TY - JOUR A1 - Lozano-Martín, D. A1 - Martín, M. C. A1 - Chamorro, C. R. A1 - Tuma, Dirk A1 - Segovia, J. J. T1 - Speed of sound for three binary (CH4 + H2) mixtures from p = (0.5 up to 20) MPa at T = (273.16 to 375) K N2 - Speed of sound is one of the thermodynamic properties that can be measured with least uncertainty and is of great interest in developing equations of state. Moreover, accurate models are needed by the H2 industry to design the transport and storage stages of hydrogen blends in the natural gas network. This research aims to provide accurate data for (CH4 + H2) mixtures of nominal (5, 10, and 50) mol-% of hydrogen, in the p = (0.5 up to 20) MPa pressure range and with temperatures T = (273.16, 300, 325, 350, and 375) K. Using an acoustic spherical resonator, speed of sound was determined with an overall relative expanded (k = 2) uncertainty of 220 parts in 10^6 (0.022%). Data were compared to reference equations of state for natural gas-like mixtures, such as AGA8-DC92 and GERG-2008. Average absolute deviations below 0.095% and percentage deviations between 0.029% and up to 0.30%, respectively, were obtained. Additionally, results were fitted to the acoustic virial equation of state and adiabatic coefficients, molar isochoric heat capacities and molar isobaric heat capacities as perfect-gas, together with second and third acoustic virial coefficients were estimated. Density second virial coefficients were also obtained. KW - Speed of sound KW - Acoustic resonator KW - Heat capacity PY - 2020 DO - https://doi.org/10.1016/j.ijhydene.2019.12.012 SN - 0360-3199 VL - 45 IS - 7 SP - 4765 EP - 4783 PB - Elsevier Ltd. CY - Amsterdam AN - OPUS4-50454 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Lozano-Martín, D. A1 - Tuma, Dirk A1 - Vega-Maza, D. A1 - Martín, M. C. A1 - Chamorro, C. R. T1 - Thermodynamic characterization of the (CO2+ O2) binary system for the development of models for CCS processes: Accurate experimental (p, rho, T) data and virial coefficients N2 - Continuing our study on (CO2 + O2) mixtures, this work reports new experimental (p, rho, T) data for two oxygen-rich mixtures with mole fractions x(O2) = (0.50 and 0.75) mol·mol−1, in the temperature range T = (250–375) K and pressure range p = (0.5–20) MPa, using a single-sinker densimeter. Experimental density data were compared to two well-established equation-of-state models: EOS-CG and GERG-2008. In the p, T-range investigated, the EOS-CG gave a better reproduction for the equimolar mixture (x(O2) = 0.5), whereas the GERG-2008 performed significantly better for the oxygen-rich mixture (x(O2) = 0.75). The EOS-CG generally overestimates the density, while the GERG-2008 underestimates it. This complete set of new experimental data, together with previous measurements, is used to calculate the virial coefficients B(T, x) and C(T, x), as well as the second interaction virial coefficient B12(T) for the (CO2+ O2) system. KW - Binary mixtures CO2 + O2 KW - Density measurements KW - Equations of state KW - Virial coefficients PY - 2021 DO - https://doi.org/10.1016/j.supflu.2020.105074 SN - 0896-8446 VL - 169 SP - 5074 PB - Elsevier B. V. CY - Amsterdam AN - OPUS4-51670 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Martin-Sanchez, Pedro Maria A1 - Miller, A. Z. A1 - Garcia-Sanchez, A. M. A1 - Martin-Sanchez, Pedro Maria A1 - F.C. Pereira, M. A1 - Afonso, M. J. A1 - Saiz-Jimenez, C. A1 - Spangenberg, J. E. A1 - Jurado, V. A1 - Dionísio, A. A1 - Chaminé, H. I. A1 - Hermosin, B. T1 - Origin of abundant moonmilk deposits in a subsurface granitic environment N2 - Subsurface granitic environments are scarce and poorly investigated. A multi-disciplinary approach was used to characterize the abundant moonmilk deposits and associated microbial communities coating the granite walls of the 16th Century Paranhos spring water tunnel in Porto city (north-west Portugal). It is possible that this study is the first record of moonmilk in an urban subsurface granitic environment. The morphology and texture, mineralogical composition, stable isotope composition and microbial diversity of moonmilk deposits have been studied to infer the processes of moonmilk formation. These whitish secondary mineral deposits are composed of very fine needle fibre calcite crystals with different morphologies and density. Calcified filaments of fungal hyphae or bacteria were distinguished by field emission scanning electron microscopy. Stable isotope analysis revealed a meteoric origin of the needle fibre calcite, with an important contribution of atmospheric CO2, soil respiration and HCO3 − from weathering of Ca-bearing minerals. The DNA-based analyses revealed the presence of micro-organisms related to urban contamination, including Actinobacteria, mainly represented by Pseudonocardia hispaniensis, Thaumarchaeota and Ascomycota, dominated by Cladosporium. This microbial composition is consistent with groundwater pollution and contamination sources of the overlying urban area, including garages, petrol stations and wastewater pipeline leakage, showing that the Paranhos tunnel is greatly perturbed by anthropogenic activities. Whether the identified micro-organisms are involved in the formation of the needle fibre calcite or not is difficult to demonstrate, but this study evidenced both abiotic and biogenic genesis for the calcite moonmilk in this subsurface granitic environment. KW - Biomineralization KW - Carbonate precipitation KW - Granite KW - Moonmilk KW - Needle fibre calcite PY - 2017 UR - https://onlinelibrary.wiley.com/doi/full/10.1111/sed.12431 DO - https://doi.org/10.1111/sed.12431 SN - 1365-3091 VL - 65 IS - 2 SP - 1482 EP - 1503 PB - Wiley AN - OPUS4-43622 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Krause, Martin A1 - Milmann, Boris A1 - Feldmann, Rüdiger A1 - Friese, Martin A1 - Wöstmann, Jens A1 - Zoëga, Andreas A1 - Sodeikat, C. T1 - Thickness measurement & quality assurance of floor slabs & diaphragm walls T2 - Structural faults & repair 2010 - International conference and exhibition CY - Edinburgh, Scotland, UK DA - 2010-06-15 KW - Ultrasonic echo KW - Radar KW - Impact-echo KW - Synthetic aperture focusing technique (SAFT) KW - Compaction faults PY - 2010 SN - 0-947644-67-9 SP - 1 EP - 9 PB - Engineering Technics Press CY - Edinburgh, Scotland AN - OPUS4-22897 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Tuma, Dirk A1 - Lozano-Martín, D. A1 - Vega-Maza, D. A1 - Moreau, A. A1 - Martín, M. C. A1 - Segovia, J. J. T1 - Speed of sound data, derived perfect-gas heat capacities, and acoustic virial coefficients of a calibration standard natural gas mixture and a low-calorific H2-enriched mixture N2 - This work aims to address the technical aspects related to the thermodynamic characterization of natural gas mixtures blended with hydrogen for the introduction of alternative energy sources within the Power-to-Gas framework. For that purpose, new experimental speed of sound data are presented in the pressure range between (0.1 up to 13) MPa and at temperatures of (260, 273.16, 300, 325, and 350) K for two mixtures qualified as primary calibration standards: a 11 component synthetic natural gas mixture (11 M), and another low-calorific H2-enriched natural gas mixture with a nominal molar percentage x(H2) = 3 %. Measurements have been gathered using a spherical acoustic resonator with an experimental expanded (k = 2) uncertainty better than 200 parts in 106 (0.02 %) in the speed of sound. The heat capacity ratio as perfect-gas gammapg, the molar heat capacity as perfect-gas Cp,m pg, and the second betaa and third gammaa acoustic virial coefficients are derived from the speed of sound values. All the results are compared with the reference mixture models for natural gas-like mixtures, the AGA8-DC92 EoS and the GERG-2008 EoS, with Special attention to the impact of hydrogen on those properties. Data are found to be mostly consistent within the model uncertainty in the 11 M synthetic mixture as expected, but for the hydrogen-enriched mixture in the limit of the model uncertainty at the highest measuring pressures. KW - Natural gas mixtures KW - Speed-of-sound measurements KW - Equations of state KW - Acoustic virial coefficients PY - 2021 DO - https://doi.org/10.1016/j.jct.2021.106434 SN - 0021-9614 VL - 158 SP - 106434 PB - Elsevier Ltd. CY - Amsterdam AN - OPUS4-52292 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Segovia, J. J. A1 - Tuma, Dirk A1 - Lozano-Martín, D. A1 - Moreau, A. A1 - Martín, M. C. A1 - Vega-Maza, D. T1 - Speed of sound data and acoustic virial coefficients of two binary (N2 + H2) mixtures at temperatures between (260 and 350) K and at pressures between (0.5 and 20) MPa N2 - This work aims to address the technical concerns related to the thermodynamic characterization of gas mixtures blended with hydrogen for the implementation of hydrogen as a new energy vector. For this purpose, new experimental speed of sound measurements have been done in gaseous and supercritical phases of two binary mixtures of nitrogen and hydrogen using the most accurate technique available, i.e., the spherical acoustic resonator, yielding an experimental expanded (k = 2) uncertainty of only 220 parts in 106 (0.022%). The measurements cover the pressure range between (0.5 and 20) MPa, the temperature range between (260 and 350) K, and the composition range with a nominal mole percentage of hydrogen of (5 and 10) mol%, respectively. From the speed of sound data sets, thermophysical properties that are relevant for the characterization of the mixture, namely the second βa and third γa acoustic virial coefficients, are derived. These results are thoroughly compared and discussed with the established reference mixture models valid for mixtures of nitrogen and hydrogen, such as the AGA8-DC92 EoS, the GERG-2008 EoS, and the recently developed adaptation of the GERG-2008 EoS, here denoted GERG-H2_improved EoS. Special attention has been given to the effect of hydrogen concentration on those properties, showing that only the GERG-H2_improved EoS is consistent with the data sets within the experimental uncertainty in most measuring conditions. KW - Speed of sound KW - Acoustic resonance KW - Binary gas mixture PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-551482 DO - https://doi.org/10.1016/j.jct.2022.106791 SN - 0021-9614 VL - 171 SP - 1 EP - 13 PB - Elsevier B. V. CY - Amsterdam AN - OPUS4-55148 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Nilsson, R. H. A1 - Taylor, A. F. S. A1 - Adams, R. I. A1 - Baschien, C. A1 - Bengtsson-Palme, J. A1 - Cangren, P. A1 - Coleine, C. A1 - Iršėnaitė, R. A1 - Martin-Sanchez, Pedro Maria A1 - Meyer, W. A1 - Oh, S.-Y. A1 - Sampaio, J. P. A1 - Seifert, K. A. A1 - Sklenář, F. A1 - Stubbe, D. A1 - Suh, S.-O. A1 - Summerbell, R. A1 - Svantesson, S. A1 - Unterseher, M. A1 - Visagie, C. M. A1 - Weiss, M. A1 - Woudenberg, J. HC. A1 - Wurzbacher, C. A1 - Van den Wyngaert, S. A1 - Yilmaz, N. A1 - Yurkov, A. A1 - Kõljalg, U. A1 - Abarenkov, K. A1 - Daniel, H.-M. A1 - Glassman, S. I. A1 - Hirooka, H. A1 - Irinyi, L. T1 - Taxonomic annotation of public fungal ITS sequences from the built environment – a report from an April 10–11, 2017 workshop (Aberdeen, UK) N2 - Recent DNA-based studies have shown that the built environment is surprisingly rich in fungi. These indoor fungi – whether transient visitors or more persistent residents – may hold clues to the rising levels of human allergies and other medical and building-related health problems observed globally. The taxo¬nomic identity of these fungi is crucial in such pursuits. Molecular identification of the built mycobiome is no trivial undertaking, however, given the large number of unidentified, misidentified, and technically compromised fungal sequences in public sequence databases. In addition, the sequence metadata required to make informed taxonomic decisions – such as country and host/substrate of collection – are often lacking even from reference and ex-type sequences. Here we report on a taxonomic annotation workshop (April 10–11, 2017) organized at the James Hutton Institute/University of Aberdeen (UK) to facilitate reproducible studies of the built mycobiome. The 32 participants went through public fungal ITS bar¬code sequences related to the built mycobiome for taxonomic and nomenclatural correctness, technical quality, and metadata availability. A total of 19,508 changes – including 4,783 name changes, 14,121 metadata annotations, and the removal of 99 technically compromised sequences – were implemented in the UNITE database for molecular identification of fungi (https://unite.ut.ee/) and shared with a range of other databases and downstream resources. Among the genera that saw the largest number of changes were Penicillium, Talaromyces, Cladosporium, Acremonium, and Alternaria, all of them of significant importance in both culture-based and culture-independent surveys of the built environment. KW - Indoor mycobiome KW - Built environment KW - Molecular identification KW - Fungi KW - Taxonomy KW - Systematics KW - Sequence annotation KW - Metadata KW - Open data PY - 2018 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-438949 DO - https://doi.org/10.3897/mycokeys.28.20887 SN - 1314-4049 SN - 1314-4057 VL - 28 SP - 65 EP - 82 PB - Pensoft Publishers CY - Washington, DC AN - OPUS4-43894 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Bothe, Martin A1 - Mya, K.Y. A1 - Lin, E.M.J. A1 - Yeo, C. C. A1 - Lu, X. A1 - He, C. A1 - Pretsch, Thorsten T1 - Triple-shape properties of star-shaped POSS-polycaprolactone polyurethane networks N2 - Here, we present an investigation of the triple-shape properties of star-shaped polyhedral oligomeric silsesquioxane-poly(ε-caprolactone) polyurethanes (SPOSS-PUs), which have three-dimensional network structures. In a typical 'triple-shape functionalization process', mostly consisting of two tensile deformations at different temperatures, chain immobilization of the polymer network component poly(ε-caprolactone) (PCL) was successfully realized first through crystallization and then through vitrification. Subsequently, large parts of the respective strains were released under stress-free recovery conditions. The two-fold fixed ('programmed') specimens responded to heating with two independent length contractions (switching steps); the first shape change was associated with PCL devitrification and the second one with the melting of hitherto crystalline PCL. It was revealed that the triple-shape properties of SPOSS-PU networks considerably depend on PCL network chain length. When applying exactly the same 'triple-shape creation procedure', larger strain releases were detected in the first transition for polymers with a higher PCL network chain length, whereas the second transition was more accentuated for SPOSS-PU networks with a shorter PCL chain length. In the course of thermo-mechanical cycling, the formation of a neck during the second tensile deformation was repeatedly detected for SPOSS-PUs with higher PCL network chain length; in the subsequent recovery process the specimens even exhibited the highest total strain recoverability. Finally, gradual strain release could be achieved at temperatures below the PCL melting transition through the selection of up to four temperature holding steps, at which every time stable shapes were formed. KW - Shape memory polymer KW - Active polymer KW - Triple-shape polymer KW - Hybrid star-shaped polymer KW - POSS-polycaprolactone polyurethanes KW - Thermo-mechanical properties PY - 2012 DO - https://doi.org/10.1039/c1sm06474f SN - 1744-683X VL - 8 IS - 4 SP - 965 EP - 972 PB - RSC Publ. CY - Cambridge AN - OPUS4-25260 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Fischer, C. A1 - Wu, J. A1 - Meyer, U. A1 - Kong, B. A1 - Schmidt, Martin A1 - Wuttke, M. A1 - Drebenstedt, C. A1 - Barth, Uli A1 - Rüter, H. T1 - Eight years of successful bilateral cooperation: Milestones of sino-german research T2 - 2nd International conference on coal fire research (ICCFR2) CY - Berlin, Germany DA - 2010-05-19 KW - Underground coal fires KW - Sino-german cooperation PY - 2010 SN - 978-3-86012-397-3 IS - Introduction SP - 3 EP - 18 AN - OPUS4-21460 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Fischer, C. A1 - Schmidt, Martin A1 - Meyer, U. A1 - Barth, Uli A1 - Drebenstedt, C. A1 - Wuttke, M. W. T1 - Innovative Technologien für die Erkundung, Löschung und Beobachtung von Kohlebränden - Phase B - N2 - Aufbauend auf den Erkenntnissen der Phase A, die sich auf das grundlegende Verständnis von Kohlebränden, sowie der Voraussetzung und des prinzipiellen Ablaufs der physikalischchemischen Brandprozesse konzentriert haben, erfolgte in Phase B eine Fokussierung auf Methoden zur Vermeidung von Kohlebränden, sowie der Löschung und Überwachung von Kohlebrandzonen, um einen Beitrag zur Verminderung von C02-Emissionen und zum Erhalt der nutzbaren Energieressourcen leisten zu können. Diese Arbeiten erfolgten insbesondere mit Bezug zu den „Clean Development Mechanisms“ (CDM), die im Rahmen des Kyoto-Protokolls entwickelt worden sind. Eine Zertifizierung von Löschaktivitäten im Rahmen des Kyoto-Protokolls setzt dabei eine nachvollziehbare Ermittlung der kohlebrandbezogenen C02-Emissionen und eine belastbare Abschätzung der durch die Löschung verringerten Emissionsmengen voraus. Wesentliche Arbeiten konzentrierten sich auf die Entwicklung von Verfahren, die eine solche Abschätzung gewährleisten können. Dazu wurden unterschiedliche Ansätze entwickelt und anhand der erhobenen Felddaten überprüft. Die untersuchten Ansätze konzentrierten sich dabei auf Verfahren, die eine Ermittlung des vorhandenen Kohlevolumens, die Erfassung der emittierten Gase und die durch die Kohlebrände verursachten Temperaturanomalien an der Tagesoberfläche ermöglichen. Die direkten Arbeiten zum Thema CDM wurden dabei in einem Arbeitspaket unter Federführung der BGR gebündelt. Die deutsche Initiative zur Erforschung der Kohlenbrände in der V.R. China leistete zweifelsfrei signifikante Beiträge zu den oben genannten Zielen. Durch die inventiven Ansätze im Bereich der Brandbewältigung konnte darüber hinaus auch in Teilen die ökonomischen Chancen für ein Engagement deutscher Unternehmen aufgezeigt werden. KW - Kohlebrände KW - Brandbekämpfung KW - Branderkundung PY - 2011 DO - https://doi.org/10.2314/GBV:664529690 SP - 1 EP - 39 AN - OPUS4-25013 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Mans, C. A1 - Simons, C. A1 - Hanning, S. A1 - Janßen, A. A1 - Alber, D. A1 - Radtke, Martin A1 - Reinholz, Uwe A1 - Bühler, A. A1 - Kreyenschmidt, M. T1 - New polymeric candidate reference materials for XRF and LA-ICP-MS - development and preliminary characterization N2 - A set of ten calibration materials based on acrylonitrile-butadiene-styrene terpolymer (ABS) containing the elements Br, Pb, Cd, Cr, and Hg was produced in order to control polymer samples in regard to the restriction on the use of certain hazardous substances (RoHS) directive. The materials were produced with respect to the special demands of X-ray fluorescence analysis (XRF) and inductively coupled plasma mass spectrometry in combination with laser ablation (LA-ICP-MS). The mass fractions of all elements were 0-1500 mg/kg and the materials were produced as granulates and solid discs with a diameter of 40 mm and thicknesses of 1, 2, and 6 mm. It could be shown that the signals measured by XRF strongly depend on the thickness of polymeric samples. Macroscopic homogeneity was assessed with XRF measuring a total of 180 samples. The microscopic homogeneities were determined for a material with average elemental mass fractions with the aid of synchrotron radiation (SR) µ-XRF and LA-ICP-MS. Sufficient macroscopic and microscopic homogeneities for all elements could be achieved. It was observed that organic additives show a better homogeneity than oxides. XRF and LA-ICP-MS were successfully calibrated with the new materials. Limits of detection were in the range of 0.4-22 mg/kg for XRF and 2.3-26.8 mg/kg for LA-ICP-MS. The materials are considered as candidate reference materials (RM) by the Federal Institute of Materials Research and Testing (BAM, Germany). KW - XRF KW - LA.ICP-MS Plastics KW - RoHS KW - CRM PY - 2009 DO - https://doi.org/10.1002/xrs.1120 SN - 0049-8246 VL - 38 IS - 1 SP - 52 EP - 57 PB - Wiley CY - Chichester AN - OPUS4-18681 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Simons, C. A1 - Mans, C. A1 - Hanning, S. A1 - Janßen, A. A1 - Radtke, Martin A1 - Reinholz, Uwe A1 - Ostermann, Markus A1 - Michaelis, Matthias A1 - Wienold, Julia A1 - Alber, D. A1 - Kreyenschmidt, M. T1 - Study on microscopic homogeneity of polymeric candidate reference materials BAM H001-BAM H010 by means of synchrotron µ-XRF and LA-ICP-MS N2 - In this study the microscopic homogeneity of the newly developed plastic reference materials BAM H001-BAM H010 was investigated. The materials consist of an acrylonitryle-butadien-styrene terpolymer, doped with different amounts of the elements Br, Cd, Cr, Hg and Pb. For the quantitative determination of the degree of homogeneity, a procedure proposed by Kempenaers et al. (Fresenius J. Anal. Chem., 2001, 369, 733-737) was used. On every sample an extensive number of different points were analyzed and standard deviation for every element mentioned above was used to calculate a minimal sampling mass that is necessary to reach a certain level of uncertainty caused by inhomogeneity (mmin,5%). The experiments were taken out with synchrotron µ-XRF (SR µ-XRF) at BESSYII in Berlin and by laser ablation inductively coupled plasma mass spectroscopy (LA-ICP-MS). The calculated values for mmin,5% of both techniques showed comparable results for all elements. It could be shown that the materials are suitable for calibration of micro analytic techniques if at least 64 µg are used. KW - XRF KW - LA-ICP-MS KW - RoHS KW - CRM PY - 2010 DO - https://doi.org/10.1039/b917008a SN - 0267-9477 SN - 1364-5544 VL - 25 SP - 40 EP - 43 PB - Royal Society of Chemistry CY - London AN - OPUS4-20938 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Fiedler Bremer, C. A1 - Scholz, R. A1 - Myslicki, S. A1 - Starke, P. A1 - Boller, C. A1 - Walther, F. A1 - Krause, Martin T1 - NDT-based characteriazation of timber and vulcanized fiber for civil infrastructure N2 - The paper addresses beech wood as well as vulcanized fiber and discusses the results obtained when using acoustic emission and thermography as non-destructive testing techniques along tensile and load increase fatigue tests to characterize the wooden material’s behavior under increasing fatigue loads to get enhanced information regarding the fatigue behavior of both materials. Reference is mainly made to the materials’ anisotropic and microstructural behavior and what implications this has with respect to the materials’ strength. The influence of moisture is discussed, as well as parameters that may deserve monitoring in the sense of structural health monitoring to be applied in timber structures in general. T2 - NDT-CE 2015 - International symposium non-destructive testing in civil engineering CY - Berlin, Germany DA - 15.09.2015 KW - Ermüdung KW - Belastungsversuch KW - Thermographie KW - ZfP KW - Timber PY - 2015 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-346377 UR - https://www.ndt.net/?id=18419 SN - 1435-4934 VL - 20 IS - 11 SP - 1 EP - 11 PB - NDT.net CY - Kirchwald AN - OPUS4-34637 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - de O. Primo, J. A1 - Horsth, D.F. A1 - de S. Correa, J. A1 - Das, A. A1 - Bittencourt, C. A1 - Umek, P. A1 - de Oliveira Guilherme Buzanich, Ana A1 - Radtke, Martin A1 - Yusenko, Kirill A1 - Zanetta, C. A1 - Anaissi, F.J. T1 - Synthesis and Characterization of Ag/ZnO Nanoparticles for Bacteria Disinfection in Water N2 - n this study, two green synthesis routes were used for the synthesis of Ag/ZnO nanoparticles, using cassava starch as a simple and low-cost effective fuel and Aloe vera as a reducing and stabilizing agent. The Ag/ZnO nanoparticles were characterized and used for bacterial dis- infection of lake water contaminated with Escherichia coli (E. coli). Characterization indicated the formation of a face-centered cubic structure of metallic silver nanoparticles with no insertion of Ag into the ZnO hexagonal wurtzite structure. Physicochemical and bacteriological analyses described in “Standard Methods for the Examination of Water and Wastewater” were used to evaluate the efficiency of the treatment. In comparison to pure ZnO, the synthesized Ag/ZnO nanoparticles showed high efficiencies against Escherichia coli (E. coli) and general coliforms present in the lake water. These pathogens were absent after treatment using Ag/ZnO nanoparticles. The results indicate that Ag/ZnO nanoparticles synthesized via green chemistry are a promising candidate for the treatment of wastewaters contaminated by bacteria, due to their facile preparation, low-cost synthesis,and disinfection efficiency. KW - Synchrotron KW - BAMline PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-562440 DO - https://doi.org/10.3390/nano12101764 SN - 2079-4991 VL - 12 IS - 10 SP - 1 EP - 18 PB - MDPI CY - Basel AN - OPUS4-56244 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Förste, F. A1 - Bauer, L. A1 - Streeck, C. A1 - Radtke, Martin A1 - Reinholz, Uwe A1 - Kadow, D. A1 - Keil, C. A1 - Mantouvalou, I. T1 - Quantitative Analysis and 2D/3D Elemental Imaging of Cocoa Beans Using X‑ray Fluorescence Techniques N2 - As an important raw material for the confectionery industry, the cocoa bean (Theobroma cacao L.) has to meet certain legal requirements in terms of food safety and maximum contaminant levels in order to enter the cocoa market. Understanding the enrichment and distribution of essential minerals but also toxic metals is of utmost importance for improving the nutritional quality of this economically important raw food material. We present three X-ray fluorescence (XRF) techniques for elemental bio-imaging of intact cocoa beans and one additional XRF technique for quantitative analysis of cocoa pellets. The interrelation of all the methods presented gives a detailed picture of the content and 3D-resolved distribution of elements in complete cocoa beans for the first time. KW - BAMline KW - Synchrotron KW - XRF KW - CXC KW - Cocoa PY - 2023 DO - https://doi.org/10.1021/acs.analchem.2c05370 VL - 95 SP - 5627 EP - 5635 PB - ACS Publications AN - OPUS4-57832 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Steglich, P. A1 - Rabus, D. G. A1 - Sada, C. A1 - Paul, Martin A1 - Weller, Michael G. A1 - Mai, C. A1 - Mai, A. T1 - Silicon Photonic Micro-Ring Resonators for Chemical and Biological Sensing: A Tutorial N2 - Silicon photonic micro-ring resonators (MRR) developed on the silicon-on-insulator (SOI) platform, owing to their high sensitivity and small footprint, show great potential for many chemical and biological sensing applications such as label-free detection in environmental monitoring, biomedical engineering, and food analysis. In this tutorial,we provide the theoretical background and give design guidelines for SOI-based MRR as well as examples of surface functionalization procedures for label-free detection of molecules. After introducing the advantages and perspectives of MRR, fundamentals of MRR are described in detail, followed by an introduction to the fabrication methods, which are based on a complementary metal-oxide semiconductor (CMOS) technology. Optimization of MRR for chemical and biological sensing is provided, with special emphasis on the optimization of waveguide geometry. At this point, the difference between chemical bulk sensing and label-free surface sensing is explained, and definitions like waveguide sensitivity, ring sensitivity, overall sensitivity as well as the limit of detection (LoD) of MRR are introduced. Further, we show and explain chemical bulk sensing of sodium chloride (NaCl) in water and provide a recipe for label-free surface sensing. KW - Biosensors KW - Biophotonics KW - Chemosensor KW - Biosensor KW - Microresonator KW - Nanophotonics KW - Optical sensors KW - Photonic sensors KW - Optoelectronic KW - Ring resonator KW - Silicon photonics KW - Miniaturization KW - Lab-on-a-chip KW - Lab-on-chip KW - Waveguide KW - Surface chemistry KW - Silanization KW - Glutaraldehyde KW - Affinity immobilization KW - Antibody KW - Oriented immobilization KW - Real-time measurement PY - 2022 DO - https://doi.org/10.1109/JSEN.2021.3119547 SN - 1530-437X VL - 22 IS - 11 SP - 10089 EP - 10105 PB - IEEE AN - OPUS4-55147 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Tannenberg, Robert A1 - Paul, Martin A1 - Röder, Bettina A1 - Gande, S. L. A1 - Sreeramulu, S. A1 - Saxena, K. A1 - Richter, C. A1 - Schwalbe, H. A1 - Swart, C. A1 - Weller, Michael G. T1 - Chemiluminescence biosensor for the determination of cardiac troponin I (cTnI) N2 - Cardiac troponin I (cTnI) is a crucial biomarker for diagnosing cardiac vascular diseases, including acute myocardial infarction (AMI). This study presents a proof-of-concept chemiluminescence-based immunosensor for rapid and accurate measurement of cTnI, with the potential for online monitoring. The immunosensor incorporates a flow cell design and a sensitive complementary metal-oxide-semiconductor (CMOS) camera for optical readout. A microfluidic setup was established to enable selective and quasi-online determination of cTnI within ten minutes. The sensor was tested with recombinant cTnI in phosphate buffer, demonstrating measurements in the concentration range of 2–25 µg/L, with a limit of detection (LoD) of 0.6 µg/L (23 pmol/L) achieved using the optimized system. The immunosensor exhibited high selectivity, as no cross-reactivity was observed with other recombinant proteins such as cTnT and cTnC at a concentration of 16 µg/L. Measurements with diluted blood plasma and serum yielded an LoD of 60 µg/L (2.4 nmol/L) and 70 µg/L (2.9 nmol/L), respectively. This biosensor offers a promising approach for the rapid and sensitive detection of cTnI, contributing to the diagnosis and management of acute myocardial infarction and other cardiac vascular diseases. N2 - Das kardiale Troponin I (cTnI) ist ein wichtiger Biomarker für die Diagnose von Herz-Kreislauf-Erkrankungen, einschließlich des akuten Myokardinfarkts (AMI). In dieser Studie wird ein auf Chemilumineszenz basierender Immunsensor für die schnelle und genaue Messung von cTnI vorgestellt, der das Potenzial für eine Online-Überwachung hat. Der Immunsensor besteht aus einer Durchflusszelle und einer empfindlichen CMOS-Kamera (Complementary Metal-Oxide-Semiconductor) zur optischen Detektion. Es wurde ein mikrofluidischer Aufbau entwickelt, der eine selektive und quasi Online-Bestimmung von cTnI innerhalb von zehn Minuten ermöglicht. Der Sensor wurde mit rekombinantem cTnI in Phosphatpuffer getestet und zeigte einen Messbereich von 2-25 µg/L, wobei mit dem optimierten System eine Nachweisgrenze (LoD) von 0,6 µg/L (23 pmol/L) erreicht wurde. Der Immunsensor zeigte eine hohe Selektivität, da keine Kreuzreaktivität mit anderen rekombinanten Proteinen wie cTnT und cTnC bei einer Konzentration von 16 µg/L beobachtet wurde. Messungen mit verdünntem Blutplasma und Serum ergaben einen LoD von 60 µg/L (2,4 nmol/L) bzw. 70 µg/L (2,9 nmol/L). Dieser Biosensor bietet einen vielversprechenden Ansatz für den schnellen und empfindlichen Nachweis von cTnI, der zur Diagnose und Behandlung des akuten Myokardinfarkts und anderer kardialer Gefäßerkrankungen beitragen kann. KW - Acute myocardial infarction KW - Heart attack KW - Emergency KW - Diagnosis KW - Cardiac troponin KW - Biomarker KW - Immunosensor KW - Biosensor KW - Chemiluminescence KW - Luminol KW - Peroxidase KW - Monoclonal antibodies KW - Flow injection immunoassay KW - Immunometric assay KW - Immunometric biosensor KW - Microfluidic system KW - Monolithic column KW - Online biosensor PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-575471 DO - https://doi.org/10.3390/bios13040455 SN - 2079-6374 VL - 13 IS - 4 SP - 1 EP - 20 PB - MDPI CY - Basel AN - OPUS4-57547 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Steglich, P. A1 - Rabus, D. G. A1 - Sada, C. A1 - Paul, Martin A1 - Weller, Michael G. A1 - Mai, C. A1 - Mai, A. T1 - Silicon Photonic Micro-Ring Resonators for Chemical and Biological Sensing: A Tutorial N2 - Silicon photonic micro-ring resonators (MRR) developed on the silicon-on-insulator (SOI) platform, owing to their high sensitivity and small footprint, show great potential for many chemical and biological sensing applications such as label-free detection in environmental monitoring, biomedical engineering, and food analysis. In this tutorial, we provide the theoretical background and give design guidelines for SOI-based MRR as well as examples of surface functionalization procedures for label-free detection of molecules. After introducing the advantages and perspectives of MRR, fundamentals of MRR are described in detail, followed by an introduction to the fabrication methods, which are based on a complementary metal-oxide semiconductor (CMOS) technology. Optimization of MRR for chemical and biological sensing is provided, with special emphasis on the optimization of waveguide geometry. At this point, the difference between chemical bulk sensing and label-free surface sensing is explained, and definitions like waveguide sensitivity, ring sensitivity, overall sensitivity as well as the limit of detection (LoD) of MRR are introduced. Further, we show and explain chemical bulk sensing of sodium chloride (NaCl) in water and provide a recipe for label-free surface sensing. KW - Lab on a chip KW - Biosensor KW - Cmos KW - Silanization KW - Surface derivatization KW - Evanescent wave PY - 2021 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-529360 DO - https://doi.org/10.36227/techrxiv.14909901.v1 SP - 1 EP - 18 PB - IEEE CY - Piscataway Township AN - OPUS4-52936 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Coutinho, M.L. A1 - Miller, A. Z. A1 - Martin-Sanchez, Pedro Maria A1 - Mirao, J. A1 - Gomez-Bolea, A. A1 - Machado-Moreira, B. A1 - Cerqueira-Alves, L. A1 - Jurado, V. A1 - Saiz-Jimenez,, C. A1 - Lima, A. A1 - Phillips, A. J. L. A1 - Pina, F. A1 - Macedo, M. F. T1 - A multiproxy approach to evaluate biocidal treatments on biodeteriorated majolica glazed tiles N2 - The Fishing House located on the grounds of the Marquis of Pombal Palace, Oeiras, Portugal, was built in the 18th century. During this epoch, Portuguese gardens, such as the one surrounding the Fishing House, were commonly ornamented with glazed wall tile claddings. Currently, some of these outdoor tile panels are covered with dark colored biofilms, contributing to undesirable aesthetic changes and eventually inducing chemical and physical damage to the tile surfaces. Phylogenetic analyses revealed that the investigated biofilms are mainly composed of green algae, cyanobacteria and dematiaceous fungi. With the aim of mitigating biodeterioration, four different biocides (TiO2 nanoparticles, Biotin® T, Preventol® RI 80 and Albilex Biostat®) were applied in situ to the glazed wall tiles. Their efficacy was monitored by visual examination, epifluorescence microscopy and DNA-based analysis. Significant changes in the microbial community composition were observed 4 months after treatment with Preventol® RI 80 and Biotin® T. Although the original community was inactivated after these treatments, an early stage of re-colonization was detected 6 months after the biocide application. TiO2 nanoparticles showed promising results due to their self-cleaning effect, causing the detachment of the biofilm from the tile surface, which remained clean 6 and even 24 months after biocide application. KW - Biofilm KW - Glazed tiles KW - Fungi PY - 2016 DO - https://doi.org/10.1111/1462-2920.13380 SN - 1462-2912 SN - 1462-2920 VL - 18 IS - 12 SP - 4794 EP - 4816 PB - Society for Applied Microbiology and John Wiley & Sons Ltd AN - OPUS4-37380 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - De la Rosa, J. M. A1 - Martin-Sanchez, Pedro Maria A1 - Santiago-Cortes, S. A1 - Hermosin, B. A1 - Knicker, H. A1 - Saiz-Jimenez, C. ED - De la Rosa, J. M. T1 - Structure of melanins from the fungi Ochroconis lascauxensis and Ochroconis anomala contaminating rock art in the Lascaux Cave N2 - Two novel species of the fungal genus Ochroconis, O. lascauxensis and O. anomala have been isolated from the walls of the Lascaux Cave, France. The interest in these fungi and their melanins lies in the formation of black stains on the walls and rock art which threatens the integrity of the paintings. Here we report solid-state cross polarization magic-angle spinning 13C and 15N nuclear magnetic resonance (NMR) spectroscopy and surface-enhanced Raman spectroscopy (SERS) of the melanins extracted from the mycelia of O. lascauxensis and O. anomala in order to known their chemical structure. The melanins from these two species were compared with those from other fungi. The melanins from the Ochroconis species have similar SERS and 13C and 15N NMR spectra. Their chemical structures as suggested by the data are not related to 3,4-dihydroxyphenylalanine, 5,6-dihydroxyindole or 1,8-dihydroxynaphthalene precursors and likely the building blocks from the melanins have to be based on other phenols that react with the N-terminal amino acid of proteins. The analytical pyrolysis of the acid hydrolysed melanin from O. lascauxensis supports this assumption. KW - Microbiology KW - Biodeterioration KW - Melanins KW - Fungi PY - 2017 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-435345 DO - https://doi.org/10.1038/s41598-017-13862-7 SN - 2045-2322 VL - 7 SP - 13441, 1 EP - 13441, 11 PB - Nature AN - OPUS4-43534 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Hernández-Gómez, R. A1 - Tuma, Dirk A1 - Lozano-Martín, D. A1 - Chamorro, C. R. T1 - Accurate experimental (p, rho, T) data of natural gas mixtures for the assessment of reference equations of state when dealing with hydrogen-enriched natural gas N2 - The GERG-2008 equation of state is the approved ISO standard (ISO 20765-2) for the calculation of thermophysical properties of natural gas mixtures. The composition of natural gas can vary considerably due to the diversity of origin. Further diversification was generated by adding hydrogen, biogas, or other non-conventional energy gases. In this work, high-precision experimental (p, rho, T) data for two gravimetrically prepared synthetic natural gas mixtures are reported. One mixture resembled a conventional natural gas of 11 components (11 M) with a nominal mixture composition (amount-of-substance fraction) of 0.8845 for methane as the matrix compound with the other compounds being 0.005 for oxygen, 0.04 for nitrogen, 0.015 for carbon dioxide, 0.04 for ethane, 0.01 for propane, 0.002 each for n- and isobutane, and ultimately 0.0005 each for isopentane, n-pentane, and nhexane. The other mixture was a 13-component hydrogen-enriched natural gas with a low calorific value featuring a nominal composition of 0.7885 for methane, 0.03 for hydrogen, 0.005 for helium, 0.12 for nitrogen, 0.04 for carbon dioxide, 0.0075 for ethane, 0.003 for propane, 0.002 each for n- and isobutane, and 0.0005 each for neopentane, isopentane, npentane, and n-hexane. Density measurements were performed in an isothermal operational mode at temperatures between 260 and 350 K and at pressures up to 20 MPa by using a single-sinker densimeter with magnetic suspension coupling. The data were compared with the corresponding densities calculated from both GERG-2008 and AGA8-DC92 equations of state to test their performance on real mixtures. The average absolute Deviation from GERG-2008 (AGA8-DC92) is 0.027% (0.078%) for 11 M and 0.095% (0.062%) for the 13-component H2-enriched mixture, respectively. The corresponding maximum relative Deviation from GERG-2008 (AGA8-DC92) amounts to 0.095% (0.127%) for 11 M and 0.291% (0.193%) for the H2-enriched mixture. KW - Hydrogen-enriched natural gas KW - Gravimetric preparation KW - Volumetric data KW - GERG-2008 equation of state PY - 2018 DO - https://doi.org/10.1016/j.ijhydene.2018.10.027 SN - 0360-3199 SN - 1879-3487 VL - 43 IS - 49 SP - 21983 EP - 21998 PB - Elsevier CY - Amsterdam AN - OPUS4-46686 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Trela, C. A1 - Kind, Thomas A1 - Günther, Martin T1 - Ground penetrating radar in reflection vs transmission mode for void detection in concrete structures N2 - The concreting of prefabricated concrete structures can lead to insufficient bonding or even to remaining cavities. Honeycombs (aggregate clusters without cement) represent potential weakening of the structure and need to be detected non-destructively. In our study we tested the capability of ground penetrating radar (GPR)techniques for this purpose. We applied GPR in reflection mode and zero-offset profiling (ZOP) Transmission mode on a precast concrete twin wall with built-in honeycombs. GPR measurements were performed as twochannel measurement with ground coupled antennas with centre frequencies of 1.5 GHz and 2.6 GHz mounted to an automated scanner system. Our findings show that ZOP transmission measurements are a more efficient method to detect voids in reinforced concrete structures compared to reflection mode measurements. This holds for both the effort needed for the measurement and the evaluation as well as the validity of the data. Honeycombs (basically representing voids) are usually characterized by strongly reduced amplitudes and earlier arrivals of the transmitted wave. T2 - NDT-CE 2015 - International symposium non-destructive testing in civil engineering CY - Berlin, Germany DA - 15.09.2015 KW - Ground penetrating radar KW - Reflection KW - Transmission KW - Reinforced concrete KW - Prefabricated wall KW - Void detection PY - 2015 SN - 1435-4934 SP - 324 EP - 344 PB - Technische Universität Berlin / Bundesanstalt für Materialforschung und -prüfung CY - Berlin, Germany AN - OPUS4-40006 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Dippong, Martin A1 - Carl, Peter A1 - Lenz, C. A1 - Schenk, J. A. A1 - Hoffmann, Katrin A1 - Schwaar, Timm A1 - Schneider, Rudolf A1 - Kuhne, Maren T1 - Hapten-specific single-cell selection of hybridoma clones by fluorescence-activated cell sorting for the generation of monoclonal antibodies N2 - The conventional hybridoma screening and subcloning process is generally considered to be one of the most critical steps in hapten-specific antibody production. It is time-consuming, monoclonality is not guaranteed, and the number of clones that can be screened is limited. Our approach employs a novel hapten-specific labeling technique of hybridoma cells. This allows for fluorescence-activated cell sorting (FACS) and single-cell deposition and thereby eliminates the above-mentioned problems. A two-step staining approach is used to detect antigen specificity and antibody expression: in order to detect antigen specificity, hybridoma cells are incubated with a hapten−horseradish peroxidase conjugate (hapten−HRP), which is subsequently incubated with a fluorophore-labeled polyclonal anti-peroxidase antibody (anti-HRP−Alexa Fluor 488). To characterize the expression of membrane-bound immunoglobulin G (IgG), a fluorophore-labeled anti-mouse IgG antibody (anti-IgG−Alexa Fluor 647) is used. Hundreds of labeled hybridoma cells producing monoclonal antibodies (mAbs) specific for a hapten were rapidly isolated and deposited from a fusion mixture as single-cell clones via FACS. Enzyme-linked immunosorbent assay (ELISA) measurements of the supernatants of the sorted hybridoma clones revealed that all hapten-specific hybridoma clones secrete antibodies against the target. There are significant improvements using this high-throughput technique for the generation of mAbs including increased yield of antibody-producing hybridoma clones, ensured monoclonality of sorted cells, and reduced development times. KW - Monoclonal antibodies KW - FACS KW - Hybridoma cells PY - 2017 DO - https://doi.org/10.1021/acs.analchem.6b04569 SN - 0003-2700 SN - 1520-6882 VL - 89 IS - 7 SP - 4007 EP - 4012 PB - ACS Publications AN - OPUS4-40320 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Martin, S. A1 - Walnsch, A. A1 - Nolze, Gert A1 - Leineweber, A. A1 - Léaux, F. A1 - Scheuerlein, C. T1 - The crystal structure of (Nb0.75Cu0.25)Sn-2 in the Cu-Nb-Sn system N2 - During the processing of superconducting Nb3Sn wire, several intermediate intermetallic phases including a previously encountered Cu-Nb-Sn phase show up. The yet unknown crystal structure of this phase is now identified by a combination of different experimental techniques and database search to be of the hexagonal NiMg2 type with a proposed composition of about (Nb0.75Cu0.25)Sn2. The structure determination started from an evaluation of the lattice parameters from EBSD Kikuchi patterns from quenched material suggesting hexagonal or orthorhombic symmetry. A database search then led to the hexagonal NiMg2 type structure, the presence of which was confirmed by a Rietveld analysis on the basis of high energy synchrotron X-ray powder diffraction data. Assuming a partial substitution of Nb in orthorhombic NbSn2 by Cu, the change of the valence electron concentration provokes a structural transformation from the CuMg2 type for NbSn2 to the NiMg2 type for (Nb0.75Cu0.25)Sn2. In the previous literature the (Nb0.75Cu0.25)Sn2 phase described here has occasionally been referred to as Nausite. KW - Electron backscatter diffraction KW - X-ray diffraction KW - Intermetallic compound KW - Structure solution KW - Superconductor PY - 2017 DO - https://doi.org/10.1016/j.intermet.2016.09.008 SN - 0966-9795 SN - 1879-0216 VL - 80 SP - 16 EP - 21 PB - Elsevier Ltd. AN - OPUS4-37874 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Maierhofer, Christiane A1 - Krause, Martin A1 - Wöstmann, Jens A1 - Röllig, Mathias A1 - Arndt, Ralf A1 - Streicher, Doreen A1 - Kohl, C. ED - L. Binda, ED - M. di Prisco, ED - R. Felicetti, T1 - Influence of concret properties on the calibration of radar, ultrasonics and active thermography T2 - 1st International RILEM Conference, on Site Assessment of Concrete, Masonry and Timber Structures (SACoMaTiS 2008) CY - Varenna, Italy DA - 2008-09-01 KW - Concrete KW - Radar KW - Ultrasonics KW - Active thermography KW - Velocity calibration PY - 2008 SN - 978-2-35158-062-2 VL - 1 IS - PRO 59 SP - 15 EP - 24 PB - RILEM Publications AN - OPUS4-18033 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Hasenstab, Andreas A1 - Krause, Martin A1 - Hillemeier, B. A1 - Rieck, C. T1 - Ultraschallecho-Messungen an Holz N2 - In der Praxis kann Fäulnis in Holzkonstruktionen ein großes Problem darstellen. Ein Fäulnisbefall kann zu einer Schädigung in der Gesamtkonstruktion führen. Zusammen mit der TU Berlin wurden an der Bundesanstalt für Materialforschung und -prüfung (BAM) Versuche mit Ultraschallecho zur Detektion von Bauteilrückwänden und verdeckten Hohlstellen durchgeführt. Hierbei werden Sender und Empfänger auf einer Bauteilseite angekoppelt, was eine große Anwendungsvielfalt ermöglicht. Im Rahmen der Versuche an der BAM wurden zylindrische Longitudinalwellenprüfköpfe in Zweikopftechnik mit 100 kHz angeregt und an den Probekörpern mit verschiedenen Koppelmitteln angekoppelt. Die Messergebnisse wurden graphisch als B-Bilder dargestellt und ausgewertet. Dabei zeigte sich, dass die Rückwand der fehlerfreien Probekörper klar geortet wird und eingebrachte Hohlstellen besonders gut detektiert werden können. KW - Zerstörungsfreie Prüfung KW - Ultraschallecho KW - Holz PY - 2006 DO - https://doi.org/10.1007/s00107-006-0124-x SN - 0018-3768 VL - 64 SP - 475 EP - 481 PB - Springer CY - Berlin AN - OPUS4-23056 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Friese, Martin A1 - Roder, C. A1 - Effner, Ute A1 - Mielentz, Frank T1 - Quality control for crack repair - a new approach using ultrasonic imaging T2 - NDE/NDT for highways and bridges - Structural materials technology CY - New York, NY, USA DA - 2010-08-16 KW - Zerstörungsfreie Prüfung KW - Ultraschall KW - Risse KW - Erfolgskontrolle Rissinjektion PY - 2010 SN - 978-1-57117-211-2 SP - 374 EP - 382 AN - OPUS4-22549 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Mya, K.Y. A1 - Gose, H.B. A1 - Pretsch, Thorsten A1 - Bothe, Martin A1 - He, C. T1 - Star-shaped POSS-polycaprolactone polyurethanes and their shape memory performance N2 - Star-shaped polyhedral oligomeric silsesquioxane (SPOSS)-based multi-arm poly(ε-caprolactones) (PCLs) with various arm lengths were synthesized by ring opening polymerization of ε-caprolactone. Increasing the PCL arm lengths was observed to increase the melting temperature and also the melt crystallization temperature in SPOSS-PCLs. Star-shaped POSS-PCL polyurethanes (SPOSS-PUs) were then prepared by cross-linking SPOSS-PCLs with hexamethylene diisocyanate (HMDI) and their shape memory (SM) behaviour was determined. For this purpose two cyclic thermo-mechanical testing concepts with similar programming (deformation and shape fixing) but different recovery strategies (free strain versus fixed-strain constrained stress recovery) were used and the synthesized polymers were systematically investigated around the crystallization and melting temperatures of PCL. SPOSS-PU with the highest POSS content exhibited remarkable cycles-averaged (N = 2–5) shape fixities and strain recoverabilities of 98% and stress recoverabilities close to 100%. The main structural factors that were expected to reduce the SM performances with increasing PCL arm lengths were a lowering of cross-link density (content of octasubstituted POSS) and an increase in chain flexibility/molecular mobility. KW - Shape memory polymer KW - Active polymer KW - Hybrid star-shaped polymer KW - POSS-polycaprolactone polyurethanes KW - Thermo-mechanical properties PY - 2011 DO - https://doi.org/10.1039/c0jm04459h SN - 0959-9428 SN - 1364-5501 VL - 21 IS - 13 SP - 4827 EP - 4836 PB - Royal Society of Chemistry CY - Cambridge AN - OPUS4-23479 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Hasenstab, Andreas A1 - Krause, Martin A1 - Rieck, C. A1 - Hillemeier, B. T1 - Use of Low Frequency Ultrasound Echo Technique to Determine Cavities in Wooden Construction Composites T2 - 6th International Symposium Non-Destructive Testing in Civil Engineering (NDT-CE) CY - Berlin, Germany DA - 2003-09-16 PY - 2003 UR - http://www.ndt.net/article/ndtce03/papers/p051/p051.htm SN - 3-931381-49-8 SP - 1(?) EP - 9(?) PB - DGZfP CY - Berlin AN - OPUS4-3230 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Hertwig, Andreas A1 - Martin, Sven A1 - Krüger, Jörg A1 - Spielmann, C. A1 - Lenner, M. A1 - Kautek, Wolfgang ED - Dausinger, F. ED - Lichtner, F. ED - Lubatschowski, H. T1 - Primary hazards and reliability of protective materials N2 - Femtosecond laser pulses are close to industrial use. The advantages of ultrashort laser pulses for micromachining applications especially in the case of dielectric and biological samples down to pulse durations of 5 fs have been established. The current international standards of laser safety are primarily concerned with CW and pulsed lasers down to the nanosecond range. Therefore, human tissue and laser-protection equipment was investigated with respect to its resistance and protection performance for femtosecond laser illumination down to 30 fs. This included filter glasses for laser protection eyewear, polymer and textile materials used in curtains and guards. Bulk absorber filters can provide enough protection against laser radiation, give a sufficiently broad absorption spectrum. Materials are damaged more easily by femtosecond laser radiation. The need for sufficient spectral broadness as well as the different damage thresholds have to be included in international laser safety standards. This work should trigger the development of novel eye-protection devices that are lighter and ergonomically more acceptable than present commercial models. KW - Lasersicherheit KW - Kurzpulslaser KW - Femtosekunden KW - Lasertechnik KW - Materialbearbeitung PY - 2004 SN - 3-540-20114-9 DO - https://doi.org/10.1007/b96440 SN - 0303-4216 N1 - Serientitel: Topics in applied physics – Series title: Topics in applied physics IS - 96 SP - 287 EP - 307 PB - Springer CY - Berlin AN - OPUS4-4661 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Hattwig, Martin A1 - Krause, Ulrich A1 - Proust, C. ED - Hattwig, M. T1 - Explosion Venting PY - 2004 SN - 3-527-30718-4 SP - 493 EP - 530 PB - Wiley-VCH CY - Weinheim AN - OPUS4-6896 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Hattwig, Martin A1 - Krause, Ulrich A1 - Proust, C. ED - Steen, H. T1 - Explosionsdruckentlastung PY - 2000 SN - 3-527-29848-7 SP - 577 EP - 618 PB - Wiley-VCH CY - Weinheim AN - OPUS4-6894 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Starke, K. A1 - Ristau, D. A1 - Martin, Sven A1 - Hertwig, Andreas A1 - Krüger, Jörg A1 - Allenspacher, P. A1 - Riede, W. A1 - Meister, S. A1 - Theiss, C. A1 - Sabbah, A. A1 - Rudolph, W. A1 - Raab, V. A1 - Grigonis, R. A1 - Rakickas, T. A1 - Sirutkaitis, V. ED - Exarhos, G. J. T1 - Results of a round-robin experiment in multiple-pulse LIDT measurement with ultrashort pulses T2 - 35th Annual Boulder Damage Symposium ; 35th Annual Symposium on Optical Materials for High-Power Lasers CY - Boulder, CO, USA DA - 2003-09-22 KW - Multiple-pulse damage KW - ISO 11254-2 KW - S on 1-LIDT KW - Round-robin experiment KW - CHOCLAB PY - 2004 SN - 0-8194-5163-0 DO - https://doi.org/10.1117/12.525135 SN - 0038-7355 N1 - Serientitel: Proceedings of SPIE – Series title: Proceedings of SPIE IS - 5273 SP - 388 EP - 395 PB - SPIE, the International Society for Optical Engineering CY - Bellingham, Wash. AN - OPUS4-4948 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Kautek, Wolfgang A1 - Hertwig, Andreas A1 - Martin, Sven A1 - Krüger, Jörg A1 - Lenzner, Matthias A1 - Spielmann, C. A1 - Lenner, M. A1 - Bunte, J. A1 - Puester, T. A1 - Burmester, T. A1 - Fiedler, A. A1 - Heberer, E. A1 - Brose, M. A1 - Stingl, A. A1 - Kiehl, P. A1 - Hönigsmann, H. A1 - Trautinger, F. A1 - Grabner, G. T1 - Safety in Femtosecond Laser Technology - Recent Results of a European Research Project (406) T2 - International Laser Safety Conference 2003 ; ILSC 2003 CY - Jacksonville, FL, USA DA - 2003-03-10 PY - 2003 SN - 0-912035-38-2 SP - 1(?) EP - 10(?) PB - Laser Institute of America CY - Orlando, Fla. AN - OPUS4-2259 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Hasenstab, Andreas A1 - Krause, Martin A1 - Rieck, C. A1 - Hillemeier, B. T1 - Materialuntersuchung an Holz mit niederfrequenter Ultraschall-Echotechnik N2 - Kurzfassung Die Anwendung niederfrequenter Ultraschall-Echotechnik mit Longitudinal- und Transversalwellen für die Materialuntersuchung von Holzbauteilen wird beschrieben. Weiterhin wird der Einfluss der Holzfasern auf die Schallgeschwindigkeiten und Oberflächenwellen an Hand von Messergebnissen aufgezeigt. Die Leistungsfähigkeit des Ultraschall-Echoverfahrens an ungeschädigten Holzkörpern und Körpern mit eingebrachten Bohrungen in Faserrichtung (Kernfäulnissimulation) wird dargestellt. Es ist zudem möglich, bei koppelmittelfreier Ankopplung mit Transversalwellen indirekt Fäulnis von der ungeschädigten Bauteilseite aus zu orten. Als Referenzverfahren werden die Bohrwiderstandsmethode oder die Röntgendurchstrahlung eingesetzt. T2 - Jahrestagung Zerstörungsfreie Materialprüfung 2004 CY - Salzburg, Österreich DA - 2004-05-17 PY - 2004 UR - http://www.ndt.net/article/dgzfp04/papers/v87/v87.htm SN - 3-931381-55-2 SP - 1(?) EP - 9(?) PB - DGZfP CY - Berlin AN - OPUS4-5216 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Hasenstab, Andreas A1 - Krause, Martin A1 - Lutz, J. A1 - Hillemeier, B. A1 - Rieck, C. T1 - Niederfrequente Ultraschall-Echo-Verfahren und Bohrwiderstandsmessung zur Untersuchung von Holzbauteilen T2 - DGZfP Jahrestagung CY - Rostock, Deutschland DA - 2005-05-02 KW - ZfP an Holzbauteilen KW - Fehlstellen KW - Minderdicken KW - Ultraschallecho-Experimente an Probekörpern KW - Ultraschall-Echo KW - Fäulnis KW - Bauwesen PY - 2005 SN - 3-931381-64-1 N1 - Serientitel: Berichtsband / Deutsche Gesellschaft für zerstörungsfreie Prüfung e. V. – Series title: Berichtsband / Deutsche Gesellschaft für zerstörungsfreie Prüfung e. V. IS - 94-CD SP - 1(?) EP - 11(?) PB - DGZfP CY - Berlin AN - OPUS4-11960 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Hasenstab, Andreas A1 - Krause, Martin A1 - Hillger, w. A1 - Bühling, L. A1 - Ilse, D. A1 - Hillemeier, B. A1 - Rieck, C. T1 - Luftultraschall und Ultraschall-Echo-Technik an Holz T2 - DGZfP Jahrestagung CY - Rostock, Deutschland DA - 2005-05-02 KW - ZfP an Holzbauteilen KW - Fehlstellen KW - Minderdicken KW - Ultraschallecho-Experimente an Probekörpern KW - Ultraschall-Echo KW - Fäulnis KW - Bauwesen KW - Luftultraschall PY - 2005 SN - 3-931381-64-1 N1 - Serientitel: Berichtsband / Deutsche Gesellschaft für zerstörungsfreie Prüfung e. V. – Series title: Berichtsband / Deutsche Gesellschaft für zerstörungsfreie Prüfung e. V. IS - 94-CD SP - 1(?) EP - 15(?) PB - DGZfP CY - Berlin AN - OPUS4-11961 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Hasenstab, Andreas A1 - Krause, Martin A1 - Scheer, C. T1 - Zerstörungsfreie Integritätsprüfung von Holz mit dem Ultraschallecho-Verfahren T2 - Forschungskolloquium "Holzbau Forschung + Praxis" CY - Stuttgart, Deutschland DA - 2006-02-23 PY - 2006 SP - 33 EP - 40 PB - Technische Universität Stuttgart CY - Stuttgart AN - OPUS4-12242 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Bunte, J. A1 - Barcikowski, S. A1 - Burmester, T. A1 - Püster, T. A1 - Hertwig, Andreas A1 - Kautek, Wolfgang A1 - Krüger, Jörg A1 - Martin, Sven A1 - Spielmann, C. A1 - Lenner, M. A1 - Brose, M. T1 - Sicherer Umgang mit Ultrakurzpuls-Lasern, Teil 1: Primäre Gefährdungen PY - 2005 SN - 0945-8875 IS - 2 SP - 6 EP - 11 PB - Magazin-Verl. CY - Bad Nenndorf AN - OPUS4-11001 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Bunte, J. A1 - Barcikowski, S. A1 - Burmester, T. A1 - Püster, T. A1 - Hertwig, Andreas A1 - Kautek, Wolfgang A1 - Krüger, Jörg A1 - Martin, Sven A1 - Spielmann, C. A1 - Lenner, M. A1 - Brose, M. T1 - Sicherer Umgang mit Ultrakurzpuls-Lasern, Teil 2: Sekundäre Gefährdungen PY - 2005 SN - 0945-8875 IS - 4 SP - 13 EP - 18 PB - Magazin-Verl. CY - Bad Nenndorf AN - OPUS4-11002 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Frunza, L. A1 - Schönhals, Andreas A1 - Frunza, S. A1 - Parvulescu, V.I. A1 - Cojocaru, B. A1 - Carriazo, D. A1 - Martín, C. A1 - Rives, V. T1 - Rotational Fluctuations of Water Confined to Layered Oxide Materials - Nonmonotonous Temperature Dependence of Relaxation Times N2 - The rotational molecular dynamics of water confined to layered oxide materials with brucite structure was studied by dielectric spectroscopy in the frequency range from 10-2 to 107 Hz and in a broad temperature interval. The layered double hydroxide samples show one relaxation process, which was assigned to fluctuations of water molecules forming a layer, strongly adsorbed to the oxide surface. The temperature dependence of the relaxation rates has an unusual saddlelike shape characterized by a maximum. The model of Ryabov et al. (J. Phys. Chem. B 2001, 105, 1845) recently applied to describe the dynamics of water molecules in porous glasses is employed also for the layered materials. This model assumes two competing effects: rotational fluctuations of water molecules that take place simultaneously with defect formation, allowing the creation of free volume necessary for reorientation. The activation energy of rotational fluctuations, the energy of defect formation, a pre-exponential factor, and the defect concentration are obtained as main parameters from a fit of this model to the data. The values of these parameters were compared with those found for water confined to nanoporous molecular sieves, porous glasses, or bulk ice. Several correlations were discussed in detail, such as the lower the value of the energy of defect formation, the higher the number of defects. The pre-exponential factor increases with increasing activation energy, as an expression of the compensation law, and indicates the cooperative nature of the motional process. The involvement of the surface OH groups and of the oxygen atoms of the interlayer anions in the formation of hydrogen bonds was further discussed. For the birnessite sample, the relaxation processes are probably overlaid by a dominating conductivity contribution, which is analyzed in its frequency and temperature dependence. It is found that the conductivity of birnessite obeys the characteristics of semiconducting disordered materials. Especially the Barton/Nakajima/Namikawa relationship is fulfilled. Analyzing the temperature dependence of the direct current (dc) conductivity σ0 in detail gives some hint that σ0(T) has also an unusual saddlelike form. PY - 2007 DO - https://doi.org/10.1021/jp0717140 SN - 1089-5639 SN - 1520-5215 VL - 111 IS - 24 SP - 5166 EP - 5175 PB - Soc. CY - Washington, DC AN - OPUS4-15718 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schmidt, Martin A1 - Wanke, C. A1 - Krause, U. T1 - Determination of measurement uncertainties in adiabatic hot-storage experiments for reactive dusts N2 - The formal kinetics of self-ignition of solid bulk materials theoretically can be derived from just one single adiabatic hot-storage test. The question arises how uncertainties in the measurements can be quantified and how these uncertainties affect the results of the subsequent predictions. Adiabatic and isoperibolic hot-storage basket tests were performed for samples of lignite coal, black coal, cork dust, a polymer dust, and wax-coated silicid acid. In the adiabatic experiments, the starting temperature and the temperature control of the oven were varied systematically to study the uncertainty margin of adiabatic tests. The apparent activation energy and the pre-exponential factor of the lumped reaction were derived from the adiabatic tests including average values and standard deviations and compared to isoperibolic experiments performed according to the European standard EN 15188. It could be shown that with a precise temperature control of the adiabatic oven combined with an automated computation of the maximum rate of temperature rise the uncertainty of the apparent activation energy can be limited to less than 10%. KW - Adiabatic test KW - Bulk materials KW - Hot-storage test KW - Reactive dust KW - Self-ignition PY - 2013 DO - https://doi.org/10.1002/ceat.201300068 SN - 0930-7516 SN - 1521-4125 VL - 36 IS - 10 SP - 1 EP - 10 PB - Wiley-VCH Verl. CY - Weinheim AN - OPUS4-29036 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Lenke, Karoline A1 - Schmidt, R. A1 - Märtin, J. A1 - Hoffmann, G. A1 - Cherif, C. T1 - Simulation of the yarn transportation dynamics in a warp knitting machine N2 - To date, in the textile manufacturing process of warp knitting, trouble-shooting and process optimization mainly rely on empirical knowledge and experiments. This factor limits the achievable increase in productivity and quality. On the other hand, using simulations, different phenomena that affect the quality of the knitted fabric and the knitting process can be clarified in the run-up of the experiments. Consequently, an increase in quality and flexibility can be reached with reduced experimental effort. This paper presents a process simulation of the warp thread dynamics in the thread feeding system of a warp knitting machine. For this purpose, a continuum model of the warp thread that includes the spatial dynamics of the thread and the axial transport movement has been developed. KW - Simulation of yarn transportation KW - Yarn transportation model KW - Warp knitting machine KW - Continuum model KW - Process optimization KW - Knitting PY - 2013 DO - https://doi.org/10.1177/0040517512470197 SN - 0040-5175 N1 - Geburtsname von Lenke, Karoline: Metzkes, K. - Birth name of Lenke, Karoline: Metzkes, K. VL - 83 IS - 12 SP - 1251 EP - 1262 PB - Sage Publ. CY - London AN - OPUS4-28381 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Krüger, Jörg A1 - Lenzner, Matthias A1 - Martin, Sven A1 - Lenner, M. A1 - Spielmann, C. A1 - Fiedler, A. A1 - Kautek, Wolfgang ED - Phipps, C. R. T1 - Femtosecond laser induced damage in absorbing filters used for laser protection N2 - Damage experiments of absorbing filters (Schott BG18 and BG36) were performed with Ti:sapphire laser pulses with durations from 30 fs to 340 fs (800 nm, 1 kHz) in air. The direct focusing technique was employed under single- and multi-pulse irradiation conditions. Ablation threshold fluences were determined from a semi-logarithmic plot of the ablation crater diameter vs. laser fluence. The damage threshold fluence decreases for shorter pulse durations. In the investigated pulse duration range, the measured multi-pulse ablation threshold fluences are practically similar to those of undoped glass material (~1 Jcm-2). That means that the multi-pulse ablation threshold is independent on the doping level of the filters. For more than 100 pulses per spot and all pulse durations applied, the threshold fluence saturates. This leads to technically relevant damage threshold values in the femtosecond laser pulse duration domain. T2 - 4th SPIE's International Conference on High-Power Laser Ablation CY - Taos, NM, USA DA - 2002-04-22 KW - Ablation KW - Damage KW - Eye protection KW - Femtosecond pulse laser KW - Incubation KW - Laser safety KW - Threshold fluence PY - 2002 SN - 0-8194-4524-X DO - https://doi.org/10.1117/12.482109 SN - 1605-7422 N1 - Serientitel: SPIE proceedings series – Series title: SPIE proceedings series VL - 1 IS - 4760 SP - 398 EP - 405 PB - SPIE CY - Bellingham, Wash. AN - OPUS4-1550 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kautek, Wolfgang A1 - Krüger, Jörg A1 - Lenzner, Matthias A1 - Martin, Sven A1 - Lenner, M. A1 - Spielmann, C. A1 - Fiedler, A. ED - Meunier, M. T1 - Single- and multi-pulse femtosecond laser ablation of optical filter materials N2 - Commercially available absorption filters (Schott BG18 and BG36) were investigated with respect to their single- and multi-pulse ablation threshold using laser pulses from a Ti:Sapphire laser in the range between 30 and 340 fs. It could be observed, that the threshold fluence decreases for shorter pulse durations. The similarity of the measured multi-pulse threshold fluences with those of undoped glass material (around 1 J/cm^2 for a pulse duration of 30 fs) suggests that, for very short pulses, the threshold is independent on the doping level and therefore, linear absorption does not significantly contribute to laser-induced damage. For >100 pulses per spot and all pulse durations applied, the threshold fluences saturate. This independence on the number of applied pulses leads to technically relevant damage threshold values. T2 - Symposium D - European Materials Research Society CY - Strasbourg, France DA - 2002-06-18 PY - 2002 UR - http://www.emrs-strasbourg.com/files/pdf/2002_SPRING/02_Prog_Dv2.pdf N1 - Serientitel: Applied surface science – Series title: Applied surface science VL - 208/209.2003,1 IS - 1 SP - 1(?) PB - Elsevier CY - Amsterdam AN - OPUS4-1588 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Hasenstab, Andreas A1 - Rieck, C. A1 - Hillemeier, B. A1 - Krause, Martin T1 - Hohlstellenortung in Holzbalken mit dem Ultraschallverfahren N2 - Zusammenfassung Die Anwendung des Ultraschallecho-Verfahrens zur Hohlstellenortung in Holzbalken wird beschrieben. An Hand der Versuchsergebnisse wird der Einfluss der Anisotropie des Holzes auf die Messkopfanordnung und Schallgeschwindigkeit dargestellt. Mit der optimierten Messanordnung ist die erfolgreiche Detektierung von Nachbildungen von Minderdicken und Kernfäule möglich. Besonders klar sind Schäden in Faserrichtung (Kernfäulenachbildung) nachzuweisen. Die sehr guten Ergebnisse zeigen die Anwendbarkeit des Ultraschallecho-Verfahrens an Holz. T2 - Jahrestagung Zerstörungsfreie Materialprüfung 2002 CY - Weimar, Deutschland DA - 2002-05-06 KW - ZfP an Holzbauteilen KW - Fehlstellen KW - Minderdicken KW - Ultraschallecho-Experimente an Probekörpern PY - 2002 UR - http://www.ndt.net/article/dgzfp02/papers/p32/p32.htm SN - 3-931381-39-0 N1 - Serientitel: Berichtsband / Deutsche Gesellschaft für zerstörungsfreie Prüfung e. V. – Series title: Berichtsband / Deutsche Gesellschaft für zerstörungsfreie Prüfung e. V. IS - 80-CD PB - DGZfP CY - Berlin AN - OPUS4-1937 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Beutel, R. A1 - Reinhardt, H.-W. A1 - Grosse, C. U. A1 - Glaubitt, A. A1 - Krause, Martin A1 - Maierhofer, Christiane A1 - Algernon, Daniel A1 - Wiggenhauser, Herbert A1 - Schickert, M. T1 - Performance Demonstration of Non-Destructive Testing Methods T2 - 9th European Conference on NDT CY - Berlin, Germany DA - 2006-09-25 KW - NDT-CE KW - Concrete KW - Ultrasonic echo KW - Impact-echo KW - Radar KW - Concrete cover of tendon ducts KW - Thickness measurement KW - Concrete slabs PY - 2006 SN - 3-931381-86-2 SP - 1(?) EP - 9(?) PB - European Federation for Non-Destructive Testing CY - Berlin AN - OPUS4-14382 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CHAP A1 - Beutel, R. A1 - Reinhardt, H.-W. A1 - Große, C. A1 - Krause, Martin A1 - Algernon, Daniel A1 - Streicher, Doreen A1 - Maierhofer, Christiane A1 - Glaubitt, A. T1 - Quantitativer Verfahrensvergleich KW - ZfPBau KW - Ultraschallecho KW - Radar KW - Impact-Echo KW - Dickenmessung KW - Betondeckung KW - Hüllrohrortung KW - Betonbauteile PY - 2006 SN - 978-3-433-01833-0 SN - 0342-7617 VL - 1 IS - Kap. V / Abschnitt 11 SP - 567 EP - 573 PB - Ernst CY - Berlin AN - OPUS4-14379 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Lozano-Martín, D. A1 - Akubue, G. U. A1 - Moreau, A. A1 - Tuma, Dirk A1 - Chamorro, C. R. T1 - Accurate experimental (p, rho, T) data of the (CO2 + O2) binary system for the development of models for CCS processes N2 - The limited availability of accurate experimental data in wide ranges of pressure, temperature, and composition is the main constraining factor for the proper development and assessment of thermodynamic models and equations of state. In the particular case of carbon capture and storage (CCS) processes, there is a clear need for data sets related to the (carbon dioxide + oxygen) mixtures that this work aims to address. This work provides new experimental (p, rho, T) data for three binary (CO2 + O2) mixtures with mole fractions of oxygen x(O2) = (0.05, 0.10, and 0.20) mol/mol, in the temperature range T = (250 to 375) K and pressure range p = (0.5 to 13) MPa. The measurements were performed with a high-precision single-sinker densimeter with magnetic suspension coupling. The density data were obtained with estimated expanded relative uncertainties of 0.02 % for the highest densities and up to 0.3 % for the lowest ones.The results were compared to the corresponding results calculated by the current reference equations of state for this kind of mixtures, namely the EOS-CG (combustion gases) and the GERG-2008 equation of state, respectively. The EOS-CG yields better estimations in density than the GERG-2008 equation of state. The results from the EOS-GC model show no systematic temperature dependence. For the GERG-2008 model, however, this criterion is significantly less fulfilled. KW - carbon capture and storage KW - single-sinker densimeter KW - equation of state PY - 2020 DO - https://doi.org/10.1016/j.jct.2020.106210 SN - 0021-9614 VL - 150 SP - 106210 PB - Elsevier Ltd. CY - Amsterdam AN - OPUS4-50925 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Krause, Martin A1 - Borchardt, Kerstin A1 - Lange, Marco A1 - Behrens, Matthias A1 - Maack, Stefan A1 - Mielentz, Frank A1 - Milmann, Boris A1 - Schaurich, Dieter A1 - Wöstmann, Jens A1 - Hintzpeter, F. A1 - Sodeikat, C. T1 - Kosteneinsparung durch Anwendung zerstörungsfreier Prüfverfahren für Betonbauteile beim Bauen im Bestand N2 - In Zeiten knapper Kassen wird überall nach Wegen gesucht Kosten einzusparen. Im Bauwesen geht es dabei um Kosteneinsparungen ohne Reduktion der Sicherheit und Dauerhaftigkeit des Bauwerks. Beim Bauen im Bestand können mit einer zerstörungsfreien Prüfung von Bauwerken die Weiternutzung oder die erforderlichen Umbauten optimiert werden und so Kosten eingespart werden. KW - Zerstörungsfreie Prüfung KW - Bauen im Bestand KW - Radar KW - Ultraschallecho KW - Kosteneinsparung PY - 2011 SN - 978-3-8167-8611-5 VL - 101 SP - 1 EP - 95 PB - Fraunhofer IRB Verl. CY - Stuttgart ET - Abschlussbericht AN - OPUS4-26649 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Lozano-Martín, D. A1 - Tuma, Dirk A1 - Kipphardt, Heinrich A1 - Khanipour, Peyman A1 - Chamorro, C. R. T1 - Thermodynamic characterization of the (H2 + C3H8) system significant for the hydrogen economy: Experimental (p, rho, T) determination and equation-of-state modelling N2 - For the gradual introduction of hydrogen in the energy market, the study of the properties of mixtures of hydrogen with typical components of natural gas (NG) and liquefied petroleum gas (LPG) is of great importance. This work aims to provide accurate experimental (p, rho, T) data for three hydrogen-propane mixtures with nominal compositions (amount of substance, mol/mol) of (0.95 H2 + 0.05 C3H8), (0.90 H2 + 0.10 C3H8), and (0.83 H2 + 0.17 C3H8), at temperatures of 250, 275, 300, 325, 350, and 375 K, and pressures up to 20 MPa. A single-sinker densimeter was used to determine the density of the mixtures. Experimental density data were compared to the densities calculated from two reference equations of state: the GERG-2008 and the AGA8-DC92. Relative deviations from the GERG-2008 EoS are systematically larger than those from the AGA8-DC92. They are within the ±0.5% band for the mixture with 5% of propane, but deviations are higher than 0.5% for the mixtures with 10% and 17% of propane, especially at low temperatures and high pressures. Finally, the sets of new experimental data have been processed by the application of two different statistical equations of state: the virial equation of state, through the second and third virial coefficients, B(T, x) and C(T, x), and the PC-SAFT equation of state. KW - Hydrogen-containing gas mixture KW - Density data KW - Equation of state KW - Virial coefficients PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-570056 DO - https://doi.org/10.1016/j.ijhydene.2022.11.170 SN - 0360-3199 VL - 48 IS - 23 SP - 8645 EP - 8667 PB - Elsevier B. V. CY - Amsterdam AN - OPUS4-57005 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -