flip chip configuration. This so-called unified constitutive model is able to describe the Bauschinger effect as well as the creep/plasticity interaction. Herewith the influence of the substrate material on the inelastic deformation behaviour of a tin-lead solder bump was analysed. A comparison is given with respect to the influence of the two substrate materials namely Al2O3 and our self-developed Low Temperature Co-fired Ceramics (LTCC) on the inelastic response of the Sn60Pb40 eutectic solder material. It may be shown that the thermoelastic behaviour of the LTCC substrate significantly reduces the cyclic stresses in the bump compared to Al2O3 as well as the cumulative inelastic strain which is responsible for the development of damage and hence flip chip failure T2 - International symposium on advanced packaging materials 2000 CY - Braselton, Georgia, USA DA - 06.03.2000 PY - 2000 SN - 0-930815-59-9 DO - https://doi.org/10.1109/ISAPM.2000.869253 SP - 112 EP - 117 AN - OPUS4-33716 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Reinsch, Stefan A1 - Eberstein, Markus A1 - Müller, Ralf A1 - Schiller, Wolfgang Arno A1 - Schweiger, M. T1 - Lastabhängige Schwindung von Glaspulvern N2 - Glasig-kristalline Sinterwerkstoffe werden für vielfältige Anwendungen eingesetzt. Bei einem hohen Glasanteil ist ein Einfluss geringer Lasten auf das Schwindungsverhalten möglich, so dass es zu Fehlinterpretationen des Schwindungsverhaltens bei gebräuchlichen Horizontaldilatometer kommen kann. T2 - 75. Glasetechnische Tagung CY - Wernigerode, Germany DA - 21.05.2001 KW - Glasig-kristalline Sinterwerkstoffe KW - Schwindungsverhalten KW - Horizontaldilatometer PY - 2001 AN - OPUS4-35786 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -