TY - CONF A1 - Wäsche, Rolf T1 - Dispersion and Characterisation of Nanoscale Particle Suspensions T2 - International Symposium on Smart Processing Technology (ISMPT) CY - Osaka, Japan DA - 2005-11-14 PY - 2005 AN - OPUS4-11828 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Woydt, Mathias A1 - Dörfel, Ilona T1 - Interface formation by tribo-oxidation in SiC based ceramics T2 - AIST-BAM Symposium on Materials Surface Technology in Twin Institute Programme CY - Tsukuba, Japan DA - 2003-02-18 PY - 2003 SP - 1 EP - 4 AN - OPUS4-12051 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Woydt, Mathias A1 - Dörfel, Ilona T1 - Structure of the interface in SiC-based ceramic composites formed by tribo-oxidation under dry sliding conditions PY - 2004 SN - 1042-1122 VL - 146 SP - 401 EP - 407 PB - American Ceramic Society CY - Westerville, Ohio AN - OPUS4-12053 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Yarim, Rasim A1 - Nicolaides, Dagmar T1 - Influence of Green Compaction on the Sintering Behaviour of SiC-TiC-TiB2 Composites KW - Pressureless sintering KW - SiC KW - TiC KW - TiB2 KW - Green compaction KW - Particle size KW - Microstructure PY - 2004 SN - 1013-9826 VL - 264-268 SP - 213 EP - 218 PB - Trans Tech Publ. CY - Aedermannsdorf AN - OPUS4-12054 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Yarim, Rasim A1 - Wäsche, Rolf A1 - Woydt, Mathias A1 - Dörfel, Ilona T1 - Analysis of wear protecting oxide layers in the system SiC-TiC-TiB2 formed in-situ at high temperatures T2 - AIST-BAM Symposium on Materials Surface Technology in Twin Institute Programme CY - Tsukuba, Japan DA - 2003-02-18 PY - 2003 SP - 5 EP - 8 AN - OPUS4-12057 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Steinborn, Gabriele ED - Bartz, Wilfried J. T1 - Tribological investigations on infiltrated zirconia T2 - 15th International colloquium tribology - Automotive and Industrial Lubrication CY - Ostfildern, Germany DA - 2006-01-17 KW - Friction KW - Wear infiltration KW - Zirconia KW - Alcaline earth fluorides PY - 2006 SN - 3-924813-62-0 SP - 1(?) EP - 7(?) CY - Ostfildern AN - OPUS4-12165 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Klaffke, Dieter A1 - Wäsche, Rolf ED - Bartz, Wilfried J. T1 - Tribological Characterisation of ceramics in fretting tests at room temperature T2 - 15th International colloquium tribology - Automotive and Industrial Lubrication CY - Ostfildern, Germany DA - 2006-01-17 KW - Silicon nitride KW - Silicon carbide KW - Composits KW - Friction KW - Wear KW - Fretting PY - 2006 SN - 3-924813-62-0 SP - 1(?) EP - 10(?) CY - Ostfildern AN - OPUS4-12167 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Klaffke, Dieter A1 - Wäsche, Rolf A1 - Janakiraman, N. A1 - Aldinger, F. T1 - Tribological characterisation of siliconcarbonitride ceramics derived from preceramic polymers N2 - Amorphous SiCN ceramics were prepared in a laboratory scale as disk shaped specimens with 10 mm diameter and 0.3 mm thickness. The friction and wear behaviour was characterised in gross slip fretting tests under unlubricated conditions at room temperature against steel (100Cr6) and ceramic (Al2O3). Tests with a ball-on-disk contact were performed in laboratory air with different content of water vapour. The results show clearly that the relative humidity has a significant effect on friction and wear behaviour. All tests in dry air lead to higher friction and higher wear rate than in normal air. Improved friction and wear behaviour was observed with increasing pyrolysis temperature up to 1100 °C of the SiCN specimens. This is attributed to increasingly better mechanical properties and higher stiffness of the amorphous network due to the evaporation of gaseous organic species and the formation of free graphite like carbon. KW - Ceramics KW - Preceramic polymer KW - Siliconcarbonitride KW - Friction KW - Wear PY - 2006 DO - https://doi.org/10.1016/j.wear.2005.04.031 SN - 0043-1648 VL - 260 IS - 7-8 SP - 711 EP - 719 PB - Elsevier CY - Amsterdam AN - OPUS4-12302 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Steinborn, Gabriele T1 - Tribological testing of Ca-Ba infiltrated zirconia KW - Friction KW - Wear KW - Ca-Ba fluoride KW - Infiltration KW - Porous zirconia PY - 2005 UR - http://www.om.ugal.ro/AnnalsFasc8Tribology/pdf/2005/9-Annals2005-3-Wasche.pdf SN - 1221-4590 SN - 1220-0824 SP - 53 EP - 59 CY - Gala¸ti AN - OPUS4-12365 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Tribological investigations on siliconcarbonitride ceramics derived from preceramic T2 - 14th International Colloquium Tribology CY - Ostfildern, Germany DA - 2004-01-13 PY - 2004 AN - OPUS4-11057 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Oscicalling sliding wear behaviour of SiC, TiC, TiB2 59SiC-41TiB2 and 52SiC-24TiC-24TiB2 T2 - 14th International Colloquium Tribology CY - Ostfildern, Germany DA - 2004-01-13 PY - 2004 AN - OPUS4-11062 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kloß, Heinz A1 - Wäsche, Rolf T1 - Analytical approach for wear prediction of metallic and ceramic materials in tribological applications T2 - ECOTRIB 2007 CY - Ljubljana, Slovenia DA - 2007-06-12 KW - Wear KW - Surface temperature KW - Activation energy KW - Simulation KW - Movable cellular automata (MCA) PY - 2007 VL - I SP - 223 EP - 234 PB - Slovenská Akadémia Vied CY - Ljubljana AN - OPUS4-14972 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Gräber, H.-G. A1 - Klaffke, Dieter T1 - Tribologische Untersuchung zum Verschleißverhalten von keramischen Zahnersatzwerkstoffen KW - Dentalkeramik KW - Bearbeitbarkeit KW - Zwischenmedium KW - pH-Wert KW - Dental ceramic KW - Machinability KW - Liquid media KW - pH-value PY - 2007 SN - 0724-3472 VL - 54 IS - 3 SP - 29 EP - 32 PB - Expert Verlag CY - Renningen AN - OPUS4-15737 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Springborn, U. A1 - Köster, K. A1 - Bewilogua, K. T1 - Schwingungsverschleiß von Kohlenstoffnitridschichten CNx gegen Aluminiumoxid in Luft T2 - 48. Tribologie-Fachtagung CY - Göttingen, Deutschland DA - 2007-09-24 KW - Schwingungsverschleiß KW - CNx Schichten KW - Magnetronsputtern KW - Reibung KW - Keramik PY - 2007 SN - 978-3-00-022603-8 SP - 27/1 EP - 27/11 CY - Aachen AN - OPUS4-15921 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Djahanbakhsh, Mohammad A1 - Österle, Werner T1 - Vergleich von Standard-Modell- und HIP-Simulator-Untersuchungen an Verschleißschutzschichten für Metall-Keramik-Paarungen bei Endoprothesen T2 - 48. Tribologie-Fachtagung "Reibung, Schmierung und Verschleiß - Forschung und praktische Anwendungen" CY - Göttingen, Deutschland DA - 2007-09-24 KW - Reibung KW - Verschleiß KW - Beschichtung KW - HIP-Simulation PY - 2007 SN - 978-3-00-022603-8 VL - 1 SP - 8/1 EP - 8/10 CY - Aachen AN - OPUS4-16102 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Steinborn, Gabriele A1 - Wäsche, Rolf T1 - Charakterisierung der Dispergiereigenschaften von keramischen nanodispersen Suspensionen mit der Ultraschallspektroskopie N2 - Die Dispergiereigenschaften von verschiedenen nanoskaligen Pulvern mit unterschiedlicher Kornfraktion im Bereich von 10 bis 250 nm werden in verdünnten und konzentrierten keramischen Schlickern mit der Ultraschallspektroskopie untersucht. Alle stabilen Suspensionen weisen im entsprechenden pH-Bereich eine monomodale Partikelgrößenverteilung auf. Durch die Charakterisierung der Suspensionen mit der Ultraschallspektroskopie kann eine verbesserte Bewertung hinsichtlich Homogenität und Agglomeratbildung auch für nanoskalige Pulver erhalten werden. Dies ermöglicht eine bessere Qualitätskontrolle prozessrelevanter Schritte bei der Verarbeitung. KW - Dispergieren KW - Nanopartikel KW - Suspensionen KW - Folie KW - Nanopulver KW - Dispergierung PY - 2007 DO - https://doi.org/10.1002/cite.200600141 SN - 0009-286X SN - 1522-2640 VL - 79 IS - 3 SP - 257 EP - 265 PB - Wiley-VCH Verl. CY - Weinheim AN - OPUS4-16271 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Steinborn, Gabriele A1 - Fritz, Ulrich A1 - Rabe, Torsten A1 - Wäsche, Rolf ED - Kriegesmann, J. T1 - Dispergierung von Nanopulvern in Foliengießschlickern KW - Dispergierung KW - Nanopulver KW - Foliengiessen PY - 2005 SN - 3-87156-091-X IS - Kap. 3.3.3.5 SP - 1 EP - 16 PB - Deutscher Wirtschaftsdienst CY - Köln AN - OPUS4-16272 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf ED - Pohl, M. T1 - Schwingungsverschleißprüfung als Werkzeug für die Werkstoffentwicklung T2 - Tagung "Werkstoffprüfung 2007" CY - Neu-Ulm, Deutschland DA - 2007-11-29 KW - Verschleißfestigkeit KW - Werkstoffentwicklung KW - Keramik KW - Reibungsverhalten KW - Stahl PY - 2007 SN - 978-3-514-00753-6 SP - 299 EP - 304 PB - Verl. Stahleisen CY - Düsseldorf AN - OPUS4-16426 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Urchegui, M.A. A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Gómez, X. T1 - Analysis of different strategies to reduce fretting wear in thin steel roping wires N2 - After having checked in a previous study the influence of stroke and normal load in laboratory fretting tests accomplished with thin steel roping wires, in this paper the effect of the contact pressure (test configuration), environmental conditions (relative humidity) and reduction of the friction coefficient (lubricants) on the wear behaviour were analysed. The wires were 0.45 mm in diameter and the material was a cold-drawn eutectoid carbon steel (0.8% C) with a Tensile Strength over 2800 MPa. The tests were performed on an oscillating test rig and the volumetric wear of both specimens of the tribocouple was determined separately from three-dimensional topographies of the wear scars acquired by means of a confocal profiler, and a calculation algorithm developed in using MATLAB®. The strong effect of humidity and lubrication on wear behaviour was proved, whereas a slight effect of contact pressure was derived. KW - Wires KW - Fretting test KW - Contact pressure PY - 2008 DO - https://doi.org/10.1002/tt.52 SN - 1354-4063 SN - 1557-685X VL - 14 IS - 1 SP - 43 EP - 57 PB - Coppin CY - Deal AN - OPUS4-16677 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Podgursky, V. A1 - Adoberg, E. A1 - Surzenkov, A. A1 - Kimmari, E. A1 - Viljus, M. A1 - Mikli, V. A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Síma, M. A1 - Kulu, P. T1 - Dependence of the friction coefficient on roughness parameters during early stage fretting of (Al,Ti)N coated surfaces N2 - Main focus was on the correlation of the coefficient of friction (COF) with the geometrical parameters of the surface during early stage of the running-in period. TiN, TiAlN and AlTiN coatings were prepared by using rotating cathode arc evaporation unit. The roughness of the WC-Co substrate Ra ranged from 0.05 to 0.2 µm and the coating thickness was 2.3 ± 0.2 µm. Part of the samples were subjected to the surface modification by the drag grinding finishing. Geometrical parameters of the surface were evaluated by means of atomic force microscopy (AFM) and fretting tests were conducted with 10 mm diameter alumina ball under 2 N load, 100 µm slip distance and the frequency of 10 Hz. It was found that the distribution of macroparticles strongly influences the geometrical parameters of the surface and the number of macroparticles increases with increasing Al content in the coating. In the case of the positive skewness Ssq of the coating surface, the kurtosis Sku provides a statistically significant effect on the COF, namely the COF depends inversely on the kurtosis Sku. The kurtosis value for TiN was the highest among as-deposited coatings, subsequently, the slowest increase rate in the COF was observed for the TiN coating. KW - PVD coatings KW - AFM KW - Surface topography KW - COF PY - 2011 DO - https://doi.org/10.1016/j.wear.2011.03.006 SN - 0043-1648 VL - 271 IS - 5-6 SP - 853 EP - 858 PB - Elsevier CY - Amsterdam AN - OPUS4-24497 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Oxidative wear in gross slip fretting of thin steel wires T2 - ITC Hiroshima Satellite Symposium, Tribochemistry Hagi 2011 CY - Hagi, Japan DA - 2011-10-25 PY - 2011 AN - OPUS4-24609 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - The history of the Stribeck curve and the role of Adolf Martens T2 - Int. Tribology Congress / ITC Hiroshima CY - Hiroshima, Japan DA - 2011-10-30 PY - 2011 AN - OPUS4-24610 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Alumina and zirconia as tribomaterials - a review T2 - The Fourth International Conference on The Characterization and Control of Interfaces for High Quality Advanced Materials (ICCCI 2012) CY - Kurashiki, Japan DA - 2012-09-02 PY - 2012 AN - OPUS4-24612 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hartelt, Manfred A1 - Wäsche, Rolf T1 - Verschleißuntersuchungen an Dental-Implantat-Werkstoffen unter partial slip Bedingungen N2 - Im Vortrag wird neben der apparativen Prüftechnik das allgemeine methodische Vorgehen für Modell-Verschleißuntersuchungen im Bereich des partial slip vorgestellt. Im Detail wird für Dental-Implantat-Werkstoffe eine Rangfolge aufgestellt, die vergleichend die Verschleißresistenz unterschiedlicher Ti-basierter Werkstoffe zeigt. Wird durch die Kaubewegung eine mehrachsige Beanspruchung in die Kontaktflächen der Schraubverbindung eingeleitet, kann durch partial slip im Randbereich dieser Kontaktfläche ein Verschleißprozess initiiert werden, der die Lockerung des Implantats begünstigt. Eine gute Verschleißresistenz verhindert oder schiebt die vorzeitige Lockerung hinaus. Um das Werkstoffverhalten in Bezug auf eine vorzeitige Lockerung der Implantatkrone bei geschraubten zweiteiligen Implantaten zu charakterisieren, wurden zylindrische Probekörper unter partial slip Fretting-Bedingungen mit Zyklenzahlen bis n = 200 000 beansprucht. Die Frequenz der aufgebrachten Tangentialkraft betrug 2 Hz, um die Kaubewegung zu simulieren. Die tribologischen Untersuchungen wurden auf einem Eigenbau-Tribometer mit der Kontaktgeometrie „gekreuzte Zylinder“ durchgeführt. Die zylindrischen Proben wurden aus den Werkstoffen Titan Grade 4 und der Ti-Legierung Ti6AI4V gefertigt. Ein Teil dieser Ti-basierten Proben wurde oberflächengehärtet. Die bisher erzielten Ergebnisse zeigen, dass die oberflächenbehandelten Proben dazu neigen, unter der Belastung die Kontaktfläche zu vergrößern. Dies deutet auf einen Effekt bekannt als „junction growth“ und damit auf eine erhöhte Versetzungsbeweglichkeit der randschichtgehärteten Proben hin. Einen Einfluss der Zwischenstoffe konnte nicht nachgewiesen werden. T2 - 52. Tribologie-Fachtagung - Reibung, Schmierung und Verschleiß - Forschung und praktische Anwendungen CY - Göttingen, Germany DA - 26.09.2011 KW - Partial slip KW - Schwingungsverschleiß PY - 2011 SN - 978-3-00-035439-7 VL - I SP - 14/1 EP - 14/11 AN - OPUS4-24813 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Hartelt, Manfred A1 - Wäsche, Rolf T1 - Verschleißuntersuchungen an Dental-Implantat-Werkstoffen unter partial slip Bedingungen KW - Modellsystem KW - Partial slip KW - Fretting regime KW - Implantat KW - Titan PY - 2012 SN - 0724-3472 VL - 59 IS - 3 SP - 18 EP - 23 PB - Expert Verlag CY - Renningen AN - OPUS4-26003 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Wear behaviour of yttrium titanate ceramics under gross slip fretting conditions T2 - Int. Conf. Nordic Countries (NordTrib 2012) CY - Trondheim, Norway DA - 2012-06-12 PY - 2012 AN - OPUS4-26014 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Tribological behaviour of polyurethane under oscillating sliding conditions against cast iron T2 - 18. Int. Colloq. Tribology - Industrial and Automotive Lubrication CY - Ostfildern, Germany DA - 2012-01-10 PY - 2012 AN - OPUS4-25343 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kovalev, Alexander A1 - Hartelt, Manfred A1 - Spaltmann, Dirk A1 - Wäsche, Rolf A1 - Woydt, Mathias T1 - Zero wear (Null Verschleiß) N2 - Während des Gleitreibens auftretende, plastische Deformationen im oberen Bereich der Kontaktspitzen werden als „Null-Verschleiß“ bezeichnet. Um diesen zu quantifizieren, werden in dieser Arbeit statt der üblichen, statistischen Rauheitsparameter die Flächen solcher Kontaktspitzenbefrachtet. Dabei liegen diesen Befrachtungen AFM-Bilder von realen Oberflächentopografien auf der Mikro-/Nanoskala als Ausgangspunkt für die Simulationen zugrunde. In den Simulationen wird berücksichtigt, dass die Flächen während der Gleitreibung in den Kontaktspitzen elastisch und plastisch verformt werden können. Ebenso wird der Effekt des Einsatzhärtens in die Befrachtungen eingeschlossen. Die Ergebnisse der Computersimulation stellen einen Weg zur Untersuchung der Reibkräfte zu Beginn des EinlaufVorgangs dar, insbesondere dann, wenn sich dabei die wahre Kontaktfläche verändert hat. Die Ergebnisse der Simulation belegen klar, dass das Vorliegen von „Null-Verschleiß“ stark von der Veränderung der Oberfläche abhängt und nicht von der Erzeugung von Verschleißpartikel begleitet wird. N2 - Recent developments in contact mechanics and microfribology have shown that it is very important to study surface modification effects for quantification of „Zero wear“ (plastic deformation of upper parts of asperities) during sliding friction. The present work considers experimental and Simulation data on the Formation of elastic and plastic contact areas during sliding friction on rough surfaces. The Simulation of discrete contact was carried out using as a source the AFMimages of real surface topography at micro/nanoscale. The approach for quantification of „zero wear“, proposed here, is not using common Statistical Parameters of roughness, but it considers contact areas on asperities. In these areas some regions are undergoing plastic deformation which influences surface Transformation during sliding friction. Also, the workhardening effect was taken into account in the Simulation of sliding friction. This enabled a rnore successful fit of experimental data. The results obtained of the Computer simulations will provide a way of studying friction force at the initial stage of the running-in process. T2 - 53. Tribologie-Fachtagung - Reibung, Schmierung und Verschleiß CY - Göttingen, Germany DA - 24.09.2012 PY - 2012 SN - 978-3-00-039201-6 VL - II SP - 43/1 EP - 43/13 CY - Aachen AN - OPUS4-26640 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Scholz, Christian A1 - Wäsche, Rolf T1 - Stick-slip and wear behavior of ceramic and polymer materials under reciprocating sliding conditions N2 - In many technical applications not only the actual friction coefficient is of importance, but rather the constancy relevant for the functionality. Due to inconstant ffiction values, positioning processes can be substantially influenced as well as vibrations can be induced. The appearance of this tribological effect, named stick-slip, depends on different factors such as sliding speed, relative humidity and ambient temperature occurring primarily after long operating periods. Beside ambient conditions the choice of materials in contact is the main influencing factor of an inconstant coefficient of friction during operating. Certain polymers are well known for their stick-slip tendencies in technical applications. These are on the one hand different modifications of PTFE (polytetrafluoroethylene) reinforced with glass fibers, bronze or graphite and on the other hand thermoplastics such as PE (polyester) or Pf (polyimide). The difference between static and dynamic values of the ffiction force is decisive for stick-slip phenomena. Furthermore, the stick-slip tendency of polymers strongly depends on the elastic material properties. Main softening material areas, which can be found in the contact, represent particularly vulnerable areas. The high friction value in the contact area decreases in most cases by increasing sliding speeds. However, beside polymers ceramic materials can also offer tendencies to stick-slip motion. Klaffke et al. already investigated the influence of ceramic materials on the stick-slip behavior in. T2 - WTC 2013 - 5th World tribology congress CY - Torino, Italy DA - 08.09.2013 KW - Stick-slip KW - Sliding speed KW - Polymers KW - Ceramics KW - Humidity PY - 2013 SP - 1 EP - 4 AN - OPUS4-29091 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kovalev, Alexander A1 - Hartelt, Manfred A1 - Spaltmann, Dirk A1 - Wäsche, Rolf A1 - Woydt, Mathias T1 - Zero wear (Null Verschleiß) KW - Reibung KW - Null-Verschleiß KW - Rauhigkeit KW - Kontaktmechanik KW - Modellierung KW - DLC KW - Friction KW - Zero-wear KW - Roughness KW - Contact mechanics KW - Simulation PY - 2013 SN - 0724-3472 VL - 60 IS - 2 SP - 5 EP - 12 PB - Expert Verlag CY - Renningen AN - OPUS4-28979 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Aiming at zero wear - Where are we right now? T2 - International Conference on Industrial Tribology (ICIT 2012) CY - Pune, India DA - 2012-12-07 PY - 2012 AN - OPUS4-27364 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hartelt, Manfred A1 - Cappella, Brunero A1 - Wäsche, Rolf T1 - Verschleißbestimmung im nm-Bereich N2 - Die Verschleißbeträge können im nm-Bereich quantifiziert werden durch die Berechnung eines Mittelwert-Profils. Grundlage dieser Berechnung ist die hochauflösende Erfassung der 3D-Topographiedaten, die tribologisch beanspruchte und nichtbeanspruchte Oberflächenbereiche gleichermaßen beinhalten. Ein bestimmtes Messverfahren (taktil oder optisch) wird nicht favorisiert. Die vertikale Auflösung des Messverfahrens sollte im nm-Bereich liegen. N2 - The wear rates can be quantified in the nm range by calculating a mean profile. Based on this calculation is the high-resolution recording of the 3D topography data containing tribologically worn and unworn surface areas alike. A specific measurement method (tactile or visual) is not favored. The vertical resolution of the measurement process should be in the nm range. T2 - 54. Tribologie-Fachtagung - Reibung, Schmierung und Verschleiß - Forschung und praktische Anwendungen CY - Göttingen, Germany DA - 30.09.2013 PY - 2013 SN - 978-3-00-022603-8 VL - I SP - 31/1 EP - 31/10 AN - OPUS4-29640 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Klaffke, Dieter A1 - Wäsche, Rolf ED - Franek, F. T1 - Friction and wear behaviour of ceramic SiC-TiC-TiB2 composites under unlubricated oscillating sliding conditions T2 - 2nd World Tribology Congress ; 2nd WTC 2001 CY - Vienna, Austria DA - 2001-09-03 KW - Silicon carbide KW - Titanium carbide KW - Titanium diboride KW - Alumina KW - Oscillating sliding KW - Humidity PY - 2001 SN - 3-901657-07-X SP - 140 PB - ÖTG CY - Wien AN - OPUS4-1172 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Klaffke, Dieter A1 - Wäsche, Rolf T1 - Friction and wear testing can steer the development of ceramic tribo materials T2 - 2nd World Tribology Congress ; 2nd WTC 2001 CY - Vienna, Austria DA - 2001-09-03 KW - Friction KW - Wear quantities KW - Humidity KW - Ball-on-disk KW - Wear particles PY - 2001 SN - 3-901657-09-6 SP - 141 PB - ÖTG CY - Vienna AN - OPUS4-1152 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Klaffke, Dieter A1 - Wäsche, Rolf T1 - Tribological Performance of SiC and TiB2 sliding against SiC and Al2O3 T2 - 10th Nordic Symposium on Tribology ; 10th Nordtrib 2002 CY - Stockholm, Sweden DA - 2002-06-09 PY - 2002 SP - 1(?) EP - 10(?) PB - Royal Institute of Technology CY - Stockholm AN - OPUS4-1386 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Klaffke, Dieter A1 - Yarim, Rasim A1 - Wäsche, Rolf T1 - Effect of pre-oxidation on friction and wear behaviour of a SiC-TiC-TiB2 composite T2 - 10th Nordic Symposium on Tribology ; 10th Nordtrib 2002 CY - Stockholm, Sweden DA - 2002-06-09 PY - 2002 SP - 1 EP - 10(?) PB - Royal Institute of Technology CY - Stockholm AN - OPUS4-1387 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Steinborn, Gabriele A1 - Klaffke, Dieter ED - Somiya, S. T1 - Gas pressure sintering of SiCp-alumina composites made by gelcasting and their tribological properties N2 - COMPOSITE MATERIALS OF A 99.7 % ALPHA-ALUMINA MATRIX WITH PLATELETS OF SILICON CARBIDE (SICP) HAVE BEEN PREPARED BY GELCASTING. DENSIFICATION WAS CARRIED OUT BY GAS-PRESSURE SINTERING WITHOUT FURTHER SINTERING AIDS. FIVE DIFFERENT COMPOSITIONS WITH 0, 5, 10, 15, AND 20 VOL.% SICP RESP. HAVE BEEN INVESTIGATED AND TRIBOLOGICAL PROPERTIES WERE CHARACTERIZED. INCREASING AMOUNT OF SICP AS RIGID PARTICLES IN THE FINE GRAINED MATRIX COMPLICATE THE DENSIFICATION PROCESS. WITH THE APPLICATION OF 50 BAR AR PRESSURE DURING THE FINAL SINTERING STEP AT A TEMPERATURE OF 1700 DEGREE C THE DENSITY OF THE SAMPLES COULD BE INCREASED BY 3-5%. INVESTIGATION OF THE TRIBOLOGICAL PROPERTIES AGAINST STEEL AS A COUNTERBODY UNDER UNLUBRICATED OSCILLATING SLIDING CONDITIONS SHOWED A HIGH COEFFICIENT OF FRICTION AND AN INCREASING WEAR RATE UP TO A SICP CONTENT OF 10 VOL. % . AT 15 AND 20 VOL. % SICP RESP. BOTH THE COEFFICIENT OF FRICTION AND THE COEFFICIENT OF WEAR DROP DOWN. T2 - 3rd IUMRS International Conference on Advanced Materials (ICAM) CY - Tokyo, Japan DA - 1993-08-31 PY - 1994 SN - 0-444-81993-2 N1 - Serientitel: Transactions of the Materials Research Society of Japan – Series title: Transactions of the Materials Research Society of Japan IS - 16B SP - 791 EP - 794 PB - Elsevier CY - Amsterdam AN - OPUS4-1433 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Steinborn, Gabriele T1 - Characterisation of the secondary properties of alumina - measuring the isoelectric point by a streaming potential method PY - 1997 SN - 0173-9913 SN - 0196-6219 VL - 74 IS - 5 SP - 235 EP - 239 PB - Göller CY - Baden-Baden AN - OPUS4-1434 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Steinborn, Gabriele T1 - Influence of Slip Viscosity on the Mechanical Properties of High Purity Alumina made by Gelcasting KW - High purity alumina KW - Gelcasting KW - Solid content KW - Viscosity KW - Deairing KW - Bending strenght KW - Microstructure KW - Computertomography KW - Defect type PY - 1997 SN - 1013-9826 VL - 132 SP - 374 EP - 377 PB - Trans Tech Publ. CY - Aedermannsdorf AN - OPUS4-1435 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Abe, H. A1 - Naito, M. A1 - Hackley, V. A1 - Hotta, Y. T1 - Influence of particle size and solid loading on the determination of the isoelectric point (IEP) of ceramics powders by different methods N2 - The isoelectric point is a material property for the characterization of acid-base behavior of the powder surface. The IEP of two alumina powders (AKP-30, Grade A) with different particle size characteristics in aqueous suspension has been determined by colloid vibration current (CVI) and particle charge detection (PCD) methods in moderately concentrated suspensions in order to qualify these methods for a future standardization. The solid loading of the suspensions were 1 and 5 vol%. The comparison of the IEP determined by PCD and CVI was in good agreement. However, the solid loading dependence of IEP and a large IEP hysteresis (at 1 vol%) were observed, which do not allow a proper determination of the IEP. The recording of the potential curve and therfore the determination of the IEP with CVI was difficult for the suspension of Grade A powder due to formation of agglomerates at pH values near the pHIEP. T2 - 7th Euro Ceramics - Conference and Exhibition of the European Ceramic Society (ECerS) CY - Brugge, Belgium DA - 2001-09-09 KW - Isoelectric point (IEP) KW - Alumina powder KW - Particle charge detection (PCD) KW - Colloid vibration current (CVI) PY - 2002 UR - http://ois.nist.gov/nistpubs/technipubs/recent/search.cfm?dbibid=9289 DO - https://doi.org/10.4028/www.scientific.net/KEM.206-213.3 SN - 1013-9826 VL - 206-213 SP - 3 EP - 6 PB - Trans Tech Publ. CY - Aedermannsdorf AN - OPUS4-1437 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Yarim, Rasim A1 - Wäsche, Rolf A1 - Woydt, Mathias ED - Franek, F. T1 - Wear Behaviour of SiC-TiC-TiB2 Ceramic Composites Sliding against SiC up to 800°C and 2m/s T2 - 2nd World Tribology Congress ; 2nd WTC 2001 CY - Vienna, Austria DA - 2001-09-03 KW - Dry sliding KW - Tribochemistry KW - Silicon carbide KW - Titanium carbide KW - Titanium boride KW - High temperature KW - Ceramic composites PY - 2001 SN - 3-901657-07-X SP - 1(?) EP - 4(?) PB - ÖTG CY - Wien AN - OPUS4-1438 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Klaffke, Dieter ED - Andersson, P. T1 - Tribological Behaviour of Multiphase Ceramic Composites in the System Si-Ti-B-C Containing Free Carbon T2 - 9th Nordic Symposium on Tribology ; 9th NORDTRIB 2000 CY - Porvoo, Finland DA - 2000-06-11 PY - 2000 SN - 951-38-5276-8 SN - 0357-9387 N1 - Serientitel: VTT Symposium – Series title: VTT Symposium VL - 1 IS - 200 SP - 186 EP - 195 PB - VTT, Technical Research Centre of Finland CY - Espoo AN - OPUS4-1439 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter T1 - Ceramic particulate composites in the system SiC-TiC-TiB2 sliding against SiC and Al2O3 under water N2 - The tribological behaviour of SiC, SiC-TiC and SiC-TiC-TiB2 was determined in oscillating sliding against SiC and -Al2O3 in water at room temperature. The tribo-systems with the composite materials containing TiC and TiB2 differ significantly from the systems with the single phase SiC: The wear is reduced and the friction is increased. The wear reduction up to a factor of 10 is mainly due to the formation of an oxide film containing titanium oxides which is soft, stable in water and well adhering to the bulk material. This oxide film is transferred to the alumina ball but not to the silicon carbide ball. KW - Silicon carbide KW - Titanium carbide KW - Titanium boride KW - Ceramic KW - Particulate composites KW - Oscillating sliding KW - Water lubrication KW - Friction KW - Wear PY - 1999 DO - https://doi.org/10.1016/S0301-679X(99)00033-X SN - 0301-679X VL - 32 IS - 4 SP - 197 EP - 206 PB - Butterworth-Heinemann CY - Oxford AN - OPUS4-1440 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Naito, M. ED - Puri, V. ED - Adair, J. ED - Knobloch, C. ED - Huang, C. T1 - Electrokinetic Characterization of Aqueous Ceramic Suspensions T2 - Fine Powder Processing Conference '99 CY - State University, PA, USA DA - 1999-09-20 KW - Meßverfahren KW - Zeta Potenzial KW - Hochleistungskeramik PY - 1999 SP - 177 EP - 183 AN - OPUS4-1441 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Czichos, Horst T1 - Wear behaviour of i-carbon coatings PY - 1992 SN - 0043-1648 VL - 153 SP - 149 EP - 162 PB - Elsevier CY - Amsterdam AN - OPUS4-1428 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Steinborn, Gabriele T1 - Influence of the Dispersants in Gelcasting of Nanosized TiN PY - 1997 SN - 0955-2219 SN - 1873-619X IS - 17 SP - 421 EP - 426 PB - Elsevier CY - Oxford AN - OPUS4-1429 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Naito, M. A1 - Hackley, V.A. T1 - Experimental study on zeta potential and streaming potential of advanced ceramic powders N2 - Zeta potential as measured with the electrokinetic sonic amplitude (ESA) method has been compared to streaming potential as measured with the particle charge detection (PCD) method. The measurements have been carried out on identical suspensions of a-Al2O3, SiC and Si3N4 with a solids volume fraction of 1% and 10%. Zeta potential and streaming potential are related by a linear function. The correlation coefficients for this relationship are better than 0.99 for the suspensions with 1% solids loading. For the suspensions with 10% solids loading, correlation coefficients are slightly lower due to the influence of increasing viscosity. Regardless of lower correlation at the higher solids loading, the isoelectric pH is constant within the limits of accuracy of the pH measurements. KW - Zeta potential KW - Streaming potential KW - Ceramic powders KW - Correlation of measurement PY - 2002 DO - https://doi.org/10.1016/S0032-5910(01)00462-4 SN - 0032-5910 SN - 1873-328X VL - 123 SP - 275 EP - 281 PB - Elsevier CY - Amsterdam AN - OPUS4-1430 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf T1 - Keramische Supraleiter - Kristallstruktur, Gefüge und Eigenschaften PY - 1988 SN - 0340-7551 VL - 18 IS - 2 SP - 128 EP - 133 PB - Bundesanstalt für Materialprüfung CY - Berlin AN - OPUS4-1431 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf T1 - Feste Schmierstoffe für hohe Temperaturen - Eine Literaturübersicht PY - 1989 SN - 0724-3472 VL - 36 IS - 3 SP - 145 EP - 151 PB - Expert Verlag CY - Renningen AN - OPUS4-1432 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kautek, Wolfgang A1 - Rudolph, Pascale A1 - Brzezinka, Klaus-Werner A1 - Wäsche, Rolf ED - Meunier, M. T1 - Physical chemistry of the femtosecond and nanosecond laser-material-interaction with SiC and a SiC-TiC-TiB2 composite ceramic compound N2 - The interaction of nanosecond laser pulses in the ultraviolet wavelength range and femtosecond laser pulses in the near-infrared region with the direct semiconductor SiC and the composite compound SiC-TiC-TiB2 was investigated in respect to resulting physicochemical processes. Surface analytical techniques, such as XPS, µ-Raman, and EDX were used to identify the chemical changes between untreated and laser-treated areas. Single-pulse irradiation led to material modifications in the condensed state in most instances. Multi-pulse results differed depending on the pulse duration. In the nanosecond case, melting of the surface and redeposited material (debris) were observed. With femtosecond pulses instead, only negligible melting and few debris could be detected. Additionally, periodic structures (ripples) appeared, with parallel orientation and in most cases two different periodicities for a particular material. Laser ablation of all the studied compound materials exhibited preferential ablation of the lighter component elements. Crystal structure changes of the irradiated surface were observed as a consequence of laser-induced melting and resolidification. An oxidation process interfered with all this processes so that unstoichiometric oxides were formed. T2 - Symposium D - European Materials Research Society CY - Strasbourg, France DA - 2002-06-18 PY - 2002 UR - http://www.emrs-strasbourg.com/files/pdf/2002_SPRING/02_Prog_Dv2.pdf N1 - Serientitel: Applied surface science – Series title: Applied surface science VL - 208/209.2003,1 IS - 1 SP - 1 PB - Elsevier CY - Amsterdam AN - OPUS4-1732 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Steinborn, Gabriele A1 - Wäsche, Rolf A1 - Reichel, U. T1 - Fabrication of porous ceramics made from nano sized alumina powder by gelcasting N2 - The gelcasting process was used for manufacturing porous ceramic bodies from nano sized powders. 3 different powders with specific surface areas between 12 and 30 m²/g were used. Solid content of the corresponding slurries was dependent on the milling procedure and the use of a suitable dispersant. For bimodal GradeA powder solid content was as high as 58 vol%. For sintering temperatures between 1250 and 1600°C the porosity varied between 45 and 20%, whereas the pore radii varied between 50 and 91nm. The grain size of crystallites in the sintered microstructures was about 1um. The reflection ratio for visible light increased in comparison to a reference sample made from conventional powder from 0.8 to 0.95 in the wavelenght range around 400nm. T2 - 2nd International Conference on Shaping of Advanced Ceramics CY - Gent, Belgium DA - 2002-10-24 PY - 2002 SP - 103 EP - 108 AN - OPUS4-1813 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Suchantke, Christian A1 - Yarim, Rasim ED - Schulte, K. ED - Kainer, K. T1 - Sintern von Verbundwerkstoffen im System SiC-TiC-TiB2 T2 - 12. Tagung "Verbundwerkstoffe und Werkstoffverbunde" CY - Hamburg, Deutschland DA - 1999-10-05 KW - Sintern KW - Verbundwerkstoffe KW - Thermochemische Analyse PY - 1999 SN - 3-527-29967-X SP - 189 EP - 194 PB - Wiley-VCH CY - Weinheim AN - OPUS4-720 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter T1 - High temperature tribological behaviour of particulate composites in the system SiC-TiC-TiB2 during dry oscillating sliding KW - Ceramic Composites KW - High temperatures KW - Tribo-oxidation KW - Dry-slidins KW - Friction KW - Wear PY - 1999 SN - 1225-9381 VL - 5 IS - 2 SP - 155 EP - 161 PB - Han'guk-Seramik-Hakhoe CY - Seoul AN - OPUS4-761 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Klaffke, Dieter A1 - Wäsche, Rolf ED - Schulte, K. ED - Kainer, K. T1 - Tribologische Prüfungen als begleitende Maßnahme zur Entwicklung von keramischen Tribowerkstoffen T2 - 12. Tagung "Verbundwerkstoffe und Werkstoffverbunde" CY - Hamburg, Deutschland DA - 1999-10-05 KW - Tribologie KW - Reibung KW - Verschleiß PY - 1999 SN - 3-527-29967-X SP - 423 EP - 428 PB - Wiley-VCH CY - Weinheim AN - OPUS4-723 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Naito, M. A1 - Jahanmir, S. T1 - TWA 27 Characterization Methods for Ceramic Powders and Green Bodies KW - Standardisierung KW - Keramische Pulver KW - Grünkörper PY - 2000 SN - 1016-2178 IS - 23 SP - 21 EP - 27 PB - National Institute of Standards and Technology AN - OPUS4-979 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter T1 - Wear of multiphase SiC based ceramic composites containing free carbon N2 - Ceramics are of increasing interest for application in many branches of technique. In order to improve the tribological performance of ceramic materials, composites on the basis of silicon carbide with different amounts of titanium carbide, boron carbide, titanium diboride and free carbon in the form of graphite were manufactured by a reaction sintering process. The friction and wear behaviour of these composites was investigated with oscillating sliding motion in unlubricated tests at room temperature on different levels of relative humidity. Additional tests were performed under water lubrication, revealing the superior behaviour of composites for special test conditions. A major influence of the free carbon on friction or wear behaviour was not observed. The tribological behaviour in air as well as under water is mainly dependant on the amount of titanium phases. KW - Siliziumkarbid KW - Verbundwerkstoffe KW - Tribooxidation KW - Silicon carbide KW - Ceramic composites KW - Humidity water KW - Lubrication PY - 2001 DO - https://doi.org/10.1016/S0043-1648(01)00566-X SN - 0043-1648 VL - 249 SP - 220 EP - 228 PB - Elsevier CY - Amsterdam AN - OPUS4-900 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Wäsche, Rolf A1 - Habig, Karl-Heinz T1 - Physikalisch-chemische Grundlagen der Feststoffschmierung - Literaturübersicht - N2 - Die für einen erfolgreichen Einsatz von Festschmierstoffen zur Minderung von Reibung und Verschleiß systembestimmender Parameter wie Last, Geschwindigkeit, Temperatur, umgebende Atmosphäre, Filmbildung und -haltung sowie die Anwendungstechnologien werden dargestellt, ferner Modellvorstellungen zum Verschleißverhalten von Festschmierstoffen im Hinblick auf konkrete Anwendungsfälle diskutiert. T3 - BAM Forschungsberichtreihe - 158 KW - Festschmierstoff KW - Transferschmierung KW - Hohe Temperaturen KW - Graphit KW - Reibung KW - Verschleißmodelle KW - gebundene Filme KW - Synergieeffekte PY - 1989 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-2921 SN - 978-3-88314-889-X SN - 0938-5533 VL - 158 SP - 1 EP - 112 PB - Wirtschaftsverlag NW CY - Bremerhaven AN - OPUS4-292 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Wäsche, Rolf A1 - Köse, Fatma T1 - Einfluß der Verfahrensparameter beim Gelcasting auf die Entstehung bruchauslösender Gefügefehler in hochreinen Aluminiumoxidkeramiken N2 - Es wird die Untersuchung des Entlüftungsvorgangs in Keramikschlickern beschrieben, die Teil des Gelcastingprozesses zur Herstellung hochfester Aluminiumoxidkeramiken sind. Ziel der Untersuchung war es, den Einfluss von Viskosität und Entlüftungszeit als prozessvariablen auf die Entstehung von bruchauslösenden Fehlern im Gefüge zu verdeutlichen. T3 - BAM Forschungsberichtreihe - 221 PY - 1997 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-2294 SN - 978-3-89429-036-4 SN - 0938-5533 VL - 221 SP - 1 EP - 54 PB - Wirtschaftsverlag NW CY - Bremerhaven AN - OPUS4-229 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Dörfel, Ilona A1 - Wäsche, Rolf A1 - Rabe, Torsten A1 - Steinborn, Gabriele T1 - Tribological Induced Microstructural Changes in Subsurface Layers of Si3N4-Based Materials KW - Tribologie PY - 1994 SN - 1013-9826 VL - 89-91 SP - 763 EP - 767 PB - Trans Tech Publ. CY - Aedermannsdorf AN - OPUS4-577 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Klaffke, Dieter A1 - Hartelt, Manfred A1 - Wäsche, Rolf ED - Bartz, Wilfried J. T1 - Non-Oxide Ceramics as Tribo Materials - Analysis of Wear Mechanisms under Oscillating Sliding Conditions in Various Atmospheres T2 - 12th International Colloquium Tribology CY - Esslingen, Germany DA - 2000-01-11 KW - Tribologie PY - 2000 SN - 3-924813-44-2 VL - 3 SP - 1755 EP - 1763 PB - Techn. Akad. Esslingen CY - Ostfildern AN - OPUS4-848 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Characterisation of tribological interface in low wear magneli type ceramics T2 - International Conference on Characterisation and Control of Interfaces (ICCC 2009) CY - Kurashiki, Japan DA - 2009-09-06 PY - 2009 AN - OPUS4-22871 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Woydt, Mathias A1 - Rehmer, Birgit ED - Ewsuk, K. ED - Naito, M. ED - Kakeshita, T. ED - Kirihara, S. ED - Uematsu, K. ED - Abe, H. T1 - Characterization of the tribological interface in low wear Magneli type ceramics N2 - The tribological behaviour under dry sliding conditions of Magneli phase Ti4O7 and e-phase Ti2Cr2O7 with α-alumina as a sliding partner has been characterised at room temperature by oscillating sliding. The mechanical properties as well as Vickers hardness measurements do not reveal big differences between the materials, and 4-point bending strengths are around 200 MPa for both materials. Although the friction coefficients are in the medium range of 0.6 and do not differ much between the materials, the wear behaviour is very different. At room temperature, the wear coefficient of Ti2O7 is strongly dependent on relative humidity, and wear is highest under dry conditions when relative humidity is low as it is typically found for many ceramic materials. Ti2Cr2O7 shows remarkably different wear behaviour with the lowest wear in dry conditions. The measured coefficients of wear at low relative humidity of 4% are more than 2 orders of magnitude lower than those for Ti2O7. T2 - 3rd International conference on characterization and control of interfaces for high quality advanced materials CY - Kurashiki, Japan DA - 2009-09-06 PY - 2009 SN - 978-0-470-90917-1 VL - 219 SP - 111 EP - 116 PB - John Wiley & Sons CY - Hoboken, New Jersey, USA AN - OPUS4-21842 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Salge, T. A1 - Wäsche, Rolf A1 - Hodoroaba, Vasile-Dan T1 - Advanced light element and low energy X-ray analysis of a TiB2 – TiC – SiC ceramic material using EDS spectrum imaging N2 - The accurate EDS microanalysis of light elements such as boron and carbon by spectrum imaging will be demonstrated using a sintered hard ceramic material composed of the three major phases titanium boride (TiB2), titanium carbide (TiC), silicon carbide (SiC) and minor phases, sub-μm in size. The combination of these three materials leads to improved mechanical and tribological properties. Silicon carbide is a material used for mechanical seals. It has the disadvantage of reduced failsafe running functions, causing increased wear when running dry. The added titanium components (TiC and TiB2) improve the failsafe running functions. This technology has already been transferred to industrial applications. KW - EDS KW - Spectrum imaging KW - Ceramic KW - Phase analysis KW - Light elements PY - 2018 UR - https://www.bruker.com/fileadmin/user_upload/8-PDF-Docs/X-rayDiffraction_ElementalAnalysis/Microanalysis_EBSD/LabReports/App_eds_10_LE_keramik_Rev1_1_lores.pdf SP - 1 EP - 5 CY - Berlin AN - OPUS4-44622 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - A study on wear particle analysis in lubricated steel-steel contacts T2 - International Tribology Congress/ITC 2015 CY - Tokyo, Japan DA - 2015-09-15 PY - 2015 AN - OPUS4-34324 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Hodoroaba, Vasile-Dan T1 - Verschleißpartikel-Analyse mit Rasterelektronenmikroskopie und energiedispersiver Röntgenspektrometrie im Transmissionsmodus (TSEM/EDX) N2 - Untersucht wurden Verschleißpartikel als elektronen-transparente Proben auf dünnen Trägerfolien mit einem hochauflösendem Rasterelektronenmikroskop und energiedispersiver Röntgenspektrometrie im Transmissionsmodus. Die hohe laterale Auflösung dieser modernen Methoden ermöglicht eine morphologische Charakterisierung der Verschleißpartikel bis in den nm-Bereich. Die hochauflösende Elementanalyse erlaubt eine Interpretation der Zusammensetzung und damit Rückschlüsse auf die Verschleißpartikelbildung. Die tribologischen Untersuchungen sind an einem Modell-Verschleißtribometer nach DIN 51834-2 geschmiert, aber ohne Ölkreislauf, durchgeführt worden. Die Präparation der Verschleißpartikel über eine Entnahme und Übertragung einer geringen Schmierstoffmenge mit einer Mikropipette auf eine TEM-Trägerfolie ist mit einem geringen Aufwand möglich. Der präparative Aufwand ist relativ gering. Das benötigte Schmierstoffvolumen beträgt wenige Mikroliter (0,001ml). Die Untersuchung zeigt die geringe geometrische Größe der Verschleißpartikel und bestätigt indirekt die These der Reaktionsschichtbildung mit einer geringen Schichtdicke, die ständig verschleißt und sich stetig neu bildet. Die beschriebenen Verschleißprozesse sind in der Modell-Verschleiß-Prüfung mit sehr hohen Pressungen am Versuchsbeginn nachweisbar. T2 - 55. Tribologie-Fachtagung - Reibung, Schmierung und Verschleiß - Forschung und praktische Anwendungen CY - Göttingen, Germany DA - 22.09.2014 PY - 2014 SN - 978-3-00-046545-1 VL - I SP - 05/1 EP - 05/10 AN - OPUS4-31528 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Sato, K. A1 - Brandt, Guido A1 - Schmid, Thomas A1 - Sasaki, S. A1 - Woydt, Mathias T1 - Wear behaviour of MgO stabilized zirconia in hot steam environment up to 400°C N2 - Self-mated magnesia stabilized zirconia (Mg-PSZ) ceramic sliding couples have been investigated at 100 N load (P0max= 1324 MPa) in oscillating sliding conditions in different humidity conditions in air and in hot steam. Temperatures have been varied up to 400 °C and pressures up to 6 bars. The results show that the wear behavior of MgO-ZrO2 under high Hertzian contact pressures is strongly dependent on temperature and is similar for both dry oscillating and oscillating in hot steam. However, although the evolution in wear rates on temperature is similar and the wear rates of MgO-ZrO2 plunged above 300 °C in hot steam and air by nearly three orders of magnitude, SEM micrographs revealed in hot steam at 400 °C smooth wear tracks. In contrast, hot steam enhanced the tribochemistry of self-mated alumina couples and reduced wear rates. Hot steam decreased the coefficients of friction of MgO-ZrO2 with increasing temperature, but not the wear rates. KW - Hot steam KW - Zirconia KW - Friction KW - Wear KW - Tribofilm KW - Raman spectroscopy PY - 2019 DO - https://doi.org/10.1016/j.wear.2019.01.047 VL - 426-427 SP - 428 EP - 432 PB - Elsevier B.V. AN - OPUS4-47873 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Harsha, A. P. A1 - Wäsche, Rolf A1 - Joyce, T. J. T1 - Wear of biopolymers under reciprocating sliding conditions against different counterfaces N2 - In the present work it was shown the investigation of wear resistance of ultrahigh-molecular weight polyethylene (UHMWPE) and crosslinked polyethylene (XLPE) against different counterfaces. Friction and wear studies were evaluated under dry reciprocating sliding conditions at room temperature. KW - Biopolymers KW - Wear KW - Friction KW - UHMWPE PY - 2019 DO - https://doi.org/10.1002/pen.25239 VL - 59 IS - 11 SP - 2356 EP - 2366 PB - Society of Plastics Engineers AN - OPUS4-49779 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Analysing wear particles on the nano scale N2 - A novel method for preparation and chracterisation of nano scale wear particles by means of TSEM was presented. The tribological tests were carried out in a lubricated system at a temperature of 80°C. T2 - The 17th Nordic Symposium on Tribology - NORDTRIB 2016 CY - Hämeenlinna, Finland DA - 14.06.2016 KW - Nano scale KW - Wear particles KW - Tribology KW - Steel KW - SEM PY - 2016 AN - OPUS4-38209 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Hodoroaba, Vasile-Dan T1 - Analysis of nanoscale wear particles from lubricated steel-steel contacts N2 - A new method for sampling wear particles directly from the lubricant reservoir has been developed and applied successfully for analyzing wear particles by high-resolution scanning electron microscopy in transmission mode having coupled energy-dispersive X-ray spectroscopy. The lubricated tribological testing was carried out with fully formulated as well as with non-formulated synthetic base oil. It was possible to analyze individual particles with dimensions as small as about 5–30 nm which are likely the 'primary' wear particles. A majority of the particles, however, are agglomerated and, thus, lead to the formation of larger agglomerates of up to a few micrometers. Chemical analysis led to the conclusion that most of the observed particles generated in formulated oil, especially the larger ones, are composed of the additives of the lubricant oil. In non-formulated base oil, the primary particles are of similar dimensions but contain only iron, chromium and oxygen, but most likely stem from the mating materials. This finding points to the fact that the main wear mechanism under lubricated conditions with fully formulated oil is more like a continuous shearing process rather than a catastrophic failure with the generation of larger primary particles. When the oil is non-formulated, however, several wear mechanisms act simultaneously and the wear rate is increased significantly. Generated larger primary particles are milled down to the nanoscale. When the oil is fully formulated, wear mainly takes places at the additive layer or tribofilm; thus, the steel surface is protected. KW - Particle KW - Wear particle analysis KW - Lubricated contact KW - Bearing steel KW - Nanoscale T-SEM KW - Nanoscale EDX analysis PY - 2015 DO - https://doi.org/10.1007/s11249-015-0534-1 SN - 1023-8883 SN - 1573-2711 VL - 58 IS - 3 SP - 49-1 - 49-10 PB - Springer Science Business Media B.V. CY - Dordrecht AN - OPUS4-33525 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Hodoroaba, Vasile-Dan T1 - Verschleißpartikel-Analyse mit Rasterelektronenmikroskopie und energiedispersiver Röntgenspektrometrie im Transmissionsmodus (TSEM/EDX) N2 - Untersucht wurden Verschleißpartikel als elektronentransparente Proben auf dünnen Trägerfolien mit einem hochauflösendem Rasterelektronenmikroskop und energiedispersiver Röntgenspektrometrie im Transmissionsmodus. Die hohe laterale Auflösung dieser modernen Methoden ermöglicht eine morphologische Charakterisierung der Verschleißpartikel bis in den nm-Bereich. Die hochauflösende Elementanalyse erlaubt eine Interpretation der Zusammensetzung und damit Rückschlüsse auf die Verschleißpartikelbildung. Die tribologischen Untersuchungen sind an einem Modell-Verschleißtribometer nach DIN 51834-2 geschmiert, aber ohne Ölkreislauf, durchgeführt worden. Die Präparation der Verschleißpartikel über eine Entnahme und Übertragung einer geringen Schmierstoffmenge mit einer Mikropipette auf eine TEM-Trägerfolie ist mit einem geringen Aufwand möglich. Der präparative Aufwand ist relativ gering. Das benötigte Schmierstoffvolumen beträgt wenige Mikroliter (0,001 ml). Die Untersuchung zeigt die geringe geometrische Größe der Verschleißpartikel und bestätigt indirekt die These der Reaktionsschichtbildung mit einer geringen Schichtdicke, die ständig verschleißt und sich stetig neu bildet. Die beschriebenen Verschleißprozesse sind in der Modell-Verschleiß-Prüfung mit sehr hohen Pressungen am Versuchsbeginn nachweisbar. KW - Modellverschleißprüfung KW - Verschleißpartikel-Analyse KW - TSEM PY - 2015 SN - 0724-3472 VL - 62 IS - 6 SP - 5 EP - 11 PB - Expert Verlag CY - Renningen AN - OPUS4-35043 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kaltzakorta, O. A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Aginagalde, A. A1 - Tato, W. T1 - Influence of polymer filler on tribological properties of thermoplastic polyurethane under oscillating sliding conditions against cast iron N2 - The tribological behaviour of unfilled thermoplastic polyurethane (TPU) and a polymer sphere filled (TPUG) thermoplastic polyurethane have been studied under oscillating sliding condition against cast iron as a counterpart. In the case of unfilled TPU, the wear mechanisms are dominated by particle detachment and roll formation. In principle, TPUG also showed a similar wear mechanism as that of unfilled TPU; in addition, particle pull-out and delamination are also observed. Wear volume of TPUG was significantly higher than that for the unfilled TPU and this is attributed to the different material removal processes taking place in the material during sliding. The polymer spheres as a filler material deteriorated the wear resistance of TPU because of improper adhesion and bonding of filler in the TPU matrix and therefore it contributed to more wear. In case of TPU the friction behaviour was strongly dependant on the temperature and surface roughness of the counter body. The results showed that below the glass transition temperature higher friction values are observed with higher counter body surface roughness. However, above the glass transition temperature, higher friction values are observed with a smoother surface roughness of the counter body. In case of TPUG, the friction behaviour was not significantly dependent on surface roughness of the counter body. KW - Dry sliding KW - Polymers KW - Cast iron KW - Temperature PY - 2012 DO - https://doi.org/10.1007/s11249-012-0017-6 SN - 1023-8883 SN - 1573-2711 VL - 48 IS - 2 SP - 209 EP - 216 PB - Springer Science Business Media B.V. CY - Dordrecht AN - OPUS4-27272 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -