TY - JOUR A1 - Richter, Matthias A1 - Jann, Oliver A1 - Horn, Wolfgang A1 - Pyza, Lars A1 - Wilke, Olaf T1 - System to generate stable long-term VOC gas mixtures of concentrations in the ppb range for test and calibration purposes N2 - The development of a gas mixing system (GMS) that enables dynamic and retraceable production of stable long-term VOC gas mixtures within the ppb range is discussed. In this system pure liquid substances are kept separately at a constant temperature, evaporated according to their vapour pressure and removed by a small inert gas flow. A modular set-up allows flexible handling. All vapours generated are finally united in a mixing chamber. Any concentration level of the gas mixture can be produced by a suitable combination of evaporation temperature, carrier and dilution gas flows. Test results from continuous operation over six weeks are presented. The equipment was tested on seven volatile organic compounds (VOC) of different vapour pressure ranges. It was possible to establish stable operation for the equipment during the entire period and reproducible gas concentrations which were traceable to the mass as an SI unit, thus the system is suitable for long-term tests.--------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------- Im Beitrag wird die Entwicklung eines Gasmischsystems (GMS) beschrieben, das die dynamische und rückführbare Generierung von langzeitstabilen VOC-Gasgemischen im ppb-Bereich erlaubt. Dabei werden Reinsubstanzen separat temperiert, ihrem Dampfdruck entsprechend verdampft und durch einen kleinen Inertgasstrom abgeführt. In einer Mischkammer werden sie schließlich zusammengeführt. Durch die Kombination von Verdampfungstemperatur, Träger- und Verdünnungsgasflüssen ist die Einstellung eines beliebigen Konzentrationsniveaus des Gasgemischs möglich. Aus einem Dauerbetrieb von sechs Wochen werden Untersuchungsergebnisse gezeigt. Dabei wurde die Apparatur mit insgesamt sieben flüchtigen organischen Verbindungen (VOC) unterschiedlicher Dampfdruckbereiche betrieben. Die Anlage lief über den gesamten Zeitraum stabil und lieferte reproduzierbare und auf die Masse als SI-Einheit rückführbare Gaskonzentrationen. Somit ist das Verfahren für Langzeitanwendungen geeignet. KW - Gas mixing system KW - VOC gas mixtures KW - Low gas concentrations KW - Evaporation KW - Dynamic gas generation PY - 2013 SN - 0949-8036 SN - 0039-0771 SN - 1436-4891 VL - 73 IS - 3 SP - 103 EP - 106 PB - Springer-VDI-Verl. CY - Düsseldorf AN - OPUS4-27903 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Richter, Matthias A1 - Horn, Wolfgang A1 - Nohr, Michael T1 - Approach to the improvement of the traceability for (S)Voc-measurement T2 - 7th Gas Analysis Symposium & Exhibition CY - Rotterdam, Netherlands DA - 2013-06-05 PY - 2013 AN - OPUS4-29625 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Richter, Matthias A1 - Jann, Oliver T1 - Determination of radon exhalation from building materials using emission test chambers T2 - IAQ 2013 Environmental Health in Low Energy Buildings CY - Vancouver, Canada DA - 2013-10-15 PY - 2013 AN - OPUS4-29627 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Meyer, S. A1 - Richter, S. A1 - Balski, Matthias A1 - Hagendorf, C. ED - Thirsk, M. T1 - Trace element analysis in crystalline silicon PY - 2013 SN - 978-0-9565331-3-5 SP - 34 EP - 38 PB - Photovoltaics International CY - London, UK AN - OPUS4-29823 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Richter, Matthias A1 - Jann, Oliver T1 - Determination of radon exhalation rates from construction materials using VOC emission test chambers T2 - IAQ 2013 - Environmental health in low energy buildings CY - Vancouver, British Columbia, Canada DA - 2013-10-15 KW - Radon exhalation KW - Radon measurement KW - Construction material KW - Emission test chamber KW - Indoor air quality PY - 2013 SN - 2166-4870 SP - 508 EP - 512 AN - OPUS4-29407 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Richter, Matthias A1 - Jann, Oliver A1 - Kemski, J. A1 - Schneider, Uwe A1 - Krocker, Christian A1 - Hoffmann, B. T1 - Determination of radon exhalation from construction materials using VOC emission test chambers N2 - The inhalation of 222Rn (radon) decay products is one of the most important reasons for lung cancer after smoking. Stony building materials are an important source of indoor radon. This article describes the determination of the exhalation rate of stony construction materials by the use of commercially available measuring devices in combination with VOC emission test chambers. Five materials – two types of clay brick, clinker brick, light-weight concrete brick, and honeycomb brick – generally used for wall constructions were used for the experiments. Their contribution to real room concentrations was estimated by applying room model parameters given in ISO 16000-9, RP 112, and AgBB. This knowledge can be relevant, if for instance indoor radon concentration is limited by law. The test set-up used here is well suited for application in test laboratories dealing with VOC emission testing. KW - Radon exhalation KW - Radon measurement KW - Building material KW - Emission test chamber KW - Indoor air quality KW - Real room radon concentrations PY - 2013 U6 - https://doi.org/10.1111/ina.12031 SN - 0905-6947 SN - 1600-0668 VL - 23 IS - 5 SP - 397 EP - 405 PB - Danish Techn. Pr. CY - Copenhagen AN - OPUS4-29408 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Richter, Matthias A1 - Wilke, Olaf A1 - Jann, Oliver T1 - Use of emission test chambers for the determination of chemical emissions from construction materials T2 - 1st International conference on the chemistry of construction materials CY - Berlin, Germany DA - 2013-10-07 KW - VOC KW - Emission from materials KW - Construction materials KW - Emission test chamber PY - 2013 SN - 978-3-936028-75-1 N1 - Serientitel: GDCh-Monographien – Series title: GDCh-Monographien VL - 46 SP - 259 EP - 262 AN - OPUS4-29480 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Richter, Matthias A1 - Jann, Oliver A1 - Wilke, Olaf T1 - Use of emission test chambers for the determination of chemical emissions from construction materials T2 - 1st International Conference on the Chemistry of Construction Materials CY - Berlin, Germany DA - 2013-10-07 PY - 2013 AN - OPUS4-29626 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -