TY - JOUR A1 - Österle, Werner A1 - Dörfel, Ilona A1 - Prietzel, Claudia A1 - Rooch, Heidemarie A1 - Cristol-Bulthé, A.-L. A1 - Defallaix, G. A1 - Desplanques, Y. T1 - A comprehensive microscopic study of third body formation at the interface between a brake pad and brake disc during the final stage of a pin-on-disc test KW - Brake KW - Third body KW - Wear KW - Friction KW - Nano-scale KW - TEM PY - 2009 U6 - https://doi.org/10.1016/j.wear.2008.11.023 SN - 0043-1648 VL - 267 IS - 5-8 SP - 781 EP - 788 PB - Elsevier CY - Amsterdam AN - OPUS4-19450 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Österle, Werner T1 - Bohrer für den Nanometerbereich - Mikrobearbeitung und Gefügedarstellung mit der Technik des fokussierten Ionenstrahls (FIB) KW - FIB KW - Mikrobearbeitung KW - TEM KW - Nanotechnologie PY - 2004 U6 - https://doi.org/10.3139/120.100573 SN - 0025-5300 VL - 46 IS - 3 SP - 113 EP - 117 PB - Carl Hanser Verlag CY - München AN - OPUS4-3495 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Österle, Werner A1 - Dörfel, Ilona A1 - Gesatzke, Wolfgang A1 - Rooch, Heidemarie A1 - Urban, Ingrid T1 - Charakterisierung tribologischer Kontakte mit FIB und TEM KW - FIB KW - TEM KW - Verbundwerkstoff KW - Bremse KW - Diamantschicht PY - 2004 SN - 0032-678X N1 - Sprachen: Deutsch/Englisch - Languages: German/English VL - 41 IS - 4 SP - 166 EP - 179 PB - Hanser CY - München AN - OPUS4-3496 LA - mul AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Österle, Werner A1 - Dmitriev, A.I. A1 - Gradt, Thomas A1 - Häusler, Ines A1 - Hammouri, Basem A1 - Morales Guzman, Pablo Israel A1 - Wetzel, B. A1 - Yigit, D. A1 - Zhang, G. T1 - Exploring the beneficial role of tribofilms formed from an epoxy-based hybrid nanocomposite N2 - The composition and nanostructure of a beneficial tribofilm formed during sliding of a hybrid nanocomposite against steel were characterized comprehensively. A similar nanostructure was produced by high energy ball milling of the three identified tribofilm constituents: silica, hematite and graphite. By supplying powders to a pin-on-disc test it has been shown that neither silica, nor hematite, nor a mixture of both provide the low coefficient of friction (COF) observed for the hybrid composite. Only if graphite was blended with the oxides, the low COF was obtained. Thus, a film of finely dispersed stable inorganic wear products containing 15 vol% graphite provides low friction and wear in the considered case. KW - TEM KW - Nanocomposite KW - Tribofilm KW - Ball milling KW - Pin-on-disc test PY - 2015 U6 - https://doi.org/10.1016/j.triboint.2015.03.006 SN - 0301-679X VL - 88 SP - 126 EP - 134 PB - Butterworth-Heinemann CY - Oxford AN - OPUS4-33035 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Engelhardt, Monika A1 - Gesatzke, Wolfgang A1 - Österle, Werner A1 - Müller, Urs A1 - Rooch, Heidemarie A1 - Saliwan Neumann, Romeo A1 - Urban, Ingrid T1 - Makro- und Mikrogefüge von Bremsbelägen KW - Bremsbelag KW - Polymermatrix-Verbundstoff KW - Röntgenfluoreszenzanalyse KW - REM KW - FIB KW - TEM PY - 2005 SN - 3-88355-343-3 SN - 0343-3579 N1 - Serientitel: Sonderbände der praktischen Metallographie – Series title: Sonderbände der praktischen Metallographie IS - 37 SP - 105 EP - 110 PB - Werkstoff-Informationsges. CY - Frankfurt AN - OPUS4-10996 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Dörfel, Ilona A1 - Österle, Werner A1 - Urban, Ingrid A1 - Bouzy, E. T1 - Microstructural characterization of binary and ternary hard coating systems for wear protection - Part I: PVD coatings N2 - Different wear-resistant coatings produced by physical vapour deposition (PVD) were characterized with the aid of cross-sectional transmission electron microscopy (XTEM). All coating systems were optimized by the producers and exhibited good properties with respect to their special applications. The microstructure, texture and chemical composition of binary and ternary systems produced by the arc process [TiN, CrN, Cr2N (Ti, Cr)N on steel substrates] and magnetron sputtering process [TiN, CrN on steel substrates, (Ti, Al)N on Si-substrate] were investigated. All coatings had a more or less columnar microstructure, which was interrupted by interlayers in some cases. Whereas arc coatings always did show some kind of substrate modification, the latter was not observed after magnetron sputtering. Electron diffraction normally revealed a mono-phase fcc structure, except at sites very near to the interface. Only for the systems Cr–N and (Ti, Cr)–N were different additional phases observed at low nitrogen partial pressures. KW - Arc bond sputtering KW - Arc deposition KW - Magnetron sputtering KW - TEM KW - XTEM PY - 1999 UR - http://www.sciencedirect.com/science?_ob=ArticleURL&_udi=B6TVV-3VTRSCY-G&_user=963821&_coverDate=01%2F29%2F1999&_rdoc=14&_fmt=summary&_orig=browse&_srch=doc-info(%23toc%235544%231999%23998889997%2360972%23FLA%23display%23Volume)&_cdi=5544&_sort=d&_docanch U6 - https://doi.org/10.1016/S0257-8972(98)00735-X SN - 0257-8972 VL - 111 IS - 2-3 SP - 199 EP - 209 PB - Elsevier Science CY - Lausanne AN - OPUS4-2364 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Österle, Werner A1 - Griepentrog, Michael A1 - Klaffke, Dieter T1 - Microstructural characterization of wear particles formed during tribological stressing of TiC and Ti(C,N) coatings N2 - An attempt was undertaken to obtain a better understanding of the tribological properties of two wear-resistant coatings on tool steel by structural and microchemical analysis of wear particles using a transmission electron microscope. Coatings were deposited by physical vapor deposition and plasma-assisted chemical vapor deposition techniques and tribological properties were derived from reciprocating sliding tests of the coatings against alumina balls. Three types of wear particles were identified by electron diffraction and energy dispersive X-ray spectroscopy: nanocrystalline rutile (TiO2), nanocrystalline graphite and microcrystalline graphite. Low coefficients of friction, of the order of 0.2, were attributed to the formation of solid lubricant films of sub-stoichiometric TiO2-x Magnéli phases and/or graphite. KW - Third body KW - Solid lubrication KW - Coating, debris KW - Wear particle KW - TEM PY - 2002 U6 - https://doi.org/10.1023/A:1015491027710 SN - 1023-8883 SN - 1573-2711 VL - 12 IS - 4 SP - 229 EP - 234 PB - Springer Science Business Media B.V. CY - Dordrecht AN - OPUS4-1379 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Grulke, E. A. A1 - Yamamoto, K. A1 - Kumagai, K. A1 - Häusler, Ines A1 - Österle, Werner A1 - Ortel, Erik A1 - Hodoroaba, Vasile-Dan A1 - Brown, S. C. A1 - Chan, C. A1 - Zheng, J. A1 - Yamamoto, K. A1 - Yashiki, K. A1 - Song, N. W. A1 - Kim, Y. H. A1 - Stefaniak, A. B. A1 - Schwegler-Berry, D. A1 - Coleman, V. A. A1 - Jämting, Å. K. A1 - Herrmann, J. A1 - Arakawa, T. A1 - Burchett, W. W. A1 - Lambert, J. W. A1 - Stromberg, A. J. T1 - Size and shape distributions of primary crystallites in titania aggregates N2 - The primary crystallite size of titania powder relates to its properties in a number of applications. Transmission electron microscopy was used in this interlaboratory comparison (ILC) to measure primary crystallite size and shape distributions for a commercial aggregated titania powder. Data of four size descriptors and two shape descriptors were evaluated across nine laboratories. Data repeatability and reproducibility was evaluated by analysis of variance. One-third of the laboratory pairs had similar size descriptor data, but 83% of the pairs had similar aspect ratio data. Scale descriptor distributions were generally unimodal and were well-described by lognormal reference models. Shape descriptor distributions were multi-modal but data visualization plots demonstrated that the Weibull distribution was preferred to the normal distribution. For the equivalent circular diameter size descriptor, measurement uncertainties of the lognormal distribution scale and width parameters were 9.5% and 22%, respectively. For the aspect ratio shape descriptor, the measurement uncertainties of the Weibull distribution scale and width parameters were 7.0% and 26%, respectively. Both measurement uncertainty estimates and data visualizations should be used to analyze size and shape distributions of particles on the nanoscale. KW - Measurement uncertainty KW - Size distribution KW - Shape distribution KW - TEM KW - Titania PY - 2017 U6 - https://doi.org/10.1016/j.apt.2017.03.027 SN - 0921-8831 VL - 28 IS - 7 SP - 1647 EP - 1659 PB - Elsevier B.V. AN - OPUS4-40478 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Seah, M.P. A1 - Spencer, S.J. A1 - Bensebaa, F. A1 - Vickridge, I. A1 - Danzebrink, H. A1 - Krumrey, M. A1 - Gross, Thomas A1 - Österle, Werner A1 - Wendler, E. A1 - Rheinländer, B. A1 - Azuma, Y. A1 - Kojima, I. A1 - Suzuki, N. A1 - Suzuki, M. A1 - Tanuma, S. A1 - Moon, D.W. A1 - Lee, H.J. A1 - Cho, H.M. A1 - Chen, H.Y. A1 - Wee, A. T. S. A1 - Osipowicz, T. A1 - Pan, J.S. A1 - Jordaan, W.A. A1 - Hauert, R. A1 - Klotz, U. A1 - van der Marel, C. A1 - Verheijen, M. A1 - Tamminga, Y. A1 - Jeynes, C. A1 - Bailey, P. A1 - Biswas, S. A1 - Falke, U. A1 - Nguyen, N.V. A1 - Chandler-Horowitz, D. A1 - Ehrstein, J.R. A1 - Muller, D. A1 - Dura, J.A. T1 - Ultra-thin SiO2 on Si, Part V: Results of a CCQM Pilot Study of Thickness Measurements KW - SiO2 KW - Thin films KW - Thickness KW - XPS KW - Ellipsometry KW - TEM PY - 2003 SN - 1473-2734 SP - 57 pages AN - OPUS4-4118 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Bettge, Dirk A1 - Österle, Werner T1 - “Cube slip” in near-[111] oriented specimens of a single-crystal nickel-base superalloy N2 - In the past few years, it has been discussed with increasing frequency, whether cube slip does occur in gamma' hardened nickel-base superalloys. Occurrence of cube slip has consequences for the modeling of orientation dependence of the CRSS. Until now, there are only few experimental investigations. In principle, cube slip should be possible in primitive cubic lattices (e.g. L12 ordered gamma' phase) but not in face centered cubic ones (e.g. Ni solid solution). The most favourable specimen orientations are near [111], where the Schmid factors for this type of glide exceed those for octahedral systems. There are two basic methods to detect cube slip: macroscopic slip trace analysis and Transmission electron microscopy (TEM) investigation of the dislocation structure. Few observations of cube slip by macroscopic slip traces are reported in the literature. But it is still uncertain under which test conditions cube slip occurs and what the dislocation mechanisms are. Cube slip was observed during tensile or compression tests of several first generation superalloys, but it seems not to occur during shear creep deformation (e.g. CMSX-4 at 980°C), and it is also lacking under conventional tensile or compression loading, if the gmma' particles are small. No observations were ever reported of dislocations gliding on {001} planes in matrix channels. KW - Cube slip KW - Nickel-base superalloy KW - Dislocations KW - TEM PY - 1999 U6 - https://doi.org/10.1016/S1359-6462(98)00446-1 SN - 1359-6462 VL - 40 IS - 4 SP - 389 EP - 395 PB - Elsevier AN - OPUS4-38220 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -