TY - JOUR A1 - Liehr, Alexander A1 - Dingel, Kristina A1 - Kottke, Daniel A1 - Degener, Sebastian A1 - Meier, David A1 - Sick, Bernhard A1 - Niendorf, Thomas T1 - Data selection strategies for minimizing measurement time in materials characterization N2 - Every new material needs to be assessed and qualified for an envisaged application. A steadily increasing number of new alloys, designed to address challenges in terms of reliability and sustainability, poses significant demands on well-known analysis methods in terms of their efficiency, e.g., in X-ray diffraction analysis. Particularly in laboratory measurements, where the intensities in diffraction experiments tend to be low, a possibility to adapt the exposure time to the prevailing boundary conditions, i.e., the investigated microstructure, is seen to be a very effective approach. The counting time is decisive for, e.g., complex texture, phase, and residual stress measurements. Traditionally, more measurement points and, thus, longer data collection times lead to more accurate information. Here, too short counting times result in poor signal-to-background ratios and dominant signal noise, respectively, rendering subsequent evaluation more difficult or even impossible. Then, it is necessary to repeat experiments with adjusted, usually significantly longer counting time. To prevent redundant measurements, it is state-of-the-art to always consider the entire measurement range, regardless of whether the investigated points are relevant and contribute to the subsequent materials characterization, respectively. Obviously, this kind of approach is extremely time-consuming and, eventually, not efficient. The present study highlights that specific selection strategies, taking into account the prevailing microstructure of the alloy in focus, can decrease counting times in X-ray energy dispersive diffraction experiments without any detrimental effect on data quality for the subsequent analysis. All relevant data, including the code, are carefully assessed and will be the basis for a widely adapted strategy enabling efficient measurements not only in lab environments but also in large-scale facilities. KW - Materials characterization KW - Machine learning KW - X-ray diffraction KW - Measurement optimization PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-630831 DO - https://doi.org/10.1038/s41598-025-96221-1 SN - 2045-2322 VL - 15 IS - 1 SP - 1 EP - 12 PB - Springer Science and Business Media LLC AN - OPUS4-63083 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schepers, Winfried A1 - Brinkgreve, Ronald B. J. A1 - Holtzendorff, Kira A1 - Wegener, Dirk A1 - Appel, Silke A1 - Efthymiou, Georgia A1 - Krajewski, Wolfgang A1 - Machaček, Jan A1 - Meier, Thomas A1 - Nseir, Bashar A1 - Rangelow, Peter A1 - Schmitt, Jürgen A1 - Staubach, Patrick A1 - Vrettos, Christos T1 - Numerische Ermittlung von Baugrundschwingungen bei dynamisch belasteten Fundamenten: Empfehlungen zur Modellierung T1 - Numerical analysis of soil vibrations due to vibrating foundations: Guidance for model design N2 - AbstractIn der Praxis tätige geotechnisch Planende kommen in zunehmendem Maße mit dynamischen Fragestellungen in Berührung. Hersteller von geotechnischer Berechnungssoftware haben entsprechend ihre ursprünglich für statische Aufgabenstellungen konzipierten Produkte um die Möglichkeit zur Lösung von Wellenausbreitungsproblemen im Baugrund erweitert. Den Anwendern fehlt aber häufig die notwendige Erfahrung zur Durchführung dieser Art von numerischen Berechnungen. Die Arbeitskreise 1.4 „Baugrunddynamik“ und 1.6 „Numerik in der Geotechnik“ der Deutschen Gesellschaft für Geotechnik (DGGT) haben diese Entwicklung aufgegriffen und einen gemeinsamen Unterarbeitskreis „Numerik in der Baugrunddynamik“ gegründet. Der vorliegende Beitrag stellt die aktuellen Ergebnisse der Arbeit des Unterarbeitskreises vor und fasst die gewonnenen Erkenntnisse in Form von Empfehlungen zusammen. N2 - Geotechnical engineers are increasingly concerned with wave propagation problems. Manufacturers of geotechnical analysis software added features for soil dynamic analyses to their products initially devised for static geotechnical analyses. Though, users often lack the experience for conducting such advanced numerical analyses. Working groups 1.4 "Soil dynamics" and 1.6 "Numerical analyses in geotechnical engineering" of DGGT German Society for Geotechnical Engineering established a joint subgroup "Numerical analyses in soil dynamics" to address this shortcoming. The present paper presents the work of the subgroup so far and provides some guidance on conducting numerical analyses in soil dynamics. KW - Wellenausbreitung KW - Numerische Methoden KW - Empfehlungen KW - Modellgröße KW - Zeitschrittweite PY - 2024 DO - https://doi.org/10.1002/gete.202400016 SN - 0172-6145 VL - 47 IS - 4 SP - 254 EP - 268 PB - Ernst CY - Berlin AN - OPUS4-62078 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kipphardt, Heinrich A1 - Dudzus, Thomas A1 - Meier, Klaus A1 - Recknagel, Sebastian A1 - Hedrich, Martina A1 - Matschat, Ralf T1 - Measurement of oxygen and nitrogen in high purity metals used as national standards for elemental analysis in Germany by classical carrier gas hot extraction (HE) and HE after activation with photons N2 - The special importance of the analysis of non-metals in high purity metals, which will serve as national standards for elemental analysis in Germany, is illustrated for oxygen and nitrogen. The typical range of the mass fraction of oxygen and nitrogen in these materials is below 10.MU.g/g, often close to 1.MU.g/g. The two methods applied at BAM for these measurements are classical carrier gas hot extraction (HE) and carrier gas hot extraction after activation with photons (PAA-HE). The approach, the methods and their advantages and limitations are discussed. Comparative results from the measurement of oxygen and nitrogen in Cu, Fe, Ga, Pb, Sn and W are presented. (author abst.) T2 - 8th International Conference on Ultra-High Purity Base Metals (UHPM-2001) CY - Berlin, Germany DA - 2001-06-25 KW - Oxygen determination KW - Nitrogen determination KW - High purity metals KW - Carrier gas hot extraction KW - Photon activation analysis PY - 2002 DO - https://doi.org/10.2320/matertrans.43.98 SN - 1345-9678 SN - 1347-5320 VL - 43 IS - 2 SP - 98 EP - 100 PB - Japan Institute of Metals CY - Sendai AN - OPUS4-1361 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -