TY - CONF A1 - Werner, Jan T1 - "Nicht ganz dicht" - Dichtheitsprobleme bei Ausrüstungsteilen von Eisenbahnkesselwagen T2 - 11. Gefahrgut Technik-Tage, BAM CY - Berlin, Germany DA - 2008-11-20 PY - 2008 AN - OPUS4-18337 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Pötzsch, Klaus-Michael A1 - Jochems, Frank A1 - Werner, Jan T1 - Dichtheit von Eisenbahnkesselwagen N2 - Zur Gewährleistung der Dichtheit von Eisenbahnkesselwagen während des Betriebs stellt das europäische Gefahrgutrecht für den Eisenbahnverkehr (RID) sowohl bauliche, konstruktive Anforderungen an die Ausrüstung wie auch an die Verwendung, den Betrieb dieser Kesselwagen und deren Ausrüstungsteile. Das Ziel des Projekts bestand in der Ermittlung der Ursachen für auftretende Undichtigkeiten an den unteren Füll- und Entleerungseinrichtungen von Kesselwagen im Betrieb (zum Transport von Gefahrgütern der Klasse 3 in Deutschland) und der Ausarbeitung entsprechender Vorschläge in technischer und organisatorischer Richtung sowie zur zugehörenden Rechtslage zur Vermeidung dieser Undichtigkeiten. KW - Dichtheit KW - Tropfleckagen KW - Füll- und Entleerungseinrichtungen an Tanks KW - Eisenbahnkesselwagen KW - Mineralöl KW - Verschlusseinrichtungen PY - 2007 SN - 0937-9762 IS - 668-1 SP - 1 EP - 71 CY - Hamburg AN - OPUS4-19515 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Pötzsch, Klaus-Michael A1 - Werner, Jan T1 - Gefährliche Güter in loser Schüttung - das neue Kapitel 6.11 im RID/ADR 2005 KW - Bulktransport KW - Zulassungsverfahren KW - Container PY - 2005 SN - 0944-6117 VL - 13 IS - April SP - 3 Seiten PB - Vogel CY - München AN - OPUS4-7022 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Werner, Jan A1 - Pötzsch, Klaus-Michael A1 - Würsig, Andreas A1 - Miethe, Sylvia T1 - Wieso, weshalb, warum? (Erfahrungsaustausch Tank 2005 - Teil I) KW - Protokoll zur Diskussion aktueller Problemfelder des Tankbaus KW - Tankzulassung KW - Gefahrgut-Verkehrsrecht PY - 2005 SN - 0016-5808 VL - 50 IS - 7 SP - 8 EP - 9 PB - Storck CY - Hamburg AN - OPUS4-10854 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Werner, Jan A1 - Pötzsch, Klaus-Michael A1 - Würsig, Andreas A1 - Miethe, Sylvia T1 - Wieso, weshalb, warum? (Erfahrungsaustausch Tank 2005 - Teil II) KW - Protokoll zur Diskussion aktueller Problemfelder des Tankbaus KW - Tankzulassung KW - Gefahrgut-Verkehrsrecht PY - 2005 SN - 0016-5808 VL - 50 IS - 8 SP - 10 EP - 12 PB - Storck CY - Hamburg AN - OPUS4-10866 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Werner, Jan T1 - Schüttgutcontainer für Gefahrgut BK 1/BK 2 T2 - Entsorga-Enteco, Messe Köln CY - Cologne, Germany DA - 2006-10-24 PY - 2006 AN - OPUS4-13451 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Werner, Jan T1 - BK? VV? Gefahrgut: nicht gerührt, sondern geschüttet T2 - 16. Berlin-Brandenburger Gefahrguttage CY - Berlin, Germany DA - 2007-11-29 PY - 2007 AN - OPUS4-16185 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Werner, Jan T1 - ISO-Container CSC T2 - ERFA Tanks, BK-Schüttgut-Container und MEMU, BAM CY - Berlin, Germany DA - 2011-10-20 PY - 2011 AN - OPUS4-24606 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Werner, Jan T1 - Gefahrguttransport im Schienengüterverkehr: Gefahrgutumschließung und -transport in loser Schüttung: BK-Container als Bindeglied zwischen den Verkehrsträgern unter besonderer Berücksichtigung der Bauvorschriften für BK-Container T2 - Moderner Schienengüterverkehr 2012 und intermodaler Verkehr: Herausforderung für den Güterverkehrssektor: CY - Berlin, Germany DA - 2012-03-29 PY - 2012 AN - OPUS4-25667 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Konersmann, Rainer A1 - Werner, Jan A1 - Jochems, Frank T1 - Pipelineversagen durch Erdarbeiten N2 - Fast alle zu errichtenden Bauwerke benötigen ein entsprechendes Fundament, was bedeutet, dass die Erde aufgegraben werden muss. Beim Bodenaushub kann es aber Schwierigkeiten geben, denn es können z. B. tonnenschwere Steine im Untergrund liegen oder Kabel und Rohre, die niemand dort vermutet hat und von denen man nicht sofort weiß, ob sie noch in Betrieb sind. Oftmals werden Rohrleitungen, die Flüssigkeiten oder Gase befördern, 'angebaggert.' Über diese Pipelines sollten zwar Pläne existieren, aus denen die Lage eindeutig hervorgeht. Doch Theorie und Praxis streben oftmals weit auseinander. Nachfolgender Beitrag geht der Frage nach, warum es bei Grabungsarbeiten in der Peripherie von Pipelinetrassen – oftmals auch erst nach Jahren – zu Produktfreisetzungen kommt. KW - Pipeline KW - Erdarbeiten KW - Schädigungsmechanismus KW - Überwachung PY - 2013 SN - 2191-0073 VL - 3 IS - 9 SP - 54 EP - 58 PB - Springer-VDI-Verl. CY - Düsseldorf AN - OPUS4-29050 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Weltschev, Margit A1 - Werner, Jan A1 - Heming, Frank A1 - Haufe, Manuela T1 - Compatibility of sealing materials with biodiesel, bioethanol-gasoline and biodiesel-heating oil blends N2 - Biofuels including ethanol and biodiesel (fatty acid methyl ester) represent an impor-tant renewable fuel alternative to petroleum-derived transport fuels. Increasing bio-fuel use would bring some benefits, such as a reduction in oil demands and green-house gas emissions, and an improvement in air quality. Materials compatibility is a major concern whenever the fuel composition is changed in a fuel system. The aim of this work is to study the interaction between sealing materials such as FKM (fluorocarbon rubber), EPDM (ethylene-propylene-diene rubber), CR (chloro-prene rubber), CSM (chlorosulfonated polyethylene), NBR (acrylonitrile-butadiene rubber), IIR (butyl rubber), VMQ (methyl-vinyl-silicone rubber) and FVMQ (methyl-fluoro-silicone rubber) and biofuels such as biodiesel, E85 (fuel with 85% ethanol) and B10 (heating oil with 10% biodiesel) at 70°C for 84 days. Experiments were con-ducted with tests specimens of theses elastomers to document the changes in the mass and tensile properties of these sealing materials according to ISO 1817. The exposure tests of the elastomers in E85 at 70°C showed that the weight gain caused by swelling of the test specimens was in the range of 3% to 12%. However, the weight gain of the fluorinated elastomers was at the lower end of this range. Tensile strength and breaking elongation decreased by 22% to 61% or 13% to 77%. The lowest decrease in the tensile properties was determined for FKM, EPDM und IIR. These sealing materials were evaluated as resistant to E85 up to a temperature of 70°C. Biodiesel absorbed water more quickly and aged faster than conventional diesel fuel. The weight loss of the elastomers varied between 9% (FKM) and 126% (CSM) in biodiesel. FKM was evaluated as resistant with a 16% reduction in tensile strength, a 2% reduction in breaking elongation and low weight loss. NBR, EPDM, CSM and VMQ were evaluated as not resistant. CSM even lost 84% of its original tensile strength and 78% of its breaking elongation. The highest weight gain as a result of swelling was measured for CSM with 86%, for EPDM with 84% and for VMQ with 54% in B10, while the fluorine-containing elasto-mers FKM (1%) and FVMQ (3%) absorbed much less B10 and swelled less. FKM lost 23% in tensile strength and 17% in breaking elongation; FMVQ lost 29% in ten-sile strength and 36% in breaking elongation. FMVQ was, therefore, only limited in its resistance to B10. The elastomers NBR, EPDM, CSM and VMQ were not resistant to B10 at all as the decrease in the tensile properties was significantly over 50%. NBR lost about 93% and CSM about 100% of its breaking elongation. The conclusion of the investigations at 70°C is that FKM is the most resistant sealing material in biodiesel, E85 (fuel with 85% ethanol) and B10 (heating oil with 10% biodiesel). T2 - EUROCORR 2013 - The European corrosion congress CY - Estoril, Portugal DA - 01.09.2013 KW - Compatibility KW - Sealing materials KW - Biodiesel KW - E85 KW - B10 KW - Mass loss KW - Tensile properties PY - 2013 SN - 978-989-8601-31-5 SP - 1 EP - 6 AN - OPUS4-29150 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Weltschev, Margit A1 - Kohl, Anka A1 - Haufe, Manuela A1 - Werner, Jan T1 - Use of Fourier transform infrared spectroscopy to characterize nitric acid oxidation of polyethylene grades N2 - Resistance to oxidative degradation by nitric acid has been selected for a comparison of polyethylene grades in a European standard on suitability proof for alternative plastic resins used for packagings and intermediate bulk containers (IBCs) for the transport of dangerous goods. Measurements of the infrared (IR) absorption spectra of microtome slices cut from the walls of jerricans, which were pre-stored with 55% nitric acid for 21 and 42 days at 40°C, showed changes in the structure of the polyethylene. The penetration depths of 55% nitric acid into the polyethylene grades are, in principle, suitable for evaluating the resistance to oxidative degradation of polyethylene grades after pre-storage of the packagings for 21 days. After this period the packaging wall is not fully penetrated. The intensities of the IR bands at 1565 cm-1 (-NO2), 1630 cm-1 (-C=C) and 1654 cm-1 (-O-NO2) increased with the treatment time with 55% nitric acid as a result of oxidative damage by the nitric acid. The high increase in absorbance of the -C=C band in the region 1630 - 1690 cm-1 is attributable to paraffinic chain cracks. The absorbance of the -O-NO2 band, formed as result of the nitration process was still low at a test temperature of 40°C. T2 - NACE International Corrosion Conference 2013 CY - Orlando, FL, USA DA - 17.03.2013 KW - Polyethylenformstoffe KW - Beständigkeit gegen oxidativen Abbau KW - Salpetersäure KW - Eindringtiefen KW - FTIR KW - Verpackungen zum Transport von Gefahrgütern PY - 2013 SN - 978-1-627-48145-8 SP - 1 EP - 11 (Paper No. 2070) PB - Curran CY - Red Hook, NY AN - OPUS4-27981 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Weltschev, Margit A1 - Werner, Jan A1 - Haufe, Manuela A1 - Heyer, Martina T1 - Compatibility of high-density polyethylene grades with biofuels N2 - The aim of this work was to study the interaction between high-density polyethylene (HDPE) grades as material for dangerous goods packagings and biofuels such as E85 and biodiesel. Jerricans made of two polyethylene (PE) grades were filled with these fuels and exposed to temperatures of 20°C and 40°C for 1 year. Tensile properties (tensile strength, breaking elongation and elasticity modulus) and melt flow rate (MFR) were determined once a month, and Fourier transform infrared (FTIR) spectroscopy was used to evaluate changes in the chemical structure. Measurements of the MFR and tensile properties of the PE grades after 1 year of exposure to E85 showed only a slightly damaging influence. An increase in the peak of 1585 cm-1 (C=C) stretching vibrations is visible in the FTIR spectra after the immersion tests with E85. Therefore, packagings made of HDPE grades are suitable for the transport of E85. An increase in the MFR with immersion time of the grades in biodiesel was measured, in particular, after 1 year of exposure. The elasticity modulus of the PE grades was reduced with immersion time. The FTIR spectra showed a broadening of the CO peak of 1740 cm-1 and the appearance of the hydroxyl group at 3500 cm-1. Both results are explained by secondary degradation products of the PE decomposition process caused by increasing unsaturated fatty acid content in the biodiesel. In light of the above mentioned, it was concluded that HDPE grades are not suitable as packaging materials for the transport of biodiesel. T2 - IAPRI 2013 - 26th Symposium on packaging CY - Espoo, Finland DA - 10.06.2013 KW - Polyethylene grades KW - Biodiesel KW - E85 KW - Tensile properties KW - FTIR analysis PY - 2013 DO - https://doi.org/10.1002/pts.2028 SN - 0894-3214 VL - 27 SP - 231 EP - 240 PB - Wiley CY - Chichester, UK AN - OPUS4-28696 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Weltschev, Margit A1 - Niebergall, Ute A1 - Werner, Jan T1 - Comparison of the material parameters of polyethalene grades with the test performance behaviour of packagings for the transport of dangerous goods in relation to the pre-storage time with 55% nitric acid N2 - The material parameters melt flow rate (MFR), density (D), notched impact strength (NIS) at –30°C, stress crack resistance [determined with the Full Notch Creep Test (FNCT)] and resistance to oxidative degradation (Ox) have been selected for a comparison of polyethylene grades in the European standard EN 15507. These parameters have a relationship with design type tests of packagings for the transport of dangerous goods. This paper presents the results of additional investigations to determine the impact of the pre-storage time of jerricans with 55% nitric acid at 40°C and 23°C on the marginal drop heights in drop tests at –18°C, on the MFR and on the tensile properties. Jerricans made of different polyethylene grades were pre-stored with 55% nitric acid for 21, 42 and 84 days at 40°C and for six months at 23°C. The tests showed that the NIS values at –30°C of polyethylene grades were not comparable with marginal drop heights determined in drop tests at –18°C. Pre-damage with 55% nitric acid for 21 days at 40°C led to an increase in the marginal drop heights of the jerricans. Altering the test regulations by increasing pre-storage time with 55% nitric acid to 42 days would be an alternative. The test results demonstrated clearly that pre-storage of the jerricans for six months at 23°C caused a higher increase in the MFR and lower marginal drop heights for the jerricans when compared with pre-stored jerricans for 21 days at 40°C. KW - Polyethylene grades KW - Resistance to oxidative degradation KW - Nitric acid KW - Tensile properties KW - Packagings for the transport of dangerous goods KW - Drop tests PY - 2013 DO - https://doi.org/10.1002/pts.2037 SN - 0894-3214 VL - 27 SP - 409 EP - 421 PB - Wiley CY - Chichester, UK AN - OPUS4-28731 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Werner, Jan T1 - Ausführungen zum Gefahrgutrecht T2 - Gefahrgutseminar der AREVA GmbH CY - Erlangen, Germany DA - 2013-11-20 PY - 2013 AN - OPUS4-29670 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Jochems, Frank A1 - Werner, Jan T1 - Fachkenntnisse gefragt - Prüfstellen N2 - Die neue BAM-GGR 014 beschreibt ein Verfahren zur Anerkennung und Überwachung von Prüfstellen zur Prüfung von Tanks nach der GGVSee. PY - 2013 SN - 0944-6117 IS - 9 SP - 26 EP - 27 PB - Vogel CY - München AN - OPUS4-29423 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Quercetti, Thomas A1 - Feldkamp, Martin A1 - Gleim, Tobias A1 - Musolff, André A1 - Werner, Jan A1 - Wille, Frank T1 - Fire Test Stand for Thermal Testing of Large Packages for the Transport of Radioactive Materials N2 - Packages for the transport of high level radioactive materials are designed to withstand severe accidents. These packages must comply with the specific safety requirements SSR 6 [ of the International Atomic Energy Agency (IAEA). To guarantee compliance with these requirements, specific mechanical and thermal tests need to be addressed r egard ing the package type. Typically, the r egulations prescribe mechanical tests followed by a thermal test as part of a cumulative test scenario. The thermal test is specified by the exposure of a test specimen for a period of 30 minutes to a thermal environment that provides a heat flux equivalent to that of a hydrocarbon fuel air fire with an av erage fire temperature of at least 800 °C fully flame engulfing the test specimen. The Federal Institute for Materials Research and Testing (BAM) operates various test facilities for this purpose at their Test Site for Technical Safety (near Berlin in Germany). Thermal tests for large packages are conducted in an established fire test stand that may be adapted by the test setup to the geometric boundary conditions of a test specimen. This fire test stand is built for test specimens with masses up to 200,000 kg an d geometric dimensions relating to large transport packages including their impact limiters. The test specimen is usually placed on a water cooled support frame in the middle of the test stand. The fire is realized by burning propane gas which is released in liquid state from an array of gas nozzles arranged in the form of a burner ring surrounding the test specimen. For particularly extra large test specimens, two burner rings are used on top of each other and at different heights to firstly achieve full f ire engulfment with a significantly larger volume of fire and secondly to achieve the required heat output , cf. In advance of a regular thermal test BAM usually performs so called fire reference tests to determine the test conditions for compliance with the IAEA requirements. These tests are performed using a generic package which corresponds to the external geometr ic dimensions of the test specimen used later in the approval test. Then, this reference package is exposed to a fire under defined test parameters whereas the corresponding heat input determined from the temperature changes measured is regarded as main cr iterion for proofing compliance with the IAEA criteria. The paper shows the experimental proof of the suitability of BAM’s fire test stand for thermal testing of extra large packages. The heat input and fire temperatures fully meet the IAEA criteria and can also be set significantly higher for example for extra regulatory testing. T2 - PATRAM 2025 CY - San Antonio, TX, USA DA - 27.07.2025 KW - IAEA Regu-lations KW - Fire Test Stand KW - Accident Scenario KW - Fire Qualification PY - 2025 SP - 1 EP - 10 CY - Institute of Nuclear Materials Management (INMM) AN - OPUS4-63872 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Weltschev, Margit A1 - Werner, Jan A1 - Brandt, S. T1 - Compatibility of high density polyethylene grades with bioethanol-gasoline blends and biodiesel N2 - Biofuels including ethanol and biodiesel (fatty acid methyl ester) represent an important renewable fuel alternative to petroleum-derived transport fuels. Increasing biofuels use would have some benefits, such as a reduction in oil demand and greenhouse gas emissions, and an improvement in air quality. Materials compatibility is a major concern whenever the fuel composition is changed in a fuel System. The aim of this work is to study the interaction between high density polyethylene (HDPE) grades and biofuels such as E85 (fuel with 85 % ethanol) and biodiesel. 10 I jerricans made of two different polyethylene grades were filled with E85 and biodiesel and exposed to temperatures of 20°C and 40°C for one year. Tensile properties (tensile strength, breaking elongation and elasticity modulus) were determined in accordance with EN ISO 527-2 at 23±2 °C once a month, and Fourier Transform Infrared Spectroscopy (FTIR) was used to evaluate possible changes. The tensile properties of HDPE jerrican cuttings decreased, but not significantly, after immersion in E85 and biodiesel. In particular, the elasticity modulus of the polyethylene grades was reduced after exposure to biodiesel. Pin impression tests according to EN ISO 16101 were performed with test specimens of a HDPE grade in White Spirit, E85 and biodiesel. Measurements of the remaining tensile strength showed that biofuels had a stronger effect than White Spirit. The FTIR spectra of HDPE jerrican cuttings showed that immersion tests for one year with E85 at 20°C and 40°C only caused an increase in the peak of 1585 cm'1 (C=C Stretching vibrations) in the Chemical structure of HDPE. The FTIR spectra of HDPE jerrican cuttings showed that immersion tests for one year with biodiesel at 20°C and 40°C led to a broadening of the C=O peak of 1740 cm'1 and the appearance of the hydroxyl group at 3500 cm'1. Both results are explained by secondary degradation products of the polyethylene decomposition process caused by the temperature and unsaturated fatty acid content in the biodiesel since biodiesel decomposes quickly at elevated temperatures. The broadening of the C=O peak to 1740 cm'1 can be attributed to aldehyde carbonyl and ester Carbonyl groups mutually overlapping. Measurements of the melt flow rate (MFR) showed an increase in the MFR with immersion time in biodiesel due to the unsaturated fatty acid formed in the biodiesel. Diffusions of oxygen and rapeseed methyl ester increase the Chemical impact on polyethylene grades. T2 - EUROCORR 2012 - The European corrosion congress CY - Istanbul, Turkey DA - 09.09.2012 PY - 2012 SP - 1 EP - 12 AN - OPUS4-26534 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Quercetti, Thomas A1 - Feldkamp, Martin A1 - Gleim, Tobias A1 - Musolff, Andre A1 - Werner, Jan A1 - Wille, Frank T1 - A fire test stand for thermal testing of extra-large packages N2 - Packages for the transport of high-level radioactive materials are designed to withstand severe accidents. These packages must adhere to the specification-based criteria of the International Transport Regulations of the International Atomic Energy Agency (IAEA). To ensure compliance with these requirements, specific mechanical and thermal tests need to be addressed with respect to the package type. Typically, the Regulations prescribe mechanical tests followed by a thermal test as part of a cumulative test scenario. The thermal test is specified by the exposure of a test specimen for a period of 30 minutes to a thermal invironment that provides a heat flux equivalent to that of a hydrocarbon fuel-air fire with an average fire temperature of at least 800 °C fully flame engulfing the test specimen. The Federal Institute for Materials Research and Testing (BAM) operates various test facilities for this purpose at their test site (TTS) near Berlin in Germany. Thermal tests for large packages are carried out in an established fire test stand that can be adapted by the test-setup to the geometric boundary conditions of a test specimen. This fire test stand is built for test specimens with masses up to 200,000 kg and geometric dimensions relating to large transport packages including their impact limiters. The test specimen is usually placed on a water-cooled support frame in the middle of the test-stand. The fire is realized by burning propane gas which is released in liquid state from an array of gas nozzles arranged in the form of a burner ring surrounding the test specimen. For particularly extra-large test specimens, two burner rings are used on top of each other and at different heights in order to firstly achieve full fire engulfment with a significantly larger volume of fire and secondly to achieve the required heat output. In advance of a regular thermal test BAM usually performs so-called fire reference tests to determine the test conditions for compliance with the IAEA requirements. These tests are performed using a generic package which corresponds to the external geometric dimensions of the test specimen used later in the approval test. Then, this reference package is exposed to a fire under defined test parameters whereas the corresponding heat input determined from the temperature changes measured is regarded as main criterion for proofing compliance with the IAEA criteria.The paper shows the experimental proof of the suitability of BAM’s fire test stand for thermal testing of extra-large packages. The heat input and fire temperatures fully meet the IAEA criteria but can also be set significantly higher for e.g. extra-regulatory testing. T2 - ASME PVP 2025 CY - Montreal, Quebec, Kanada DA - 20.07.2025 KW - Test stand KW - Thermal testing KW - Package KW - Fire PY - 2025 SP - 1 EP - 6 AN - OPUS4-63892 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Werner, Jan T1 - Composite subjected to low temperatures N2 - To reduce the global emission of CO2, liquified natural gas (LNG) is increasingly used as fuel. As the pipeline network is not developed all around the globe, LNG needs to be transported via ship or truck. Double-walled tanks made of steel with a vacuum insulation are currently used to keep LNG at cryogenic temperatures (-162 °C; 111 K). The double-walled construction makes the tanks heavy and expensive. The vacuum insulation between the two walled structure ensures that the LNG stays liquid over the transportation time (boiling point of LNG: -162 ◦C). This causes a high temperature difference between the transported good and the ambient air. Furthermore, there are some restrictions in carrying out in-service inspection using a double-wall design. Therefore, alternative tank designs, such as single wall glass fiber reinforced plastics (GFRP), are of growing interest. The material properties of GFRP and tank insulation at cryogenic temperatures are investigated. Liquified nitrogen (-196 °C; 77 K) is used for all experiments at cryogenic temperatures for safety reasons. Thermal conductivity of different layers are investigated and compared. Mechanical properties are analyzed by performing 3-point bending tests on cooled specimen. When cooled, the specimens fail at a higher force, but all layers of the laminate fail at once. Further investigations into the characterization of material properties, such as CT scans are currently in preparation. Evaluation is done by FEM and in approximation via analytical solutions. T2 - ICMEA 2020 CY - Ho Chi Minh City, Vietnam DA - 06.01.2020 KW - GFRP KW - Tanks KW - Cryogenic temperatures KW - LNG KW - Composite material KW - Safety PY - 2020 AN - OPUS4-50415 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kutz, Philipp A1 - Otremba, Frank A1 - Werner, Jan T1 - Mechanical and Thermal Properties of Composite Material and Insulation for a Single Walled Tank for Cryogenic Liquids N2 - This paper describes the testing methods used to determine the thermal properties of insulation materials and mechanical properties of materials used for the load-bearing structure for pressure tanks (up to 4 bar, relative) and cryogenic liquids (LNG, −166 °C to -157 °C at atmospheric pressure). Goal is to design a transportation tank that does not exceed 4 bars (relative) within 10 h, starting at atmospheric pressure. PUR-foam is a suitable material for the insulation. A 12,5 l small scale tank prototype reached 4 bar (relative) within 87 minutes, which is, regarding the influence of the size, a satisfying result. The mechanical properties change significantly at cryogenic temperatures. The bending modulus is similar at first, but decreases at a certain point by appr. 50 %. However, the maximum stress is much higher and could not be reached within this testing setup. T2 - 26th Assembly Advanced Materials Congress CY - Stockholm, Sweden DA - 10.06.2019 KW - GFRP KW - LNG KW - Lightweight design KW - Thermal properties KW - Mechanical prtoperties PY - 2020 DO - https://doi.org/10.5185/amlett.2020.011457 VL - 11 IS - 1 SP - 1 EP - 6 PB - VBRI Press AN - OPUS4-50216 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Werner, Jan A1 - Kutz, P. W. A1 - Otremba, Frank T1 - Testing of Small Scale Tank Prototypes under Cryogenic Conditions N2 - Climate change, CO2 reduction, resource efficiency are only 3 current keywords that describe the current industrial-economic situation. In order to influence climate change effectively, the conversion of supply systems with technically usable forms of energy must succeed in the next decade. The international network founded in Baku in 2015 bundles research activities in the broad field of energy supply and energy efficiency. Discuss current research approaches and results with scientists and experts from renowned universities and follow Azerbaijan's efforts to implement the energy revolution. T2 - Neseff 2020 CY - Online meeting DA - 28.09.2020 KW - Mud pumps KW - Mud circulation system KW - Pistons KW - Hydrostatic pressure KW - Friction wear KW - Ceramic liners KW - Tribology PY - 2020 SN - 978-3-940471-59-8 SP - 4 EP - 9 AN - OPUS4-52149 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Werner, Jan T1 - Brandschutzbeschichtungen an Tanks - Prüfverfahren zur Bestimmung der Feuerwiderstandsfähigkeit von Druckbehältern mit einem Brandschutzsystem unter Standardbrandbedingungen - ISO 21843 N2 - Brandschutzbeschichtungen an Tanks können zuverlässig BLEVEs verhindern. Die ISO 21843 gibt hierzu neue Standards für Prüfverfahren vor und charakterisiert die Qualität von Unfallfeuern detaillierter als bisher. Die BAM hat auf ihren Prüfanlagen im TTS die Umsetzbarkeit dieser Anforderungen nachgewiesen. T2 - 29. Gefahrgutkongress Mecklenburg-Vorpommern CY - Rostock, Germany DA - 18.11.2025 KW - ISO 21843 KW - BLEVE KW - Brandschutz KW - Unfallfeuer KW - Wärmeübertragung PY - 2025 AN - OPUS4-64806 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Werner, Jan T1 - Verpackungen und Beförderungseinheiten im Zusammenspiel N2 - Die derzeitigen Explosivstoffschutz-Anforderungen des Regelwerks ADR basieren auf einem überholten Stand der Technik sowie Technologie der Baustoffe/Bauteile/Werkstoffe. Die Formulierung im entsprechenden Abschnitt des ADR (9.3.4.2) ist nicht eindeutig und verweist auf eine Norm, welche als kritisch angesehen wird. Diese Unklarheiten führen bei den Ausrüstern und Betreibern der Gefahrgutfahrzeuge zu Unsicherheiten mit existenziellen Risiken und Kosten. Es ist hier sowohl aus wirtschaftlicher als auch aus sicherheitstechnischer Sicht vordringlicher Klärungsbedarf erkennbar. Eine Klärung ist zudem dringlich, weil sich auch international bei den beteiligten Akteuren der ADR-Vertragsparteien Fragen zur Klärung der Technologieentwicklung und dem Stand der Technik ergeben haben. Um eine Überarbeitung der ergänzenden Vorschriften für EX/III-Fahrzeuge zur Beförderung von explosiven Stoffen und Gegenständen der Klasse 1 in Versandstücken voranzutreiben, ist deshalb eine Untersuchung der Gefahren erforderlich, denen explosive Stoffe und Gegenstände während der Beförderung ausgesetzt sind. Die beschriebenen Unschärfen der heutigen Vorschriften sollten im Rahmen eines Forschungsvorhabens des Bundesministeriums für Digitales und Verkehr (BMDV) durch eine neuerliche Untersuchung beseitigt werden. Hierzu wurden auf Grundlage der heutigen Vorschriften bestehende konstruktive Lösungen untersucht und deren Wirksamkeit gegenüber einer typischen Wärmebelastung von außen festgestellt. Erforderlich dafür war zunächst die Charakterisierung der Wärmeeinträge durch Versuche mit typischen Unfallbelastungen. Daraus abzuleiten waren dann idealisierte Belastungsszenarien, welche als Voraussetzung für eine Normungsarbeit angesehen werden sollen. Im letzten Schritt soll ein Textentwurf für die Erneuerung der bestehenden Vorschriften des ADR verfasst und im Anschluss international abgestimmt werden. Es soll ein völlig neuer Ansatz zur Auslegung und Bewertung von Bauteilen von EX/III-Fahrzeugen für den Einsatz als Schutzschild gegenüber externer Wärmebelastung gefunden werden. Dieser begründet sich auf neuen technischen Erkenntnissen, welche eine Feuerbelastung heute nicht mehr allein durch eine Einheits-Temperaturkurve (ETK), sondern differenziert nach konvektiven und strahlenden Anteilen betrachtet. Mit ähnlicher technischer Zielrichtung wurde international der neue Standard „Bestimmung der Beständigkeit von Brandschutzmaterialien und -systemen für Druckbehälter gegenüber Kohlenwasserstoffpoolbränden“ als ISO 21843 in Jahr 2018 verabschiedet. Die jeweilige Wärmeleistung bzw. Wärmestromdichte soll mittels Kalorimeterversuchen bestimmt werden. Es gilt den Wärmeeintrag ins Innere der Ladeabteile zu begrenzen. Hierbei stellt sich nicht nur die Frage nach Isolationswirkung sowie Wärmeübergängen und ob dies nur durch Wandung sowie Boden sicherzustellen ist, sondern ob weitere Maßnahmen, wie Reifenschutz, automatische Feuerlöscheinrichtungen, etc. benötigt werden. Letztlich soll durch die Präzisierung der Gefahrgutvorschriften Transparenz bei Anwendern, Zulassungs- und Kontrollbehörden geschaffen werden. T2 - Gefahrguttechniktage 2025 CY - Berlin, Germany DA - 13.11.2025 KW - Explosivstoffe KW - Unfallszenarien KW - Brandbelastungen PY - 2025 AN - OPUS4-64808 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Steinbeck, Christoph A1 - Jung, Nicole A1 - Bach, Felix A1 - Neumann, Steffen A1 - Herres-Pawlis, Sonja A1 - Liermann, Johannes A1 - Koepler, Oliver A1 - Bannwarth, Christoph A1 - Bender, Theo A1 - Bocklitz, Thomas A1 - Boehm, Franziska A1 - Bonatto Minella, Christian A1 - Biedermann, Frank A1 - Brack, Werner A1 - Cunha, Ricardo A1 - Czodrowski, Paul A1 - Eberl, Franziska A1 - Engel, Thomas A1 - Engstfeld, Albert A1 - Fischer, Tillmann G. A1 - Friedrich, Pascal A1 - Glorious, Frank A1 - Golub, Benjamin A1 - Grathwol, Christoph A1 - Haag, Rainer A1 - Hunold, Johannes A1 - Jacob, Christoph A1 - Johannsen, Jochen A1 - Jollife, John A1 - Kast, Stefan A1 - Kettner, Carsten A1 - Kuhn, Stefan A1 - Lanza, Giacomo A1 - Lisec, Jan A1 - Manolikakes, Georg A1 - Mata, Ricardo A1 - Meiler, Jens A1 - Müller, Matthias A1 - Müller-Pfefferkorn, Ralph A1 - Ortmeyer, Jochen A1 - Patterson, Wendy A1 - Pleiss, Jürgen A1 - Riedel, Annalisa A1 - Riedel, Jens A1 - Schatzschneider, Ulrich A1 - Schuster, Leonie A1 - Seeberger, Peter A1 - Seibert, Johann-Nikolaus A1 - Stadler, Peter A1 - Zeitler, Kirsten T1 - Proposal NFDI4Chem 2025-2030 In the National Research Data Infrastructure (NFDI) — Our Vision: All Chemists Publish FAIR Data N2 - The first funding period of NFDI4Chem established a robust foundation for research data management (RDM) in chemistry by promoting FAIR data principles and creating a cohesive infrastructure to capture well-annotated data early in the lab through electronic lab notebooks (ELNs) and making this data available in public repositories. Key achievements include standardised data formats and metadata, a federated repository environment, and improved data visibility and accessibility. Training programs and outreach have significantly increased awareness and adoption of best RDM practices. In the second funding period, the consortium aims to advance these achievements by consolidating this infrastructure, developing a model for its sustainable maintenance and operation, and fostering cultural change for its widespread adoption. Goals include ensuring seamless data workflows from laboratories to open repositories, enhancing interoperability, and supporting innovative research through AI-ready data. The work plan is organised into six task areas (TAs). TA1 (Management) provides leadership and supports all other TAs in achieving their objectives. TA2 (Smart Lab) aims to develop a fully digital research environment, including an ELN as a modular platform. This environment will support data collection, management, storage, analysis, and sharing. Integrating devices and external resources will enable seamless data transfer to repositories. TA3 (Repositories) will consolidate the repository ecosystem. The goal is to integrate repositories into a federated system for better accessibility and interoperability, ensuring long-term data availability and sustainability. TA4 (Metadata, Data Standards, and Publication Standards) focuses on developing and promoting new data and metadata standards in an international community process. This includes applying ontologies to create a semantic foundation for linking research data, making it machine-readable and enabling knowledge graphs. TA5 (Community and Training) is dedicated to fostering a cultural shift towards digital chemistry through continuous engagement, collecting requirements, and providing extensive training and support through workshops and open education resources. It will promote FAIR-compliant machine learning applications, embedding RDM into academic curricula to ensure future scientists are well-versed in these practices. TA6 (Synergies and Cross-Cutting Topics) aims to enhance collaboration across NFDI consortia and beyond. This includes developing ontologies, terminology services, the search service, and other cross-cutting solutions, integrating these developments into existing infrastructure, enabling interdisciplinary data harmonisation and fostering machine learning applications. KW - Research Data Management KW - FAIR KW - Chemistry PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-648540 DO - https://doi.org/10.3897/rio.11.e177037 SN - 2367-7163 VL - 11 SP - 1 EP - 100 PB - Pensoft Publishers AN - OPUS4-64854 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eberwein, Robert A1 - Heßmann, Jennifer A1 - Werner, Jan A1 - Scarponi, Giordano Emrys A1 - Cozzani, Valerio A1 - Otremba, Frank T1 - Investigation of realistic fire scenarios involving cryogenic storage tanks N2 - The number of vehicles using or transporting cryogenic fuels such as Liquefied Hydrogen (LH2) or Liquefied Natural Gas (LNG) increases fast in the land transportation sector. Does this also entail new risks for instance from a BLEVE? A key to answer this question is to research representative fires by its characterization and its effect on the insulation. At BAM’s technical test side in Germany, a test series was started to answer this question among others. This paper presents results on a pool fire under a colorimeter, that simulates a tank. The investigation points out, that the full fire characterization approach allows to represent the fire. The findings are relevant for the investigation of a representative design fire that is applicable for the approval and improvement of tanks as well as to research accident scenarios and their consequences. T2 - 18th EFCE International Symposium on Loss Prevention and Safety Promotion in the Process Industries CY - Bologna, Italy DA - 08.06.2025 KW - LH2 KW - Insulation KW - Fire KW - Liquefied Natural Gas KW - Safety PY - 2025 AN - OPUS4-63425 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Werner, Jan T1 - Formale Pflichterfüllung N2 - Darstellung der Probleme im Zulassungsverfahren von Gefahrguttanks unter Berücksichtigung aktueller Regelwerksänderungen und daraus folgender Konsequenzen T2 - 23. Gefahrgutkongress Mecklenburg-Vorpommern CY - Rostock, Germany DA - 07.11.2019 KW - Baumusterzulassung KW - Tanks KW - Gefahrgut KW - Regelwerk KW - Antragsteller KW - Behörde KW - Prüfstelle PY - 2019 AN - OPUS4-50409 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Werner, Jan T1 - Formale Pflichterfüllung N2 - Probleme mit der Einhaltung formaler Anforderungen bei der Beantragung von Baumusterzulassungen können für Verärgerung sorgen – nicht nur beim Antragsteller, sondern auch bei der Zulassungsbehörde. Warum die Formalitäten aber so wichtig sind, welche Spielräume die Behörden tatsächlich haben und wie Sorgfalt und Gründlichkeit zu mehr Planungssicherheit innerhalb eines komplexen Systems führen, möchte dieser Beitrag anhand einiger Beispiele zeigen. KW - Baumusterzulassung KW - Tanks KW - Gefahrgut KW - Regelwerk KW - Antragsteller KW - Behörde KW - Prüfstelle KW - Sicherheit PY - 2019 SN - 0941-6080 VL - 2 SP - 18 EP - 21 PB - TÜV MEDIA GmbH CY - Köln AN - OPUS4-50413 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Werner, Jan T1 - ERFA BAM - BAG N2 - Darstellung des Fachbereichs 3.2 und der vielfältigen Aufgaben im Zulassungsverfahren von Gefahrguttanks sowie Grundlagen und zu Gefahrgutvorschriften. Betrachtung sicherheitsrelevanter Problemstellungen beim Gefahrguttransport. T2 - ERFA BAM - BAG CY - BAM TTS, Germany DA - 03.04.2019 KW - Baumusterzulassung KW - Tanks KW - Gefahrgut KW - Regelwerk KW - Ausrüstung KW - Behörde KW - Prüfstelle KW - Sicherheit PY - 2019 AN - OPUS4-50412 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kutz, Philipp A1 - Werner, Jan A1 - Otremba, Frank T1 - Testing of Composite Material for Transport Tanks for LNG N2 - To reduce the emission of carbondyoxide (CO2) of combustion engines, liquefied natural gas (LNG) is used as an alternative fuel. LNG is transported via truck, ship or railway for long distances. Double walled stainless steel tanks are used for transportation, which are heavy and expensive. The vacuum insulation between the two walled structure ensures that the LNG stays liquid over the transportation time (boiling point of LNG: -162 ◦C). This causes a high temperature difference between the transported good and the ambient air. A simplified tank construction is used to reduce the weight and price of the tank. Instead of stainless steel, glass fiber reinforced plastic (GFRP) is used. The design is changed to a single walled construction with a solid insulation material outside on the GFRP structure. Goal of this work is the characterization of a suitable insulation material and configuration as well as the analysis of the mechanical properties of GFRP under cryogenic conditions. Several experiments are carried out. Numerical models of these experiments can then be used for parameter studies. KW - GFRP KW - Lightweight design KW - LNG PY - 2019 DO - https://doi.org/10.4028/www.scientific.net/KEM.809.625 SN - 1662-9795 VL - 809 SP - 625 EP - 629 PB - Trans Tech Publications Ltd. AN - OPUS4-48271 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Werner, Jan T1 - Fire tests on BAM TTS test facilities N2 - Overview Test facilities TTS Division 3.2 for ´visit of IRSN T2 - Technical Exchange IRSN – BAM CY - BAM TTS, Germany DA - 12.09.2019 KW - FIRE TESTS BAM TTS TEST FACILITIES PY - 2019 AN - OPUS4-49194 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Eberwein, Robert A1 - Heßmann, Jennifer A1 - Werner, Jan A1 - Scarponi, Giordano Emrys A1 - Cozzani, Valerio A1 - Otremba, Frank T1 - Investigation of Realistic Fire Scenarios Involving Cryogenic Storage Tanks N2 - The number of vehicles using or transporting cryogenic fuels such as Liquefied Hydrogen (LH2) or Liquefied Natural Gas (LNG) increases fast in the land transportation sector. Does this also entail new risks for instance from a BLEVE? A key to answer this question is to research representative fires by its characterization and its effect on the insulation. At BAM’s technical test side in Germany, a test series was started to answer this question among others. This paper presents results on a pool fire under a colorimeter, that simulates a tank. The investigation points out, that the full fire characterization approach allows to represent the fire. The findings are relevant for the investigation of a representative design fire that is applicable for the approval and improvement of tanks as well as to research accident scenarios and their consequences. T2 - Loss Prevention 2025 CY - Bologna, Italien DA - 09.06.2025 KW - LH2 KW - LNG KW - Fire KW - Tank KW - Safety PY - 2025 DO - https://doi.org/10.3303/CET25116031 SN - 2283-9216 IS - 116 SP - 181 EP - 186 PB - AIDIC AN - OPUS4-63738 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Werner, Jan A1 - Böttcher, Nils A1 - Soderer, Hannes T1 - Batterieelektrisch betriebene FL/AT-Fzg.-Vorschriften und Sicherheit N2 - Überblick über Vorschriftenlage, Technik der Batterien und aktuelle Forschung. Aufzeigen bestehender Unschärfen in der Rechtslage, Sicherheitsfragestellungen zu Batterietechnik sowie Interaktion mit Gefahrgut. T2 - E-Mobilität in der Chemielogistik CY - Duisburg, Germany DA - 04.03.2026 KW - Batterieelektrische Antriebe KW - Gefahrgut KW - ADR KW - Unfallfeuer KW - Wärmeübertragung KW - Lithium Ionen Batterien PY - 2026 AN - OPUS4-65663 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -