TY - JOUR A1 - Rawat, S. S. A1 - Harsha, A. P. A1 - Khatri, O. P. A1 - Wäsche, Rolf T1 - Pristine, reduced, and alkylated graphene oxide as additives to paraffin grease for enhancement of tribological properties N2 - Pristine, reduced, and alkylated graphene oxides are applied as lubricating additives in paraffin grease. It has revealed that their crystalline structure governs the tribological properties of grease for steel tribo-pair. The microstructural analyses of grease samples showed that a loose fiber network of soap in the presence of graphene-based additive allows their facile release for efficient lubrication. The surface analyses based on the microscopic and elemental mapping show the development of a graphene-derived protective film on the worn scars, which protected the tribo-surfaces and subsided the wear. The reduced graphene oxide (rGO) with the interlamellar distance of 0.35 nm in the (002) plane provided minimum resistance to shear and exhibited maximum reduction in coefficient of friction (COF) for the paraffin grease. The presence of oxygen functionalities in the basal of pristine and alkylated graphene oxide (GO) compromised the interlamellar shearing under tribo-stress; consequently, higher COF than that of rGO. KW - Coefficient of friction KW - Graphene oxide KW - Grease KW - Nanoadditive KW - Tribo-film KW - Wear KW - Boundary lubrication KW - Grease lubrication KW - Lubricant additives KW - Lubricants PY - 2021 DO - https://doi.org/10.1115/1.4047952 VL - 143 IS - 2 SP - 021903-1 EP - 021903-11 PB - ASME AN - OPUS4-51170 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Harsha, A. P. A1 - Wäsche, Rolf A1 - Joyce, T. J. T1 - Friction and wear of two polyethylenes under different tribological contact conditions N2 - Tribological properties of ultrahigh-molecular weight polyethylene (UHMWPE) and cross-linked polyethylene (XLPE) were studied in two different wear modes. Firstly, reciprocating sliding wear studies under non-conformal contact investigated the effects of counterface surface roughness (polished, lapped and ground) of Ti6Al4V on the friction and wear of the polyethylenes. Secondly, two-body abrasive wear studies in conformal contact against different abrasive grit size papers were also carried out to ascertain the wear sensitivity of the polyethylenes under these adverse conditions. Wear mechanisms were studied using optical and scanning electron micrographs. The results of the reciprocating sliding wear studies showed that surface roughness of the counterface influenced friction and wear characteristics although no correlation was found between the coefficient of friction and specific wear rate. XLPE demonstrated wear sensitivity, particularly under severe abrasive wear condition. The results indicated that the performance of the polyethylenes greatly depends upon the tribological system under which it is operating. KW - Abrasive wear KW - Polyethylene KW - Reciprocating sliding wear KW - Surface roughness KW - Wear mechanism PY - 2021 DO - https://doi.org/10.1177/0967391120920130 SN - 0967-3911 SN - 1478-2391 VL - 29 IS - 5 SP - 393 EP - 404 PB - Sage Publishing CY - London AN - OPUS4-56903 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Tribological studies on polyetherimide composites sliding against steel under reciprocating conditions N2 - Results of tribological tests on polyetherimide composites were presented. The tests were carried out at room temperature as well as at 120°C. Counter body was steel 100Cr6. T2 - PolyTrib 2016. 2nd International Conference on Polymer Tribology CY - Ljubljana, Slovenia DA - 15.09.2016 KW - PEI KW - Composites KW - Polyetherimide KW - Temperature KW - Steel PY - 2016 AN - OPUS4-38690 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Harsha, A. P. A1 - Wäsche, Rolf T1 - Tribological studies on polyetherimide composites sliding against steel under reciprocating conditions N2 - The friction and wear properties of polyetherimide composites under dry oscillating sliding condition at room temperature (RT) as well as at elevated temperature (120 °C) was investigated. The polymer specimens were made to oscillate against steel cylinder as a counterpart. The friction and wear properties of PEI and composites were strongly influenced by the temperature. In case of carbon fiber composite abrasive action of carbon fibers has severely damaged the counterpart and resulted in accelerated wear of the composite at RT. Solid lubricants filled (PTFE, MoS2, graphite) along with glass fiber is beneficial in improving the friction and wear performance of the PEI composite at RT, whereas at elevated temperature wear performance was deteriorated. T2 - 2nd International Conference on Polymer Tribology CY - Ljubljana, Slovenia DA - 15.09.2016 KW - Polyetherimide KW - Composites KW - Friction KW - Wear KW - Temperature KW - Oscillating sliding KW - Solid lubricant KW - Fibers PY - 2016 AN - OPUS4-38135 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Woydt, Mathias A1 - Wäsche, Rolf A1 - Brandt, Guido A1 - Ehrke, Roman A1 - Yano, S. A1 - Sasaki, S. T1 - Tribology in hot steam for energy recovery N2 - The wear rates of self-mated alumina couples show that friction as well as wear is largely determined by the above-mentioned hydro-thermal conditions. The presence of water and its amount available in the surrounding system either in liquid or in gaseous form plays a key role for friction and wear behavior and can be beneficial for the tribological profile of steam degradation resistant materials. Hot steam enhances the tribo-chemical formations of oxides and hydroxides on MgO-ZrO2 alumina and antimony impregnated carbon. T2 - 21th International Colloquium Tribology CY - Stuttgart/Ostfildern, Germany DA - 09.01.2018 KW - Tribology KW - Friction KW - Alumina KW - Hot steam PY - 2018 SP - 1 EP - 2 AN - OPUS4-43896 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Brandt, Guido A1 - Ehrke, Roman A1 - Nolze, Gert A1 - Schmid, Thomas A1 - Sasaki, S. A1 - Woydt, Mathias T1 - Wear behaviour of alpha-alumina in hot steam at high contact pressure N2 - The work examines the wear behaviour of α-aluminium oxide by combining thermodynamic modelling with advanced wear testing as well as analytical methods to get a better understanding of this structural ceramic material wear behavior and its possible use in high temperature steam environment. KW - Aluminium oxide KW - Temperature KW - Hot steam KW - Diaspore KW - Ceramic KW - Wear PY - 2018 DO - https://doi.org/10.1016/j.wear.2018.02.012 SN - 0043-1648 SN - 1873-2577 VL - 404-405 SP - 22 EP - 30 PB - Elsevier B.V. AN - OPUS4-44449 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Colloidal processing of Nbc cermets with Ni binder N2 - Niobium-titanium carbide cermets with nickel binder have been prepared by colloidal processing in water without a milling step by using Poly-diallyl-dimethyl-ammonium chloride (Poly-DADMAC) as a dispersant. Homogeneous microstructures with relative densities larger than 99% of the theoretical density have been achieved by gas pressure sintering in argon atmosphere. However, mechanical properties like hardness and strength were slightly decreased due to precipitation of free carbon. T2 - ISNT2017 & ISSNOX5 - 9th International Symposium on Nitrides & 5th International Symposium on SiAlONS and Non-Oxides CY - Sapporo, Japan DA - 27.08.2017 KW - Niobium carbide KW - Colloidal processing KW - Nckel binder KW - Hardness PY - 2017 AN - OPUS4-42152 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Niobium carbide, a new cermet material with excellent properties N2 - Niobium carbide is a ceramic material which can be used with excellent results to replace tungsten carbide with cobalt binder. Furthermore, it might be manufactured by classic ceramic technologies and even colloidal processing. To achieve high toughness and strength, it is necessary to have a perfect mix of hard phase and binder, which is mainly achieved by ball milling. Mechanical and physical properties as well as results on different tribological and application-oriented machining tests are presented. The results have been compared with results obtained with NbC grades with Co and Fe3Al binders as well as with pure binderless hot-pressed NbC and SPS sintered Nb2O5. T2 - ICCCI 2018 - 6th Int. Conf. on the Characterization and Control of Interfaces for High Quality Advanced Materials and 54th Summer Symposium on Powder Technology CY - Kurashiki, Japan DA - 09.07.2018 KW - Niobium carbide KW - Cermet KW - Microstructure KW - Properties PY - 2018 AN - OPUS4-45643 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Harsha, A. P. A1 - Wäsche, Rolf T1 - Influence of temperature on friction and wear characteristic of polyaryletherketones and their composites under reciprocating sliding condition N2 - In the present work it was shown the tribological behavior of different polyaryletherketones (PAEKs) and their composites under reciprocating sliding conditions at room temperature as well as at elevated temperature (120°C). KW - Composite KW - PAEKs KW - Reciprocating sliding KW - Solid lubricants KW - Wear mechanisms PY - 2018 DO - https://doi.org/10.1007/s11665-018-3633-y SN - 1059-9495 VL - 27 IS - 10 SP - 5438 EP - 5449 PB - Springer AN - OPUS4-46430 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Jayachandran, Ashok Raj A1 - Brandt, Guido A1 - Schmid, Thomas A1 - Tamura, T. A1 - Nakase, T. T1 - Tribofilm formation of a-C:H coatings under influence of temperature in boundary lubricated oscillating sliding against alumina and silicon nitride N2 - Gegenstand dieses Beitrags ist der Einfluss von Temperatur und Gegenkörperwerkstoff auf die Bildung von Tribofilmen auf a-C:H Beschichtungen. Dies wurde mit einer Kugel-Ebene Anordnung im geschmierten Kontakt untersucht. KW - a-C:H KW - Temperature KW - Tribofilm KW - Lubricated sliding KW - Alumina KW - Silicon nitride PY - 2018 SN - 0724-3472 VL - 65 IS - 5 SP - 28 EP - 37 PB - expert Verlag CY - Tübingen AN - OPUS4-46034 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Influence of temperature on tribological behaviour of DLC coatings under lubricated conditions up to 250°C N2 - The lecture deals with both friction and wear processes in ceramic - a-C:H Systems. T2 - AsiaTrib 2018 CY - Kuching, Malaysia DA - 16.09.2018 KW - Temperature KW - Lubricated sliding KW - Tribofilm PY - 2018 AN - OPUS4-46036 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Ehrke, R. A1 - Kramer, R. A1 - Jayachandran, A. R. A1 - Brandt, G. T1 - Influence of temperature on tribological behaviour of DLC coatings under lubricated conditions up to 250°C N2 - In the present work it was shown that there is an influence of temperature and counter body material on the tribological properties of a-C:H coatings deposited on Cronidur 30 steel in a lubricated ball on disk contact situation. T2 - ASIATRIB 2018 CY - Kuching, Sarawak, Malaysia DA - 17.09.2018 KW - DLC KW - Temperature KW - Lubricated sliding PY - 2018 SP - 253 EP - 254 AN - OPUS4-46213 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Rabe, Torsten A1 - Wäsche, Rolf T1 - Sintering behaviour of nanocrystalline titanium nitride powders N2 - The sintering behaviour of one microcrystalline and several nanocrystalline TiN powders was investigated by means of a gas pressure furnace with an integrated dilatometer. The investigated nanocrystalline powders strongly differ in the sintering activity. It can be concluded from the experiments, that small grain size, narrow grain size distribution and a low oxygen content are the most important prerequisites for high sintering activity of the nanocrystalline TiN powders. The extraordinary sintering activity of the best TiN powder makes it possible to produce a dense (< 2 % porosity), pure (no sintering aids) and nanostructured (mean diameter of crystals about 100 nm) TiN bodies. PY - 1995 SN - 0965-9773 VL - 6 IS - 1-4 SP - 357 EP - 360 PB - Pergamon Press CY - New York, NY AN - OPUS4-32975 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Rabe, Torsten A1 - Prümmer, R. A1 - Wäsche, Rolf T1 - Explosive compaction of nanosized TiN-powders KW - Explosive compaction KW - Nanocrystalline powder KW - Shaping methods KW - Sintering KW - Titanium nitride PY - 1997 DO - https://doi.org/10.4028/www.scientific.net/MSF.235-238.285 SN - 0255-5476 VL - 235-238 SP - 285 EP - 290 PB - Trans Tech Publications CY - Aedermannsdorf, Switzerland AN - OPUS4-32976 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Yarim, Rasim A1 - Klaffke, Dieter A1 - Hartelt, Manfred T1 - Oscillating sliding wear behaviour of SiC, TiC, TiB2, 59SiC-41TiB2 and 52SiC-24TiC-24TiB2 materials up to 750°C in air N2 - The tribological behaviour of different monolithic and composite ceramics was evaluated in the temperature range between room temperature and 750°C. The test method was oscillating sliding with a ball-on-disk arrangement in an SRV machine. Alumina balls were used as counter body. The friction behaviour was determined on-line, and the wear behaviour was determined from calculations on the basis of wear scar dimensions and profilometric measurements. The friction depends on temperature and shows an increase for most materials for increasing temperature; the smallest friction at all temperatures is found for monolithic TiC. The wear behaviour shows different trends for the different materials. In tests against SiC a maximum of wear is found at 500°C, for TiC at 200°C and for TiB2 at 750°C. The composite ceramics suffer the smallest wear of all materials in the range from 200°C to 500°C. PY - 2006 DO - https://doi.org/10.1002/tt.8 SN - 1354-4063 SN - 1557-685X VL - 12 SP - 99 EP - 111 PB - Coppin CY - Deal AN - OPUS4-32977 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kimmari, E. A1 - Podgursky, V. A1 - Simunin, M. A1 - Adoberg, E. A1 - Surzenkov, A. A1 - Viljus, M. A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Sildos, I. A1 - Kulu, P. T1 - Tribological behavior of carbon nanofibers deposited on hard nanocomposite (nc-Ti1 - xAlxN)/(a-Si3N4) coating N2 - Main focus was on the deposition of carbon nanofibers (CNFs) onto the hard nanocomposite (nc-Ti1 - xAlxN)/(a-Si3N4) (nACo®) coating surface and the investigation of the structure and tribological properties of CNFs. The alcohol chemical vapor deposition (ACCVD) method was employed to prepare CNFs and the deposition temperatures were 600 and 700 °C, respectively. Prior to the CNF deposition, Ni catalyst was deposited onto the nACo® surface using the magnetron sputtering. The influence of the deposition temperature on the carbon nanofibers structure was investigated by Raman spectroscopy and scanning electron microscopy (SEM). The higher order degree of CNF structure is observed with increasing deposition temperature. Tribological tests were carried out under fretting contact conditions against Al2O3 ball. It is shown that the coefficient of friction (COF) decreases from 1.0 to 1.2 for the clean nACo® surface to 0.2–0.4 for the CNF layers deposited on the nACo® surface. The roughness of the nACo® surface was varied and a higher durability of the CNF layers deposited on the rougher nACo® surface is found. KW - Carbon nanofiber KW - Coating KW - Fretting KW - Roughness KW - Solid lubrication PY - 2013 DO - https://doi.org/10.1016/j.surfcoat.2013.03.011 SN - 0257-8972 VL - 225 SP - 21 EP - 25 PB - Elsevier Science CY - Lausanne AN - OPUS4-32978 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Gräber, H.-G. A1 - Klaffke, Dieter T1 - Experimentelle Untersuchungen zum Abriebverhalten von keramischen Werkstoffen für dentale Restaurationen T2 - 47. Tribologie-Fachtagung - Reibung, Schmierung und Verschleiß - Forschung und praktische Anwendungen CY - Göttingen, Germany DA - 2006-09-25 KW - Dentalkeramik KW - Bearbeitbarkeit KW - Abriebverhalten PY - 2006 SN - 3-00-019670-6 VL - I SP - 36/1 EP - 36/9 CY - Aachen AN - OPUS4-31751 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Scholz, Christian A1 - Wäsche, Rolf ED - Bartz, Wilfried J. T1 - Effect of sliding speed and relative humidity on the tribological behavior of ceramic and polymer materials T2 - 19th International colloquium Tribology - Industrial and automotive lubrication CY - Stuttgart/Ostfildern, Germany DA - 2014-01-21 PY - 2014 SN - 978-3-943563-10-8 SP - Paper 08_11_Scholz_Man, 1 EP - 6 CY - Stuttgart/Ostfildern AN - OPUS4-31743 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Cruzado, A. A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Urchegui, M.A. A1 - Gómez, X. T1 - Fretting wear of thin steel wires. Part 2: Influence of crossing angle N2 - The wear behaviour of thin steel wires has been analyzed under oscillating sliding conditions in crossed cylinders contact geometry. The focus of this analysis was the influence of the crossing angle between the wires on the wear. The wires used had 0.45 mm in diameter and the material was cold-drawn eutectoid carbon steel (0.8% C) with a tensile strength higher than 2800 MPa. Two different types of tests were carried out, the first one representing the influence of the crossing angle for a constant load and the second one representing the influence of the crossing angle with constant contact pressure. In the first type of tests it was seen that as the contact angle decreases the contact pressure decreases too and hence less energy specific wear resistance is observed. As a consequence less wear is produced, thus increasing the life of the wires. In the second type of tests it was seen that with constant contact pressure but different crossing angles, nearly the same energy specific wear resistance was observed. This points at an identical wear behaviour in both type of tests but with a running-in and a steady state period as two different wear periods. The tests showed that the running in period may play an important role in the overall wear particle generation and hence the wear occurring in the steady state period is rather mild. KW - Fretting KW - Wires KW - Contact pressure KW - Crossing angle PY - 2011 DO - https://doi.org/10.1016/j.wear.2011.04.012 SN - 0043-1648 VL - 273 IS - 1 SP - 60 EP - 69 PB - Elsevier CY - Amsterdam AN - OPUS4-31762 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Hartelt, Manfred ED - Mang, T. T1 - Fretting N2 - The importance of lubricants in virtually all fields of the engineering industry is reflected by an increasing scientific research of the basic principles. Energy efficiency and material saving are just two core objectives of the employment of high-tech lubricants. The encyclopedia presents a comprehensive overview of the current state of knowledge in the realm of lubrication. All the aspects of fundamental data, underlying concepts and use cases, as well as theoretical research and last but not least terminology are covered in hundreds of essays and definitions, authored by experts in their respective fields, from industry and academic institutes. KW - Fretting corrosion KW - Fretting fatigue KW - Fretting regimes KW - Fretting wear KW - Mixed fretting regime PY - 2014 SN - 978-3-642-22646-5 SN - 978-3-642-22647-2 DO - https://doi.org/10.1007/978-3-642-22647-2 VL - 2 SP - 680 EP - 687 PB - Springer CY - Heidelberg AN - OPUS4-30497 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Woydt, Mathias ED - Mang, T. T1 - Stribeck curve N2 - The importance of lubricants in virtually all fields of the engineering industry is reflected by an increasing scientific research of the basic principles. Energy efficiency and material saving are just two core objectives of the employment of high-tech lubricants. The encyclopedia presents a comprehensive overview of the current state of knowledge in the realm of lubrication. All the aspects of fundamental data, underlying concepts and use cases, as well as theoretical research and last but not least terminology are covered in hundreds of essays and definitions, authored by experts in their respective fields, from industry and academic institutes. PY - 2014 SN - 978-3-642-22646-5 SN - 978-3-642-22647-2 DO - https://doi.org/10.1007%2F978-3-642-22647-2 VL - 4 SP - 1998 EP - 2005 PB - Springer CY - Heidelberg AN - OPUS4-30499 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Steinborn, Gabriele T1 - Wear behaviour of low IR-emission titanate ceramics under gross slip fretting conditions against steel and alpha-alumina N2 - The tribological behavior of different low infrared (IR) emission ceramic materials from the titanate group has been investigated at room temperature under gross slip fretting conditions against 100Cr6 ball bearing steel and α-alumina as the counterface materials. For all material pairs, friction and wear depended largely on the relative humidity of the environment. When paired with steel the low IR-emission ceramic disks showed higher wear resistance. Under dry conditions, almost no wear was found on the low IR-emission ceramic specimen. The high wear on the steel counter body is caused not only by tribo-oxidation, which is the main wear mechanism, but also by abrasion. In dry conditions a COF of 0.6 and in humid conditions a COF of 0.2 have been measured. When paired with α-alumina the results on wear are just opposite to those with steel counterbody and the low IR-emission ceramic materials show much lower wear resistance under all conditions. This is explained by the predominance of abrasion and the relatively large difference in hardness between the low IR-emission ceramic and α-alumina. In high humidity environments the results point to the formation of stable reaction layers causing lower friction and wear. KW - Gross slip fretting KW - Ceramic wear KW - Yttrium titanate KW - Zirconium titanate KW - Low IR-emission ceramics PY - 2014 DO - https://doi.org/10.1016/j.wear.2014.03.006 SN - 0043-1648 VL - 315 IS - 1-2 SP - 11 EP - 16 PB - Elsevier B.V. CY - Amsterdam AN - OPUS4-30504 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Colloidal processing of metal bonded niobium carbide (NbC-Ni) N2 - The manufacturing of NbC with Ni binder with addition of titanium carbide by using a colloidal process for blending the different powders without a milling step were investigated. The the sintering process and formation of the resulting microstructures, the phase relations and the hardness of the produced cermet materials are characterized. T2 - 19. Plansee Seminar CY - Reutte, Austria DA - 29.05.2017 KW - Niobium carbide (NbC) KW - Cermets KW - Hardness PY - 2017 AN - OPUS4-40513 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Woydt, Mathias T1 - Tribological characterization of niobium carbide with different binder materials N2 - Wear of Niobium carbide with nickel binder has been experimentally characterized under dry, oscillating sliding conditions against steel and a-alumina up to 600°C. T2 - National Tribology Conference/NTC-2016 CY - Varanasi, India DA - 08.12.2016 KW - Niobium carbide KW - Wear resistance KW - Binder PY - 2016 SP - 1 EP - 2 AN - OPUS4-38879 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Ehrke, Roman ED - Silva Gomes, J. F. ED - Meguid, S. A. T1 - A study on tribological behaviour of a-C:H coatings under lubricated conditions up to 250°C N2 - The influence of temperature and counterbody material on the tribological properties of a-C:H coatings deposited on Cronidur 30 steel has been investigated in a lubricated ball on disk contact situation with alpha-alumina and silicon nitride as counterbodies. The results show, that the wear volumes of the systems increase exponentially with increasing temperature, for alpha-alumina more than for silicon nitride. Two different wear mechanisms seem to have a major influence: First, the abrasive action due to materials hardness and second, the tribo-oxidation when silicon nitride is counter material. T2 - 6th International Conference on Mechanics and Materials Design CY - P. Delgada/Azores, Portugal DA - 26.07.2015 KW - Diamond like carbon KW - Ceramics KW - Wear KW - Friction KW - Temperature PY - 2015 SP - Paper 5395, 445 EP - 446 AN - OPUS4-37014 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Ehrke, Roman ED - Silva Gomes, J.F. ED - Meguid, S.A. T1 - A study on tribological behaviour of a-C:H coatings under lubricated conditions up to 250 °C N2 - The influence of temperature and counterbody material on the tribological properties of a-C:H coatings deposited on Cronidur 30 steel has been investigated in a lubricated ball on disk contact situation. The results show, that the wear volumes of the system increase exponentially with increasing temperature. Two different wear mechanisms seem to have a major influence: First, the abrasive action due to materials hardness and second, the tribooxidation when silicon nitride is counter material. T2 - M2D2015 - 6th International conference on mechanics and materials in design CY - Ponta Delgada, Azores DA - 26.07.2015 KW - Diamond like carbon KW - Ceramics KW - Wear KW - Friction KW - Temperature PY - 2015 SN - 978-989-98832-3-9 SP - 445 EP - 446 AN - OPUS4-33808 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - A study of tribological behaviour of a-C:H coatings under lubricated conditions up to 250°C T2 - 6. International Conference on Mechanics and Materials in Design CY - P. Delgada/Azores, Portugal DA - 2015-07-26 PY - 2015 AN - OPUS4-33761 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Harsha, A.P. A1 - Wäsche, Rolf A1 - Hartelt, Manfred T1 - Friction and wear studies of polyetherimide composites under oscillating sliding condition against steel cylinder N2 - Tribological properties of neat polyetherimide (PEI), glass, carbon fiber, and solid lubricants filled PEI composites are presented in this article. The aim of this study was to investigate the friction and wear properties of these composites under dry oscillating sliding condition at room temperature (RT) as well as at elevated temperature (120 °C). The polymer specimens were made to oscillate against steel cylinder as a counterpart. The friction and wear properties of PEI and composites were strongly influenced by the temperature. Incorporation of carbon fiber in the PEI matrix has increased the wear rate at RT, while at elevated temperature this trend was opposite. Abrasive action of carbon fibers has severely damaged the counterpart and resulted in accelerated wear of the composite at RT. Solid lubricants filled (PTFE, MoS2, graphite) along with glass fiber is beneficial in improving the friction and wear performance of the PEI composite at RT, whereas at elevated temperature wear performance was deteriorated. Tribological performance of neat PEI and glass fiber composite was similar with each other at RT. Scanning electron micrographs and optical micrographs of the worn polymer specimens and the steel cylinders was used to study the possible wear mechanisms. The present test results were also compared with data available on the reciprocating wear of PEI and composites in the literature and trends have been reported. PY - 2015 DO - https://doi.org/10.1002/pc.23559 SN - 0272-8397 SN - 1548-0569 VL - 38 IS - 1 SP - 48 EP - 60 PB - Society of Plastics Engineers CY - Manchester, NH AN - OPUS4-34921 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Steinborn, Gabriele A1 - Woydt, Mathias T1 - Colloidal processing of metal bonded niobium carbide N2 - Manufacturing of Niobium carbide cermets with nickel binder and different additions of titanium carbide has been realized by colloidal processing in aqueous environment. T2 - 19. Plansee Seminar CY - Reutte, Austria DA - 29.05.2017 KW - NbC KW - TiC KW - Ni KW - Colloidal processing KW - Gas pressure sintering KW - Hardness PY - 2017 SP - HM 135/1 EP - HM 135/11 AN - OPUS4-40596 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Wear of alpha-Alumina in hot steam up to 300°C N2 - Selfmated alpha-alumina sliding couples habe been investigated under oscillating sliding at 100 N load in different humidity conditions in air as well as in hot steam up to temperatures of 300°C and ambient pressures up to 4 bar. T2 - 7th International Conference on Mechanics and Materials in Design CY - Albufeira, Portugal DA - 11.06.2017 KW - Alpha-alumina KW - Wear KW - Temperature KW - Abrasion PY - 2017 AN - OPUS4-41127 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Ehrke, Roman A1 - Woydt, Mathias T1 - Wear of alpha-alumina in hot steam up to 300°C N2 - Selfmated alpha-alumina sliding couples have been investigated under oscillating sliding at 100 N load in different humidity conditions in air as in hot steam up to temperatures of 300°C and ambient pressures up to 4 bar. T2 - 7th International Conference on Mechanics and Materials in Design CY - Albufeira, Portugal DA - 11.06.2017 KW - Apha-alumina KW - Wear KW - Steam KW - Temperature KW - Abrasion PY - 2017 SN - 978-989-98832-6-0 SP - 265 EP - 266 PB - LusoImpress S.A. CY - Avintes, Portugal AN - OPUS4-41128 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Klaffke, Dieter ED - Christophe Donnet, ED - Erdemir, Ali T1 - Tribology of DLC Films Under Fretting Conditions KW - DLC KW - Oscillation sliding KW - Counterbody KW - Relative humidity KW - Temperature KW - Lubrication PY - 2008 SN - 978-0-387-30264-5 SP - 362 EP - 382 PB - Springer Science + Business Media AN - OPUS4-18571 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kloß, Heinz A1 - Wäsche, Rolf T1 - Analytical approach for wear prediction of metallic and ceramic materials in tribological applications N2 - Wear mechanisms, as adhesion, abrasion, fatigue and tribochemical wear, are complex in their physical and chemical nature. A theoretical description and prediction of wear are in most cases still far from reality. It is, therefore, important to use test rigs before a practical application of a given material combination under tribological loading. On the other hand, model equations can be helpful for wear description, if a single wear mechanism is dominant. Under oscillating and continuous sliding contact conditions, equations for wear calculation are presented to describe running-in and stationary wear behaviour of metals and ceramics. By using shear energy density, real area of contact, flash temperature, activation energy and numerical simulations with the method of movable cellular automata (MCA), wear data were calculated and compared to experimental laboratory results. KW - Wear KW - Surface temperature KW - Activation energy KW - Simulation KW - Movable cellular automata (MCA) PY - 2009 DO - https://doi.org/10.1016/j.wear.2008.04.034 SN - 0043-1648 VL - 266 IS - 3-4 SP - 476 EP - 481 PB - Elsevier CY - Amsterdam AN - OPUS4-18651 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Wear of thin steel wires T2 - Nordtrib 2010 CY - Luleå, Sweden DA - 2010-06-08 PY - 2010 AN - OPUS4-22874 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Wear of SiC-TiC-TiB2 ceramics at high temperatures and sliding speeds in air T2 - Asiatrib 2010 CY - Perth, Australia DA - 2010-12-05 PY - 2010 AN - OPUS4-22875 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Analysis of oxidative processes in SiC-TiC-TiB2 ceramic composites during tribological loading T2 - Tribochemistry 2009 CY - Kyoto, Japan DA - 2009-09-02 PY - 2009 AN - OPUS4-22870 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Extended tribological study on carbon nitride coatings under oscillating sliding conditions T2 - World Tribology Congress (WTC) CY - Kyoto, Japan DA - 2009-09-09 PY - 2009 AN - OPUS4-22872 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Experimental study on wear of dental ceramic materials - tests in artificial saliva T2 - 17. International Colloquium on Tribology CY - Filderstadt, Germany DA - 2010-01-19 PY - 2010 AN - OPUS4-22873 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Wötting, G. T1 - Tribological behaviour of structural Si-based ceramics in fretting tests at room temperature N2 - The friction and wear behaviour of SiC, Si3N4 and SiC/Si3N4 composite ceramics were investigated with oscillating sliding (gross slip fretting) at room temperature. The influence of counter body material and the humidity of the surrounding air was studied with a ball-on-disc configuration with different ball materials (1000Cr6, Al2O3 SiC and Si3N4). The effect of RH on friction is marginal with exception of SiC (low friction) as counter body material. The wear behaviour, however, is strongly affected by humidity, showing inverse trends for different counter body materials. Consequently, the wear behaviour of a tribo couple can be improved by selecting an adequate mating material. The results reveal the necessity to control RH in tribological tests. For estimation of the performance of tribo couples under varying environmental conditions, a variation of RH is required. In tribo couples with single phase SiC, either as ball or disc, the tribological behaviour of the system is dominated by SiC. The friction behaviour of the composite material is in between the behaviour of the two single phase materials, Si3N4 and SiC, whereas the wear behaviour is very similar to that of single phase Si3N4. KW - Silicon carbide KW - Silicon nitride KW - Particulate composite KW - Fretting KW - Humidity KW - Mating material PY - 2009 DO - https://doi.org/10.1007/s11249-009-9413-y SN - 1023-8883 SN - 1573-2711 VL - 33 IS - 3 SP - 211 EP - 219 PB - Springer Science Business Media B.V. CY - Dordrecht AN - OPUS4-19000 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Paulick, Carl A1 - Steinborn, Gabriele A1 - Richter, V. A1 - Werner, M. T1 - Joining of ceramic components in the green state via LPIM N2 - It has been successfully demonstrated that ceramic materials can be joined in the green state without a second phase by using low pressure injection molded parts. The investigation of the joining interface revealed that a high quality interface can be achieved by carefully adjusting the different manufacturing steps. The use of monomodal particle size distribution in the used powder CT3000SG is inferior to a broader particle size distribution obtained by replacing 33% of the finer alumina powder by coarser CT1200SG. In this way the dewaxing process is significantly improved when the wall thickness of the part exceeds 3 mm. The investigation of the mechanical properties of the joined and sintered parts revealed, that the bending strength of the joined specimens achieved about 80 % of the unjoined, monolithic specimens. T2 - 4th International Conference on Advanced Materials and Processing CY - Hamilton, New Zealand DA - 2006-12-10 KW - Joining KW - Ceramics KW - Green state KW - Interface KW - Bending strength KW - Low pressure injection molding PY - 2005 UR - http://www.scientific.net/3-908453-89-5/207/ SN - 1022-6680 SN - 1662-8985 VL - 29-30 SP - 207 EP - 210 PB - Trans Tech Publ. CY - Zurich AN - OPUS4-19001 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Hartelt, Manfred A1 - Wäsche, Rolf T1 - Volumetrische Verschleiß-Berechnung an gekrümmten Kontaktgeometrien T2 - 50. Tribologie-Fachtagung - Reibung, Schmierung und Verschleiß - Forschung und praktische Anwendung CY - Göttingen, Deutschland DA - 2009-09-21 KW - Verschleißberechnung KW - Calculation of wear volume PY - 2009 SN - 978-3-00-028824-1 VL - I SP - 3-1 - 3-9 CY - Aachen AN - OPUS4-20023 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Weihnacht, V. T1 - Influence of counterbody material on wear of ta-C coatings under fretting conditions at elevated temperatures N2 - The high temperature tribological performance of tetrahedral amorphous carbon coatings has been analyzed at elevated temperatures up to 250 °C in air against three different counterbody materials-steel 100Cr6, a-alumina and silicon nitride. The results show that the counterbody material influences the friction and wear behavior and therefore coating life time strongly. This effect is well known for these coatings at room temperature under dry environmental conditions, equivalent to conditions above 100 °C when water molecules desorb from the surface. However, the sharp difference in tribological performance between silicon nitride on the one hand and alumina and steel on the other hand cannot be understood in this context. Analyzing the friction behavior during the running-in phase, it is evident that only alumina and steel form a stable interface with constant low friction and relatively low wear rates. Silicon nitride forms an unstable interface with fluctuating COF and relatively high wear rates due to its own inherent tendency to tribo-oxidation. KW - Fretting KW - Hard carbon coatings KW - ta-C KW - High temperature KW - Counterbody influence PY - 2009 DO - https://doi.org/10.1016/j.wear.2009.08.041 SN - 0043-1648 VL - 267 IS - 12 SP - 2208 EP - 2215 PB - Elsevier CY - Amsterdam AN - OPUS4-20344 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Gräber, H.G. T1 - Experimental study on wear of dental ceramic materials - tests in artificial saliva T2 - 17th International colloquium tribology - Solving friction and wear problems CY - Stuttgart/Ostfildern, Germany DA - 2010-01-19 KW - Fretting KW - Life science KW - Wear KW - Dental materials PY - 2010 SN - 3-924813-80-9 IS - Special aspects of tribology SP - 1 EP - 7 AN - OPUS4-21070 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Woydt, Mathias A1 - Wäsche, Rolf T1 - The history of the Stribeck curve and ball bearing steels: The role of Adolf Martens N2 - The historical development on the discoveries of lubrication regimes for lubricated sliding contacts has been reviewed from the very beginning. It was found that the functional relationship between the coefficient of friction and the product of sliding speed and viscosity divided by the normal load well known as the Stribeck curve has been experimentally explored much earlier by Adolf Martens in 1888 long before Richard Stribeck did his pioneering measurements in 1902. However, basic work in this field of experimental hydrodynamics was done and results were published even earlier than that back in 1854 by Gustave A. Hirn, in 1879 by Robert H. Thurston and in 1883 by Beauchamp Tower. KW - Stribeck curve KW - Martens KW - Stribeck KW - Thurston KW - Gümbel KW - Hirn PY - 2010 DO - https://doi.org/10.1016/j.wear.2010.02.015 SN - 0043-1648 VL - 268 IS - 11-12 SP - 1542 EP - 1546 PB - Elsevier CY - Amsterdam AN - OPUS4-21180 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Cruzado, A. A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Urchegui, M.A. A1 - Gómez, X. T1 - Fretting wear of thin steel wires. Part 1: Influence of contact pressure N2 - Different fretting tests of thin steel wires under different conditions (loads, strokes, number of cycles and mean pressures) were performed. The wires used had 0.45 mm in diameter and the material was a cold-drawn eutectoid carbon steel (0.8% C) with a tensile strength over 2800 MPa. The tests were carried out with 90° "crossed cylinders" configuration varying the stroke, normal load and testing time (number of cycles). Afterwards the volumetric wear was obtained using surface profilometry with diamond stylus. With a classical study of the coefficient of wear with respect to the sliding distance, the results show that the wear coefficient increases with normal load and stroke, consequently, for the same sliding distance, the wear produced was higher when the load and/or stroke is increased. In this work, the coefficient of wear is decreasing continuously as the test is running. In order to analyze better the wear behaviour, another method, in which the volumetric wear is compared with respect to the Archard's loading factor, is proposed. As result of this method, two distinctive behaviours were detected; one corresponds to the running-in period with a more aggressive wear behaviour and the second one to the stable steady state period. In all the tests the running-in period was similar with regard to the wear rates but in the stable period the wear rates were increasing with higher loads or strokes. KW - Fretting KW - Wear KW - Wires KW - Contact pressure KW - Unlubricated tests PY - 2010 DO - https://doi.org/10.1016/j.wear.2010.02.017 SN - 0043-1648 VL - 268 IS - 11-12 SP - 1409 EP - 1416 PB - Elsevier CY - Amsterdam AN - OPUS4-21181 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Djahanbakhsh, Mohammad A1 - Österle, Werner T1 - Vergleich von Standard-Modell- und HIP-Simulator-Untersuchungen an Verschleißschutzschichten für Metall-Keramik-Paarungen bei Endoprothesen KW - Beschichtung KW - Reversierender Gleitverschleiß KW - HIP-Simulation KW - Coating KW - Reciprocating sliding KW - HIP-Simulation PY - 2008 SN - 0724-3472 VL - 55 IS - 1 SP - 21 EP - 25 PB - Expert Verlag CY - Renningen AN - OPUS4-17133 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Tribotesting with small loads and amplitudes - how does it compare to normal conditions in oscillating sliding? T2 - 27th Meeting of the International Research Group on Wear of Engineering Materials CY - Berlin, Germany DA - 2008-09-30 PY - 2008 AN - OPUS4-18215 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Tribological behavior of hard carbon coatings sliding against aluminum oxide, silicon nitride and steel up to 250 °C in air T2 - NORDTRIB 2008, 13th Nordic Symposium on Tribology CY - Tampere, Finland DA - 2008-06-10 PY - 2008 AN - OPUS4-18217 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Physikalisch-chemische Grundlagen der Festschmierstoffe T2 - TAE Esslingen: Lehrgang: Reibungs- und Verschleißminderung durch Festschmierstoffe CY - Ostfildern, Germany DA - 2008-03-31 PY - 2008 AN - OPUS4-18316 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Grundlagen der Schwingungsverschleißprüfung T2 - TAE Esslingen + GfT: Seminar: Reibung und Verschleiß von Werkstoffen, Bauteilen und Konstruktion CY - Ostfildern, Germany DA - 2008-04-08 PY - 2008 AN - OPUS4-18317 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -