TY - GEN A1 - Neuhaus, B. A1 - Allspach, A. A1 - Bartsch, P. A1 - Burckhardt, D. A1 - Coleman, C.O. A1 - Fries, I. A1 - Fuchs, R. A1 - Gudo, M. A1 - Kotrba, M. A1 - Mentjes, M. A1 - Moore, S. A1 - Neumann, D. A1 - Oberer, C. A1 - Potthast, A. A1 - Riedel, Juliane A1 - Rudolf, R. A1 - Schnalke, T. A1 - Schönbohm, D. A1 - Schuda, M. A1 - van Dam, A. A1 - Widulin, N. T1 - KUR-Projekt: Aufbau und öffentliche Kommunikation eines wissenschafts-basierten Sammlungsmanagements für naturkundliche Nasssammlungen N2 - Im Rahmen eines von der Kulturstiftung des Bundes und der Kulturstiftung der Länder geförderten Projektes zum Erhalt naturkundlicher Nasssammlungen wurden 1) der Zustand der Sammlungen bewertet (Profiling; Analyse der Vergällungsmittel), 2) über Workshops Expertenwissen in das Projekt gebracht, 3) neue archivbeständige Materialien und Managementmaßnahmen eingeführt (Borosilikat-Gläser und - Röhrchen, Augenwatte, Tefloneinlagen, Japanpapier, archivbeständige Kleber und Papier, Etikettenaufbewahrung; digitales Dichtemessgerät, Alcomon-Indikator, Kontrollintervalle), 4) Erhaltungsmaßnahmen zur langfristigen Konservierung in großem Umfange durchgeführt (Messen der Alkoholkonzentration, Umsetzen von Präparaten in geeignetere Gefäße, Wiederverschluss von Schaugläsern) und 5) Erfahrungen und Diskussionsergebnisse zusammengestellt, nicht ohne auf Wissenslücken und wünschenswerte Forschungsaspekte hinzuweisen. Das Projekt profitierte besonders von der Expertise aus den Materialwissenschaften und der Papierrestaurierung. Das Museum für Naturkunde Berlin kooperierte eng mit dem Berliner Medizinhistorischen Museum der Charité, der Zoologischen Staatssammlung München und dem Forschungsinstitut Senckenberg in Frankfurt. Letzteres Museum führte ein eigenes, themenverwandtes KUR-Projekt Restauration der Sammlungen 'Vergleichende Anatomie, Embryologie und Histologie' des Naturmuseums Senckenberg durch. KW - Nasssammlung KW - Ethanol KW - Vergällungsmittel PY - 2012 DO - https://doi.org/10.5165/hawk-hhg/epublication/44 SP - 1 EP - 32 AN - OPUS4-25491 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Waiblinger, H. U. A1 - Bartsch, D. A1 - Brockmeyer, J. A1 - Bruenen-Nieweler, C. A1 - Busch, U. A1 - Haase, I. A1 - Hahn, A. A1 - Haarmann, M. A1 - Hauser, W. A1 - Huber, I. A1 - Jany, K. D. A1 - Kirmse, N. A1 - Lindeke, S. A1 - Neumann, K. A1 - Naumann, H. A1 - Paschke, A. A1 - Pietsch, K. A1 - Pöpping, B. A1 - Reiting, R. A1 - Schroeder, U. A1 - Schwägele, F. A1 - Weller, Michael G. A1 - Zagon, J. T1 - Methods of differentiating animal species in foods – Status quo N2 - Work on standardising methods in the field of animal species differentiation has been intensified in Germany in recent years, not least due to the horsemeat scandal in 2013. Even though there are now hardly ever any positive findings any more in examinations to detect horse adulterations in foods such as lasagne, animal species differentiation altogether ranks high in detecting adulteration of foods. This article therefore summarises the current status of analytical techniques used in Germany with standardisation at German level. It has been established by the working group “Biochemical and Molecular Biological Analytics” of the Lebensmittelchemische Gesellschaft (Food Chemistry Society within the German Chemical Society) with support of experts in the working group “Molecular biology techniques for differentiating plant and animal species” (§ 64 of the German Food and Feed Code – LFGB) and the “Immunology and molecular biology” task force of the food hygiene and Food of animal origin working group (ALTS), both from Germany. KW - Animal species differentiation KW - Fish species KW - PCR KW - Standardisation KW - DNA chip KW - Multiplex methods KW - Digital PCR KW - ELISA methods KW - Immunoassays KW - LC-MS/MS KW - Reference materials KW - Microarrays KW - LAMP KW - Interlaboratory studies PY - 2017 SN - 0179-2415 VL - 97 IS - 1 SP - 50 EP - 55 PB - Deutscher Fachverlag GmbH CY - Frankfurt AN - OPUS4-39264 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Waiblinger, H. U. A1 - Bartsch, D. A1 - Brockmeyer, J. A1 - Bruenen-Nieweler, C. A1 - Busch, U. A1 - Haase, I. A1 - Hahn, A. A1 - Haarmann, M. A1 - Hauser, W. A1 - Huber, I. A1 - Jany, K. D. A1 - Kirmse, N. A1 - Lindeke, S. A1 - Neumann, K. A1 - Naumann, H. A1 - Paschke, A. A1 - Pietsch, K. A1 - Pöpping, B. A1 - Reiting, R. A1 - Schroeder, U. A1 - Schwägele, F. A1 - Weller, Michael G. A1 - Zagon, J. T1 - Methods of differentiating animal species in food - Status quo N2 - In the field of animal species differentiation, work on standardizing methods has been intensified in Germany in recent years, not least due to the horsemeat scandal in 2013. Even though there are now hardly ever any positive findings anymore in examinations to detect horse adulterations in foods such as lasagne, animal species differentiation altogether ranks high in detecting adulteration of foods. This article, therefore, summarises the current status of analytical techniques used in Germany with standardization at German level. It has been established by the working group "Biochemical and Molecular Biological Analytics" of the Lebensmittelchemische Gesellschaft (Food Chemistry Society within the German Chemical Society) with support of experts in the working group “Molecular biology techniques for differentiating plant and animal species" (§64 of the German Food and Feed Code - LFGB) and the "Immunology and molecular biology" task force of the food hygiene and food of animal origin working group (ALTS), both from Germany. KW - Animal species differentiation KW - Fish species KW - PCR KW - ELISA KW - LC-MS/MS PY - 2017 IS - 3 SP - 29 EP - 36 PB - Deutscher Fachverlag GmbH CY - Frankfurt am Main AN - OPUS4-43485 LA - mul AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Neumann, Patrick P. A1 - Bartholmai, Matthias A1 - Lazik, D. T1 - Near real-time reconstruction of 2D soil gas distribution from a regular network of linear gas sensors N2 - A monitoring method is introduced that creates, in near real-time, two-dimensional (2D) maps of the soil gas distribution. The method combines linear gas sensing technology for in-situ monitoring of gases in soil with the mapping capabilities of Computed Tomography (CT) to reconstruct spatial and temporal resolved gas distribution maps. A weighted iterative algebraic reconstruction method based on Maximum Likelihood with Expectation Maximization (MLEM) in combination with a source-by-source reconstruction approach is introduced that works with a sparse setup of orthogonally-aligned linear gas sensors. The reconstruction method successfully reduces artifact production, especially when multiple gas sources are present, allowing the discrimination between true and non-existing so-called ghost source locations. A first experimental test indicates the high potential of the proposed method for, e.g., rapid gas leak localization. T2 - IEEE Sensors 2015 CY - Busan, South Korea DA - 01.11.2015 KW - Distributed linear sensor KW - Membrane-based gas sensing KW - Subsurface monitoring KW - Gas storage areas KW - Computed tomography PY - 2015 SN - 978-1-4799-8202-8 SN - 1930-0395 SP - 1550 EP - 1553 PB - IEEE AN - OPUS4-34849 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Petrov, Sergej A1 - Neumann, Patrick P. A1 - Werner, Klaus-Dieter A1 - Wosniok, Aleksander A1 - Lazik, D. A1 - Bartholmai, Matthias ED - Nicoletto, G. ED - Pastrama, S.D. ED - Emri, I. T1 - Concept for investigating mechanical and thermal impacts on distributed subsurface gas monitoring N2 - A multifunctional sensor in line shape was developed and introduced in previous work for measuring of gas concentrations, temperature change, and strain. A current field study focuses on a spatially distributed monitoring of subsurface CO 2 gas storage sites in near real time. Mechanical impacts, e.g., caused by construction work, denudation, and seismic activity, can affect the integrity of underground gas storage sites. Thermal or moisture impacts, e.g., caused by weather conditions, can influence the gas Distribution behavior. In this paper, we briefly describe the setup of a CO 2 injection soil test field. This setup contains actuating elements for the investigation of mechanical and thermal impacts on distributed subsurface gas monitoring. A concept is given for evaluating these impacts and first experimental results are presented. T2 - 32nd DANUBIA ADRIA SYMPOSIUM on Advances in Experimental Mechanics CY - Starý Smokovec, Slovakia DA - 22.09.2015 KW - Linear sensor KW - Distributed sensor KW - Monitoring of CO 2 KW - Subsurface monitoring KW - Gas storage areas KW - Membrane-based gas sensing KW - Fibre optical sensing PY - 2016 DO - https://doi.org/10.1016/j.matpr.2016.03.060 SN - 2214-7853 VL - 3 IS - 4 SP - 1124 EP - 1128 PB - Elsevier Ltd. AN - OPUS4-35688 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Neumann, Patrick P. A1 - Ebert, S. A1 - Lazik, D. A1 - Bartholmai, Matthias ED - Nicoletto, G. ED - Dan Pastrama, S. ED - Emri, I. T1 - Inverse calibration routine for linear soil gas sensors N2 - Gas sensors in linear form based on the measuring principle of gas selective permeability through a membrane were developed and introduced for the detection and quantification of gas concentrations. A current field study focuses on measuring CO2 concentrations for a spatially distributed monitoring of subsurface CO2 gas storage sites in near real time. A 400 m² test site and a corresponding laboratory system were built up to characterize, validate, and optimize the sensor. A calibration routine was developed, which can be applied subsequently to underground installation. First measurement results indicate the potential of the method. T2 - 32nd Danubia Adria Symposium on Advances in Experimental Mechanics CY - Starý Smokovec, Slovakia DA - 22.09.2015 KW - Linear sensor KW - Distributed sensor KW - Subsurface monitoring KW - Gas storage areas KW - Membrane-based gas sensing KW - Calibration PY - 2016 UR - http://www.sciencedirect.com/science/article/pii/S221478531600256X DO - https://doi.org/doi:10.1016/j.matpr.2016.03.051 SN - 2214-7853 VL - 3 IS - 4 SP - 1074 EP - 1078 PB - Elsevier Ltd. AN - OPUS4-35633 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Neumann, Patrick P. A1 - Lazik, D. A1 - Bartholmai, Matthias T1 - Tomographic reconstruction of soil gas distribution from multiple gas sources based on sparse sampling N2 - A monitoring method is introduced that creates twodimensional (2D) maps of the soil gas distribution. The method combines linear gas sensing technology for in-situ monitoring of gases in soil with the mapping capabilities of Computed Tomography (CT) to reconstruct spatial and temporal resolved gas distribution maps. A weighted iterative algebraic reconstruction method based on Maximum Likelihood with Expectation Maximization (MLEM) in combination with a source-by-source reconstruction approach is introduced that works with a sparse setup of orthogonally-aligned linear gas sensors. The reconstruction method successfully reduces artifact production, especially when multiple gas sources are present, allowing the discrimination between true and non-existing so-called ghost source locations. Experimental validation by controlled field experiments indicates the high potential of the proposed method for rapid gas leak localization and quantification with respect to Pipeline or underground gas storage issues. KW - Computed tomography KW - Gas distribution mapping and gas source localization KW - Discrimination of multiple gas sources KW - Distributed linear sensor KW - Membrane-based gas sensing KW - Subsurface monitoring KW - Gas storage areas PY - 2016 DO - https://doi.org/10.1109/JSEN.2016.2545103 SN - 1530-437X VL - 16 IS - 11 SP - 4501 EP - 4508 PB - IEEE - Inst. Electrical Electronics Engineers Inc CY - Hoes Lane, NJ, USA AN - OPUS4-36228 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Lazik, D. A1 - Ebert, S. A1 - Neumann, Patrick P. A1 - Bartholmai, Matthias T1 - Characteristic length measurement of a subsurface gas anomaly - A monitoring approach for heterogeneous flow path distributions N2 - Geogenic gases from natural sources, carbon dioxide (CO2) from a geological repository (carbon capture and storage - CCS) or a leaking gas pipeline can present serious risks in industrial and urban areas. To extend the lead time for risk treatment in such critical regions, reliable detection of gases within the shallow subsurface is required to observe critical gas accumulations before degassing into the atmosphere. A near real-time monitoring approach is introduced to determine the volumetric expansion of a leakinggas in the subsurface. Considering the pressure relaxation with the ambient air pressure, the approach enables the forecasting of the final size of a pressurized gas body in terms of characteristic lengths. According to theoretical basics, such a characteristic length, which enables us to perform a gas (safety) measurement based on a purely geometrical measure, behaves independently of subsurface properties,i.e., it enables a reliable quantification of the escaping gas irrespective of its heterogeneous or changingflow path distribution. A field test for a 10 l/min pinhole leakage injected into a 10 m long, 0.4 m wide, 0.95 m deep soil-filled trench that was equipped with linear sensors shows the lateral-vertical volumetric gas expansion along these sensors, and demonstrates the applicability of the characteristic length approach. KW - Monitoring KW - Carbon capture and storage KW - Leakage KW - Quantification KW - Subsurface KW - CO2 PY - 2016 DO - https://doi.org/10.1016/j.ijggc.2016.02.008 SN - 1750-5836 VL - 2016 IS - 47 SP - 330 EP - 341 PB - Elsevier B.V. AN - OPUS4-35425 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Neumann, Patrick P. A1 - Lazik, D. A1 - Bartholmai, Matthias T1 - Leak detection with linear soil gas sensors under field conditions - First experiences running a new measurement technique N2 - A 400 m² soil test field with gas injection system was built up, which enables an experimental validation of linear gas sensors for specific applications and gases in an application-relevant scale. Several injection and soil watering experiments with carbon dioxide (CO2) at different days with varying boundary conditions were performed indicating the potential of the method for, e.g., rapid leakage detection with respect to Carbon Capture and Storage (CCS) issues. T2 - IEEE Sensors 2016 CY - Orlando, FL, USA DA - 30.10.2016 KW - Soil test field KW - Membrane-based linear gas sensor KW - Leak detection KW - Field conditions PY - 2016 SN - 978-1-4799-8287-5 SN - 1930-0395 SP - B-3-65, 757 EP - 759 PB - IEEE AN - OPUS4-38244 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Neumann, Patrick P. A1 - Werner, Klaus-Dieter A1 - Petrov, Sergej A1 - Bartholmai, Matthias A1 - Lazik, D. ED - Puente León, F. ED - Zagar, B. T1 - Aufbau eines großflächigen Testfeldes für verteilte Bodengassensorik und Untersuchung einer Monitoringmethode basierend auf Tomographie T1 - Setup of a large-scale test field for distributed soil gas sensors and testing of a monitoring method based on tomography N2 - A 400 m² soil test field with gas injection system was built up for the purpose of large-scale validation, optimization, and characterization of a novel comprehensive monitoring method for underground gas storage areas. The method combines gas sensing technology with linear form factor for in-situ monitoring of gases in soil with the mapping capabilities of Computed Tomography (CT) to reconstruct time-series of gas distribution maps based on samples of orthogonally-aligned linear gas sensors. Several injection experiments with carbon dioxide (CO2) at different days with varying boundary conditions indicates the potential of the method for, e.g., rapid leakage detection with respect to Carbon Capture and Storage (CCS) issues. N2 - Zur Validierung, Optimierung und praxisnahen Demonstration eines flächendeckenden Monitoringverfahrens für Untergrundgasspeichern wurde ein 400 m² großes Testfeld mit Gasinjektionssystem auf dem BAM Testgelände Technische Sicherheit aufgebaut. Die Methode kombiniert verteilte, linienförmige Gassensorik für die In-situ-Überwachung von Gasen im Boden mit den Mapping-Fähigkeiten der Computertomographie (CT). Auf Basis von orthogonal zueinander ausgerichteten linearen Gassensoren können mit diesem Verfahren so Zeitreihen der Gasverteilung rekonstruiert werden. Experimente mit Kohlendioxid (CO2) zeigen das Potential des Verfahrens zur schnellen Lokalisierung von Leckagen auf. KW - Soil test field KW - Distributed linear sensor KW - Membrane-based gas sensing KW - Subsurface monitoring KW - Gas storage areas KW - Computed tomography PY - 2016 DO - https://doi.org/10.1515/teme-2016-0015 SN - 2196-7113 SN - 0171-8096 VL - 83 IS - 10 SP - 606 EP - 615 PB - Walter de Gruyter GmbH CY - Berlin, Deutschland AN - OPUS4-37653 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Neumann, Patrick P. A1 - Lazik, D. A1 - Bartholmai, Matthias ED - Aulova, Alexandra ED - Rogelj Ritonja, A. ED - Emri, I. T1 - Validation of membrane-based linear soil gas sensors – results from repetitive CO2 injection experiments performed in the field N2 - This work presents first results from repetitive CO2 injection experiments performed on a recently built-up 400 m² soil test field with gas injection system. The test field contains 48 membrane-based linear gas sensors that were installed in several depths of the test field. Sensors for measuring meteorological parameters (e.g., wind / rain) and the parameters soil temperature, soil moisture, and groundwater level were installed additionally. T2 - 33rd Danubia- Adria Symposium on Advances in Experimental Mechanics CY - Portorož, Slovenia DA - 20.09.2016 KW - Distributed linear sensor KW - Gas distribution mapping and gas source localization KW - Gas storage areas KW - Membrane-based gas sensing KW - Subsurface monitoring PY - 2016 SN - 978-961-94081-0-0 SP - 174 EP - 175 CY - Ljubljana AN - OPUS4-37644 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Moraleja, I. A1 - Mena, M. L. A1 - Lázaro, A. A1 - Neumann, B. A1 - Tejedor, A. A1 - Jakubowski, Norbert A1 - Gómez-Gómez, M. M. A1 - Esteban-Fernández, D. T1 - An approach for quantification of platinum distribution in tissues by LA-ICP-MS imaging using isotope dilution analysis N2 - Laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) has been revealed as a convenient technique for trace elemental imaging in tissue sections, providing elemental 2D distribution at a quantitative level. For quantification purposes, in the last years several approaches have been proposed in the literature such as the use of CRMs or matrix matched standards. The use of Isotope Dilution (ID) for quantification by LA-ICP-MS has been also described, being mainly useful for bulk analysis but not feasible for spatial measurements so far. In this work, a quantification method based on ID analysis was developed by printing isotope-enriched inks onto kidney slices from rats treated with antitumoral Pt-based drugs using a commercial ink-jet device, in order to perform an elemental quantification in different areas from bio-images. For the ID experiments ¹⁹⁴Pt enriched platinum was used. The methodology was validated by deposition of natural Pt standard droplets with a known amount of Pt onto the surface of a control tissue, where could be quantified even 50 pg of Pt, with recoveries higher than 90%. The amount of Pt present in the whole kidney slices was quantified for cisplatin, carboplatin and oxaliplatin-treated rats. The results obtained were in accordance with those previously reported. The amount of Pt distributed between the medullar and cortical areas was also quantified, observing different behavior for the three drugs. KW - Isotopic dilution KW - LA-ICP-MS KW - Quantification KW - Imaging KW - Kidney KW - Pt-based drugs PY - 2018 DO - https://doi.org/10.1016/j.talanta.2017.09.031 SN - 0039-9140 VL - 178 SP - 166 EP - 171 PB - Elsevier AN - OPUS4-43627 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schaepe, Kaija A1 - R. Bhandari, D. A1 - Werner, J. A1 - Henss, A. A1 - Pirkl, A. A1 - Kleine-Boymann, M. A1 - Rohnke, M. A1 - Wenisch, S. A1 - Neumann, E. A1 - Janek, J. A1 - Spengler, B. T1 - Imaging of lipids in native human bone sections using TOF-secondary ion mass spectrometry, atmospheric pressure scanning microprobe matrix-assisted laser desorption/ionization orbitrap mass spectrometry, and orbitrap-secondary ion mass spectrometry N2 - A method is described for high-resolution label-free molecular imaging of human bone tissue. To preserve the lipid content and the heterogeneous structure of osseous tissue, 4 μm thick human bone sections were prepared via cryoembedding and tape-assisted cryosectioning, circumventing the application of organic solvents and a decalcification step. A protocol for comparative mass spectrometry imaging (MSI) on the same section was established for initial analysis with time-of-flight secondary ion mass spectrometry (TOF-SIMS) at a lateral resolution of 10 μm to <500 nm, followed by atmospheric pressure scanning microprobe matrix-assisted laser desorption/ionization (AP-SMALDI) Orbitrap MSI at a lateral resolution of 10 μm. This procedure ultimately enabled MSI of lipids, providing the lateral localization of major lipid classes such as glycero-, glycerophospho-, and sphingolipids. Additionally, the applicability of the recently emerged Orbitrap-TOF-SIMS hybrid system was exemplarily examined and compared to the before-mentioned MSI methods. KW - ToF-SIMS KW - MALDI KW - Mass spectrometry imaging KW - Lipids KW - Osteoporosis KW - Bone KW - Surface analysis PY - 2018 UR - https://pubs.acs.org/doi/10.1021/acs.analchem.8b00892 DO - https://doi.org/10.1021/acs.analchem.8b00892 SN - 0003-2700 SN - 1520-6882 VL - 90 IS - 15 SP - 8856 EP - 8864 PB - ACS Publ. CY - Washington, DC AN - OPUS4-45730 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Budnik, J. A1 - Betz, T. A1 - Fromm, A. A1 - Gerdes, A. A1 - Gerlach, J. A1 - Götz, M. A1 - Hintzen, W. A1 - Hüttl, R. A1 - Kämpfer, W. A1 - König, A. A1 - Kühner, S. A1 - Lohaus, L. A1 - Meng, Birgit A1 - Neumann, T. A1 - Patzer, M. A1 - Schaab, A. A1 - Schauerte, J. A1 - Siebert, B. A1 - Stephan, D. A1 - Tebbe, H. A1 - Wagner, J.-P. ED - Siebert, B. T1 - Chemischer Angriff auf Betonbauwerke - Bewertung des Angriffsgrads und geeignete Schutzprinzipien N2 - In verschiedenen Bereichen des Betonbaus ist Beton einem chemischen Angriff von außen ausgesetzt, der die Dauerhaftigkeit des betreffenden Bauteils bzw. des gesamten Bauwerks beeinträchtigen kann. Für einen chemischen Angriff in natürlichen Böden und Grundwässern bestehen normative Vorgaben in DIN 4030-1 [R10] bzw. DIN 1045-2 [R19], um den Angriffsgrad anhand der Art und Konzentration der angreifenden Stoffe in Expositionsklassen XA1 (schwach angreifend) bis XA3 (stark angreifend) einzustufen. Hinsichtlich weiterer maßgeblicher Einflussfaktoren wird an dieser Stelle nicht näher differenziert, ob und inwieweit die Regelungen für Böden und Grundwässer auch auf andere Bereiche mit chemischem Angriff auf Beton zu übertragen sind, ist stets im Einzelfall zu überprüfen. Ebenfalls sind die zu treffenden Maßnahmen über die Vorgaben der DIN EN 206-1/DIN 1045-2 [R19] hinaus anwendungsspezifisch festzulegen. Der Hauptausschuss Baustofftechnik (HABT) des DBV hat daher den Arbeitskreis "Chemischer Angriff auf Beton" beauftragt, dieses Merkblatt zu erarbeiten, das Hilfestellung bei der Bewertung einer projektspezifischen chemischen Angriffssituation auf Beton sowie bei der Planung und Ausführung von Schutzprinzipien leisten soll. KW - Beton KW - Betonangriff KW - Dauerhaftigkeit KW - Säureangriff KW - Sulfatangriff PY - 2014 SP - 1 EP - 101 PB - Eigenverlag Deutscher Beton- und Bautechnik-Verein e. V. CY - Berlin AN - OPUS4-44662 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Budnik, J. A1 - Betz, T. A1 - Brameshuber, W. A1 - Fromm, A. A1 - Gerdes, A. A1 - Gerlach, J. A1 - Götz, M. A1 - Hart, R. A1 - Heese, C. A1 - Hintzen, W. A1 - Hüttl, R. A1 - Kämpfer, W. A1 - König, A. A1 - Kühner, S. A1 - Lohaus, L. A1 - Meng, Birgit A1 - Neumann, T. A1 - Remus, R. A1 - Schaab, A. A1 - Schäffel, P. A1 - Schauerte, J. A1 - Schönborn, A. A1 - Siebert, B. A1 - Stephan, D. A1 - Tebbe, H. A1 - Wagner, J.-P. ED - Siebert, B. T1 - Chemischer Angriff auf Beton - Empfehlungen zur Prüfung und Bewertung N2 - ln den letzten Jahren wurden diverse Prüfverfahren und Methoden entwickelt, um die Leistungsfähigkeit von Beton bzw. Bindemittel hinsichtlich des Widerstands gegenüber betonaggressiven Einwirkungen beurteilen zu können. Ein wesentliches Ziel von Prüfverfahren zur Beurteilung der Dauerhaftigkeit von Baustoffen ist, die im Laufe der Nutzungsdauer zu erwartenden Einwirkungen auf den Baustoff realitätsnah abzubilden. Dazu sind die Prüfparameter auf die im jeweiligen Anwendungsbereich vorherrschenden Umgebungs- und Randbedingungen anzupassen. Daneben sind auch die Bewertungskriterien individuell unter Berücksichtigung der im Einzelfall geforderten Nutzungsdauer eines Bauwerks festzulegen. Eine systematische Zuordnung von adäquaten Prüfverfahren bzw. Prüfparametem und Bewertungskriterien für die verschiedenen Anwendungsbereiche im Betonbau, in denen betonaggressive Einwirkungen auftreten, ist mit Ausnahme von Einzelfällen bislang nicht vorhanden. Daneben stellt sich in der Praxis immer wieder das Problem, das Angriffspotenzial der Umgebung eines Bauwerks (prüftechnisch) zu erfassen und zu bewerten. Der Hauptausschuss Baustofftechnik des DBV hat daher den Arbeitskreis „Chemischer Angriff auf Beton“ beauftragt, dieses Merkblatt zu erarbeiten, das auf Basis von einschlägigen Erfahrungen der Baupraxis und wissenschaftlichen Erkenntnissen Grundsätze und bewährte Methoden zur Beurteilung der Einwirkungs- und Widerstandsseite beim chemischen Angriff auf Beton aufzeigt und diesbezüglich Hinweise für verschiedene Anwendungsbereiche im Betonbau liefert. KW - Beton KW - Betonangriff KW - Dauerhaftigkeit KW - Säureangriff PY - 2017 SP - 1 EP - 65 PB - Eigenverlag Deutscher Beton- und Bautechnik-Verein e. V. CY - Berlin AN - OPUS4-44663 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bartholmai, Matthias A1 - Neumann, Patrick P. A1 - Werner, Klaus-Dieter A1 - Ebert, Sebastian A1 - Lazik, D. T1 - Linear sensor for areal subsurface gas monitoring - calibration routine and validation experiments N2 - Membrane based linear gas sensors and fiber optical sensors feature similar geometries and complement each other in quantities to be measured. To the author's best knowledge, it is the first time that these sensors are combined to a multifunctional sensor for distributed measuring of gas concentrations, temperature, and strain. Objective is a comprehensive monitoring of underground gas storage areas. In the presented project a 400 m² test site and a corresponding laboratory system were just built up to characterize, validate, and optimize the combined sensor. Application of the sensor lines in a grid structure should enable spatial resolution of the measurement data and early detection of relevant events, as gas leakage, temperature change, or mechanical impact. A Calibration routine was developed which can be applied subsequent to underground installation. First measurement results indicate the potential of the method, with regard to highly topical energy transport and storage issues. T2 - IEEE Sensors 2014 conference CY - Valencia, Spain DA - 02.11.2014 KW - Linear sensor KW - Distributed sensor KW - Monitoring of CO2 KW - Subsurface monitoring KW - Gas storage areas KW - Membrane-based gas sensing KW - Fibre optical sensing PY - 2014 SN - 978-1-4799-0161-6 DO - https://doi.org/10.1109/ICSENS.2014.6985157 SP - 942 EP - 945 AN - OPUS4-32083 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bartholmai, Matthias A1 - Ebert, Sebastian A1 - Neumann, Patrick P. A1 - Noske, Reinhard A1 - Rehak, W. A1 - Lazik, D. T1 - Linear gas sensor for methane based on a selectively permeable membrane N2 - In preliminary work, gas sensors in linear form based on the measuring principle of gas selective permeability through a membrane were developed and introduced for the detection and quantification of gas concentrations. In this study, first experimental results are presented for adapting the technology for measuring methane (CH4). A material with suitable selective permeability was identified and utilized in a sensor setup containing the gas selective membrane and a reference membrane, both integrated in a measuring cell, to which a gas stream with defined CH4 concentrations was applied. The results prove the sensor's capability for measuring methane and indicate further application potential of the method, e.g., as a robust field monitoring technology, since CH4 is the major component of natural gas, town gas, and fracking gas. T2 - AMA Conferences 2015 with SENSOR and IRS2 CY - Nuremberg, Germany DA - 19.05.2015 KW - Selective permeability KW - Quantification of gas concentrations KW - Spatially distributed monitoring KW - Gas storage sites KW - Methane measuring PY - 2015 SN - 978-3-9813484-8-4 DO - https://doi.org/10.5162/sensor2015/P8.1 SP - 833 EP - 835 AN - OPUS4-33263 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lazik, D. A1 - Ebert, Sebastian A1 - Neumann, Patrick P. A1 - Bartholmai, Matthias T1 - Pipeline monitoring with linear gas sensors N2 - Comprehensive monitoring of pipelines over their full length is technically difficult and expensive. Considering a cost-benefit ratio it is reasonable to implement monitoring solutions in pipeline segments, which bear a high risk potential, like residential areas, construction sites, slopes, street or river crossings. Still such segments can measure up to several hundred meters in length, demanding for monitoring solutions that extend along such distances and enable fast response. Point wise sensing and periodical surveillance have clear drawbacks, particularly regarding early damage detection. Fibre optic sensors enable distributed sensing of temperature and strain, but they offer very limited possibilities for measuring gas concentrations. Linear membrane-based gas sensors enable the monitoring of gas concentrations alongside a pipeline. Such line-sensors are implemented in form of flexible tubes and can be arranged inside or outside the pipeline (also underwater or within the subsurface), corresponding to the technical requirements. The measuring method combines the gas specific diffusion rates through a membrane with Dalton’s law of partial pressures and enables the calculation of gas concentrations or the detection of a change of the gas composition. The objective is to detect gas leakages fast and with high reliability. Furthermore, the calibrated system enables to estimate the spatial extent of a leakage. So far the gas concentration measurement is tested for oxygen, carbon dioxide, methane; further gases should follow, e.g. hydrogen, carbon monoxide or mixtures like natural gas. The paper introduces in the different operating modes of line-sensors. A near real-time approach will be demonstrated to quantify the impact of a gas leak on the near environment. This approach is based on a critical length describing the expansion of the leaking gas. T2 - 9th Pipeline technology conference 2014 CY - Berlin, Germany DA - 12.05.2014 KW - Multi-sensor system KW - Condition monitoring KW - Safety management KW - Hazardous scenarios KW - Data fusion PY - 2014 SP - 1 EP - 9 AN - OPUS4-30727 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Neumann, Patrick P. A1 - Kohlhoff, Harald A1 - Werner, Klaus-Dieter A1 - Erdmann, Jessica A1 - Eggeringhaus, Bärbel A1 - Kammermeier, Michael A1 - Schukar, Marcus A1 - Basedau, Frank A1 - Bartholmai, Matthias A1 - Lazik, D. A1 - Ebert, Sebastian T1 - Setup of a large scale soil test field with CO2 injection for testing a novel distributed subsurface monitoring system for gas storage areas N2 - One of the main unsolved issues of under-ground storages for, e.g., CO2, H2, and natural gas is the comprehensive surveillance of these areas with reasonable effort and costs. Conventional sensors (e.g., soil air probes or borehole probes), however, can only be used for punctual or locally limited measurements; further their application can cause structural influences (invasive application). In this paper, we describe in detail the setup of a CO2 injection soil test field. This test field will be used to enhance and validate an innovative ap-proach for distributed subsurface monitoring of gas storage areas. To the author’s knowledge, this is the first time that, for this purpose, a test field is built in an application relevant scale. T2 - 31st Danubia-Adria Symposium on advances in experimental mechanics CY - Kempten, Germany DA - 24.09.2014 KW - Large scale soil test field KW - Subsurface monitoring KW - Gas storage areas KW - Membrane-based gas sensing KW - Fiber optical sensing PY - 2014 SN - 978-3-00-046740-0 SP - 238 EP - 239 AN - OPUS4-31527 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lazik, D. A1 - Neumann, Patrick P. A1 - Bartholmai, Matthias T1 - Characteristic length measurement of a subsurface gas anomaly - an integrating monitoring approach over heterogeneous distributed gas flow paths N2 - Geogenic gases such as CH4 or CO2 from natural sources, gases (CCS-CO2, H2, Natural gas, City gas …) from a geological repository, or a leaking gas pipeline can present serious risks in industrial and urban areas where the density of infrastructural elements increases as well as above and below ground. To extend the lead time for risk treatment in such critical regions, reliable detection of gases within the shallow subsurface is required to observe critical gas accumulations before degassing into the atmosphere. A near real-time monitoring approach is introduced to determine the volumetric expansion of such a gas escaping from a leak in the subsurface. Considering the pressure relaxation with the ambient air pressure, the approach enables the forecasting of the final size of a pressurized gas body in terms of characteristic lengths. According to theoretical basics, such a characteristic length, which allows to perform a gas (safety) measurement based on a purely geometrical measure, behaves independently of subsurface properties, i.e., it enables a reliable quantification of the escaping gas, irrespective of its heterogeneous flow path distribution. A field test for a 10 l/min pinhole leakage of CO2 injected in an unsaturated Chernozemic soil (agricultural test field Bad Lauchstädt)that was equipped with linear gas sensors demonstrates the lateral-vertical volumetric gas expansion along the environment of these gas sensors, and confirms the applicability of the new characteristic length approach. T2 - UFZ EnergyDays 2017 CY - Leipzig, Germany DA - 15.03.2017 KW - CO2 KW - Carbon capture and storage KW - Leakage KW - Monitoring PY - 2017 AN - OPUS4-39400 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Petrov, Sergej A1 - Neumann, Patrick P. A1 - Werner, Klaus-Dieter A1 - Lazik, D. A1 - Bartholmai, Matthias T1 - Concept for investigating mechanical impacts on distributed subsurface gas monitoring N2 - A multifunctional sensor in line shape was developed and introduced in previous work for measuring of gas concentrations, temperature change, and strain. A current field study focuses on a spatially distributed monitoring of subsurface CO2 gas storage sites in near real time. Mechanical impacts, e.g., caused by construction work, denudation, and seismic activity, can affect the integrity of underground gas storage sites. Thermal or moisture impacts, e.g., caused by weather conditions, can influence the gas distribution behavior. In this paper, we briefly describe the setup of a CO2 injection soil test field. This setup contains actuating elements for the investigation of mechanical and thermal impacts on distributed subsurface gas monitoring. A concept is given for evaluating these impacts and first experimental results are presented. T2 - 32nd Danubia-Adria Symposium on advances in experimental mechanics CY - Starý Smokovec, Slovakia DA - 22.09.2015 PY - 2015 DO - https://doi.org/10.1016/j.matpr.2016.03.060 SN - 2214-7853 VL - 3 IS - 4 SP - 1124 EP - 1128 PB - Elsevier Science CY - Zilina AN - OPUS4-34489 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Neumann, Patrick P. A1 - Ebert, Sebastian A1 - Lazik, D. A1 - Bartholmai, Matthias T1 - Inverse calibration routine for linear soil gas sensors N2 - Gas sensors in linear form based on the measuring principle of gas selective permeability through a membrane were developed and introduced for the detection and quantification of gas concentrations. A current field study focuses on measuring CO2 concentrations for a spatially distributed monitoring of subsurface CO2 gas storage sites in near real time. A 400 m(2) test site and a corresponding laboratory system were built up to characterize, validate, and optimize the sensor. A calibration routine was developed, which can be applied subsequently to underground installation. First measurement results indicate the potential of the method. T2 - 32nd Danubia-Adria Symposium on advances in experimental mechanics CY - Starý Smokovec, Slovakia DA - 22.09.2015 PY - 2015 SN - 978-80-554-1094-4 DO - https://doi.org/10.1016/j.matpr.2016.03.051 SP - 68 EP - 69 CY - Zilina AN - OPUS4-34491 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -