TY - RPRT A1 - Wäsche, Rolf A1 - Köse, Fatma T1 - Einfluß der Verfahrensparameter beim Gelcasting auf die Entstehung bruchauslösender Gefügefehler in hochreinen Aluminiumoxidkeramiken N2 - Es wird die Untersuchung des Entlüftungsvorgangs in Keramikschlickern beschrieben, die Teil des Gelcastingprozesses zur Herstellung hochfester Aluminiumoxidkeramiken sind. Ziel der Untersuchung war es, den Einfluss von Viskosität und Entlüftungszeit als prozessvariablen auf die Entstehung von bruchauslösenden Fehlern im Gefüge zu verdeutlichen. T3 - BAM Forschungsberichtreihe - 221 PY - 1997 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-2294 SN - 978-3-89429-036-4 SN - 0938-5533 VL - 221 SP - 1 EP - 54 PB - Wirtschaftsverlag NW CY - Bremerhaven AN - OPUS4-229 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Wäsche, Rolf A1 - Habig, Karl-Heinz T1 - Physikalisch-chemische Grundlagen der Feststoffschmierung - Literaturübersicht - N2 - Die für einen erfolgreichen Einsatz von Festschmierstoffen zur Minderung von Reibung und Verschleiß systembestimmender Parameter wie Last, Geschwindigkeit, Temperatur, umgebende Atmosphäre, Filmbildung und -haltung sowie die Anwendungstechnologien werden dargestellt, ferner Modellvorstellungen zum Verschleißverhalten von Festschmierstoffen im Hinblick auf konkrete Anwendungsfälle diskutiert. T3 - BAM Forschungsberichtreihe - 158 KW - Festschmierstoff KW - Transferschmierung KW - Hohe Temperaturen KW - Graphit KW - Reibung KW - Verschleißmodelle KW - gebundene Filme KW - Synergieeffekte PY - 1989 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-2921 SN - 978-3-88314-889-X SN - 0938-5533 VL - 158 SP - 1 EP - 112 PB - Wirtschaftsverlag NW CY - Bremerhaven AN - OPUS4-292 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Dörfel, Ilona A1 - Wäsche, Rolf A1 - Rabe, Torsten A1 - Steinborn, Gabriele T1 - Tribological Induced Microstructural Changes in Subsurface Layers of Si3N4-Based Materials KW - Tribologie PY - 1994 SN - 1013-9826 VL - 89-91 SP - 763 EP - 767 PB - Trans Tech Publ. CY - Aedermannsdorf AN - OPUS4-577 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter T1 - Wear of multiphase SiC based ceramic composites containing free carbon N2 - Ceramics are of increasing interest for application in many branches of technique. In order to improve the tribological performance of ceramic materials, composites on the basis of silicon carbide with different amounts of titanium carbide, boron carbide, titanium diboride and free carbon in the form of graphite were manufactured by a reaction sintering process. The friction and wear behaviour of these composites was investigated with oscillating sliding motion in unlubricated tests at room temperature on different levels of relative humidity. Additional tests were performed under water lubrication, revealing the superior behaviour of composites for special test conditions. A major influence of the free carbon on friction or wear behaviour was not observed. The tribological behaviour in air as well as under water is mainly dependant on the amount of titanium phases. KW - Siliziumkarbid KW - Verbundwerkstoffe KW - Tribooxidation KW - Silicon carbide KW - Ceramic composites KW - Humidity water KW - Lubrication PY - 2001 DO - https://doi.org/10.1016/S0043-1648(01)00566-X SN - 0043-1648 VL - 249 SP - 220 EP - 228 PB - Elsevier CY - Amsterdam AN - OPUS4-900 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Naito, M. A1 - Jahanmir, S. T1 - TWA 27 Characterization Methods for Ceramic Powders and Green Bodies KW - Standardisierung KW - Keramische Pulver KW - Grünkörper PY - 2000 SN - 1016-2178 IS - 23 SP - 21 EP - 27 PB - National Institute of Standards and Technology AN - OPUS4-979 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kautek, Wolfgang A1 - Rudolph, Pascale A1 - Brzezinka, Klaus-Werner A1 - Wäsche, Rolf ED - Meunier, M. T1 - Physical chemistry of the femtosecond and nanosecond laser-material-interaction with SiC and a SiC-TiC-TiB2 composite ceramic compound N2 - The interaction of nanosecond laser pulses in the ultraviolet wavelength range and femtosecond laser pulses in the near-infrared region with the direct semiconductor SiC and the composite compound SiC-TiC-TiB2 was investigated in respect to resulting physicochemical processes. Surface analytical techniques, such as XPS, µ-Raman, and EDX were used to identify the chemical changes between untreated and laser-treated areas. Single-pulse irradiation led to material modifications in the condensed state in most instances. Multi-pulse results differed depending on the pulse duration. In the nanosecond case, melting of the surface and redeposited material (debris) were observed. With femtosecond pulses instead, only negligible melting and few debris could be detected. Additionally, periodic structures (ripples) appeared, with parallel orientation and in most cases two different periodicities for a particular material. Laser ablation of all the studied compound materials exhibited preferential ablation of the lighter component elements. Crystal structure changes of the irradiated surface were observed as a consequence of laser-induced melting and resolidification. An oxidation process interfered with all this processes so that unstoichiometric oxides were formed. T2 - Symposium D - European Materials Research Society CY - Strasbourg, France DA - 2002-06-18 PY - 2002 UR - http://www.emrs-strasbourg.com/files/pdf/2002_SPRING/02_Prog_Dv2.pdf N1 - Serientitel: Applied surface science – Series title: Applied surface science VL - 208/209.2003,1 IS - 1 SP - 1 PB - Elsevier CY - Amsterdam AN - OPUS4-1732 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Rudolph, Pascale A1 - Brzezinka, Klaus-Werner A1 - Wäsche, Rolf A1 - Kautek, Wolfgang T1 - Physical chemistry of the femtosecond and nanosecond laser-material interaction with SiC and a SiC-TiC-TiB2 composite ceramic compound N2 - The interaction of nanosecond laser pulses in the ultraviolet wavelength range and femtosecond laser pulses in the near-infrared region with the semiconductor SiC and the composite compound SiC–TiC–TiB2 was investigated. Surface analytical techniques, such as XPS, depth profile (DP), and micro-Raman spectroscopy (?-RS) were used to identify the chemical changes between untreated and laser-treated areas. Single-pulse irradiation led to material modifications in the condensed state in most instances. Multi-pulse results differed depending on the pulse duration. Crystal structure changes were observed as a consequence of laser-induced melting and resolidification. In air contact all components underwent oxidation reactions according to thermodynamic expectations. Exceptions were observed under exclusion of oxygen, SiC was reduced to elemental Si. KW - Femtosecond techniques KW - Nanosecond techniques KW - Ceramics KW - Raman spectra/condensed matter KW - XPS/surface analysis PY - 2003 DO - https://doi.org/10.1016/S0169-4332(02)01356-9 SN - 0169-4332 SN - 1873-5584 VL - 208-209 SP - 285 EP - 291 PB - North-Holland CY - Amsterdam AN - OPUS4-2791 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Suchantke, Christian A1 - Yarim, Rasim ED - Schulte, K. ED - Kainer, K. T1 - Sintern von Verbundwerkstoffen im System SiC-TiC-TiB2 T2 - 12. Tagung "Verbundwerkstoffe und Werkstoffverbunde" CY - Hamburg, Deutschland DA - 1999-10-05 KW - Sintern KW - Verbundwerkstoffe KW - Thermochemische Analyse PY - 1999 SN - 3-527-29967-X SP - 189 EP - 194 PB - Wiley-VCH CY - Weinheim AN - OPUS4-720 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Klaffke, Dieter A1 - Hartelt, Manfred A1 - Wäsche, Rolf ED - Bartz, Wilfried J. T1 - Non-Oxide Ceramics as Tribo Materials - Analysis of Wear Mechanisms under Oscillating Sliding Conditions in Various Atmospheres T2 - 12th International Colloquium Tribology CY - Esslingen, Germany DA - 2000-01-11 KW - Tribologie PY - 2000 SN - 3-924813-44-2 VL - 3 SP - 1755 EP - 1763 PB - Techn. Akad. Esslingen CY - Ostfildern AN - OPUS4-848 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf T1 - Feste Schmierstoffe für hohe Temperaturen - Eine Literaturübersicht PY - 1989 SN - 0724-3472 VL - 36 IS - 3 SP - 145 EP - 151 PB - Expert Verlag CY - Renningen AN - OPUS4-1432 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Steinborn, Gabriele A1 - Klaffke, Dieter ED - Somiya, S. T1 - Gas pressure sintering of SiCp-alumina composites made by gelcasting and their tribological properties N2 - COMPOSITE MATERIALS OF A 99.7 % ALPHA-ALUMINA MATRIX WITH PLATELETS OF SILICON CARBIDE (SICP) HAVE BEEN PREPARED BY GELCASTING. DENSIFICATION WAS CARRIED OUT BY GAS-PRESSURE SINTERING WITHOUT FURTHER SINTERING AIDS. FIVE DIFFERENT COMPOSITIONS WITH 0, 5, 10, 15, AND 20 VOL.% SICP RESP. HAVE BEEN INVESTIGATED AND TRIBOLOGICAL PROPERTIES WERE CHARACTERIZED. INCREASING AMOUNT OF SICP AS RIGID PARTICLES IN THE FINE GRAINED MATRIX COMPLICATE THE DENSIFICATION PROCESS. WITH THE APPLICATION OF 50 BAR AR PRESSURE DURING THE FINAL SINTERING STEP AT A TEMPERATURE OF 1700 DEGREE C THE DENSITY OF THE SAMPLES COULD BE INCREASED BY 3-5%. INVESTIGATION OF THE TRIBOLOGICAL PROPERTIES AGAINST STEEL AS A COUNTERBODY UNDER UNLUBRICATED OSCILLATING SLIDING CONDITIONS SHOWED A HIGH COEFFICIENT OF FRICTION AND AN INCREASING WEAR RATE UP TO A SICP CONTENT OF 10 VOL. % . AT 15 AND 20 VOL. % SICP RESP. BOTH THE COEFFICIENT OF FRICTION AND THE COEFFICIENT OF WEAR DROP DOWN. T2 - 3rd IUMRS International Conference on Advanced Materials (ICAM) CY - Tokyo, Japan DA - 1993-08-31 PY - 1994 SN - 0-444-81993-2 N1 - Serientitel: Transactions of the Materials Research Society of Japan – Series title: Transactions of the Materials Research Society of Japan IS - 16B SP - 791 EP - 794 PB - Elsevier CY - Amsterdam AN - OPUS4-1433 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Steinborn, Gabriele T1 - Characterisation of the secondary properties of alumina - measuring the isoelectric point by a streaming potential method PY - 1997 SN - 0173-9913 SN - 0196-6219 VL - 74 IS - 5 SP - 235 EP - 239 PB - Göller CY - Baden-Baden AN - OPUS4-1434 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Steinborn, Gabriele T1 - Influence of Slip Viscosity on the Mechanical Properties of High Purity Alumina made by Gelcasting KW - High purity alumina KW - Gelcasting KW - Solid content KW - Viscosity KW - Deairing KW - Bending strenght KW - Microstructure KW - Computertomography KW - Defect type PY - 1997 SN - 1013-9826 VL - 132 SP - 374 EP - 377 PB - Trans Tech Publ. CY - Aedermannsdorf AN - OPUS4-1435 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Abe, H. A1 - Naito, M. A1 - Hackley, V. A1 - Hotta, Y. T1 - Influence of particle size and solid loading on the determination of the isoelectric point (IEP) of ceramics powders by different methods N2 - The isoelectric point is a material property for the characterization of acid-base behavior of the powder surface. The IEP of two alumina powders (AKP-30, Grade A) with different particle size characteristics in aqueous suspension has been determined by colloid vibration current (CVI) and particle charge detection (PCD) methods in moderately concentrated suspensions in order to qualify these methods for a future standardization. The solid loading of the suspensions were 1 and 5 vol%. The comparison of the IEP determined by PCD and CVI was in good agreement. However, the solid loading dependence of IEP and a large IEP hysteresis (at 1 vol%) were observed, which do not allow a proper determination of the IEP. The recording of the potential curve and therfore the determination of the IEP with CVI was difficult for the suspension of Grade A powder due to formation of agglomerates at pH values near the pHIEP. T2 - 7th Euro Ceramics - Conference and Exhibition of the European Ceramic Society (ECerS) CY - Brugge, Belgium DA - 2001-09-09 KW - Isoelectric point (IEP) KW - Alumina powder KW - Particle charge detection (PCD) KW - Colloid vibration current (CVI) PY - 2002 UR - http://ois.nist.gov/nistpubs/technipubs/recent/search.cfm?dbibid=9289 DO - https://doi.org/10.4028/www.scientific.net/KEM.206-213.3 SN - 1013-9826 VL - 206-213 SP - 3 EP - 6 PB - Trans Tech Publ. CY - Aedermannsdorf AN - OPUS4-1437 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Yarim, Rasim A1 - Wäsche, Rolf A1 - Woydt, Mathias ED - Franek, F. T1 - Wear Behaviour of SiC-TiC-TiB2 Ceramic Composites Sliding against SiC up to 800°C and 2m/s T2 - 2nd World Tribology Congress ; 2nd WTC 2001 CY - Vienna, Austria DA - 2001-09-03 KW - Dry sliding KW - Tribochemistry KW - Silicon carbide KW - Titanium carbide KW - Titanium boride KW - High temperature KW - Ceramic composites PY - 2001 SN - 3-901657-07-X SP - 1(?) EP - 4(?) PB - ÖTG CY - Wien AN - OPUS4-1438 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Klaffke, Dieter ED - Andersson, P. T1 - Tribological Behaviour of Multiphase Ceramic Composites in the System Si-Ti-B-C Containing Free Carbon T2 - 9th Nordic Symposium on Tribology ; 9th NORDTRIB 2000 CY - Porvoo, Finland DA - 2000-06-11 PY - 2000 SN - 951-38-5276-8 SN - 0357-9387 N1 - Serientitel: VTT Symposium – Series title: VTT Symposium VL - 1 IS - 200 SP - 186 EP - 195 PB - VTT, Technical Research Centre of Finland CY - Espoo AN - OPUS4-1439 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter T1 - Ceramic particulate composites in the system SiC-TiC-TiB2 sliding against SiC and Al2O3 under water N2 - The tribological behaviour of SiC, SiC-TiC and SiC-TiC-TiB2 was determined in oscillating sliding against SiC and -Al2O3 in water at room temperature. The tribo-systems with the composite materials containing TiC and TiB2 differ significantly from the systems with the single phase SiC: The wear is reduced and the friction is increased. The wear reduction up to a factor of 10 is mainly due to the formation of an oxide film containing titanium oxides which is soft, stable in water and well adhering to the bulk material. This oxide film is transferred to the alumina ball but not to the silicon carbide ball. KW - Silicon carbide KW - Titanium carbide KW - Titanium boride KW - Ceramic KW - Particulate composites KW - Oscillating sliding KW - Water lubrication KW - Friction KW - Wear PY - 1999 DO - https://doi.org/10.1016/S0301-679X(99)00033-X SN - 0301-679X VL - 32 IS - 4 SP - 197 EP - 206 PB - Butterworth-Heinemann CY - Oxford AN - OPUS4-1440 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Naito, M. ED - Puri, V. ED - Adair, J. ED - Knobloch, C. ED - Huang, C. T1 - Electrokinetic Characterization of Aqueous Ceramic Suspensions T2 - Fine Powder Processing Conference '99 CY - State University, PA, USA DA - 1999-09-20 KW - Meßverfahren KW - Zeta Potenzial KW - Hochleistungskeramik PY - 1999 SP - 177 EP - 183 AN - OPUS4-1441 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Steinborn, Gabriele A1 - Wäsche, Rolf A1 - Reichel, U. T1 - Fabrication of porous ceramics made from nano sized alumina powder by gelcasting N2 - The gelcasting process was used for manufacturing porous ceramic bodies from nano sized powders. 3 different powders with specific surface areas between 12 and 30 m²/g were used. Solid content of the corresponding slurries was dependent on the milling procedure and the use of a suitable dispersant. For bimodal GradeA powder solid content was as high as 58 vol%. For sintering temperatures between 1250 and 1600°C the porosity varied between 45 and 20%, whereas the pore radii varied between 50 and 91nm. The grain size of crystallites in the sintered microstructures was about 1um. The reflection ratio for visible light increased in comparison to a reference sample made from conventional powder from 0.8 to 0.95 in the wavelenght range around 400nm. T2 - 2nd International Conference on Shaping of Advanced Ceramics CY - Gent, Belgium DA - 2002-10-24 PY - 2002 SP - 103 EP - 108 AN - OPUS4-1813 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Klaffke, Dieter A1 - Wäsche, Rolf A1 - Yarim, Rasim T1 - Tribological Behaviour of SiC-TiC-TiB2 Composites under Unlubricated Sliding Conditions KW - Silicon carbide KW - Titanium carbide KW - Titanium diboride KW - Alumina KW - Oscillating sliding KW - Relative humidity PY - 2003 SN - 1354-4063 SN - 1557-685X VL - 9-3 IS - 9 SP - 185 EP - 195 PB - Coppin CY - Deal AN - OPUS4-2486 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Troczynski, T. T1 - Tribological performance of SiC and TiB2 against SiC and Al2O3 at low sliding speeds N2 - The friction and wear behaviour of a new developed, pressureless sintered TiB2 ceramic was studied in comparison to SiC against SiC and Al2O3 balls under unlubricated conditions at room temperature. Special attention was paid to the influence of relative humidity on friction and wear results. For both ceramics the coefficient of friction against both ball materials decreases with increasing humidity and is higher in tests against alumina than against SiC. The wear rate is affected significantly by humidity and decreases by one order of magnitude for Al2O3/SiC system and by 2 orders of magnitude for SiC/SiC system. For TiB2 wear rates are nearly not affected by humidity against both ball materials and are much smaller than for SiC. KW - Titanium diboride KW - Friction KW - Wear KW - Relative humidity KW - Counter body material PY - 2004 DO - https://doi.org/10.1016/S0043-1648(03)00444-7 SN - 0043-1648 VL - 256 SP - 695 EP - 704 PB - Elsevier CY - Amsterdam AN - OPUS4-3481 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Klaffke, Dieter A1 - Steinborn, Gabriele A1 - Wäsche, Rolf A1 - Wötting, G. ED - Degischer, H.-P. T1 - Tribologische Untersuchungen an SiC- und Si3N4-basierten Keramiken T2 - 14. Symposium Verbundwerkstoffe und Werkstoffverbunde CY - Wien, Österreich DA - 2003-07-02 PY - 2003 SN - 3-527-30762-1 SP - 545 EP - 550 PB - Wiley-VCH CY - Weinheim AN - OPUS4-2591 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Klaffke, Dieter A1 - Yarim, Rasim A1 - Wäsche, Rolf T1 - Effect of Pre-oxidation on Friction and Wear Behaviour of a SiC-TiC-TiB2 composite PY - 2003 VL - 22 SP - 12 EP - 20 PB - Metallilaboratorio CY - Espoo AN - OPUS4-2517 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Klaffke, Dieter A1 - Yarim, Rasim A1 - Wäsche, Rolf T1 - Einfluss einer Voroxidation auf das tribologische Verhalten keramischer Komposits KW - SiC KW - TiC KW - TiB2 KW - Kompositkeramik KW - Reibung KW - Schwingungsverschleiß KW - Randzone KW - Luftfeuchte PY - 2003 SN - 0724-3472 VL - 50 IS - 2 SP - 34 EP - 39 PB - Expert Verlag CY - Renningen AN - OPUS4-2536 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Yarim, Rasim A1 - Klaffke, Dieter A1 - Hartelt, Manfred ED - Bartz, Wilfried J. T1 - Oscillating Sliding Wear Behaviour of SiC, TiC, TiB2, 59SiC-41TiB2 and 52SiC-24TiC-24TiB2 Materials up to 750°C in Air T2 - 14th International Colloquium Tribology, Tribology and Lubrication Engineering CY - Stuttgart, Deutschland DA - 2004-01-13 PY - 2004 SN - 3-924813-54-X VL - II SP - 1039 EP - 1045 PB - Techn. Akad. Esslingen CY - Ostfildern AN - OPUS4-3057 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Klaffke, Dieter A1 - Wäsche, Rolf A1 - Wötting, G. ED - Bartz, Wilfried J. T1 - Tribological Characterisation of a Sl3N4-TiN Composite Ceramic in Fretting Tests at Room Temperature T2 - 14th International Colloquium Tribology, Tribology and Lubrication Engineering CY - Stuttgart, Germany DA - 2004-01-13 PY - 2004 SN - 3-924813-54-X VL - III SP - 1413 EP - 1420 PB - Techn. Akad. Esslingen CY - Ostfildern AN - OPUS4-3058 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Klaffke, Dieter A1 - Wäsche, Rolf A1 - Aldinger, F. A1 - Janakiraman, N. ED - Bartz, Wilfried J. T1 - Tribological investigations on siliconcarbonitride ceramics derived from preceramic polymers T2 - 14th International Colloquium Tribology, Tribology and Lubrication Engineering CY - Stuttgart, Deutschland DA - 2004-01-13 PY - 2004 SN - 3-924813-54-X VL - 3 SP - 1403 EP - 1412 PB - Techn. Akad. Esslingen CY - Ostfildern AN - OPUS4-3059 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Yarim, Rasim A1 - Santner, Erich T1 - Tribological Tayloring of Ceramic Composites N2 - With respect to their excellent material properties ceramics are of interest as candidate materials for tribological applications. The friction and wear behaviour of ceramics is often superior to that of metallic materials. Furthermore, an essential improvement of tribological performance will be possible by tailoring of ceramics in the process of powder preparation and sintering technique. Silicon Carbide (SiC) shows interesting friction and wear behaviour at room temperature, even under unlubricated running conditions but is very sensitive against effects of environmental humidity and shows high friction and high wear in the absence of water vapour. The tribological performance of SiC can be improved considerably by adding substantial amounts of TiC and TiB2 to the microstructure thus creating ceramic particulate composite materials. Various composites in the quasi ternary system SiC-TiC-TiB2 were prepared by a ceramic manufacturing process including sintering temperatures up to 2180 °C. Comparative tribo tests were performed under unlubricated oscillating sliding motion in dry, normal, and moist air and under water lubrication with SiC balls and Al2O3 balls as counter bodies. The friction is affected by the relative humidity (RH) but barely at all by the composition of the composites. The wear resistance of the composites was found to be improved considerably by addition of TiB2 in the range from 20 to 60 %. The highest wear resistance of the system wear was found when Al2O3 was used as counter body material. PY - 2003 DO - https://doi.org/10.1002/mawe.200300688 SN - 0933-5137 SN - 1521-4052 VL - 34 IS - 10/11 SP - 1008 EP - 1013 PB - Wiley-VCH Verl. CY - Weinheim AN - OPUS4-3132 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Yarim, Rasim A1 - Klaffke, Dieter A1 - Hartelt, Manfred T1 - Oscillating Sliding Wear Behaviour of SiC, TiC, TiB2, 59SiC-41TiB2 and 52SiC-24TiC-24TiB2 Materials up to 750°C in Air T2 - 14th International Colloquium Tribology, Tribology and Lubrication Engineering CY - Ostfildern, Germany DA - 2004-01-13 PY - 2004 AN - OPUS4-3076 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter T1 - High temperature tribological behaviour of particulate composites in the system SiC-TiC-TiB2 during dry oscillating sliding KW - Ceramic Composites KW - High temperatures KW - Tribo-oxidation KW - Dry-slidins KW - Friction KW - Wear PY - 1999 SN - 1225-9381 VL - 5 IS - 2 SP - 155 EP - 161 PB - Han'guk-Seramik-Hakhoe CY - Seoul AN - OPUS4-761 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Klaffke, Dieter A1 - Wäsche, Rolf ED - Franek, F. T1 - Friction and wear behaviour of ceramic SiC-TiC-TiB2 composites under unlubricated oscillating sliding conditions T2 - 2nd World Tribology Congress ; 2nd WTC 2001 CY - Vienna, Austria DA - 2001-09-03 KW - Silicon carbide KW - Titanium carbide KW - Titanium diboride KW - Alumina KW - Oscillating sliding KW - Humidity PY - 2001 SN - 3-901657-07-X SP - 140 PB - ÖTG CY - Wien AN - OPUS4-1172 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Hackley, V.A. A1 - Patton, J. A1 - Lum, L.-S. H. A1 - Wäsche, Rolf A1 - Naito, M. A1 - Abe, H. A1 - Hotta, Y. A1 - Pendse, H. T1 - Analysis of the isoelectric point in moderately concentrated Alumina suspensions using electroacoustic and streaming potential methods PY - 2002 SN - 0193-2691 SN - 1532-2351 VL - 23 IS - 5 SP - 601 EP - 617 PB - Dekker CY - New York, NY AN - OPUS4-2080 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Klaffke, Dieter A1 - Wäsche, Rolf ED - Schulte, K. ED - Kainer, K. T1 - Tribologische Prüfungen als begleitende Maßnahme zur Entwicklung von keramischen Tribowerkstoffen T2 - 12. Tagung "Verbundwerkstoffe und Werkstoffverbunde" CY - Hamburg, Deutschland DA - 1999-10-05 KW - Tribologie KW - Reibung KW - Verschleiß PY - 1999 SN - 3-527-29967-X SP - 423 EP - 428 PB - Wiley-VCH CY - Weinheim AN - OPUS4-723 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Klaffke, Dieter A1 - Wäsche, Rolf T1 - Friction and wear testing can steer the development of ceramic tribo materials T2 - 2nd World Tribology Congress ; 2nd WTC 2001 CY - Vienna, Austria DA - 2001-09-03 KW - Friction KW - Wear quantities KW - Humidity KW - Ball-on-disk KW - Wear particles PY - 2001 SN - 3-901657-09-6 SP - 141 PB - ÖTG CY - Vienna AN - OPUS4-1152 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Klaffke, Dieter A1 - Wäsche, Rolf T1 - Tribological Performance of SiC and TiB2 sliding against SiC and Al2O3 T2 - 10th Nordic Symposium on Tribology ; 10th Nordtrib 2002 CY - Stockholm, Sweden DA - 2002-06-09 PY - 2002 SP - 1(?) EP - 10(?) PB - Royal Institute of Technology CY - Stockholm AN - OPUS4-1386 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Klaffke, Dieter A1 - Yarim, Rasim A1 - Wäsche, Rolf T1 - Effect of pre-oxidation on friction and wear behaviour of a SiC-TiC-TiB2 composite T2 - 10th Nordic Symposium on Tribology ; 10th Nordtrib 2002 CY - Stockholm, Sweden DA - 2002-06-09 PY - 2002 SP - 1 EP - 10(?) PB - Royal Institute of Technology CY - Stockholm AN - OPUS4-1387 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Czichos, Horst T1 - Wear behaviour of i-carbon coatings PY - 1992 SN - 0043-1648 VL - 153 SP - 149 EP - 162 PB - Elsevier CY - Amsterdam AN - OPUS4-1428 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Steinborn, Gabriele T1 - Influence of the Dispersants in Gelcasting of Nanosized TiN PY - 1997 SN - 0955-2219 SN - 1873-619X IS - 17 SP - 421 EP - 426 PB - Elsevier CY - Oxford AN - OPUS4-1429 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Naito, M. A1 - Hackley, V.A. T1 - Experimental study on zeta potential and streaming potential of advanced ceramic powders N2 - Zeta potential as measured with the electrokinetic sonic amplitude (ESA) method has been compared to streaming potential as measured with the particle charge detection (PCD) method. The measurements have been carried out on identical suspensions of a-Al2O3, SiC and Si3N4 with a solids volume fraction of 1% and 10%. Zeta potential and streaming potential are related by a linear function. The correlation coefficients for this relationship are better than 0.99 for the suspensions with 1% solids loading. For the suspensions with 10% solids loading, correlation coefficients are slightly lower due to the influence of increasing viscosity. Regardless of lower correlation at the higher solids loading, the isoelectric pH is constant within the limits of accuracy of the pH measurements. KW - Zeta potential KW - Streaming potential KW - Ceramic powders KW - Correlation of measurement PY - 2002 DO - https://doi.org/10.1016/S0032-5910(01)00462-4 SN - 0032-5910 SN - 1873-328X VL - 123 SP - 275 EP - 281 PB - Elsevier CY - Amsterdam AN - OPUS4-1430 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf T1 - Keramische Supraleiter - Kristallstruktur, Gefüge und Eigenschaften PY - 1988 SN - 0340-7551 VL - 18 IS - 2 SP - 128 EP - 133 PB - Bundesanstalt für Materialprüfung CY - Berlin AN - OPUS4-1431 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Skopp, André ED - Bartz, Wilfried J. T1 - Tribological behaviour of silicon nitride with boron nitride as a solid lubricant PY - 1992 SN - 3-924813-28-0 N1 - Serientitel: Internationales Kolloquium / Technische Akademie Esslingen – Series title: Internationales Kolloquium / Technische Akademie Esslingen IS - 8 SP - 10.2-1 - 10.2-10 PB - Techn. Akad. Esslingen CY - Ostfildern AN - OPUS4-2406 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Woydt, Mathias A1 - Skopp, André A1 - Wäsche, Rolf T1 - Ceramic-ceramic composite materials with improved friction and wear properties PY - 1992 SN - 0301-679X VL - 25 IS - 12 SP - 61 EP - 70 PB - Butterworth-Heinemann CY - Oxford AN - OPUS4-2408 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Woydt, Mathias A1 - Skopp, André A1 - Wäsche, Rolf ED - Carlsson, R. T1 - Ceramic-ceramic composite materials with improved friction and wear properties T2 - 4th International Symposium Ceramic Materials and Components for Engines CY - Göteborg, Sweden DA - 1991-01-01 PY - 1992 SN - 1-85166-776-8 SP - 1219 EP - 1239 PB - Elsevier CY - London AN - OPUS4-2409 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Yarim, Rasim A1 - Klaffke, Dieter A1 - Hartelt, Manfred T1 - Oscicalling sliding wear behaviour of SiC, TiC, TiB2 59SiC-41TiB2 and 52SiC-24TiC-24TiB2 T2 - 14th International Colloquium Tribology CY - Ostfildern, Germany DA - 2004-01-13 PY - 2004 AN - OPUS4-11062 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Woydt, Mathias A1 - Dörfel, Ilona T1 - Interface formation by tribo-oxidation in SiC based ceramics T2 - AIST-BAM Symposium on Materials Surface Technology in Twin Institute Programme CY - Tsukuba, Japan DA - 2003-02-18 PY - 2003 SP - 1 EP - 4 AN - OPUS4-12051 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Woydt, Mathias A1 - Dörfel, Ilona T1 - Structure of the interface in SiC-based ceramic composites formed by tribo-oxidation under dry sliding conditions PY - 2004 SN - 1042-1122 VL - 146 SP - 401 EP - 407 PB - American Ceramic Society CY - Westerville, Ohio AN - OPUS4-12053 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Yarim, Rasim A1 - Nicolaides, Dagmar T1 - Influence of Green Compaction on the Sintering Behaviour of SiC-TiC-TiB2 Composites KW - Pressureless sintering KW - SiC KW - TiC KW - TiB2 KW - Green compaction KW - Particle size KW - Microstructure PY - 2004 SN - 1013-9826 VL - 264-268 SP - 213 EP - 218 PB - Trans Tech Publ. CY - Aedermannsdorf AN - OPUS4-12054 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Yarim, Rasim A1 - Wäsche, Rolf A1 - Woydt, Mathias A1 - Dörfel, Ilona T1 - Analysis of wear protecting oxide layers in the system SiC-TiC-TiB2 formed in-situ at high temperatures T2 - AIST-BAM Symposium on Materials Surface Technology in Twin Institute Programme CY - Tsukuba, Japan DA - 2003-02-18 PY - 2003 SP - 5 EP - 8 AN - OPUS4-12057 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Klaffke, Dieter A1 - Wäsche, Rolf A1 - Janakiraman, N. A1 - Aldinger, F. T1 - Tribological characterisation of siliconcarbonitride ceramics derived from preceramic polymers N2 - Amorphous SiCN ceramics were prepared in a laboratory scale as disk shaped specimens with 10 mm diameter and 0.3 mm thickness. The friction and wear behaviour was characterised in gross slip fretting tests under unlubricated conditions at room temperature against steel (100Cr6) and ceramic (Al2O3). Tests with a ball-on-disk contact were performed in laboratory air with different content of water vapour. The results show clearly that the relative humidity has a significant effect on friction and wear behaviour. All tests in dry air lead to higher friction and higher wear rate than in normal air. Improved friction and wear behaviour was observed with increasing pyrolysis temperature up to 1100 °C of the SiCN specimens. This is attributed to increasingly better mechanical properties and higher stiffness of the amorphous network due to the evaporation of gaseous organic species and the formation of free graphite like carbon. KW - Ceramics KW - Preceramic polymer KW - Siliconcarbonitride KW - Friction KW - Wear PY - 2006 DO - https://doi.org/10.1016/j.wear.2005.04.031 SN - 0043-1648 VL - 260 IS - 7-8 SP - 711 EP - 719 PB - Elsevier CY - Amsterdam AN - OPUS4-12302 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Woydt, Mathias A1 - Dörfel, Ilona T1 - Structure of interface in SiC - based composites formed by tribo-oxidation under dry sliding conditions T2 - International Conference on the Characterization and Control of Interfaces for High Quality Advanced Materials (ICCCI 2003) CY - Kurashiki, Japan DA - 2003-09-24 PY - 2003 AN - OPUS4-4304 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Woydt, Mathias A1 - Dörfel, Ilona T1 - Interface formation in SiC based composites T2 - AIST-BAM Symposium on Material Surface Technology in TWIN Institute Programme CY - Tsukuba, Japan DA - 2003-02-18 PY - 2003 AN - OPUS4-4305 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Yarim, Rasim T1 - Gas pressure sintering of SiC-TiC-TiB2 ceramic composites T2 - 8. ECerS Conference of the European Ceramic Society CY - Istanbul, Turkey DA - 2003-06-29 PY - 2003 AN - OPUS4-5354 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Göbel, Thomas T1 - Laser induced thermal shock testing on Si3N4 GS44 and alumina Heratape T2 - Research and Development on Advanced Materials for Transportation Applications CY - Oakland, CA, USA DA - 2003-10-22 PY - 2003 AN - OPUS4-5361 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Göbel, Thomas T1 - Werkstoffe der hochleistungskeramik - Herstellung und Charakterisierung an der BAM T2 - Seminar für Werkstofftechnik im FB 15 der Universität Kassel CY - Kassel, Germany DA - 2003-11-17 PY - 2003 AN - OPUS4-5362 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Procop, Mathias A1 - Hübner, Wolfgang A1 - Wäsche, Rolf A1 - Nieland, S. A1 - Ehrmann, O. T1 - Fast Elemental Mapping in Materials Science KW - Electron probe microanalysis KW - EPMA KW - Energy dispersive X-ray spectroscopy KW - EDS KW - Elemental mapping PY - 2002 UR - http://www.microscopy-analysis.com/sites/default/files/magazine_pdfs/mag%20179_2002_Jan_Procop_1.pdf SN - 0958-1952 IS - January SP - 5 EP - 6 PB - Rolston Gordon Comm. CY - Bookham, Surrey AN - OPUS4-7091 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Steinborn, Gabriele A1 - Nitsche, R. T1 - Dispersion and Characterisation of Nanoscale Particle Suspensions T2 - International Symposium on Smart Processing Technology (ISMPT) CY - Osaka, Japan DA - 2005-11-14 PY - 2005 AN - OPUS4-11828 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Janakiraman, N. A1 - Aldinger, F. T1 - Tribological investigations on siliconcarbonitride ceramics derived from preceramic T2 - 14th International Colloquium Tribology CY - Ostfildern, Germany DA - 2004-01-13 PY - 2004 AN - OPUS4-11057 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Hartelt, Manfred A1 - Wäsche, Rolf T1 - Verschleißuntersuchungen an Dental-Implantat-Werkstoffen unter partial slip Bedingungen KW - Modellsystem KW - Partial slip KW - Fretting regime KW - Implantat KW - Titan PY - 2012 SN - 0724-3472 VL - 59 IS - 3 SP - 18 EP - 23 PB - Expert Verlag CY - Renningen AN - OPUS4-26003 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Czichholz, G. A1 - Steinborn, Gabriele T1 - Wear behaviour of yttrium titanate ceramics under gross slip fretting conditions T2 - Int. Conf. Nordic Countries (NordTrib 2012) CY - Trondheim, Norway DA - 2012-06-12 PY - 2012 AN - OPUS4-26014 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Podgursky, V. A1 - Adoberg, E. A1 - Surzenkov, A. A1 - Kimmari, E. A1 - Viljus, M. A1 - Mikli, V. A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Síma, M. A1 - Kulu, P. T1 - Dependence of the friction coefficient on roughness parameters during early stage fretting of (Al,Ti)N coated surfaces N2 - Main focus was on the correlation of the coefficient of friction (COF) with the geometrical parameters of the surface during early stage of the running-in period. TiN, TiAlN and AlTiN coatings were prepared by using rotating cathode arc evaporation unit. The roughness of the WC-Co substrate Ra ranged from 0.05 to 0.2 µm and the coating thickness was 2.3 ± 0.2 µm. Part of the samples were subjected to the surface modification by the drag grinding finishing. Geometrical parameters of the surface were evaluated by means of atomic force microscopy (AFM) and fretting tests were conducted with 10 mm diameter alumina ball under 2 N load, 100 µm slip distance and the frequency of 10 Hz. It was found that the distribution of macroparticles strongly influences the geometrical parameters of the surface and the number of macroparticles increases with increasing Al content in the coating. In the case of the positive skewness Ssq of the coating surface, the kurtosis Sku provides a statistically significant effect on the COF, namely the COF depends inversely on the kurtosis Sku. The kurtosis value for TiN was the highest among as-deposited coatings, subsequently, the slowest increase rate in the COF was observed for the TiN coating. KW - PVD coatings KW - AFM KW - Surface topography KW - COF PY - 2011 DO - https://doi.org/10.1016/j.wear.2011.03.006 SN - 0043-1648 VL - 271 IS - 5-6 SP - 853 EP - 858 PB - Elsevier CY - Amsterdam AN - OPUS4-24497 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Cruzado, Aitor A1 - Hartelt, Manfred A1 - Urchegui, M.A. A1 - Gomez, X. T1 - Oxidative wear in gross slip fretting of thin steel wires T2 - ITC Hiroshima Satellite Symposium, Tribochemistry Hagi 2011 CY - Hagi, Japan DA - 2011-10-25 PY - 2011 AN - OPUS4-24609 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Woydt, Mathias T1 - The history of the Stribeck curve and the role of Adolf Martens T2 - Int. Tribology Congress / ITC Hiroshima CY - Hiroshima, Japan DA - 2011-10-30 PY - 2011 AN - OPUS4-24610 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Woydt, Mathias A1 - Tato, W. T1 - Alumina and zirconia as tribomaterials - a review T2 - The Fourth International Conference on The Characterization and Control of Interfaces for High Quality Advanced Materials (ICCCI 2012) CY - Kurashiki, Japan DA - 2012-09-02 PY - 2012 AN - OPUS4-24612 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Kaltzakorta, O. A1 - Tato, W. T1 - Tribological behaviour of polyurethane under oscillating sliding conditions against cast iron T2 - 18. Int. Colloq. Tribology - Industrial and Automotive Lubrication CY - Ostfildern, Germany DA - 2012-01-10 PY - 2012 AN - OPUS4-25343 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hartelt, Manfred A1 - Wäsche, Rolf T1 - Verschleißuntersuchungen an Dental-Implantat-Werkstoffen unter partial slip Bedingungen N2 - Im Vortrag wird neben der apparativen Prüftechnik das allgemeine methodische Vorgehen für Modell-Verschleißuntersuchungen im Bereich des partial slip vorgestellt. Im Detail wird für Dental-Implantat-Werkstoffe eine Rangfolge aufgestellt, die vergleichend die Verschleißresistenz unterschiedlicher Ti-basierter Werkstoffe zeigt. Wird durch die Kaubewegung eine mehrachsige Beanspruchung in die Kontaktflächen der Schraubverbindung eingeleitet, kann durch partial slip im Randbereich dieser Kontaktfläche ein Verschleißprozess initiiert werden, der die Lockerung des Implantats begünstigt. Eine gute Verschleißresistenz verhindert oder schiebt die vorzeitige Lockerung hinaus. Um das Werkstoffverhalten in Bezug auf eine vorzeitige Lockerung der Implantatkrone bei geschraubten zweiteiligen Implantaten zu charakterisieren, wurden zylindrische Probekörper unter partial slip Fretting-Bedingungen mit Zyklenzahlen bis n = 200 000 beansprucht. Die Frequenz der aufgebrachten Tangentialkraft betrug 2 Hz, um die Kaubewegung zu simulieren. Die tribologischen Untersuchungen wurden auf einem Eigenbau-Tribometer mit der Kontaktgeometrie „gekreuzte Zylinder“ durchgeführt. Die zylindrischen Proben wurden aus den Werkstoffen Titan Grade 4 und der Ti-Legierung Ti6AI4V gefertigt. Ein Teil dieser Ti-basierten Proben wurde oberflächengehärtet. Die bisher erzielten Ergebnisse zeigen, dass die oberflächenbehandelten Proben dazu neigen, unter der Belastung die Kontaktfläche zu vergrößern. Dies deutet auf einen Effekt bekannt als „junction growth“ und damit auf eine erhöhte Versetzungsbeweglichkeit der randschichtgehärteten Proben hin. Einen Einfluss der Zwischenstoffe konnte nicht nachgewiesen werden. T2 - 52. Tribologie-Fachtagung - Reibung, Schmierung und Verschleiß - Forschung und praktische Anwendungen CY - Göttingen, Germany DA - 26.09.2011 KW - Partial slip KW - Schwingungsverschleiß PY - 2011 SN - 978-3-00-035439-7 VL - I SP - 14/1 EP - 14/11 AN - OPUS4-24813 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Steinborn, Gabriele A1 - Fritz, Ulrich A1 - Rabe, Torsten A1 - Wäsche, Rolf T1 - Dispergierung von Nanopulvern in Foliengießschlickern KW - Dispergierung KW - Nanopulver KW - Folie PY - 2004 SN - 0173-9913 SN - 0196-6219 VL - 18 IS - 1 SP - 43 EP - 50 PB - Göller CY - Baden-Baden AN - OPUS4-5219 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Yarim, Rasim T1 - Tribological Tailoring of Ceramic Composites T2 - 13th International Colloquium on Tribology CY - Esslingen am Neckar, Germany DA - 2002-01-15 PY - 2002 AN - OPUS4-6312 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Yarim, Rasim A1 - Woydt, Mathias T1 - High Temperature Tribological Behaviour of SiC Particulate Composites T2 - Austceram 2002 CY - Perth, Australia DA - 2002-09-30 PY - 2002 AN - OPUS4-6313 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Bestimmung der Thermoshockfestigkeit von Keramik mittels Laseraufzeichung T2 - DKG Bezirksgruppensutzung Berlin CY - Berlin, Germany DA - 2002-04-18 PY - 2002 AN - OPUS4-6303 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Pre- Standardisation for Powders and Green Bodies - VAMAS TWA 27 as a Tool for enhancement of Quality in the Ceramic Manufacturing Process T2 - International Workshop on Trends and Initiatives in Materials Characterisation and Processing CY - Gwangju, South Korea DA - 2002-09-02 PY - 2002 AN - OPUS4-6304 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Tribology of Advanced Ceramics III: Principles of solid lubrication - materials and mechanisms T2 - APEC workshop CY - Daejeon, South Korea DA - 2002-03-04 PY - 2002 AN - OPUS4-6305 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Jahanmir, S. T1 - Tribology of Advanced Ceramics I: Mild to severe wear transitions T2 - APEC workshop CY - Daejeon, South Korea DA - 2002-03-04 PY - 2002 AN - OPUS4-6306 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Klaffke, Dieter T1 - Tribological perfomance of SiC and TiB2 SSilding against SiC and AI2O3 T2 - NORDTRIB 2002 CY - Stockholm, Sweden DA - 2002-06-10 PY - 2002 AN - OPUS4-6307 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Klaffke, Dieter T1 - Tribology of Advanced Ceramics II: Evaluation of tribological Properties T2 - APEC workshop CY - Daejeon, South Korea DA - 2002-03-04 PY - 2002 AN - OPUS4-6308 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Steinborn, Gabriele T1 - Porous alumina from nano sized powders with improwed diffuse reflection properties T2 - Vorlesung bei Osaka University CY - Osaka, Japan DA - 2002-09-04 PY - 2002 AN - OPUS4-6309 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hackley, V. A1 - Naito, M. T1 - Promoting the infrastructure - prestandardisation endeavours for ceramic powders and green bodies T2 - Annual Meeting of the American Ceramic Society CY - St. Louis, MO, USA DA - 2002-04-30 PY - 2002 AN - OPUS4-6310 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kloß, Heinz A1 - Wäsche, Rolf T1 - Analytical approach for wear prediction of metallic and ceramic materials in tribological applications T2 - ECOTRIB 2007 CY - Ljubljana, Slovenia DA - 2007-06-12 KW - Wear KW - Surface temperature KW - Activation energy KW - Simulation KW - Movable cellular automata (MCA) PY - 2007 VL - I SP - 223 EP - 234 PB - Slovenská Akadémia Vied CY - Ljubljana AN - OPUS4-14972 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Springborn, U. A1 - Köster, K. A1 - Bewilogua, K. T1 - Schwingungsverschleiß von Kohlenstoffnitridschichten CNx gegen Aluminiumoxid in Luft T2 - 48. Tribologie-Fachtagung CY - Göttingen, Deutschland DA - 2007-09-24 KW - Schwingungsverschleiß KW - CNx Schichten KW - Magnetronsputtern KW - Reibung KW - Keramik PY - 2007 SN - 978-3-00-022603-8 SP - 27/1 EP - 27/11 CY - Aachen AN - OPUS4-15921 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Urchegui, M.A. A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Gómez, X. T1 - Analysis of different strategies to reduce fretting wear in thin steel roping wires N2 - After having checked in a previous study the influence of stroke and normal load in laboratory fretting tests accomplished with thin steel roping wires, in this paper the effect of the contact pressure (test configuration), environmental conditions (relative humidity) and reduction of the friction coefficient (lubricants) on the wear behaviour were analysed. The wires were 0.45 mm in diameter and the material was a cold-drawn eutectoid carbon steel (0.8% C) with a Tensile Strength over 2800 MPa. The tests were performed on an oscillating test rig and the volumetric wear of both specimens of the tribocouple was determined separately from three-dimensional topographies of the wear scars acquired by means of a confocal profiler, and a calculation algorithm developed in using MATLAB®. The strong effect of humidity and lubrication on wear behaviour was proved, whereas a slight effect of contact pressure was derived. KW - Wires KW - Fretting test KW - Contact pressure PY - 2008 DO - https://doi.org/10.1002/tt.52 SN - 1354-4063 SN - 1557-685X VL - 14 IS - 1 SP - 43 EP - 57 PB - Coppin CY - Deal AN - OPUS4-16677 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Physikalisch-chemische Grundlagen der Festschmierstoffe T2 - TAE Esslingen: Lehrgang: Reibungs- und Verschleißminderung durch Festschmierstoffe CY - Ostfildern, Germany DA - 2008-03-31 PY - 2008 AN - OPUS4-18316 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Grundlagen der Schwingungsverschleißprüfung T2 - TAE Esslingen + GfT: Seminar: Reibung und Verschleiß von Werkstoffen, Bauteilen und Konstruktion CY - Ostfildern, Germany DA - 2008-04-08 PY - 2008 AN - OPUS4-18317 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Verschleißprüfung als Werkzeug für die keramikbezogene Werkstoffentwicklung T2 - Hannover-Messe 2008: Werkstoff-Forum CY - Hanover, Germany DA - 2008-04-25 PY - 2008 AN - OPUS4-18318 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Djahanbakhsh, Mohammad A1 - Österle, Werner T1 - Vergleich von Standard-Modell- und HIP-Simulator-Untersuchungen an Verschleißschutzschichten für Metall-Keramik-Paarungen bei Endoprothesen T2 - 48. Tribologie-Fachtagung "Reibung, Schmierung und Verschleiß - Forschung und praktische Anwendungen" CY - Göttingen, Deutschland DA - 2007-09-24 KW - Reibung KW - Verschleiß KW - Beschichtung KW - HIP-Simulation PY - 2007 SN - 978-3-00-022603-8 VL - 1 SP - 8/1 EP - 8/10 CY - Aachen AN - OPUS4-16102 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Österle, Werner A1 - Djahanbakhsh, Mohammad A1 - Hartelt, Manfred A1 - Wäsche, Rolf T1 - Reasons for inferior performance of ceramic on a-C:H-coated Ti-6Al-4V in hip simulator testing compared to ball on flat reciprocating sliding tests N2 - The tribological performance of a hydrogenated amorphous carbon coating on Ti–6Al–4V against ceramic balls was checked by simple reciprocating sliding tests and by more complicated tests in a hip joint simulator. 3 of 4 joints failed during hip simulator testing already after approximately 100 × 10³ cycles and possibly due to coating failures caused by insufficient polishing of the metallic acetabular cups prior to coating deposition. Since such failures occurred only occasionally, the problem was not revealed by reciprocating sliding tests which are stressing a much smaller surface area compared to the tests in the hip joint simulator. Another type of failure, pits of 1–2 µm in diameter distributed randomly at the coating surface, was frequently observed by Scanning Electron Microscopy and analyzed comprehensively by Focused Ion Beam technique in combination with Transmission Electron Microscopy in one case. Although not necessarily affecting wear, such small failures might cause long-term problems in vivo, by providing access of body fluid to the substrate–coating interface making it susceptible to corrosion. KW - Hip simulator KW - Reciprocating sliding test KW - A-C:H KW - Coating failure KW - Artificial hip joint PY - 2008 DO - https://doi.org/10.1016/j.wear.2008.04.008 SN - 0043-1648 VL - 265 IS - 11-12 SP - 1727 EP - 1733 PB - Elsevier CY - Amsterdam AN - OPUS4-18439 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Gräber, H.-G. A1 - Klaffke, Dieter T1 - Tribologische Untersuchung zum Verschleißverhalten von keramischen Zahnersatzwerkstoffen KW - Dentalkeramik KW - Bearbeitbarkeit KW - Zwischenmedium KW - pH-Wert KW - Dental ceramic KW - Machinability KW - Liquid media KW - pH-value PY - 2007 SN - 0724-3472 VL - 54 IS - 3 SP - 29 EP - 32 PB - Expert Verlag CY - Renningen AN - OPUS4-15737 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Steinborn, Gabriele A1 - Wäsche, Rolf T1 - Charakterisierung der Dispergiereigenschaften von keramischen nanodispersen Suspensionen mit der Ultraschallspektroskopie N2 - Die Dispergiereigenschaften von verschiedenen nanoskaligen Pulvern mit unterschiedlicher Kornfraktion im Bereich von 10 bis 250 nm werden in verdünnten und konzentrierten keramischen Schlickern mit der Ultraschallspektroskopie untersucht. Alle stabilen Suspensionen weisen im entsprechenden pH-Bereich eine monomodale Partikelgrößenverteilung auf. Durch die Charakterisierung der Suspensionen mit der Ultraschallspektroskopie kann eine verbesserte Bewertung hinsichtlich Homogenität und Agglomeratbildung auch für nanoskalige Pulver erhalten werden. Dies ermöglicht eine bessere Qualitätskontrolle prozessrelevanter Schritte bei der Verarbeitung. KW - Dispergieren KW - Nanopartikel KW - Suspensionen KW - Folie KW - Nanopulver KW - Dispergierung PY - 2007 DO - https://doi.org/10.1002/cite.200600141 SN - 0009-286X SN - 1522-2640 VL - 79 IS - 3 SP - 257 EP - 265 PB - Wiley-VCH Verl. CY - Weinheim AN - OPUS4-16271 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Steinborn, Gabriele A1 - Fritz, Ulrich A1 - Rabe, Torsten A1 - Wäsche, Rolf ED - Kriegesmann, J. T1 - Dispergierung von Nanopulvern in Foliengießschlickern KW - Dispergierung KW - Nanopulver KW - Foliengiessen PY - 2005 SN - 3-87156-091-X IS - Kap. 3.3.3.5 SP - 1 EP - 16 PB - Deutscher Wirtschaftsdienst CY - Köln AN - OPUS4-16272 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hartelt, Manfred T1 - Tribological characterisation with crossed cylinders - comparison of methods and application examples T2 - TAE Esslingen: 16. International Colloquium Tribology 2008 CY - Ostfildern, Germany DA - 2008-01-15 PY - 2008 AN - OPUS4-18463 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - The interface as key to unclustard ceramic tribology T2 - SRV Workshop und Normungstagung CY - Nagoya, Japan DA - 2008-03-11 PY - 2008 AN - OPUS4-18464 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf ED - Pohl, M. T1 - Schwingungsverschleißprüfung als Werkzeug für die Werkstoffentwicklung T2 - Tagung "Werkstoffprüfung 2007" CY - Neu-Ulm, Deutschland DA - 2007-11-29 KW - Verschleißfestigkeit KW - Werkstoffentwicklung KW - Keramik KW - Reibungsverhalten KW - Stahl PY - 2007 SN - 978-3-514-00753-6 SP - 299 EP - 304 PB - Verl. Stahleisen CY - Düsseldorf AN - OPUS4-16426 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Djahanbakhsh, Mohammad A1 - Österle, Werner T1 - Vergleich von Standard-Modell- und HIP-Simulator-Untersuchungen an Verschleißschutzschichten für Metall-Keramik-Paarungen bei Endoprothesen KW - Beschichtung KW - Reversierender Gleitverschleiß KW - HIP-Simulation KW - Coating KW - Reciprocating sliding KW - HIP-Simulation PY - 2008 SN - 0724-3472 VL - 55 IS - 1 SP - 21 EP - 25 PB - Expert Verlag CY - Renningen AN - OPUS4-17133 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hartelt, Manfred T1 - Tribotesting with small loads and amplitudes - how does it compare to normal conditions in oscillating sliding? T2 - 27th Meeting of the International Research Group on Wear of Engineering Materials CY - Berlin, Germany DA - 2008-09-30 PY - 2008 AN - OPUS4-18215 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hartelt, Manfred T1 - Tribological behavior of hard carbon coatings sliding against aluminum oxide, silicon nitride and steel up to 250 °C in air T2 - NORDTRIB 2008, 13th Nordic Symposium on Tribology CY - Tampere, Finland DA - 2008-06-10 PY - 2008 AN - OPUS4-18217 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Steinborn, Gabriele ED - Bartz, Wilfried J. T1 - Tribological investigations on infiltrated zirconia T2 - 15th International colloquium tribology - Automotive and Industrial Lubrication CY - Ostfildern, Germany DA - 2006-01-17 KW - Friction KW - Wear infiltration KW - Zirconia KW - Alcaline earth fluorides PY - 2006 SN - 3-924813-62-0 SP - 1(?) EP - 7(?) CY - Ostfildern AN - OPUS4-12165 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Klaffke, Dieter A1 - Wäsche, Rolf ED - Bartz, Wilfried J. T1 - Tribological Characterisation of ceramics in fretting tests at room temperature T2 - 15th International colloquium tribology - Automotive and Industrial Lubrication CY - Ostfildern, Germany DA - 2006-01-17 KW - Silicon nitride KW - Silicon carbide KW - Composits KW - Friction KW - Wear KW - Fretting PY - 2006 SN - 3-924813-62-0 SP - 1(?) EP - 10(?) CY - Ostfildern AN - OPUS4-12167 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Steinborn, Gabriele T1 - Tribological testing of Ca-Ba infiltrated zirconia KW - Friction KW - Wear KW - Ca-Ba fluoride KW - Infiltration KW - Porous zirconia PY - 2005 UR - http://www.om.ugal.ro/AnnalsFasc8Tribology/pdf/2005/9-Annals2005-3-Wasche.pdf SN - 1221-4590 SN - 1220-0824 SP - 53 EP - 59 CY - Gala¸ti AN - OPUS4-12365 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Klaffke, Dieter ED - Christophe Donnet, ED - Erdemir, Ali T1 - Tribology of DLC Films Under Fretting Conditions KW - DLC KW - Oscillation sliding KW - Counterbody KW - Relative humidity KW - Temperature KW - Lubrication PY - 2008 SN - 978-0-387-30264-5 SP - 362 EP - 382 PB - Springer Science + Business Media AN - OPUS4-18571 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kovalev, Alexander A1 - Hartelt, Manfred A1 - Spaltmann, Dirk A1 - Wäsche, Rolf A1 - Woydt, Mathias T1 - Zero wear (Null Verschleiß) KW - Reibung KW - Null-Verschleiß KW - Rauhigkeit KW - Kontaktmechanik KW - Modellierung KW - DLC KW - Friction KW - Zero-wear KW - Roughness KW - Contact mechanics KW - Simulation PY - 2013 SN - 0724-3472 VL - 60 IS - 2 SP - 5 EP - 12 PB - Expert Verlag CY - Renningen AN - OPUS4-28979 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Scholz, Christian A1 - Wäsche, Rolf T1 - Stick-slip and wear behavior of ceramic and polymer materials under reciprocating sliding conditions N2 - In many technical applications not only the actual friction coefficient is of importance, but rather the constancy relevant for the functionality. Due to inconstant ffiction values, positioning processes can be substantially influenced as well as vibrations can be induced. The appearance of this tribological effect, named stick-slip, depends on different factors such as sliding speed, relative humidity and ambient temperature occurring primarily after long operating periods. Beside ambient conditions the choice of materials in contact is the main influencing factor of an inconstant coefficient of friction during operating. Certain polymers are well known for their stick-slip tendencies in technical applications. These are on the one hand different modifications of PTFE (polytetrafluoroethylene) reinforced with glass fibers, bronze or graphite and on the other hand thermoplastics such as PE (polyester) or Pf (polyimide). The difference between static and dynamic values of the ffiction force is decisive for stick-slip phenomena. Furthermore, the stick-slip tendency of polymers strongly depends on the elastic material properties. Main softening material areas, which can be found in the contact, represent particularly vulnerable areas. The high friction value in the contact area decreases in most cases by increasing sliding speeds. However, beside polymers ceramic materials can also offer tendencies to stick-slip motion. Klaffke et al. already investigated the influence of ceramic materials on the stick-slip behavior in. T2 - WTC 2013 - 5th World tribology congress CY - Torino, Italy DA - 08.09.2013 KW - Stick-slip KW - Sliding speed KW - Polymers KW - Ceramics KW - Humidity PY - 2013 SP - 1 EP - 4 AN - OPUS4-29091 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hartelt, Manfred A1 - Cappella, Brunero A1 - Wäsche, Rolf T1 - Verschleißbestimmung im nm-Bereich N2 - Die Verschleißbeträge können im nm-Bereich quantifiziert werden durch die Berechnung eines Mittelwert-Profils. Grundlage dieser Berechnung ist die hochauflösende Erfassung der 3D-Topographiedaten, die tribologisch beanspruchte und nichtbeanspruchte Oberflächenbereiche gleichermaßen beinhalten. Ein bestimmtes Messverfahren (taktil oder optisch) wird nicht favorisiert. Die vertikale Auflösung des Messverfahrens sollte im nm-Bereich liegen.--------------------------------------------------------------------------------------------------------------------------------------------------------------------- The wear rates can be quantified in the nm range by calculating a mean profile. Based on this calculation is the high-resolution recording of the 3D topography data containing tribologically worn and unworn surface areas alike. A specific measurement method (tactile or visual) is not favored. The vertical resolution of the measurement process should be in the nm range. T2 - 54. Tribologie-Fachtagung - Reibung, Schmierung und Verschleiß - Forschung und praktische Anwendungen CY - Göttingen, Germany DA - 2013-09-30 PY - 2013 SN - 978-3-00-022603-8 VL - I SP - 31/1 EP - 31/10 AN - OPUS4-29640 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Woydt, Mathias A1 - Wäsche, Rolf T1 - The history of the Stribeck curve and ball bearing steels: The role of Adolf Martens N2 - The historical development on the discoveries of lubrication regimes for lubricated sliding contacts has been reviewed from the very beginning. It was found that the functional relationship between the coefficient of friction and the product of sliding speed and viscosity divided by the normal load well known as the Stribeck curve has been experimentally explored much earlier by Adolf Martens in 1888 long before Richard Stribeck did his pioneering measurements in 1902. However, basic work in this field of experimental hydrodynamics was done and results were published even earlier than that back in 1854 by Gustave A. Hirn, in 1879 by Robert H. Thurston and in 1883 by Beauchamp Tower. KW - Stribeck curve KW - Martens KW - Stribeck KW - Thurston KW - Gümbel KW - Hirn PY - 2010 DO - https://doi.org/10.1016/j.wear.2010.02.015 SN - 0043-1648 VL - 268 IS - 11-12 SP - 1542 EP - 1546 PB - Elsevier CY - Amsterdam AN - OPUS4-21180 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Cruzado, A. A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Urchegui, M.A. A1 - Gómez, X. T1 - Fretting wear of thin steel wires. Part 1: Influence of contact pressure N2 - Different fretting tests of thin steel wires under different conditions (loads, strokes, number of cycles and mean pressures) were performed. The wires used had 0.45 mm in diameter and the material was a cold-drawn eutectoid carbon steel (0.8% C) with a tensile strength over 2800 MPa. The tests were carried out with 90° "crossed cylinders" configuration varying the stroke, normal load and testing time (number of cycles). Afterwards the volumetric wear was obtained using surface profilometry with diamond stylus. With a classical study of the coefficient of wear with respect to the sliding distance, the results show that the wear coefficient increases with normal load and stroke, consequently, for the same sliding distance, the wear produced was higher when the load and/or stroke is increased. In this work, the coefficient of wear is decreasing continuously as the test is running. In order to analyze better the wear behaviour, another method, in which the volumetric wear is compared with respect to the Archard's loading factor, is proposed. As result of this method, two distinctive behaviours were detected; one corresponds to the running-in period with a more aggressive wear behaviour and the second one to the stable steady state period. In all the tests the running-in period was similar with regard to the wear rates but in the stable period the wear rates were increasing with higher loads or strokes. KW - Fretting KW - Wear KW - Wires KW - Contact pressure KW - Unlubricated tests PY - 2010 DO - https://doi.org/10.1016/j.wear.2010.02.017 SN - 0043-1648 VL - 268 IS - 11-12 SP - 1409 EP - 1416 PB - Elsevier CY - Amsterdam AN - OPUS4-21181 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kovalev, Alexander A1 - Hartelt, Manfred A1 - Spaltmann, Dirk A1 - Wäsche, Rolf A1 - Woydt, Mathias T1 - Zero wear (Null Verschleiß) N2 - Während des Gleitreibens auftretende, plastische Deformationen im oberen Bereich der Kontaktspitzen werden als „Null-Verschleiß“ bezeichnet. Um diesen zu quantifizieren, werden in dieser Arbeit statt der üblichen, statistischen Rauheitsparameter die Flächen solcher Kontaktspitzenbefrachtet. Dabei liegen diesen Befrachtungen AFM-Bilder von realen Oberflächentopografien auf der Mikro-/Nanoskala als Ausgangspunkt für die Simulationen zugrunde. In den Simulationen wird berücksichtigt, dass die Flächen während der Gleitreibung in den Kontaktspitzen elastisch und plastisch verformt werden können. Ebenso wird der Effekt des Einsatzhärtens in die Befrachtungen eingeschlossen. Die Ergebnisse der Computersimulation stellen einen Weg zur Untersuchung der Reibkräfte zu Beginn des EinlaufVorgangs dar, insbesondere dann, wenn sich dabei die wahre Kontaktfläche verändert hat. Die Ergebnisse der Simulation belegen klar, dass das Vorliegen von „Null-Verschleiß“ stark von der Veränderung der Oberfläche abhängt und nicht von der Erzeugung von Verschleißpartikel begleitet wird. N2 - Recent developments in contact mechanics and microfribology have shown that it is very important to study surface modification effects for quantification of „Zero wear“ (plastic deformation of upper parts of asperities) during sliding friction. The present work considers experimental and Simulation data on the Formation of elastic and plastic contact areas during sliding friction on rough surfaces. The Simulation of discrete contact was carried out using as a source the AFMimages of real surface topography at micro/nanoscale. The approach for quantification of „zero wear“, proposed here, is not using common Statistical Parameters of roughness, but it considers contact areas on asperities. In these areas some regions are undergoing plastic deformation which influences surface Transformation during sliding friction. Also, the workhardening effect was taken into account in the Simulation of sliding friction. This enabled a rnore successful fit of experimental data. The results obtained of the Computer simulations will provide a way of studying friction force at the initial stage of the running-in process. T2 - 53. Tribologie-Fachtagung - Reibung, Schmierung und Verschleiß CY - Göttingen, Germany DA - 24.09.2012 PY - 2012 SN - 978-3-00-039201-6 VL - II SP - 43/1 EP - 43/13 CY - Aachen AN - OPUS4-26640 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kaltzakorta, O. A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Aginagalde, A. A1 - Tato, W. T1 - Influence of polymer filler on tribological properties of thermoplastic polyurethane under oscillating sliding conditions against cast iron N2 - The tribological behaviour of unfilled thermoplastic polyurethane (TPU) and a polymer sphere filled (TPUG) thermoplastic polyurethane have been studied under oscillating sliding condition against cast iron as a counterpart. In the case of unfilled TPU, the wear mechanisms are dominated by particle detachment and roll formation. In principle, TPUG also showed a similar wear mechanism as that of unfilled TPU; in addition, particle pull-out and delamination are also observed. Wear volume of TPUG was significantly higher than that for the unfilled TPU and this is attributed to the different material removal processes taking place in the material during sliding. The polymer spheres as a filler material deteriorated the wear resistance of TPU because of improper adhesion and bonding of filler in the TPU matrix and therefore it contributed to more wear. In case of TPU the friction behaviour was strongly dependant on the temperature and surface roughness of the counter body. The results showed that below the glass transition temperature higher friction values are observed with higher counter body surface roughness. However, above the glass transition temperature, higher friction values are observed with a smoother surface roughness of the counter body. In case of TPUG, the friction behaviour was not significantly dependent on surface roughness of the counter body. KW - Dry sliding KW - Polymers KW - Cast iron KW - Temperature PY - 2012 DO - https://doi.org/10.1007/s11249-012-0017-6 SN - 1023-8883 SN - 1573-2711 VL - 48 IS - 2 SP - 209 EP - 216 PB - Springer Science Business Media B.V. CY - Dordrecht AN - OPUS4-27272 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Woydt, Mathias T1 - Aiming at zero wear - Where are we right now? T2 - International Conference on Industrial Tribology (ICIT 2012) CY - Pune, India DA - 2012-12-07 PY - 2012 AN - OPUS4-27364 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Scholz, Christian A1 - Wäsche, Rolf ED - Bartz, Wilfried J. T1 - Effect of sliding speed and relative humidity on the tribological behaviour of ceramic and polymer materials T2 - 19th International colloquium Tribology - Industrial and automotive lubrication CY - Stuttgart/Ostfildern, Germany DA - 2014-01-21 KW - Stick slip KW - Polymer KW - Ceramic KW - Sliding speed KW - Relative humidity PY - 2014 SN - 978-3-943563-10-8 SP - Paper 8.11, 1 EP - 6 CY - Stuttgart/Ostfildern AN - OPUS4-30176 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Ehrke, Roman ED - Silva Gomes, J. F. ED - Meguid, S. A. T1 - A study on tribological behaviour of a-C:H coatings under lubricated conditions up to 250°C N2 - The influence of temperature and counterbody material on the tribological properties of a-C:H coatings deposited on Cronidur 30 steel has been investigated in a lubricated ball on disk contact situation with alpha-alumina and silicon nitride as counterbodies. The results show, that the wear volumes of the systems increase exponentially with increasing temperature, for alpha-alumina more than for silicon nitride. Two different wear mechanisms seem to have a major influence: First, the abrasive action due to materials hardness and second, the tribo-oxidation when silicon nitride is counter material. T2 - 6th International Conference on Mechanics and Materials Design CY - P. Delgada/Azores, Portugal DA - 26.07.2015 KW - Diamond like carbon KW - Ceramics KW - Wear KW - Friction KW - Temperature PY - 2015 SP - Paper 5395, 445 EP - 446 AN - OPUS4-37014 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Woydt, Mathias ED - Mang, T. T1 - Stribeck curve N2 - The importance of lubricants in virtually all fields of the engineering industry is reflected by an increasing scientific research of the basic principles. Energy efficiency and material saving are just two core objectives of the employment of high-tech lubricants. The encyclopedia presents a comprehensive overview of the current state of knowledge in the realm of lubrication. All the aspects of fundamental data, underlying concepts and use cases, as well as theoretical research and last but not least terminology are covered in hundreds of essays and definitions, authored by experts in their respective fields, from industry and academic institutes. PY - 2014 SN - 978-3-642-22646-5 SN - 978-3-642-22647-2 DO - https://doi.org/10.1007%2F978-3-642-22647-2 VL - 4 SP - 1998 EP - 2005 PB - Springer CY - Heidelberg AN - OPUS4-30499 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Steinborn, Gabriele T1 - Wear behaviour of low IR-emission titanate ceramics under gross slip fretting conditions against steel and alpha-alumina N2 - The tribological behavior of different low infrared (IR) emission ceramic materials from the titanate group has been investigated at room temperature under gross slip fretting conditions against 100Cr6 ball bearing steel and α-alumina as the counterface materials. For all material pairs, friction and wear depended largely on the relative humidity of the environment. When paired with steel the low IR-emission ceramic disks showed higher wear resistance. Under dry conditions, almost no wear was found on the low IR-emission ceramic specimen. The high wear on the steel counter body is caused not only by tribo-oxidation, which is the main wear mechanism, but also by abrasion. In dry conditions a COF of 0.6 and in humid conditions a COF of 0.2 have been measured. When paired with α-alumina the results on wear are just opposite to those with steel counterbody and the low IR-emission ceramic materials show much lower wear resistance under all conditions. This is explained by the predominance of abrasion and the relatively large difference in hardness between the low IR-emission ceramic and α-alumina. In high humidity environments the results point to the formation of stable reaction layers causing lower friction and wear. KW - Gross slip fretting KW - Ceramic wear KW - Yttrium titanate KW - Zirconium titanate KW - Low IR-emission ceramics PY - 2014 DO - https://doi.org/10.1016/j.wear.2014.03.006 SN - 0043-1648 VL - 315 IS - 1-2 SP - 11 EP - 16 PB - Elsevier B.V. CY - Amsterdam AN - OPUS4-30504 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Cruzado, A. A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Urchegui, M.A. A1 - Gómez, X. T1 - Fretting wear of thin steel wires. Part 2: Influence of crossing angle N2 - The wear behaviour of thin steel wires has been analyzed under oscillating sliding conditions in crossed cylinders contact geometry. The focus of this analysis was the influence of the crossing angle between the wires on the wear. The wires used had 0.45 mm in diameter and the material was cold-drawn eutectoid carbon steel (0.8% C) with a tensile strength higher than 2800 MPa. Two different types of tests were carried out, the first one representing the influence of the crossing angle for a constant load and the second one representing the influence of the crossing angle with constant contact pressure. In the first type of tests it was seen that as the contact angle decreases the contact pressure decreases too and hence less energy specific wear resistance is observed. As a consequence less wear is produced, thus increasing the life of the wires. In the second type of tests it was seen that with constant contact pressure but different crossing angles, nearly the same energy specific wear resistance was observed. This points at an identical wear behaviour in both type of tests but with a running-in and a steady state period as two different wear periods. The tests showed that the running in period may play an important role in the overall wear particle generation and hence the wear occurring in the steady state period is rather mild. KW - Fretting KW - Wires KW - Contact pressure KW - Crossing angle PY - 2011 DO - https://doi.org/10.1016/j.wear.2011.04.012 SN - 0043-1648 VL - 273 IS - 1 SP - 60 EP - 69 PB - Elsevier CY - Amsterdam AN - OPUS4-31762 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Hartelt, Manfred ED - Mang, T. T1 - Fretting N2 - The importance of lubricants in virtually all fields of the engineering industry is reflected by an increasing scientific research of the basic principles. Energy efficiency and material saving are just two core objectives of the employment of high-tech lubricants. The encyclopedia presents a comprehensive overview of the current state of knowledge in the realm of lubrication. All the aspects of fundamental data, underlying concepts and use cases, as well as theoretical research and last but not least terminology are covered in hundreds of essays and definitions, authored by experts in their respective fields, from industry and academic institutes. KW - Fretting corrosion KW - Fretting fatigue KW - Fretting regimes KW - Fretting wear KW - Mixed fretting regime PY - 2014 SN - 978-3-642-22646-5 SN - 978-3-642-22647-2 DO - https://doi.org/10.1007/978-3-642-22647-2 VL - 2 SP - 680 EP - 687 PB - Springer CY - Heidelberg AN - OPUS4-30497 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Hodoroaba, Vasile-Dan T1 - Verschleißpartikel-Analyse mit Rasterelektronenmikroskopie und energiedispersiver Röntgenspektrometrie im Transmissionsmodus (TSEM/EDX) N2 - Untersucht wurden Verschleißpartikel als elektronen-transparente Proben auf dünnen Trägerfolien mit einem hochauflösendem Rasterelektronenmikroskop und energiedispersiver Röntgenspektrometrie im Transmissionsmodus. Die hohe laterale Auflösung dieser modernen Methoden ermöglicht eine morphologische Charakterisierung der Verschleißpartikel bis in den nm-Bereich. Die hochauflösende Elementanalyse erlaubt eine Interpretation der Zusammensetzung und damit Rückschlüsse auf die Verschleißpartikelbildung. Die tribologischen Untersuchungen sind an einem Modell-Verschleißtribometer nach DIN 51834-2 geschmiert, aber ohne Ölkreislauf, durchgeführt worden. Die Präparation der Verschleißpartikel über eine Entnahme und Übertragung einer geringen Schmierstoffmenge mit einer Mikropipette auf eine TEM-Trägerfolie ist mit einem geringen Aufwand möglich. Der präparative Aufwand ist relativ gering. Das benötigte Schmierstoffvolumen beträgt wenige Mikroliter (0,001ml). Die Untersuchung zeigt die geringe geometrische Größe der Verschleißpartikel und bestätigt indirekt die These der Reaktionsschichtbildung mit einer geringen Schichtdicke, die ständig verschleißt und sich stetig neu bildet. Die beschriebenen Verschleißprozesse sind in der Modell-Verschleiß-Prüfung mit sehr hohen Pressungen am Versuchsbeginn nachweisbar. T2 - 55. Tribologie-Fachtagung - Reibung, Schmierung und Verschleiß - Forschung und praktische Anwendungen CY - Göttingen, Germany DA - 22.09.2014 PY - 2014 SN - 978-3-00-046545-1 VL - I SP - 05/1 EP - 05/10 AN - OPUS4-31528 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tamura, T. A1 - Nakase, Takuya A1 - Hosohata, S. A1 - Kato, S. A1 - Woydt, Mathias A1 - Wäsche, Rolf A1 - Köhler, Norbert T1 - Zero wear and low friction under dry sliding N2 - In diesem Beitrag werden ungeschmierte Gleitpaarungen auf Basis von Oxidkeramik/DLC vorgestellt, bei denen die tribologischen Kenngrößen mehr oder weniger invariant von der Gleitgeschwindigkeit sind. Die DLC-Dünnschicht besteht aus einem bestimmten Verhältnis an sp2/sp3-hybridisiertem Kohlenstoff. Im Gegensatz zu artgleichen Gleitpaarungen aus MgO-.Zr02, AI2O3 oder SSiC mit Reibungszahlen oberhalb von 0,45, zeigt die Gleitpaarungen aus MgO-Zr02/DLC und alpha-A^OVDLC Festkörpergleitreibungszahlen zwischen 0,075 und 0,15, welche mit ansteigender Gleitgeschwindigkeit leicht abnahmen. Die Verschleißkoeffizienten der DLC-Dünnschichten lagen im Bereich von kleiner als 10~7 mm3/Nm bis herunter zu 10"9 mm3/Nm. N2 - This paper presents a dry sliding tribo-couple (DLC/monolithic oxide ceramics), where the tribological quantities are more or less in a wide ränge independent of the sliding speed. The DLC film is composed of a specific mixture of sp3 /sp2 hybridized carbon. Self-mated ceramic/ceramic couples of MgO-Zr02, alpha-AI203 or SSiC are with their coefficients of friction above 0.45 not so lubricious, whereas the coefficients of friction of the tribocouples MgO-Zr02/DLC and alpha-AbOVDLC ranged between 0.075 and 0.15 under dry sliding. The coefficients of friction for these tribo-couples tend to decrease with increase sliding speed from 0.03 m/s to 6 m/s. The dry wear rates of the thin film is low (<10‘7 mm3/Nm) and perfectly independent from sliding velocity. T2 - 55. Tribologie-Fachtagung - Reibung, Schmierung und Verschleiß - Forschung und praktische Anwendungen CY - Göttingen, Germany DA - 22.09.2014 PY - 2014 SN - 978-3-00-046545-1 VL - II SP - 43/1 EP - 43/7 AN - OPUS4-31581 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hartelt, Manfred T1 - Wear testing with crossed cylinders - comparison of methods N2 - Three different contact geometries, ball on disk and two different settings with crossed cylinders have been investigated with regard to the agreement of the results of the tribological quantities determined by each method. The material combination was α-alumina as upper specimen and steel 100Cr6 as lower specimen. For each of the contact geometries 5 independent measurements were carried out and evaluated independently. The agreement between the single results of coefficient of friction and the coefficient of system wear as well as between the different groups and conditions are good. Largest scatter of the results were found in the dry air regime where both friction and wear depend strongly on the relative humidity. However, comparison of the absolute values of the coefficient of wear between the ball on disk contact geometry on one side and the 2 crossed cylinder contact geometries on the other side reveals a significant difference in that the ball on disk results are lower by about a factor of two. The results document also a high degree of repeatability of single wear tests. T2 - 16th International colloquium tribology - Lubricants, materials and lubrication engineering CY - Stuttgart/Ostfildern, Germany DA - 2008-01-15 KW - Fretting KW - Contact geometry crossed cylinders KW - Friction KW - Wear PY - 2008 SP - Paper 10_04_Wäsche, 1 EP - 6 AN - OPUS4-31602 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Scholz, Christian A1 - Wäsche, Rolf ED - Bartz, Wilfried J. T1 - Effect of sliding speed and relative humidity on the tribological behavior of ceramic and polymer materials T2 - 19th International colloquium Tribology - Industrial and automotive lubrication CY - Stuttgart/Ostfildern, Germany DA - 2014-01-21 PY - 2014 SN - 978-3-943563-10-8 SP - Paper 08_11_Scholz_Man, 1 EP - 6 CY - Stuttgart/Ostfildern AN - OPUS4-31743 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Gräber, H.-G. A1 - Klaffke, Dieter T1 - Experimentelle Untersuchungen zum Abriebverhalten von keramischen Werkstoffen für dentale Restaurationen T2 - 47. Tribologie-Fachtagung - Reibung, Schmierung und Verschleiß - Forschung und praktische Anwendungen CY - Göttingen, Germany DA - 2006-09-25 KW - Dentalkeramik KW - Bearbeitbarkeit KW - Abriebverhalten PY - 2006 SN - 3-00-019670-6 VL - I SP - 36/1 EP - 36/9 CY - Aachen AN - OPUS4-31751 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Zabler, S. A1 - Nelson, K. T1 - Wear analysis on dental implant materials under partial slip conditions T2 - VII Iberian Conference on Tribology (IBERTRIB 2013) CY - Oporto, Portugal DA - 2013-06-20 PY - 2013 AN - OPUS4-31051 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Wötting, G. T1 - Tribological behaviour of structural Si-based ceramics in fretting tests at room temperature N2 - The friction and wear behaviour of SiC, Si3N4 and SiC/Si3N4 composite ceramics were investigated with oscillating sliding (gross slip fretting) at room temperature. The influence of counter body material and the humidity of the surrounding air was studied with a ball-on-disc configuration with different ball materials (1000Cr6, Al2O3 SiC and Si3N4). The effect of RH on friction is marginal with exception of SiC (low friction) as counter body material. The wear behaviour, however, is strongly affected by humidity, showing inverse trends for different counter body materials. Consequently, the wear behaviour of a tribo couple can be improved by selecting an adequate mating material. The results reveal the necessity to control RH in tribological tests. For estimation of the performance of tribo couples under varying environmental conditions, a variation of RH is required. In tribo couples with single phase SiC, either as ball or disc, the tribological behaviour of the system is dominated by SiC. The friction behaviour of the composite material is in between the behaviour of the two single phase materials, Si3N4 and SiC, whereas the wear behaviour is very similar to that of single phase Si3N4. KW - Silicon carbide KW - Silicon nitride KW - Particulate composite KW - Fretting KW - Humidity KW - Mating material PY - 2009 DO - https://doi.org/10.1007/s11249-009-9413-y SN - 1023-8883 SN - 1573-2711 VL - 33 IS - 3 SP - 211 EP - 219 PB - Springer Science Business Media B.V. CY - Dordrecht AN - OPUS4-19000 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Paulick, Carl A1 - Steinborn, Gabriele A1 - Richter, V. A1 - Werner, M. T1 - Joining of ceramic components in the green state via LPIM N2 - It has been successfully demonstrated that ceramic materials can be joined in the green state without a second phase by using low pressure injection molded parts. The investigation of the joining interface revealed that a high quality interface can be achieved by carefully adjusting the different manufacturing steps. The use of monomodal particle size distribution in the used powder CT3000SG is inferior to a broader particle size distribution obtained by replacing 33% of the finer alumina powder by coarser CT1200SG. In this way the dewaxing process is significantly improved when the wall thickness of the part exceeds 3 mm. The investigation of the mechanical properties of the joined and sintered parts revealed, that the bending strength of the joined specimens achieved about 80 % of the unjoined, monolithic specimens. T2 - 4th International Conference on Advanced Materials and Processing CY - Hamilton, New Zealand DA - 2006-12-10 KW - Joining KW - Ceramics KW - Green state KW - Interface KW - Bending strength KW - Low pressure injection molding PY - 2005 UR - http://www.scientific.net/3-908453-89-5/207/ SN - 1022-6680 SN - 1662-8985 VL - 29-30 SP - 207 EP - 210 PB - Trans Tech Publ. CY - Zurich AN - OPUS4-19001 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Woydt, Mathias T1 - Analysis of oxidative processes in SiC-TiC-TiB2 ceramic composites during tribological loading T2 - Tribochemistry 2009 CY - Kyoto, Japan DA - 2009-09-02 PY - 2009 AN - OPUS4-22870 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Woydt, Mathias A1 - Rehmer, Birgit T1 - Characterisation of tribological interface in low wear magneli type ceramics T2 - International Conference on Characterisation and Control of Interfaces (ICCC 2009) CY - Kurashiki, Japan DA - 2009-09-06 PY - 2009 AN - OPUS4-22871 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Springborn, U. A1 - Keunike, M. A1 - Bewilogua, K. T1 - Extended tribological study on carbon nitride coatings under oscillating sliding conditions T2 - World Tribology Congress (WTC) CY - Kyoto, Japan DA - 2009-09-09 PY - 2009 AN - OPUS4-22872 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Gräber, H.-G. T1 - Experimental study on wear of dental ceramic materials - tests in artificial saliva T2 - 17. International Colloquium on Tribology CY - Filderstadt, Germany DA - 2010-01-19 PY - 2010 AN - OPUS4-22873 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Urchegui, M.A. A1 - Cruzado, A. A1 - Hartelt, Manfred A1 - Gomez, X. T1 - Wear of thin steel wires T2 - Nordtrib 2010 CY - Luleå, Sweden DA - 2010-06-08 PY - 2010 AN - OPUS4-22874 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Woydt, Mathias A1 - Yarim, Rasim T1 - Wear of SiC-TiC-TiB2 ceramics at high temperatures and sliding speeds in air T2 - Asiatrib 2010 CY - Perth, Australia DA - 2010-12-05 PY - 2010 AN - OPUS4-22875 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Springborn, U. A1 - Hartelt, Manfred A1 - Bewilogua, K. A1 - Keunecke, M. T1 - Influence of deposition parameters on tribological properties of CNx coatings T2 - WOM, 17th International Conference on Wear of Materials CY - Las Vegas, NV, USA DA - 2009-04-19 PY - 2009 AN - OPUS4-19364 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Weihnacht, V. T1 - Influence of counterbody material on wear of ta-C coatings under fretting conditions at elevated temperatures N2 - The high temperature tribological performance of tetrahedral amorphous carbon coatings has been analyzed at elevated temperatures up to 250 °C in air against three different counterbody materials-steel 100Cr6, a-alumina and silicon nitride. The results show that the counterbody material influences the friction and wear behavior and therefore coating life time strongly. This effect is well known for these coatings at room temperature under dry environmental conditions, equivalent to conditions above 100 °C when water molecules desorb from the surface. However, the sharp difference in tribological performance between silicon nitride on the one hand and alumina and steel on the other hand cannot be understood in this context. Analyzing the friction behavior during the running-in phase, it is evident that only alumina and steel form a stable interface with constant low friction and relatively low wear rates. Silicon nitride forms an unstable interface with fluctuating COF and relatively high wear rates due to its own inherent tendency to tribo-oxidation. KW - Fretting KW - Hard carbon coatings KW - ta-C KW - High temperature KW - Counterbody influence PY - 2009 DO - https://doi.org/10.1016/j.wear.2009.08.041 SN - 0043-1648 VL - 267 IS - 12 SP - 2208 EP - 2215 PB - Elsevier CY - Amsterdam AN - OPUS4-20344 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Gräber, H.G. T1 - Experimental study on wear of dental ceramic materials - tests in artificial saliva T2 - 17th International colloquium tribology - Solving friction and wear problems CY - Stuttgart/Ostfildern, Germany DA - 2010-01-19 KW - Fretting KW - Life science KW - Wear KW - Dental materials PY - 2010 SN - 3-924813-80-9 IS - Special aspects of tribology SP - 1 EP - 7 AN - OPUS4-21070 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kloß, Heinz A1 - Wäsche, Rolf T1 - Analytical approach for wear prediction of metallic and ceramic materials in tribological applications N2 - Wear mechanisms, as adhesion, abrasion, fatigue and tribochemical wear, are complex in their physical and chemical nature. A theoretical description and prediction of wear are in most cases still far from reality. It is, therefore, important to use test rigs before a practical application of a given material combination under tribological loading. On the other hand, model equations can be helpful for wear description, if a single wear mechanism is dominant. Under oscillating and continuous sliding contact conditions, equations for wear calculation are presented to describe running-in and stationary wear behaviour of metals and ceramics. By using shear energy density, real area of contact, flash temperature, activation energy and numerical simulations with the method of movable cellular automata (MCA), wear data were calculated and compared to experimental laboratory results. KW - Wear KW - Surface temperature KW - Activation energy KW - Simulation KW - Movable cellular automata (MCA) PY - 2009 DO - https://doi.org/10.1016/j.wear.2008.04.034 SN - 0043-1648 VL - 266 IS - 3-4 SP - 476 EP - 481 PB - Elsevier CY - Amsterdam AN - OPUS4-18651 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Hartelt, Manfred A1 - Wäsche, Rolf T1 - Volumetrische Verschleiß-Berechnung an gekrümmten Kontaktgeometrien T2 - 50. Tribologie-Fachtagung - Reibung, Schmierung und Verschleiß - Forschung und praktische Anwendung CY - Göttingen, Deutschland DA - 2009-09-21 KW - Verschleißberechnung KW - Calculation of wear volume PY - 2009 SN - 978-3-00-028824-1 VL - I SP - 3-1 - 3-9 CY - Aachen AN - OPUS4-20023 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Springborn, U. A1 - Bewilogua, K. A1 - Keunecke, M. T1 - Wear of carbon nitride coatings under oscillating sliding conditions N2 - An extended study on tribological properties of carbon nitride coatings under oscillating sliding conditions has been carried out. The coatings were prepared by reactive magnetron sputtering with graphite target using nitrogen as reactive gas in an argon/nitrogen atmosphere during the deposition process to deposit carbon nitride, CNx. Coating thickness was about 2 µm. A 200–300 nm thick Ti interlayer was used to enhance adhesion. The nitrogen flow during the deposition was varied to control the amount of nitrogen in the coating. Maximum amount of N-content was about 28 at%, achieved at a maximum N2 flow rate. Other deposition parameters were target to substrate distance, substrate temperature during deposition and bias voltage. The results show a large variation of hardness depending mainly on the nitrogen content and bias voltage. Higher bias voltage produced harder coatings as did lower nitrogen content. The tribological properties were tested unlubricated and lubricated by paraffin oil under gross slip fretting conditions at room temperature against alumina as counter material. Most coatings, but not all, showed a more or less pronounced dependence of wear on relative humidity with wear rates from 10-5 to 10-6 mm3/Nm. The best coatings with regard to a low wear rate and the least dependence upon relative humidity were carbon nitride coatings deposited at elevated substrate temperatures up to 350 °C. The wear resistance of these coatings was increased under the most severe conditions by about one order of magnitude. The results are discussed on the basis of a transfer layer formation. The results show clearly that wear is not significantly correlated to the coating hardness which itself is strongly dependant on the nitrogen content. However, under lubricated conditions with paraffin oil, wear rates were generally very low with wear coefficients at about 10-8 mm3/Nm. KW - Carbon nitride KW - Wear KW - Fretting KW - Dry sliding KW - Paraffin oil PY - 2010 DO - https://doi.org/10.1016/j.wear.2010.08.010 SN - 0043-1648 VL - 269 IS - 11-12 SP - 816 EP - 825 PB - Elsevier CY - Amsterdam AN - OPUS4-22208 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Hodoroaba, Vasile-Dan T1 - Analysing wear particles on the nano scale N2 - A novel method for preparation and chracterisation of nano scale wear particles by means of TSEM was presented. The tribological tests were carried out in a lubricated system at a temperature of 80°C. T2 - The 17th Nordic Symposium on Tribology - NORDTRIB 2016 CY - Hämeenlinna, Finland DA - 14.06.2016 KW - Nano scale KW - Wear particles KW - Tribology KW - Steel KW - SEM PY - 2016 AN - OPUS4-38209 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Harsha, A. P. A1 - Wäsche, Rolf T1 - Tribological studies on polyetherimide composites sliding against steel under reciprocating conditions N2 - The friction and wear properties of polyetherimide composites under dry oscillating sliding condition at room temperature (RT) as well as at elevated temperature (120 °C) was investigated. The polymer specimens were made to oscillate against steel cylinder as a counterpart. The friction and wear properties of PEI and composites were strongly influenced by the temperature. In case of carbon fiber composite abrasive action of carbon fibers has severely damaged the counterpart and resulted in accelerated wear of the composite at RT. Solid lubricants filled (PTFE, MoS2, graphite) along with glass fiber is beneficial in improving the friction and wear performance of the PEI composite at RT, whereas at elevated temperature wear performance was deteriorated. T2 - 2nd International Conference on Polymer Tribology CY - Ljubljana, Slovenia DA - 15.09.2016 KW - Polyetherimide KW - Composites KW - Friction KW - Wear KW - Temperature KW - Oscillating sliding KW - Solid lubricant KW - Fibers PY - 2016 AN - OPUS4-38135 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Ehrke, Roman T1 - A study of tribological behaviour of a-C:H coatings under lubricated conditions up to 250°C T2 - 6. International Conference on Mechanics and Materials in Design CY - P. Delgada/Azores, Portugal DA - 2015-07-26 PY - 2015 AN - OPUS4-33761 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Pfeffer, D. A1 - Scholz, Christian A1 - Belly, C. A1 - Wäsche, Rolf A1 - Schlaak, H.F. A1 - Pott, P.P. T1 - Influence of the actuation waveform on the performance of piezoelectric stick-slip actuators N2 - Performance and efficiency of piezo-electric stick-slip actuators are dependent on the waveform of the electrical actuation of the piezo-stack. This paper compares between a conventional saw-tooth actuation with two waveforms that feature softer acceleration in order to minimize the duration of the slip-phase. It is shown that the proposed waveforms increase both maximum mechanical output power (by 43%) and overall efficiency (by 25%) of the examined actuator. T2 - IKMT 2015 - Innovative Klein- und Mikroantriebstechnik CY - Köln, Germany DA - 14.09.2015 PY - 2015 SN - 978-3-8007-4072-7 N1 - Serientitel: ETG-Fachbericht – Series title: ETG-Fachbericht VL - 146 SP - 100 EP - 104 AN - OPUS4-34883 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Harsha, A.P. A1 - Wäsche, Rolf A1 - Hartelt, Manfred T1 - Friction and wear studies of polyetherimide composites under oscillating sliding condition against steel cylinder N2 - Tribological properties of neat polyetherimide (PEI), glass, carbon fiber, and solid lubricants filled PEI composites are presented in this article. The aim of this study was to investigate the friction and wear properties of these composites under dry oscillating sliding condition at room temperature (RT) as well as at elevated temperature (120 °C). The polymer specimens were made to oscillate against steel cylinder as a counterpart. The friction and wear properties of PEI and composites were strongly influenced by the temperature. Incorporation of carbon fiber in the PEI matrix has increased the wear rate at RT, while at elevated temperature this trend was opposite. Abrasive action of carbon fibers has severely damaged the counterpart and resulted in accelerated wear of the composite at RT. Solid lubricants filled (PTFE, MoS2, graphite) along with glass fiber is beneficial in improving the friction and wear performance of the PEI composite at RT, whereas at elevated temperature wear performance was deteriorated. Tribological performance of neat PEI and glass fiber composite was similar with each other at RT. Scanning electron micrographs and optical micrographs of the worn polymer specimens and the steel cylinders was used to study the possible wear mechanisms. The present test results were also compared with data available on the reciprocating wear of PEI and composites in the literature and trends have been reported. PY - 2015 DO - https://doi.org/10.1002/pc.23559 SN - 0272-8397 SN - 1548-0569 VL - 38 IS - 1 SP - 48 EP - 60 PB - Society of Plastics Engineers CY - Manchester, NH AN - OPUS4-34921 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Hodoroaba, Vasile-Dan T1 - A study on wear particle analysis in lubricated steel-steel contacts T2 - International Tribology Congress/ITC 2015 CY - Tokyo, Japan DA - 2015-09-15 PY - 2015 AN - OPUS4-34324 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hartelt, Manfred T1 - Ceramics and DLC - influence of tribochemistry on sliding under lubricated conditions at elevated temperatures T2 - Satelite Symposium on Tribochemistry CY - Nikko, Japan DA - 2015-09-13 PY - 2015 AN - OPUS4-34325 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Hodoroaba, Vasile-Dan T1 - Verschleißpartikel-Analyse mit Rasterelektronenmikroskopie und energiedispersiver Röntgenspektrometrie im Transmissionsmodus (TSEM/EDX) N2 - Untersucht wurden Verschleißpartikel als elektronentransparente Proben auf dünnen Trägerfolien mit einem hochauflösendem Rasterelektronenmikroskop und energiedispersiver Röntgenspektrometrie im Transmissionsmodus. Die hohe laterale Auflösung dieser modernen Methoden ermöglicht eine morphologische Charakterisierung der Verschleißpartikel bis in den nm-Bereich. Die hochauflösende Elementanalyse erlaubt eine Interpretation der Zusammensetzung und damit Rückschlüsse auf die Verschleißpartikelbildung. Die tribologischen Untersuchungen sind an einem Modell-Verschleißtribometer nach DIN 51834-2 geschmiert, aber ohne Ölkreislauf, durchgeführt worden. Die Präparation der Verschleißpartikel über eine Entnahme und Übertragung einer geringen Schmierstoffmenge mit einer Mikropipette auf eine TEM-Trägerfolie ist mit einem geringen Aufwand möglich. Der präparative Aufwand ist relativ gering. Das benötigte Schmierstoffvolumen beträgt wenige Mikroliter (0,001 ml). Die Untersuchung zeigt die geringe geometrische Größe der Verschleißpartikel und bestätigt indirekt die These der Reaktionsschichtbildung mit einer geringen Schichtdicke, die ständig verschleißt und sich stetig neu bildet. Die beschriebenen Verschleißprozesse sind in der Modell-Verschleiß-Prüfung mit sehr hohen Pressungen am Versuchsbeginn nachweisbar. KW - Modellverschleißprüfung KW - Verschleißpartikel-Analyse KW - TSEM PY - 2015 SN - 0724-3472 VL - 62 IS - 6 SP - 5 EP - 11 PB - Expert Verlag CY - Renningen AN - OPUS4-35043 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Ehrke, Roman ED - Silva Gomes, J.F. ED - Meguid, S.A. T1 - A study on tribological behaviour of a-C:H coatings under lubricated conditions up to 250 °C N2 - The influence of temperature and counterbody material on the tribological properties of a-C:H coatings deposited on Cronidur 30 steel has been investigated in a lubricated ball on disk contact situation. The results show, that the wear volumes of the system increase exponentially with increasing temperature. Two different wear mechanisms seem to have a major influence: First, the abrasive action due to materials hardness and second, the tribooxidation when silicon nitride is counter material. T2 - M2D2015 - 6th International conference on mechanics and materials in design CY - Ponta Delgada, Azores DA - 26.07.2015 KW - Diamond like carbon KW - Ceramics KW - Wear KW - Friction KW - Temperature PY - 2015 SN - 978-989-98832-3-9 SP - 445 EP - 446 AN - OPUS4-33808 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Harsha, A. P. T1 - Tribological studies on polyetherimide composites sliding against steel under reciprocating conditions N2 - Results of tribological tests on polyetherimide composites were presented. The tests were carried out at room temperature as well as at 120°C. Counter body was steel 100Cr6. T2 - PolyTrib 2016. 2nd International Conference on Polymer Tribology CY - Ljubljana, Slovenia DA - 15.09.2016 KW - PEI KW - Composites KW - Polyetherimide KW - Temperature KW - Steel PY - 2016 AN - OPUS4-38690 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Woydt, Mathias T1 - Tribological characterization of niobium carbide with different binder materials N2 - Wear of Niobium carbide with nickel binder has been experimentally characterized under dry, oscillating sliding conditions against steel and a-alumina up to 600°C. T2 - National Tribology Conference/NTC-2016 CY - Varanasi, India DA - 08.12.2016 KW - Niobium carbide KW - Wear resistance KW - Binder PY - 2016 SP - 1 EP - 2 AN - OPUS4-38879 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Woydt, Mathias A1 - Wäsche, Rolf A1 - Brandt, Guido A1 - Ehrke, Roman A1 - Yano, S. A1 - Sasaki, S. T1 - Tribology in hot steam for energy recovery N2 - The wear rates of self-mated alumina couples show that friction as well as wear is largely determined by the above-mentioned hydro-thermal conditions. The presence of water and its amount available in the surrounding system either in liquid or in gaseous form plays a key role for friction and wear behavior and can be beneficial for the tribological profile of steam degradation resistant materials. Hot steam enhances the tribo-chemical formations of oxides and hydroxides on MgO-ZrO2 alumina and antimony impregnated carbon. T2 - 21th International Colloquium Tribology CY - Stuttgart/Ostfildern, Germany DA - 09.01.2018 KW - Tribology KW - Friction KW - Alumina KW - Hot steam PY - 2018 SP - 1 EP - 2 AN - OPUS4-43896 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Brandt, Guido A1 - Ehrke, Roman A1 - Nolze, Gert A1 - Schmid, Thomas A1 - Sasaki, S. A1 - Woydt, Mathias T1 - Wear behaviour of alpha-alumina in hot steam at high contact pressure N2 - The work examines the wear behaviour of α-aluminium oxide by combining thermodynamic modelling with advanced wear testing as well as analytical methods to get a better understanding of this structural ceramic material wear behavior and its possible use in high temperature steam environment. KW - Aluminium oxide KW - Temperature KW - Hot steam KW - Diaspore KW - Ceramic KW - Wear PY - 2018 DO - https://doi.org/10.1016/j.wear.2018.02.012 SN - 0043-1648 SN - 1873-2577 VL - 404-405 SP - 22 EP - 30 PB - Elsevier B.V. AN - OPUS4-44449 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Salge, T. A1 - Wäsche, Rolf A1 - Hodoroaba, Vasile-Dan T1 - Advanced light element and low energy X-ray analysis of a TiB2 – TiC – SiC ceramic material using EDS spectrum imaging N2 - The accurate EDS microanalysis of light elements such as boron and carbon by spectrum imaging will be demonstrated using a sintered hard ceramic material composed of the three major phases titanium boride (TiB2), titanium carbide (TiC), silicon carbide (SiC) and minor phases, sub-μm in size. The combination of these three materials leads to improved mechanical and tribological properties. Silicon carbide is a material used for mechanical seals. It has the disadvantage of reduced failsafe running functions, causing increased wear when running dry. The added titanium components (TiC and TiB2) improve the failsafe running functions. This technology has already been transferred to industrial applications. KW - EDS KW - Spectrum imaging KW - Ceramic KW - Phase analysis KW - Light elements PY - 2018 UR - https://www.bruker.com/fileadmin/user_upload/8-PDF-Docs/X-rayDiffraction_ElementalAnalysis/Microanalysis_EBSD/LabReports/App_eds_10_LE_keramik_Rev1_1_lores.pdf SP - 1 EP - 5 CY - Berlin AN - OPUS4-44622 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Rawat, S. S. A1 - Harsha, A. P. A1 - Khatri, O. P. A1 - Wäsche, Rolf T1 - Pristine, reduced, and alkylated graphene oxide as additives to paraffin grease for enhancement of tribological properties N2 - Pristine, reduced, and alkylated graphene oxides are applied as lubricating additives in paraffin grease. It has revealed that their crystalline structure governs the tribological properties of grease for steel tribo-pair. The microstructural analyses of grease samples showed that a loose fiber network of soap in the presence of graphene-based additive allows their facile release for efficient lubrication. The surface analyses based on the microscopic and elemental mapping show the development of a graphene-derived protective film on the worn scars, which protected the tribo-surfaces and subsided the wear. The reduced graphene oxide (rGO) with the interlamellar distance of 0.35 nm in the (002) plane provided minimum resistance to shear and exhibited maximum reduction in coefficient of friction (COF) for the paraffin grease. The presence of oxygen functionalities in the basal of pristine and alkylated graphene oxide (GO) compromised the interlamellar shearing under tribo-stress; consequently, higher COF than that of rGO. KW - Coefficient of friction KW - Graphene oxide KW - Grease KW - Nanoadditive KW - Tribo-film KW - Wear KW - Boundary lubrication KW - Grease lubrication KW - Lubricant additives KW - Lubricants PY - 2021 DO - https://doi.org/10.1115/1.4047952 VL - 143 IS - 2 SP - 021903-1 EP - 021903-11 PB - ASME AN - OPUS4-51170 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Rabe, Torsten A1 - Wäsche, Rolf T1 - Sintering behaviour of nanocrystalline titanium nitride powders N2 - The sintering behaviour of one microcrystalline and several nanocrystalline TiN powders was investigated by means of a gas pressure furnace with an integrated dilatometer. The investigated nanocrystalline powders strongly differ in the sintering activity. It can be concluded from the experiments, that small grain size, narrow grain size distribution and a low oxygen content are the most important prerequisites for high sintering activity of the nanocrystalline TiN powders. The extraordinary sintering activity of the best TiN powder makes it possible to produce a dense (< 2 % porosity), pure (no sintering aids) and nanostructured (mean diameter of crystals about 100 nm) TiN bodies. PY - 1995 SN - 0965-9773 VL - 6 IS - 1-4 SP - 357 EP - 360 PB - Pergamon Press CY - New York, NY AN - OPUS4-32975 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Rabe, Torsten A1 - Prümmer, R. A1 - Wäsche, Rolf T1 - Explosive compaction of nanosized TiN-powders KW - Explosive compaction KW - Nanocrystalline powder KW - Shaping methods KW - Sintering KW - Titanium nitride PY - 1997 DO - https://doi.org/10.4028/www.scientific.net/MSF.235-238.285 SN - 0255-5476 VL - 235-238 SP - 285 EP - 290 PB - Trans Tech Publications CY - Aedermannsdorf, Switzerland AN - OPUS4-32976 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Yarim, Rasim A1 - Klaffke, Dieter A1 - Hartelt, Manfred T1 - Oscillating sliding wear behaviour of SiC, TiC, TiB2, 59SiC-41TiB2 and 52SiC-24TiC-24TiB2 materials up to 750°C in air N2 - The tribological behaviour of different monolithic and composite ceramics was evaluated in the temperature range between room temperature and 750°C. The test method was oscillating sliding with a ball-on-disk arrangement in an SRV machine. Alumina balls were used as counter body. The friction behaviour was determined on-line, and the wear behaviour was determined from calculations on the basis of wear scar dimensions and profilometric measurements. The friction depends on temperature and shows an increase for most materials for increasing temperature; the smallest friction at all temperatures is found for monolithic TiC. The wear behaviour shows different trends for the different materials. In tests against SiC a maximum of wear is found at 500°C, for TiC at 200°C and for TiB2 at 750°C. The composite ceramics suffer the smallest wear of all materials in the range from 200°C to 500°C. PY - 2006 DO - https://doi.org/10.1002/tt.8 SN - 1354-4063 SN - 1557-685X VL - 12 SP - 99 EP - 111 PB - Coppin CY - Deal AN - OPUS4-32977 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kimmari, E. A1 - Podgursky, V. A1 - Simunin, M. A1 - Adoberg, E. A1 - Surzenkov, A. A1 - Viljus, M. A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Sildos, I. A1 - Kulu, P. T1 - Tribological behavior of carbon nanofibers deposited on hard nanocomposite (nc-Ti1 - xAlxN)/(a-Si3N4) coating N2 - Main focus was on the deposition of carbon nanofibers (CNFs) onto the hard nanocomposite (nc-Ti1 - xAlxN)/(a-Si3N4) (nACo®) coating surface and the investigation of the structure and tribological properties of CNFs. The alcohol chemical vapor deposition (ACCVD) method was employed to prepare CNFs and the deposition temperatures were 600 and 700 °C, respectively. Prior to the CNF deposition, Ni catalyst was deposited onto the nACo® surface using the magnetron sputtering. The influence of the deposition temperature on the carbon nanofibers structure was investigated by Raman spectroscopy and scanning electron microscopy (SEM). The higher order degree of CNF structure is observed with increasing deposition temperature. Tribological tests were carried out under fretting contact conditions against Al2O3 ball. It is shown that the coefficient of friction (COF) decreases from 1.0 to 1.2 for the clean nACo® surface to 0.2–0.4 for the CNF layers deposited on the nACo® surface. The roughness of the nACo® surface was varied and a higher durability of the CNF layers deposited on the rougher nACo® surface is found. KW - Carbon nanofiber KW - Coating KW - Fretting KW - Roughness KW - Solid lubrication PY - 2013 DO - https://doi.org/10.1016/j.surfcoat.2013.03.011 SN - 0257-8972 VL - 225 SP - 21 EP - 25 PB - Elsevier Science CY - Lausanne AN - OPUS4-32978 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Pfeffer, D. A1 - Scholz, Christian A1 - Belly, C. A1 - Wäsche, Rolf A1 - Schlaak, H.F. A1 - Pott, P.P. T1 - Modular test bed for performance assessment of piezoelectric stick-slip actuators N2 - Stepping piezoelectric actuators based on the stick-slip effect inherently make use of a friction contact between strator and rotor. This contact defines not only the actuator's performance but also is prone to wear and tear. For broad use, the actuator has to be able to perform around 1 million strokes. To assess the actuator's performance in terms of force, speed, mechanical output, electrical input, and long-term stability under different load- and environmental conditions, as well as different friction partners, a dedicated test-bed for a LSPA30µXS motor by Cedrat Technologies has been set up. T2 - Actuator 2014 - 14th International conference on new actuators & 8th International exhibition on smart actuators and drive systems CY - Bremen, Germany DA - 2014-06-23 KW - Piezoelectric actuator KW - Test bed KW - Stick-slip KW - Performance test KW - Micro positioning PY - 2014 SN - 978-3-933339-22-5 SN - 978-3-933339-23-2 SP - P 50, 617 EP - 620 AN - OPUS4-33498 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Hodoroaba, Vasile-Dan T1 - Analysis of nanoscale wear particles from lubricated steel-steel contacts N2 - A new method for sampling wear particles directly from the lubricant reservoir has been developed and applied successfully for analyzing wear particles by high-resolution scanning electron microscopy in transmission mode having coupled energy-dispersive X-ray spectroscopy. The lubricated tribological testing was carried out with fully formulated as well as with non-formulated synthetic base oil. It was possible to analyze individual particles with dimensions as small as about 5–30 nm which are likely the 'primary' wear particles. A majority of the particles, however, are agglomerated and, thus, lead to the formation of larger agglomerates of up to a few micrometers. Chemical analysis led to the conclusion that most of the observed particles generated in formulated oil, especially the larger ones, are composed of the additives of the lubricant oil. In non-formulated base oil, the primary particles are of similar dimensions but contain only iron, chromium and oxygen, but most likely stem from the mating materials. This finding points to the fact that the main wear mechanism under lubricated conditions with fully formulated oil is more like a continuous shearing process rather than a catastrophic failure with the generation of larger primary particles. When the oil is non-formulated, however, several wear mechanisms act simultaneously and the wear rate is increased significantly. Generated larger primary particles are milled down to the nanoscale. When the oil is fully formulated, wear mainly takes places at the additive layer or tribofilm; thus, the steel surface is protected. KW - Particle KW - Wear particle analysis KW - Lubricated contact KW - Bearing steel KW - Nanoscale T-SEM KW - Nanoscale EDX analysis PY - 2015 DO - https://doi.org/10.1007/s11249-015-0534-1 SN - 1023-8883 SN - 1573-2711 VL - 58 IS - 3 SP - 49-1 - 49-10 PB - Springer Science Business Media B.V. CY - Dordrecht AN - OPUS4-33525 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Harsha, A.P. A1 - Wäsche, Rolf A1 - Hartelt, Manfred T1 - Tribological studies on polyetherketone composite under reciprocating sliding condition against steel cylinder N2 - Tribological studies on neat polyetherketone (PEK) and glass fiber reinforced PEK composite were carried out at room and elevated temperature (120 °C). The objective of this study was to characterize for friction and wear properties under dry reciprocating sliding condition at different experimental conditions. The polymer specimens were made to oscillate against steel cylinder as a counterpart. This kind of contact condition are frequently found in bushes, sliding bearing, electronic parts, seals, etc. The friction and wear behavior of neat PEK and composite was quite different at room temperature and elevated temperature. It was observed that glass fiber reinforcement is beneficial in controlling the wear of PEK matrix at room temperature than at elevated temperature. The test results are discussed by considering the surface properties i.e. material removal and film transfer formation. Scanning electron micrographs and optical micrographs of the worn polymer and steel cylinder was used to study the wear mechanisms. KW - Dry oscillating sliding KW - Polyetherketone composite KW - Wear mechanism KW - Contact geometry PY - 2015 DO - https://doi.org/10.1177/1350650115570403 SN - 1350-6501 VL - 229 IS - 7 SP - 795 EP - 806 PB - Institution of Mechanical Engineers CY - London AN - OPUS4-33526 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Cappella, Brunero A1 - Hartelt, Manfred A1 - Wäsche, Rolf T1 - High resolution imaging of macroscopic wear scars in the initial stage N2 - The topography of wear scars on the surface of a steel disc coated with a diamond-like carbon (DLC) layer has been investigated with an Atomic Force Microscope (AFM). AFM topography images have been combined together taking advantage of the stitching technique for the study of wear scars in their initial stage. Moreover, the topography of the sample has been acquired before and after the sliding tests. In this way even very small changes of the sample surface (<10 nm) can be detected. Three main phenomena taking place at the very initial stage of wear could be identified: the abrasion of small asperities bulging out of the sample surface, the carving of swallow grooves with depth under 20 nm, and the partial or total closure of cavities present on the surface. This last phenomenon shows that, before the carving of a wear scar, the plastic deformation of particular regions of the sample, i.e. the volume around the cavities, takes place already after few cycles (in this case between 400 and 800) in the initial phase of the sliding test. KW - Atomic force microscopy KW - Stitching technique KW - Running in KW - Plastic deformation PY - 2015 DO - https://doi.org/10.1016/j.wear.2015.07.013 SN - 0043-1648 VL - 338-339 SP - 372 EP - 378 PB - Elsevier B.V. CY - Amsterdam AN - OPUS4-34734 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Cappella, Brunero T1 - The use of AFM for high resolution imaging of macroscopic wear scars N2 - In this article we demonstrate the use of atomic force microscopy (AFM) measurements for the study of macroscopic wear scars. By stitching AFM images acquired over the wear scar, the detailed structure of the scar can be characterized even when the scar is much wider than the typical maximum scan range of the AFM (50–100 µm). The results obtained by AFM are compared with those yielded by white light interferometry (WLI). The comparison validates the WLI measurements; at the same time, it shows decisive differences in the resolutions of these two methods. As a consequence, AFM measurements are necessary whenever a precise characterization of the structure of the scar is required. However, since stitching of AFM images is rather time-consuming, white light interferometry is recommended as a faster method whenever experiments are aimed at just a gross characterization of the scar and the measurement of mean quantities (e.g. the wear volume). KW - Wear scar KW - Imaging KW - Roughness KW - Wear volume KW - Atomic force microscopy KW - White light interferometry PY - 2014 DO - https://doi.org/10.1016/j.wear.2013.11.009 SN - 0043-1648 VL - 309 IS - 1-2 SP - 120 EP - 125 PB - Elsevier CY - Amsterdam AN - OPUS4-30289 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Harsha, A. P. A1 - Wäsche, Rolf A1 - Joyce, T. J. T1 - Wear of biopolymers under reciprocating sliding conditions against different counterfaces N2 - In the present work it was shown the investigation of wear resistance of ultrahigh-molecular weight polyethylene (UHMWPE) and crosslinked polyethylene (XLPE) against different counterfaces. Friction and wear studies were evaluated under dry reciprocating sliding conditions at room temperature. KW - Biopolymers KW - Wear KW - Friction KW - UHMWPE PY - 2019 DO - https://doi.org/10.1002/pen.25239 VL - 59 IS - 11 SP - 2356 EP - 2366 PB - Society of Plastics Engineers AN - OPUS4-49779 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Steinborn, Gabriele A1 - Woydt, Mathias T1 - Colloidal processing of metal bonded niobium carbide (NbC-Ni) N2 - The manufacturing of NbC with Ni binder with addition of titanium carbide by using a colloidal process for blending the different powders without a milling step were investigated. The the sintering process and formation of the resulting microstructures, the phase relations and the hardness of the produced cermet materials are characterized. T2 - 19. Plansee Seminar CY - Reutte, Austria DA - 29.05.2017 KW - Niobium carbide (NbC) KW - Cermets KW - Hardness PY - 2017 AN - OPUS4-40513 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Woydt, Mathias T1 - Niobium carbide, a new cermet material with excellent properties N2 - Niobium carbide is a ceramic material which can be used with excellent results to replace tungsten carbide with cobalt binder. Furthermore, it might be manufactured by classic ceramic technologies and even colloidal processing. To achieve high toughness and strength, it is necessary to have a perfect mix of hard phase and binder, which is mainly achieved by ball milling. Mechanical and physical properties as well as results on different tribological and application-oriented machining tests are presented. The results have been compared with results obtained with NbC grades with Co and Fe3Al binders as well as with pure binderless hot-pressed NbC and SPS sintered Nb2O5. T2 - ICCCI 2018 - 6th Int. Conf. on the Characterization and Control of Interfaces for High Quality Advanced Materials and 54th Summer Symposium on Powder Technology CY - Kurashiki, Japan DA - 09.07.2018 KW - Niobium carbide KW - Cermet KW - Microstructure KW - Properties PY - 2018 AN - OPUS4-45643 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Jayachandran, Ashok Raj A1 - Brandt, Guido A1 - Schmid, Thomas A1 - Tamura, T. A1 - Nakase, T. T1 - Tribofilm formation of a-C:H coatings under influence of temperature in boundary lubricated oscillating sliding against alumina and silicon nitride N2 - Gegenstand dieses Beitrags ist der Einfluss von Temperatur und Gegenkörperwerkstoff auf die Bildung von Tribofilmen auf a-C:H Beschichtungen. Dies wurde mit einer Kugel-Ebene Anordnung im geschmierten Kontakt untersucht. KW - a-C:H KW - Temperature KW - Tribofilm KW - Lubricated sliding KW - Alumina KW - Silicon nitride PY - 2018 SN - 0724-3472 VL - 65 IS - 5 SP - 28 EP - 37 PB - expert Verlag CY - Tübingen AN - OPUS4-46034 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Ehrke, Roman A1 - Kramer, Renee A1 - Brandt, Guido T1 - Influence of temperature on tribological behaviour of DLC coatings under lubricated conditions up to 250°C N2 - The lecture deals with both friction and wear processes in ceramic - a-C:H Systems. T2 - AsiaTrib 2018 CY - Kuching, Malaysia DA - 16.09.2018 KW - Temperature KW - Lubricated sliding KW - Tribofilm PY - 2018 AN - OPUS4-46036 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Harsha, A. P. A1 - Wäsche, Rolf T1 - Influence of temperature on friction and wear characteristic of polyaryletherketones and their composites under reciprocating sliding condition N2 - In the present work it was shown the tribological behavior of different polyaryletherketones (PAEKs) and their composites under reciprocating sliding conditions at room temperature as well as at elevated temperature (120°C). KW - Composite KW - PAEKs KW - Reciprocating sliding KW - Solid lubricants KW - Wear mechanisms PY - 2018 DO - https://doi.org/10.1007/s11665-018-3633-y SN - 1059-9495 VL - 27 IS - 10 SP - 5438 EP - 5449 PB - Springer AN - OPUS4-46430 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Ehrke, Roman A1 - Woydt, Mathias T1 - Wear of alpha-Alumina in hot steam up to 300°C N2 - Selfmated alpha-alumina sliding couples habe been investigated under oscillating sliding at 100 N load in different humidity conditions in air as well as in hot steam up to temperatures of 300°C and ambient pressures up to 4 bar. T2 - 7th International Conference on Mechanics and Materials in Design CY - Albufeira, Portugal DA - 11.06.2017 KW - Alpha-alumina KW - Wear KW - Temperature KW - Abrasion PY - 2017 AN - OPUS4-41127 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Ehrke, Roman A1 - Woydt, Mathias T1 - Wear of alpha-alumina in hot steam up to 300°C N2 - Selfmated alpha-alumina sliding couples have been investigated under oscillating sliding at 100 N load in different humidity conditions in air as in hot steam up to temperatures of 300°C and ambient pressures up to 4 bar. T2 - 7th International Conference on Mechanics and Materials in Design CY - Albufeira, Portugal DA - 11.06.2017 KW - Apha-alumina KW - Wear KW - Steam KW - Temperature KW - Abrasion PY - 2017 SN - 978-989-98832-6-0 SP - 265 EP - 266 PB - LusoImpress S.A. CY - Avintes, Portugal AN - OPUS4-41128 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Steinborn, Gabriele A1 - Woydt, Mathias T1 - Colloidal processing of metal bonded niobium carbide N2 - Manufacturing of Niobium carbide cermets with nickel binder and different additions of titanium carbide has been realized by colloidal processing in aqueous environment. T2 - 19. Plansee Seminar CY - Reutte, Austria DA - 29.05.2017 KW - NbC KW - TiC KW - Ni KW - Colloidal processing KW - Gas pressure sintering KW - Hardness PY - 2017 SP - HM 135/1 EP - HM 135/11 AN - OPUS4-40596 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Steinborn, Gabriele A1 - Woydt, Mathias T1 - Colloidal processing of Nbc cermets with Ni binder N2 - Niobium-titanium carbide cermets with nickel binder have been prepared by colloidal processing in water without a milling step by using Poly-diallyl-dimethyl-ammonium chloride (Poly-DADMAC) as a dispersant. Homogeneous microstructures with relative densities larger than 99% of the theoretical density have been achieved by gas pressure sintering in argon atmosphere. However, mechanical properties like hardness and strength were slightly decreased due to precipitation of free carbon. T2 - ISNT2017 & ISSNOX5 - 9th International Symposium on Nitrides & 5th International Symposium on SiAlONS and Non-Oxides CY - Sapporo, Japan DA - 27.08.2017 KW - Niobium carbide KW - Colloidal processing KW - Nckel binder KW - Hardness PY - 2017 AN - OPUS4-42152 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Ehrke, R. A1 - Kramer, R. A1 - Jayachandran, A. R. A1 - Brandt, G. T1 - Influence of temperature on tribological behaviour of DLC coatings under lubricated conditions up to 250°C N2 - In the present work it was shown that there is an influence of temperature and counter body material on the tribological properties of a-C:H coatings deposited on Cronidur 30 steel in a lubricated ball on disk contact situation. T2 - ASIATRIB 2018 CY - Kuching, Sarawak, Malaysia DA - 17.09.2018 KW - DLC KW - Temperature KW - Lubricated sliding PY - 2018 SP - 253 EP - 254 AN - OPUS4-46213 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Sato, K. A1 - Brandt, Guido A1 - Schmid, Thomas A1 - Sasaki, S. A1 - Woydt, Mathias T1 - Wear behaviour of MgO stabilized zirconia in hot steam environment up to 400°C N2 - Self-mated magnesia stabilized zirconia (Mg-PSZ) ceramic sliding couples have been investigated at 100 N load (P0max= 1324 MPa) in oscillating sliding conditions in different humidity conditions in air and in hot steam. Temperatures have been varied up to 400 °C and pressures up to 6 bars. The results show that the wear behavior of MgO-ZrO2 under high Hertzian contact pressures is strongly dependent on temperature and is similar for both dry oscillating and oscillating in hot steam. However, although the evolution in wear rates on temperature is similar and the wear rates of MgO-ZrO2 plunged above 300 °C in hot steam and air by nearly three orders of magnitude, SEM micrographs revealed in hot steam at 400 °C smooth wear tracks. In contrast, hot steam enhanced the tribochemistry of self-mated alumina couples and reduced wear rates. Hot steam decreased the coefficients of friction of MgO-ZrO2 with increasing temperature, but not the wear rates. KW - Hot steam KW - Zirconia KW - Friction KW - Wear KW - Tribofilm KW - Raman spectroscopy PY - 2019 DO - https://doi.org/10.1016/j.wear.2019.01.047 VL - 426-427 SP - 428 EP - 432 PB - Elsevier B.V. AN - OPUS4-47873 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Woydt, Mathias A1 - Rehmer, Birgit ED - Ewsuk, K. ED - Naito, M. ED - Kakeshita, T. ED - Kirihara, S. ED - Uematsu, K. ED - Abe, H. T1 - Characterization of the tribological interface in low wear Magneli type ceramics N2 - The tribological behaviour under dry sliding conditions of Magneli phase Ti4O7 and e-phase Ti2Cr2O7 with α-alumina as a sliding partner has been characterised at room temperature by oscillating sliding. The mechanical properties as well as Vickers hardness measurements do not reveal big differences between the materials, and 4-point bending strengths are around 200 MPa for both materials. Although the friction coefficients are in the medium range of 0.6 and do not differ much between the materials, the wear behaviour is very different. At room temperature, the wear coefficient of Ti2O7 is strongly dependent on relative humidity, and wear is highest under dry conditions when relative humidity is low as it is typically found for many ceramic materials. Ti2Cr2O7 shows remarkably different wear behaviour with the lowest wear in dry conditions. The measured coefficients of wear at low relative humidity of 4% are more than 2 orders of magnitude lower than those for Ti2O7. T2 - 3rd International conference on characterization and control of interfaces for high quality advanced materials CY - Kurashiki, Japan DA - 2009-09-06 PY - 2009 SN - 978-0-470-90917-1 VL - 219 SP - 111 EP - 116 PB - John Wiley & Sons CY - Hoboken, New Jersey, USA AN - OPUS4-21842 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Harsha, A. P. A1 - Wäsche, Rolf A1 - Joyce, T. J. T1 - Friction and wear of two polyethylenes under different tribological contact conditions N2 - Tribological properties of ultrahigh-molecular weight polyethylene (UHMWPE) and cross-linked polyethylene (XLPE) were studied in two different wear modes. Firstly, reciprocating sliding wear studies under non-conformal contact investigated the effects of counterface surface roughness (polished, lapped and ground) of Ti6Al4V on the friction and wear of the polyethylenes. Secondly, two-body abrasive wear studies in conformal contact against different abrasive grit size papers were also carried out to ascertain the wear sensitivity of the polyethylenes under these adverse conditions. Wear mechanisms were studied using optical and scanning electron micrographs. The results of the reciprocating sliding wear studies showed that surface roughness of the counterface influenced friction and wear characteristics although no correlation was found between the coefficient of friction and specific wear rate. XLPE demonstrated wear sensitivity, particularly under severe abrasive wear condition. The results indicated that the performance of the polyethylenes greatly depends upon the tribological system under which it is operating. KW - Abrasive wear KW - Polyethylene KW - Reciprocating sliding wear KW - Surface roughness KW - Wear mechanism PY - 2021 DO - https://doi.org/10.1177/0967391120920130 SN - 0967-3911 SN - 1478-2391 VL - 29 IS - 5 SP - 393 EP - 404 PB - Sage Publishing CY - London AN - OPUS4-56903 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -