TY - JOUR A1 - Schempp, Philipp A1 - Schwenk, Christopher A1 - Rethmeier, Michael A1 - Cross, C.E. T1 - Weld metal grain refinement of aluminium alloy 5083 through controlled additions of Ti and B N2 - Kornfeinung im Schweißgut kann die mechanischen Eigenschaften der Schweißnaht und die Schweißeignung des Grundwerkstoffs deutlich verbessern. Eine Möglichkeit korngefeintes Schweißgut zu erreichen, ist das Versetzen des Schmelzbades mit kornfeinenden Mitteln. In dieser Studie wird gezeigt wie Titan- und Borzusätze Korngröße und -struktur von WIG-Schweißnähten der Al-Legierung 5083 (Al Mg4,5Mn0,7) beeinflussen. Dazu wurden in einem Gießprozess stäbchenförmige Einlagen hergestellt, die aus Grundwerkstoff und definierten Zusätzen der Kornfeinungslegierung Al Ti5B1 bestanden. Sie wurden als Ersatz für einen Schweißzusatzwerkstoff in einer Nut im Grundwerkstoff untergebracht und im WIG-Verfahren überschweißt. Durch die Steigerung des Titan- und Borgehalts im Schweißgut konnte dessen mittlere Korngröße deutlich verringert werden. Außerdem wurde eine Änderung der Kornstruktur beobachtet. Die Ergebnisse können als Grundlage genutzt werden, um die empfohlene chemische Zusammensetzung von Schweißzusätzen für Lichtbogenschweißen von Aluminium anzupassen. KW - Aluminium-Legierung 5083 KW - Kornfeinung KW - WIG-Schweißen PY - 2011 DO - https://doi.org/10.3139/120.110265 SN - 0025-5300 VL - 53 IS - 10 SP - 604 EP - 609 PB - Hanser CY - München AN - OPUS4-24654 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schempp, Philipp A1 - Cross, C.E. A1 - Häcker, Ralf A1 - Pittner, Andreas A1 - Rethmeier, Michael T1 - Influence of grain size on mechanical properties of aluminium GTA weld metal N2 - Grain refinement is an important possibility to enhance the mechanical properties such as strength, ductility and toughness of aluminium weld metal. In this study, grain refinement was achieved through the addition of commercial grain refiner Al Ti5B1 to gas tungsten arc weld metal of the aluminium alloys 1050A (Al 99.5) and 5083 (Al Mg4.5Mn0.7). The grain refiner additions led to a significant reduction of the weld metal mean grain size (Alloy 1050A, 86 %; Alloy 5083, 44 %) with a change in grain shape from columnar to equiaxed. Tensile tests showed for Alloy 5083 that the weld metal's ductility can be increased through grain refinement. No improvement in weld metal strength (i.e. yield strength and ultimate tensile strength) was observed. Furthermore, tear tests with notched specimens revealed that the resistance against initiation and propagation of cracks in the weld metal can be enhanced through grain refinement. The toughness was observed to increase clearly by grain refinement in weld metal of commercial pure Al (Alloy 1050A). In Alloy 5083 weld metal, the toughness was not improved through grain refinement, likely because of a semi-continuous network of brittle intermetallic phases that facilitate crack propagation. KW - GTA welding KW - Aluminium KW - Grain size KW - Tensile tests KW - Dynamic fracture tests PY - 2013 DO - https://doi.org/10.1007/s40194-013-0026-6 SN - 0043-2288 SN - 1878-6669 VL - 57 IS - 3 SP - 293 EP - 304 PB - Springer CY - Oxford AN - OPUS4-28065 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Schempp, Philipp A1 - Pittner, Andreas A1 - Rethmeier, Michael A1 - Tang, Z. A1 - Seefeld, T. A1 - Cross, C.E. ED - Babu, S. S. ED - Bhadeshia, H.K. ED - Cross, C.E. ED - David, S.A. ED - DebRoy, T. ED - DuPont, J.N. ED - Koseki, T. ED - Liu, S. T1 - Influence of alloy and solidification parameters on grain refinement in aluminium weld metal due to inoculation N2 - Refinement of the weld metal grain structure can improve the mechanical properties of the weld and decrease the susceptibility to solidification cracking of the weld metal. In this study, commercial Al Ti5B1 grain refiner was used to refine the microstructure of LB (laser beam) and GTA (gas tungsten arc) aluminum welds by inoculation. The grain refiner additions led to a significant decrease in the weld metal mean grain size whereby a transition from columnar to equiaxed grain structure (Columnar to Equiaxed Transition, CET) was observed. The development of both grain size and shape depended upon the base metal (Al alloys 1050A, 5083 and 6082) and upon the welding process. The GTA welding process allowed a more pronounced and a more efficient refinement than in LB welds. Furthermore, the influence of the solidification conditions on the CET was investigated through temperature measurements in the weld metal. The temperature profiles revealed a faster solidification of LB welds than in GTA welds. The results from the temperature measurements were also used to estimate (according to an existing model) the critical thermal gradient at which the CET occurs. T2 - 9th International conference on trends in welding research CY - Chicago, Illinois, USA DA - 04.06.2012 KW - Aluminium KW - LBW KW - GTAW KW - Grain refinement KW - Alloy 1050A KW - Alloy 5083 KW - Alloy 6082 KW - Al Ti5B1 PY - 2013 SN - 978-1-62708-998-2 SP - 98 EP - 107 PB - ASM international AN - OPUS4-27907 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schempp, Philipp A1 - Cross, C.E. A1 - Pittner, Andreas A1 - Rethmeier, Michael T1 - Influence of solute content and solidification parameters on grain refinement of aluminum weld metal N2 - Grain refinement provides an important possibility to enhance the mechanical properties (e.g., strength and ductility) and the weldability (susceptibility to solidification cracking) of aluminum weld metal. In the current study, a filler metal consisting of aluminum base metal and different amounts of commercial grain refiner Al Ti5B1 was produced. The filler metal was then deposited in the base metal and fused in a GTA welding process. Additions of titanium and boron reduced the weld metal mean grain size considerably and resulted in a transition from columnar to equiaxed grain shape (CET). In commercial pure aluminum (Alloy 1050A), the grain-refining efficiency was higher than that in the Al alloys 6082 and 5083. Different welding and solidification parameters influenced the grain size response only slightly. Furthermore, the observed grain-size reduction was analyzed by means of the undercooling parameter P and the growth restriction parameter Q, which revealed the influence of solute elements and nucleant particles on grain size. KW - Aluminium KW - GTA welding KW - Grain refinement KW - Alloy 1050A KW - Alloy 5083 KW - Alloy 6082 KW - Al Ti5B1 PY - 2013 DO - https://doi.org/10.1007/s11661-013-1649-3 SN - 1073-5623 SN - 1543-1940 VL - 44A IS - 7 SP - 3198 EP - 3210 PB - The Minerals, Metals and Materials Society CY - Warrendale AN - OPUS4-28656 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schempp, Philipp A1 - Cross, C.E. A1 - Pittner, Andreas A1 - Rethmeier, Michael T1 - Solidification of GTA aluminium weld metal: Part 2 - Thermal conditions and model for columnar-to-equiaxed transition KW - Aluminium KW - Gas tungsten arc welding (GTAW) KW - Columnar to equiaxed transition (CET) KW - Thermal analysis PY - 2014 SN - 0043-2296 SN - 0096-7629 VL - 93 IS - March SP - 69-s - 77-s PB - American Welding Society CY - New York, NY AN - OPUS4-30415 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schempp, Philipp A1 - Cross, Carl Edward A1 - Schwenk, Christopher A1 - Rethmeier, Michael T1 - Influence of Ti and B additions on grain size and weldability of aluminium alloy 6082 N2 - Grain refinement is an important possibility to enhance the weldability of aluminium weld metal that is usually defined by its susceptibility to solidification cracking. In this study, grain refinement was achieved through the addition of commercial grain refiner containing titanium and boron to the GTA weld metal of aluminium alloy 6082. The weld metal mean grain size could be reduced significantly from about 70 µm to a saturated size of 21 µm with a change in grain shape from columnar to equiaxed. The grain refinement prevented the formation of centreline solidification cracking that was present only in welds with unrefined grain structure. A variation of torch speed led to a strong change of solidification parameters such as cooling rate that was measured in the weld metal and the corresponding solidification rate and thermal gradient. The ratio thermal gradient/growth rate (G/R) decreased from 50 K s/mm² (high torch speed) to 10 K s/mm² (low torch speed). However, the variation of torch speed did not change the tendency for solidification cracking. The microstructure of unrefined and completely refined weld metal was compared. The observed change in size and distribution of the interdendritic phases was related to the change in susceptibility to solidification cracking. KW - Aluminium KW - WIG-Schweißen KW - Kornfeinung KW - Schweißeignung KW - Heißrisse KW - Aluminium alloy KW - Solidification cracking KW - Weldability KW - GTA welding PY - 2012 SN - 0043-2288 SN - 1878-6669 VL - 56 IS - 09/10 SP - 95 EP - 104 PB - Springer CY - Oxford AN - OPUS4-26992 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schempp, Philipp A1 - Cross, C.E. A1 - Pittner, Andreas A1 - Oder, Gabriele A1 - Neumann, R. S. A1 - Rooch, Heidemarie A1 - Dörfel, Ilona A1 - Österle, Werner A1 - Rethmeier, Michael T1 - Solidification of GTA aluminium weld metal: Part I - Grain morphology dependent upon alloy composition and grain refiner content N2 - The solidification conditions during welding strongly influence the weid metal microstructure and mechanical properties of a weid. In the first part of this study, the grain morphology of gas tungsten arc (GTA) bead-on-plate welds was investigated for the aluminum Alloys 1050A (Al 99.5), 6082 (Al SifMgMn), and 5083 (AI Mg4.5Mn0.7). The experiments revealed that increasing welding speed and alloy content allow the growth of small, equiaxed grains, particularly in the weid center. Furthermore, increasing grain refiner additions led to a Strong reduction of the weid metal mean grain size and hence facilitated the columnar to equiaxed transition (CET). In addition, wavelength dispersive X-ray spectroscopy (WDS) and transmission electron microscopy (TEM) analysis revealed in the weid metal TiB2 particles that were surrounded by Al3Ti. This suggests the duplex nucleation theory for nucleation of aluminum grains in GTA weid metal. KW - Aluminium KW - Gas tungsten arc welding (GTAW) KW - Grain refinement KW - Columnar to equiaxed transition (CET) KW - Epitaxial nucleation KW - Duplex nucleation theory PY - 2014 SN - 0043-2296 SN - 0096-7629 VL - 93 SP - 53-s EP - 59-s PB - American Welding Society CY - New York, NY AN - OPUS4-30413 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -