TY - CONF A1 - Wäsche, Rolf T1 - Porous alumina from nano sized powders with improwed diffuse reflection properties T2 - Vorlesung bei Osaka University CY - Osaka, Japan DA - 2002-09-04 PY - 2002 AN - OPUS4-6309 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Promoting the infrastructure - prestandardisation endeavours for ceramic powders and green bodies T2 - Annual Meeting of the American Ceramic Society CY - St. Louis, MO, USA DA - 2002-04-30 PY - 2002 AN - OPUS4-6310 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Suchantke, Christian A1 - Yarim, Rasim ED - Schulte, K. ED - Kainer, K. T1 - Sintern von Verbundwerkstoffen im System SiC-TiC-TiB2 T2 - 12. Tagung "Verbundwerkstoffe und Werkstoffverbunde" CY - Hamburg, Deutschland DA - 1999-10-05 KW - Sintern KW - Verbundwerkstoffe KW - Thermochemische Analyse PY - 1999 SN - 3-527-29967-X SP - 189 EP - 194 PB - Wiley-VCH CY - Weinheim AN - OPUS4-720 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter T1 - High temperature tribological behaviour of particulate composites in the system SiC-TiC-TiB2 during dry oscillating sliding KW - Ceramic Composites KW - High temperatures KW - Tribo-oxidation KW - Dry-slidins KW - Friction KW - Wear PY - 1999 SN - 1225-9381 VL - 5 IS - 2 SP - 155 EP - 161 PB - Han'guk-Seramik-Hakhoe CY - Seoul AN - OPUS4-761 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kautek, Wolfgang A1 - Rudolph, Pascale A1 - Brzezinka, Klaus-Werner A1 - Wäsche, Rolf ED - Meunier, M. T1 - Physical chemistry of the femtosecond and nanosecond laser-material-interaction with SiC and a SiC-TiC-TiB2 composite ceramic compound N2 - The interaction of nanosecond laser pulses in the ultraviolet wavelength range and femtosecond laser pulses in the near-infrared region with the direct semiconductor SiC and the composite compound SiC-TiC-TiB2 was investigated in respect to resulting physicochemical processes. Surface analytical techniques, such as XPS, µ-Raman, and EDX were used to identify the chemical changes between untreated and laser-treated areas. Single-pulse irradiation led to material modifications in the condensed state in most instances. Multi-pulse results differed depending on the pulse duration. In the nanosecond case, melting of the surface and redeposited material (debris) were observed. With femtosecond pulses instead, only negligible melting and few debris could be detected. Additionally, periodic structures (ripples) appeared, with parallel orientation and in most cases two different periodicities for a particular material. Laser ablation of all the studied compound materials exhibited preferential ablation of the lighter component elements. Crystal structure changes of the irradiated surface were observed as a consequence of laser-induced melting and resolidification. An oxidation process interfered with all this processes so that unstoichiometric oxides were formed. T2 - Symposium D - European Materials Research Society CY - Strasbourg, France DA - 2002-06-18 PY - 2002 UR - http://www.emrs-strasbourg.com/files/pdf/2002_SPRING/02_Prog_Dv2.pdf N1 - Serientitel: Applied surface science – Series title: Applied surface science VL - 208/209.2003,1 IS - 1 SP - 1 PB - Elsevier CY - Amsterdam AN - OPUS4-1732 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Hackley, V.A. A1 - Patton, J. A1 - Lum, L.-S. H. A1 - Wäsche, Rolf A1 - Naito, M. A1 - Abe, H. A1 - Hotta, Y. A1 - Pendse, H. T1 - Analysis of the isoelectric point in moderately concentrated Alumina suspensions using electroacoustic and streaming potential methods PY - 2002 SN - 0193-2691 SN - 1532-2351 VL - 23 IS - 5 SP - 601 EP - 617 PB - Dekker CY - New York, NY AN - OPUS4-2080 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Klaffke, Dieter A1 - Steinborn, Gabriele A1 - Wäsche, Rolf A1 - Wötting, G. ED - Degischer, H.-P. T1 - Tribologische Untersuchungen an SiC- und Si3N4-basierten Keramiken T2 - 14. Symposium Verbundwerkstoffe und Werkstoffverbunde CY - Wien, Österreich DA - 2003-07-02 PY - 2003 SN - 3-527-30762-1 SP - 545 EP - 550 PB - Wiley-VCH CY - Weinheim AN - OPUS4-2591 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Steinborn, Gabriele A1 - Fritz, Ulrich A1 - Rabe, Torsten A1 - Wäsche, Rolf T1 - Dispergierung von Nanopulvern in Foliengießschlickern KW - Dispergierung KW - Nanopulver KW - Folie PY - 2004 SN - 0173-9913 SN - 0196-6219 VL - 18 IS - 1 SP - 43 EP - 50 PB - Göller CY - Baden-Baden AN - OPUS4-5219 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Tribological Tailoring of Ceramic Composites T2 - 13th International Colloquium on Tribology CY - Esslingen am Neckar, Germany DA - 2002-01-15 PY - 2002 AN - OPUS4-6312 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - High Temperature Tribological Behaviour of SiC Particulate Composites T2 - Austceram 2002 CY - Perth, Australia DA - 2002-09-30 PY - 2002 AN - OPUS4-6313 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Rudolph, Pascale A1 - Brzezinka, Klaus-Werner A1 - Wäsche, Rolf A1 - Kautek, Wolfgang T1 - Physical chemistry of the femtosecond and nanosecond laser-material interaction with SiC and a SiC-TiC-TiB2 composite ceramic compound N2 - The interaction of nanosecond laser pulses in the ultraviolet wavelength range and femtosecond laser pulses in the near-infrared region with the semiconductor SiC and the composite compound SiC–TiC–TiB2 was investigated. Surface analytical techniques, such as XPS, depth profile (DP), and micro-Raman spectroscopy (?-RS) were used to identify the chemical changes between untreated and laser-treated areas. Single-pulse irradiation led to material modifications in the condensed state in most instances. Multi-pulse results differed depending on the pulse duration. Crystal structure changes were observed as a consequence of laser-induced melting and resolidification. In air contact all components underwent oxidation reactions according to thermodynamic expectations. Exceptions were observed under exclusion of oxygen, SiC was reduced to elemental Si. KW - Femtosecond techniques KW - Nanosecond techniques KW - Ceramics KW - Raman spectra/condensed matter KW - XPS/surface analysis PY - 2003 DO - https://doi.org/10.1016/S0169-4332(02)01356-9 SN - 0169-4332 SN - 1873-5584 VL - 208-209 SP - 285 EP - 291 PB - North-Holland CY - Amsterdam AN - OPUS4-2791 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Woydt, Mathias A1 - Dörfel, Ilona T1 - Interface formation by tribo-oxidation in SiC based ceramics T2 - AIST-BAM Symposium on Materials Surface Technology in Twin Institute Programme CY - Tsukuba, Japan DA - 2003-02-18 PY - 2003 SP - 1 EP - 4 AN - OPUS4-12051 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Woydt, Mathias A1 - Dörfel, Ilona T1 - Structure of the interface in SiC-based ceramic composites formed by tribo-oxidation under dry sliding conditions PY - 2004 SN - 1042-1122 VL - 146 SP - 401 EP - 407 PB - American Ceramic Society CY - Westerville, Ohio AN - OPUS4-12053 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Yarim, Rasim A1 - Nicolaides, Dagmar T1 - Influence of Green Compaction on the Sintering Behaviour of SiC-TiC-TiB2 Composites KW - Pressureless sintering KW - SiC KW - TiC KW - TiB2 KW - Green compaction KW - Particle size KW - Microstructure PY - 2004 SN - 1013-9826 VL - 264-268 SP - 213 EP - 218 PB - Trans Tech Publ. CY - Aedermannsdorf AN - OPUS4-12054 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Yarim, Rasim A1 - Wäsche, Rolf A1 - Woydt, Mathias A1 - Dörfel, Ilona T1 - Analysis of wear protecting oxide layers in the system SiC-TiC-TiB2 formed in-situ at high temperatures T2 - AIST-BAM Symposium on Materials Surface Technology in Twin Institute Programme CY - Tsukuba, Japan DA - 2003-02-18 PY - 2003 SP - 5 EP - 8 AN - OPUS4-12057 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Steinborn, Gabriele A1 - Fritz, Ulrich A1 - Rabe, Torsten A1 - Wäsche, Rolf ED - Kriegesmann, J. T1 - Dispergierung von Nanopulvern in Foliengießschlickern KW - Dispergierung KW - Nanopulver KW - Foliengiessen PY - 2005 SN - 3-87156-091-X IS - Kap. 3.3.3.5 SP - 1 EP - 16 PB - Deutscher Wirtschaftsdienst CY - Köln AN - OPUS4-16272 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Oscicalling sliding wear behaviour of SiC, TiC, TiB2 59SiC-41TiB2 and 52SiC-24TiC-24TiB2 T2 - 14th International Colloquium Tribology CY - Ostfildern, Germany DA - 2004-01-13 PY - 2004 AN - OPUS4-11062 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Tribological investigations on siliconcarbonitride ceramics derived from preceramic T2 - 14th International Colloquium Tribology CY - Ostfildern, Germany DA - 2004-01-13 PY - 2004 AN - OPUS4-11057 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Gräber, H.-G. A1 - Klaffke, Dieter T1 - Tribologische Untersuchung zum Verschleißverhalten von keramischen Zahnersatzwerkstoffen KW - Dentalkeramik KW - Bearbeitbarkeit KW - Zwischenmedium KW - pH-Wert KW - Dental ceramic KW - Machinability KW - Liquid media KW - pH-value PY - 2007 SN - 0724-3472 VL - 54 IS - 3 SP - 29 EP - 32 PB - Expert Verlag CY - Renningen AN - OPUS4-15737 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Procop, Mathias A1 - Hübner, Wolfgang A1 - Wäsche, Rolf A1 - Nieland, S. A1 - Ehrmann, O. T1 - Fast Elemental Mapping in Materials Science KW - Electron probe microanalysis KW - EPMA KW - Energy dispersive X-ray spectroscopy KW - EDS KW - Elemental mapping PY - 2002 UR - http://www.microscopy-analysis.com/sites/default/files/magazine_pdfs/mag%20179_2002_Jan_Procop_1.pdf SN - 0958-1952 IS - January SP - 5 EP - 6 PB - Rolston Gordon Comm. CY - Bookham, Surrey AN - OPUS4-7091 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Djahanbakhsh, Mohammad A1 - Österle, Werner T1 - Vergleich von Standard-Modell- und HIP-Simulator-Untersuchungen an Verschleißschutzschichten für Metall-Keramik-Paarungen bei Endoprothesen T2 - 48. Tribologie-Fachtagung "Reibung, Schmierung und Verschleiß - Forschung und praktische Anwendungen" CY - Göttingen, Deutschland DA - 2007-09-24 KW - Reibung KW - Verschleiß KW - Beschichtung KW - HIP-Simulation PY - 2007 SN - 978-3-00-022603-8 VL - 1 SP - 8/1 EP - 8/10 CY - Aachen AN - OPUS4-16102 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Klaffke, Dieter A1 - Wäsche, Rolf A1 - Janakiraman, N. A1 - Aldinger, F. T1 - Tribological characterisation of siliconcarbonitride ceramics derived from preceramic polymers N2 - Amorphous SiCN ceramics were prepared in a laboratory scale as disk shaped specimens with 10 mm diameter and 0.3 mm thickness. The friction and wear behaviour was characterised in gross slip fretting tests under unlubricated conditions at room temperature against steel (100Cr6) and ceramic (Al2O3). Tests with a ball-on-disk contact were performed in laboratory air with different content of water vapour. The results show clearly that the relative humidity has a significant effect on friction and wear behaviour. All tests in dry air lead to higher friction and higher wear rate than in normal air. Improved friction and wear behaviour was observed with increasing pyrolysis temperature up to 1100 °C of the SiCN specimens. This is attributed to increasingly better mechanical properties and higher stiffness of the amorphous network due to the evaporation of gaseous organic species and the formation of free graphite like carbon. KW - Ceramics KW - Preceramic polymer KW - Siliconcarbonitride KW - Friction KW - Wear PY - 2006 DO - https://doi.org/10.1016/j.wear.2005.04.031 SN - 0043-1648 VL - 260 IS - 7-8 SP - 711 EP - 719 PB - Elsevier CY - Amsterdam AN - OPUS4-12302 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Steinborn, Gabriele T1 - Tribological testing of Ca-Ba infiltrated zirconia KW - Friction KW - Wear KW - Ca-Ba fluoride KW - Infiltration KW - Porous zirconia PY - 2005 UR - http://www.om.ugal.ro/AnnalsFasc8Tribology/pdf/2005/9-Annals2005-3-Wasche.pdf SN - 1221-4590 SN - 1220-0824 SP - 53 EP - 59 CY - Gala¸ti AN - OPUS4-12365 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Steinborn, Gabriele A1 - Wäsche, Rolf T1 - Charakterisierung der Dispergiereigenschaften von keramischen nanodispersen Suspensionen mit der Ultraschallspektroskopie N2 - Die Dispergiereigenschaften von verschiedenen nanoskaligen Pulvern mit unterschiedlicher Kornfraktion im Bereich von 10 bis 250 nm werden in verdünnten und konzentrierten keramischen Schlickern mit der Ultraschallspektroskopie untersucht. Alle stabilen Suspensionen weisen im entsprechenden pH-Bereich eine monomodale Partikelgrößenverteilung auf. Durch die Charakterisierung der Suspensionen mit der Ultraschallspektroskopie kann eine verbesserte Bewertung hinsichtlich Homogenität und Agglomeratbildung auch für nanoskalige Pulver erhalten werden. Dies ermöglicht eine bessere Qualitätskontrolle prozessrelevanter Schritte bei der Verarbeitung. KW - Dispergieren KW - Nanopartikel KW - Suspensionen KW - Folie KW - Nanopulver KW - Dispergierung PY - 2007 DO - https://doi.org/10.1002/cite.200600141 SN - 0009-286X SN - 1522-2640 VL - 79 IS - 3 SP - 257 EP - 265 PB - Wiley-VCH Verl. CY - Weinheim AN - OPUS4-16271 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Wäsche, Rolf A1 - Habig, Karl-Heinz T1 - Physikalisch-chemische Grundlagen der Feststoffschmierung - Literaturübersicht - N2 - Die für einen erfolgreichen Einsatz von Festschmierstoffen zur Minderung von Reibung und Verschleiß systembestimmender Parameter wie Last, Geschwindigkeit, Temperatur, umgebende Atmosphäre, Filmbildung und -haltung sowie die Anwendungstechnologien werden dargestellt, ferner Modellvorstellungen zum Verschleißverhalten von Festschmierstoffen im Hinblick auf konkrete Anwendungsfälle diskutiert. T3 - BAM Forschungsberichtreihe - 158 KW - Festschmierstoff KW - Transferschmierung KW - Hohe Temperaturen KW - Graphit KW - Reibung KW - Verschleißmodelle KW - gebundene Filme KW - Synergieeffekte PY - 1989 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-2921 SN - 978-3-88314-889-X SN - 0938-5533 VL - 158 SP - 1 EP - 112 PB - Wirtschaftsverlag NW CY - Bremerhaven AN - OPUS4-292 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Physikalisch-chemische Grundlagen der Festschmierstoffe T2 - TAE Esslingen: Lehrgang: Reibungs- und Verschleißminderung durch Festschmierstoffe CY - Ostfildern, Germany DA - 2008-03-31 PY - 2008 AN - OPUS4-18316 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Grundlagen der Schwingungsverschleißprüfung T2 - TAE Esslingen + GfT: Seminar: Reibung und Verschleiß von Werkstoffen, Bauteilen und Konstruktion CY - Ostfildern, Germany DA - 2008-04-08 PY - 2008 AN - OPUS4-18317 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Verschleißprüfung als Werkzeug für die keramikbezogene Werkstoffentwicklung T2 - Hannover-Messe 2008: Werkstoff-Forum CY - Hanover, Germany DA - 2008-04-25 PY - 2008 AN - OPUS4-18318 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Djahanbakhsh, Mohammad A1 - Österle, Werner T1 - Vergleich von Standard-Modell- und HIP-Simulator-Untersuchungen an Verschleißschutzschichten für Metall-Keramik-Paarungen bei Endoprothesen KW - Beschichtung KW - Reversierender Gleitverschleiß KW - HIP-Simulation KW - Coating KW - Reciprocating sliding KW - HIP-Simulation PY - 2008 SN - 0724-3472 VL - 55 IS - 1 SP - 21 EP - 25 PB - Expert Verlag CY - Renningen AN - OPUS4-17133 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter A1 - Wötting, G. T1 - Tribological behaviour of structural Si-based ceramics in fretting tests at room temperature N2 - The friction and wear behaviour of SiC, Si3N4 and SiC/Si3N4 composite ceramics were investigated with oscillating sliding (gross slip fretting) at room temperature. The influence of counter body material and the humidity of the surrounding air was studied with a ball-on-disc configuration with different ball materials (1000Cr6, Al2O3 SiC and Si3N4). The effect of RH on friction is marginal with exception of SiC (low friction) as counter body material. The wear behaviour, however, is strongly affected by humidity, showing inverse trends for different counter body materials. Consequently, the wear behaviour of a tribo couple can be improved by selecting an adequate mating material. The results reveal the necessity to control RH in tribological tests. For estimation of the performance of tribo couples under varying environmental conditions, a variation of RH is required. In tribo couples with single phase SiC, either as ball or disc, the tribological behaviour of the system is dominated by SiC. The friction behaviour of the composite material is in between the behaviour of the two single phase materials, Si3N4 and SiC, whereas the wear behaviour is very similar to that of single phase Si3N4. KW - Silicon carbide KW - Silicon nitride KW - Particulate composite KW - Fretting KW - Humidity KW - Mating material PY - 2009 DO - https://doi.org/10.1007/s11249-009-9413-y SN - 1023-8883 SN - 1573-2711 VL - 33 IS - 3 SP - 211 EP - 219 PB - Springer Science Business Media B.V. CY - Dordrecht AN - OPUS4-19000 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Paulick, Carl A1 - Steinborn, Gabriele A1 - Richter, V. A1 - Werner, M. T1 - Joining of ceramic components in the green state via LPIM N2 - It has been successfully demonstrated that ceramic materials can be joined in the green state without a second phase by using low pressure injection molded parts. The investigation of the joining interface revealed that a high quality interface can be achieved by carefully adjusting the different manufacturing steps. The use of monomodal particle size distribution in the used powder CT3000SG is inferior to a broader particle size distribution obtained by replacing 33% of the finer alumina powder by coarser CT1200SG. In this way the dewaxing process is significantly improved when the wall thickness of the part exceeds 3 mm. The investigation of the mechanical properties of the joined and sintered parts revealed, that the bending strength of the joined specimens achieved about 80 % of the unjoined, monolithic specimens. T2 - 4th International Conference on Advanced Materials and Processing CY - Hamilton, New Zealand DA - 2006-12-10 KW - Joining KW - Ceramics KW - Green state KW - Interface KW - Bending strength KW - Low pressure injection molding PY - 2005 UR - http://www.scientific.net/3-908453-89-5/207/ SN - 1022-6680 SN - 1662-8985 VL - 29-30 SP - 207 EP - 210 PB - Trans Tech Publ. CY - Zurich AN - OPUS4-19001 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Hartelt, Manfred A1 - Wäsche, Rolf T1 - Volumetrische Verschleiß-Berechnung an gekrümmten Kontaktgeometrien T2 - 50. Tribologie-Fachtagung - Reibung, Schmierung und Verschleiß - Forschung und praktische Anwendung CY - Göttingen, Deutschland DA - 2009-09-21 KW - Verschleißberechnung KW - Calculation of wear volume PY - 2009 SN - 978-3-00-028824-1 VL - I SP - 3-1 - 3-9 CY - Aachen AN - OPUS4-20023 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Woydt, Mathias A1 - Rehmer, Birgit ED - Ewsuk, K. ED - Naito, M. ED - Kakeshita, T. ED - Kirihara, S. ED - Uematsu, K. ED - Abe, H. T1 - Characterization of the tribological interface in low wear Magneli type ceramics N2 - The tribological behaviour under dry sliding conditions of Magneli phase Ti4O7 and e-phase Ti2Cr2O7 with α-alumina as a sliding partner has been characterised at room temperature by oscillating sliding. The mechanical properties as well as Vickers hardness measurements do not reveal big differences between the materials, and 4-point bending strengths are around 200 MPa for both materials. Although the friction coefficients are in the medium range of 0.6 and do not differ much between the materials, the wear behaviour is very different. At room temperature, the wear coefficient of Ti2O7 is strongly dependent on relative humidity, and wear is highest under dry conditions when relative humidity is low as it is typically found for many ceramic materials. Ti2Cr2O7 shows remarkably different wear behaviour with the lowest wear in dry conditions. The measured coefficients of wear at low relative humidity of 4% are more than 2 orders of magnitude lower than those for Ti2O7. T2 - 3rd International conference on characterization and control of interfaces for high quality advanced materials CY - Kurashiki, Japan DA - 2009-09-06 PY - 2009 SN - 978-0-470-90917-1 VL - 219 SP - 111 EP - 116 PB - John Wiley & Sons CY - Hoboken, New Jersey, USA AN - OPUS4-21842 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Springborn, U. A1 - Bewilogua, K. A1 - Keunecke, M. T1 - Wear of carbon nitride coatings under oscillating sliding conditions N2 - An extended study on tribological properties of carbon nitride coatings under oscillating sliding conditions has been carried out. The coatings were prepared by reactive magnetron sputtering with graphite target using nitrogen as reactive gas in an argon/nitrogen atmosphere during the deposition process to deposit carbon nitride, CNx. Coating thickness was about 2 µm. A 200–300 nm thick Ti interlayer was used to enhance adhesion. The nitrogen flow during the deposition was varied to control the amount of nitrogen in the coating. Maximum amount of N-content was about 28 at%, achieved at a maximum N2 flow rate. Other deposition parameters were target to substrate distance, substrate temperature during deposition and bias voltage. The results show a large variation of hardness depending mainly on the nitrogen content and bias voltage. Higher bias voltage produced harder coatings as did lower nitrogen content. The tribological properties were tested unlubricated and lubricated by paraffin oil under gross slip fretting conditions at room temperature against alumina as counter material. Most coatings, but not all, showed a more or less pronounced dependence of wear on relative humidity with wear rates from 10-5 to 10-6 mm3/Nm. The best coatings with regard to a low wear rate and the least dependence upon relative humidity were carbon nitride coatings deposited at elevated substrate temperatures up to 350 °C. The wear resistance of these coatings was increased under the most severe conditions by about one order of magnitude. The results are discussed on the basis of a transfer layer formation. The results show clearly that wear is not significantly correlated to the coating hardness which itself is strongly dependant on the nitrogen content. However, under lubricated conditions with paraffin oil, wear rates were generally very low with wear coefficients at about 10-8 mm3/Nm. KW - Carbon nitride KW - Wear KW - Fretting KW - Dry sliding KW - Paraffin oil PY - 2010 DO - https://doi.org/10.1016/j.wear.2010.08.010 SN - 0043-1648 VL - 269 IS - 11-12 SP - 816 EP - 825 PB - Elsevier CY - Amsterdam AN - OPUS4-22208 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kloß, Heinz A1 - Wäsche, Rolf T1 - Analytical approach for wear prediction of metallic and ceramic materials in tribological applications N2 - Wear mechanisms, as adhesion, abrasion, fatigue and tribochemical wear, are complex in their physical and chemical nature. A theoretical description and prediction of wear are in most cases still far from reality. It is, therefore, important to use test rigs before a practical application of a given material combination under tribological loading. On the other hand, model equations can be helpful for wear description, if a single wear mechanism is dominant. Under oscillating and continuous sliding contact conditions, equations for wear calculation are presented to describe running-in and stationary wear behaviour of metals and ceramics. By using shear energy density, real area of contact, flash temperature, activation energy and numerical simulations with the method of movable cellular automata (MCA), wear data were calculated and compared to experimental laboratory results. KW - Wear KW - Surface temperature KW - Activation energy KW - Simulation KW - Movable cellular automata (MCA) PY - 2009 DO - https://doi.org/10.1016/j.wear.2008.04.034 SN - 0043-1648 VL - 266 IS - 3-4 SP - 476 EP - 481 PB - Elsevier CY - Amsterdam AN - OPUS4-18651 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Influence of deposition parameters on tribological properties of CNx coatings T2 - WOM, 17th International Conference on Wear of Materials CY - Las Vegas, NV, USA DA - 2009-04-19 PY - 2009 AN - OPUS4-19364 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Woydt, Mathias A1 - Wäsche, Rolf T1 - The history of the Stribeck curve and ball bearing steels: The role of Adolf Martens N2 - The historical development on the discoveries of lubrication regimes for lubricated sliding contacts has been reviewed from the very beginning. It was found that the functional relationship between the coefficient of friction and the product of sliding speed and viscosity divided by the normal load well known as the Stribeck curve has been experimentally explored much earlier by Adolf Martens in 1888 long before Richard Stribeck did his pioneering measurements in 1902. However, basic work in this field of experimental hydrodynamics was done and results were published even earlier than that back in 1854 by Gustave A. Hirn, in 1879 by Robert H. Thurston and in 1883 by Beauchamp Tower. KW - Stribeck curve KW - Martens KW - Stribeck KW - Thurston KW - Gümbel KW - Hirn PY - 2010 DO - https://doi.org/10.1016/j.wear.2010.02.015 SN - 0043-1648 VL - 268 IS - 11-12 SP - 1542 EP - 1546 PB - Elsevier CY - Amsterdam AN - OPUS4-21180 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Cruzado, A. A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Urchegui, M.A. A1 - Gómez, X. T1 - Fretting wear of thin steel wires. Part 1: Influence of contact pressure N2 - Different fretting tests of thin steel wires under different conditions (loads, strokes, number of cycles and mean pressures) were performed. The wires used had 0.45 mm in diameter and the material was a cold-drawn eutectoid carbon steel (0.8% C) with a tensile strength over 2800 MPa. The tests were carried out with 90° "crossed cylinders" configuration varying the stroke, normal load and testing time (number of cycles). Afterwards the volumetric wear was obtained using surface profilometry with diamond stylus. With a classical study of the coefficient of wear with respect to the sliding distance, the results show that the wear coefficient increases with normal load and stroke, consequently, for the same sliding distance, the wear produced was higher when the load and/or stroke is increased. In this work, the coefficient of wear is decreasing continuously as the test is running. In order to analyze better the wear behaviour, another method, in which the volumetric wear is compared with respect to the Archard's loading factor, is proposed. As result of this method, two distinctive behaviours were detected; one corresponds to the running-in period with a more aggressive wear behaviour and the second one to the stable steady state period. In all the tests the running-in period was similar with regard to the wear rates but in the stable period the wear rates were increasing with higher loads or strokes. KW - Fretting KW - Wear KW - Wires KW - Contact pressure KW - Unlubricated tests PY - 2010 DO - https://doi.org/10.1016/j.wear.2010.02.017 SN - 0043-1648 VL - 268 IS - 11-12 SP - 1409 EP - 1416 PB - Elsevier CY - Amsterdam AN - OPUS4-21181 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Klaffke, Dieter A1 - Wäsche, Rolf ED - Schulte, K. ED - Kainer, K. T1 - Tribologische Prüfungen als begleitende Maßnahme zur Entwicklung von keramischen Tribowerkstoffen T2 - 12. Tagung "Verbundwerkstoffe und Werkstoffverbunde" CY - Hamburg, Deutschland DA - 1999-10-05 KW - Tribologie KW - Reibung KW - Verschleiß PY - 1999 SN - 3-527-29967-X SP - 423 EP - 428 PB - Wiley-VCH CY - Weinheim AN - OPUS4-723 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Klaffke, Dieter A1 - Hartelt, Manfred A1 - Wäsche, Rolf ED - Bartz, Wilfried J. T1 - Non-Oxide Ceramics as Tribo Materials - Analysis of Wear Mechanisms under Oscillating Sliding Conditions in Various Atmospheres T2 - 12th International Colloquium Tribology CY - Esslingen, Germany DA - 2000-01-11 KW - Tribologie PY - 2000 SN - 3-924813-44-2 VL - 3 SP - 1755 EP - 1763 PB - Techn. Akad. Esslingen CY - Ostfildern AN - OPUS4-848 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Yarim, Rasim A1 - Klaffke, Dieter A1 - Hartelt, Manfred ED - Bartz, Wilfried J. T1 - Oscillating Sliding Wear Behaviour of SiC, TiC, TiB2, 59SiC-41TiB2 and 52SiC-24TiC-24TiB2 Materials up to 750°C in Air T2 - 14th International Colloquium Tribology, Tribology and Lubrication Engineering CY - Stuttgart, Deutschland DA - 2004-01-13 PY - 2004 SN - 3-924813-54-X VL - II SP - 1039 EP - 1045 PB - Techn. Akad. Esslingen CY - Ostfildern AN - OPUS4-3057 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Klaffke, Dieter A1 - Wäsche, Rolf A1 - Wötting, G. ED - Bartz, Wilfried J. T1 - Tribological Characterisation of a Sl3N4-TiN Composite Ceramic in Fretting Tests at Room Temperature T2 - 14th International Colloquium Tribology, Tribology and Lubrication Engineering CY - Stuttgart, Germany DA - 2004-01-13 PY - 2004 SN - 3-924813-54-X VL - III SP - 1413 EP - 1420 PB - Techn. Akad. Esslingen CY - Ostfildern AN - OPUS4-3058 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Klaffke, Dieter A1 - Wäsche, Rolf A1 - Aldinger, F. A1 - Janakiraman, N. ED - Bartz, Wilfried J. T1 - Tribological investigations on siliconcarbonitride ceramics derived from preceramic polymers T2 - 14th International Colloquium Tribology, Tribology and Lubrication Engineering CY - Stuttgart, Deutschland DA - 2004-01-13 PY - 2004 SN - 3-924813-54-X VL - 3 SP - 1403 EP - 1412 PB - Techn. Akad. Esslingen CY - Ostfildern AN - OPUS4-3059 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Oscillating Sliding Wear Behaviour of SiC, TiC, TiB2, 59SiC-41TiB2 and 52SiC-24TiC-24TiB2 Materials up to 750°C in Air T2 - 14th International Colloquium Tribology, Tribology and Lubrication Engineering CY - Ostfildern, Germany DA - 2004-01-13 PY - 2004 AN - OPUS4-3076 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Gas pressure sintering of SiC-TiC-TiB2 ceramic composites T2 - 8. ECerS Conference of the European Ceramic Society CY - Istanbul, Turkey DA - 2003-06-29 PY - 2003 AN - OPUS4-5354 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Laser induced thermal shock testing on Si3N4 GS44 and alumina Heratape T2 - Research and Development on Advanced Materials for Transportation Applications CY - Oakland, CA, USA DA - 2003-10-22 PY - 2003 AN - OPUS4-5361 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wäsche, Rolf T1 - Werkstoffe der hochleistungskeramik - Herstellung und Charakterisierung an der BAM T2 - Seminar für Werkstofftechnik im FB 15 der Universität Kassel CY - Kassel, Germany DA - 2003-11-17 PY - 2003 AN - OPUS4-5362 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Klaffke, Dieter ED - Christophe Donnet, ED - Erdemir, Ali T1 - Tribology of DLC Films Under Fretting Conditions KW - DLC KW - Oscillation sliding KW - Counterbody KW - Relative humidity KW - Temperature KW - Lubrication PY - 2008 SN - 978-0-387-30264-5 SP - 362 EP - 382 PB - Springer Science + Business Media AN - OPUS4-18571 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Hartelt, Manfred A1 - Weihnacht, V. T1 - Influence of counterbody material on wear of ta-C coatings under fretting conditions at elevated temperatures N2 - The high temperature tribological performance of tetrahedral amorphous carbon coatings has been analyzed at elevated temperatures up to 250 °C in air against three different counterbody materials-steel 100Cr6, a-alumina and silicon nitride. The results show that the counterbody material influences the friction and wear behavior and therefore coating life time strongly. This effect is well known for these coatings at room temperature under dry environmental conditions, equivalent to conditions above 100 °C when water molecules desorb from the surface. However, the sharp difference in tribological performance between silicon nitride on the one hand and alumina and steel on the other hand cannot be understood in this context. Analyzing the friction behavior during the running-in phase, it is evident that only alumina and steel form a stable interface with constant low friction and relatively low wear rates. Silicon nitride forms an unstable interface with fluctuating COF and relatively high wear rates due to its own inherent tendency to tribo-oxidation. KW - Fretting KW - Hard carbon coatings KW - ta-C KW - High temperature KW - Counterbody influence PY - 2009 DO - https://doi.org/10.1016/j.wear.2009.08.041 SN - 0043-1648 VL - 267 IS - 12 SP - 2208 EP - 2215 PB - Elsevier CY - Amsterdam AN - OPUS4-20344 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Urchegui, M.A. A1 - Hartelt, Manfred A1 - Wäsche, Rolf A1 - Gómez, X. T1 - Analysis of different strategies to reduce fretting wear in thin steel roping wires N2 - After having checked in a previous study the influence of stroke and normal load in laboratory fretting tests accomplished with thin steel roping wires, in this paper the effect of the contact pressure (test configuration), environmental conditions (relative humidity) and reduction of the friction coefficient (lubricants) on the wear behaviour were analysed. The wires were 0.45 mm in diameter and the material was a cold-drawn eutectoid carbon steel (0.8% C) with a Tensile Strength over 2800 MPa. The tests were performed on an oscillating test rig and the volumetric wear of both specimens of the tribocouple was determined separately from three-dimensional topographies of the wear scars acquired by means of a confocal profiler, and a calculation algorithm developed in using MATLAB®. The strong effect of humidity and lubrication on wear behaviour was proved, whereas a slight effect of contact pressure was derived. KW - Wires KW - Fretting test KW - Contact pressure PY - 2008 DO - https://doi.org/10.1002/tt.52 SN - 1354-4063 SN - 1557-685X VL - 14 IS - 1 SP - 43 EP - 57 PB - Coppin CY - Deal AN - OPUS4-16677 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -