TY - JOUR A1 - Pott, U. A1 - Crasselt, Claudia A1 - Fobbe, N. A1 - Haist, M. A1 - Heinemann, M. A1 - Hellmann, S. A1 - Ivanov, D. A1 - Jakob, C. A1 - Jansen, D. A1 - Lei, L. A1 - Li, R. A1 - Link, J. A1 - Lowke, D. A1 - Mechtcherine, V. A1 - Neubauer, J. A1 - Nicia, D. A1 - Plank, J. A1 - Reißig, S. A1 - Schäfer, T. A1 - Schilde, C. A1 - Schmidt, Wolfram A1 - Schröfl, C. A1 - Sowoidnich, T. A1 - Strybny, B. A1 - Ukrainczyk, N. A1 - Wolf, J. A1 - Xiao, P. A1 - Stephan, D. T1 - Characterization data of reference materials used for phase II of the priority program DFG SPP 2005 “Opus Fluidum Futurum –Rheology of reactive, multiscale, multiphase construction materials” N2 - A thorough characterization of base materials is the prereq- uisite for further research. In this paper, the characterization data of the reference materials (CEM I 42.5 R, limestone pow- der, calcined clay and a mixture of these three components) used in the second funding phase of the priority program 2005 of the German Research Foundation (DFG SPP 2005) are presented under the aspects of chemical and min- eralogical composition as well as physical and chemical properties. The data were collected based on tests performed by up to eleven research groups involved in this cooperative program. KW - Portland cement KW - Limestone powder KW - Calcined clay KW - Sustainable cement KW - DFG SPP 2005 PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-569913 DO - https://doi.org/10.1016/j.dib.2023.108902 VL - 47 SP - 1 EP - 19 PB - Elsevier AN - OPUS4-56991 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Epishin, A. I. A1 - Petrushin, N. V. A1 - Link, T. A1 - Nolze, Gert A1 - Loshchinin, Yu. V. A1 - Gerstein, G. T1 - Thermal stability of the structure of a heat-resistant cobalt alloy hardened with intermetallic γ'-phase precipitates N2 - The thermal stability of the microstructure of a heat-resistant cobalt alloy, which consists of a γ solid solution strengthened with γ'-phase precipitates, has been studied. The temperature behavior of the dissolution of the hardening γ' phase and the kinetics of its coarsening at 700 and 800°C have been determined. It is found that, during prolonged annealing at 800°C, the γ' → β phase transformation occurs. KW - Superalloy KW - Microstructure KW - Hardening KW - Electron backscatter diffraction KW - TEM PY - 2016 DO - https://doi.org/10.1134/S0036029516040078 SN - 0036-0295 VL - 2016 IS - 4 SP - 286 EP - 291 PB - Pleiades Publishing AN - OPUS4-37768 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Epishin, A. A1 - Link, T. A1 - Nolze, Gert T1 - SEM investigation of interfacial dislocations in nickel-base superalloys N2 - A new technique for investigation of interfacial dislocations in nickel-base superalloys by scanning electron microscopy is presented. At high temperatures the pressure of interfacial dislocations against the gamma/gamma'-interface causes grooves. This 'fingerprint of the dislocation network' is visualized by deep selective etching, which removes the gamma'-phase down to the gamma/gamma'-interface. Compared with transmission electron microscopy, the proposed method has important advantages: observation of large sample areas, no superposition of dislocations lying in different specimen depths, possibility of three-dimensional view of dislocation configurations, information about the dislocation mobility, reduced time for preparation and visualization. The method can be applied for multiphase materials where the interface is grooved by interfacial dislocations. KW - Dislocation structure KW - Interface KW - Nickel alloys KW - SEM PY - 2007 VL - 228 IS - 2 SP - 110 EP - 117 PB - The Royal Microscopical Society AN - OPUS4-38016 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Midtlyng, Jan A1 - Epishin, A. I. A1 - Petrushin, N. V. A1 - Link, T. A1 - Nolze, Gert A1 - Svetlov, I. L. A1 - Reimers, W. T1 - Creep behavior of a γ΄-strengthened Co-base alloy with zero γ/γ΄-lattice misfit at 800 °C, 196 MPa N2 - Deformation and structural behavior of an experimental γ΄-strengthened Co-base alloy during creep at 800 °C and 196 MPa have been investigated. The characteristic features of this alloy are zero γ/γ΄-lattice misfit and a fine γ/γ΄-microstructure. In the initial condition, the γ΄-precipitates in this alloy are small (size of about 100 nm), have polyhedral morphology, and are separated by the very narrow c-channels (width of about 10 nm). The tests performed up to about 1% creep strain (about 500 h creep time) gave creep curves with a slow constant strain rate and without an apparent transient creep, typical for superalloys with nonzero misfit. In this initial stage of creep, entering of the narrow γ-channels by dislocations is blocked by a strong Orowan force. The micromechanism of creep was identified as an octahedral glide of h011i superdislocations simultaneously in two phases, γ and γ΄. The γ/γ΄-microstructure with zero misfit shows no rafting but rapidly coarsens isotropically. It is concluded that zero misfit is beneficial at the initial stages of the creep but is unfavourable for longterm creep because of the continuous microstructural coarsening. KW - Co-Basis-Legierung KW - Gitterfehlpassung KW - Kriechen KW - Ausscheidung PY - 2017 DO - https://doi.org/10.1557/jmr.2017.424 SN - 0884-2914 SN - 2044-5326 VL - 32 IS - 24 SP - 4466 EP - 4474 PB - Cambridge Univ. Press CY - Cambridge AN - OPUS4-44027 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Petrushin, N. A1 - Hvatzkiy, K. A1 - Gerasimov, V. A1 - Link, T. A1 - Epishin, A. A1 - Nolze, Gert A1 - Gerstein, G. T1 - A single-crystal co-base superalloy strengthened by gamma' precipitates: structure and mechanical properties N2 - An experimental Co-base superalloy was designed from the Ni-base system by exchange of Ni and Co concentrations. The alloy consist of a Co-matrix (γ phase) strengthened by cuboidal precipitates Co3(Al,X) (γ' phase). The γ'-solvus temperature is 1?005?°C. [001] single crystals of this alloy were solidified and tested for tension at different temperatures up to 1?000?°C. It was found that the Co-base alloy has a much lower yield stress than a corresponding Ni-base alloy, but a much higher ductility. The partitioning behaviour of the alloying elements in the Co-base alloy and the deformation mechanisms were investigated by scanning and transmission electron microscopy. KW - Microstructure KW - Precipitation KW - Stress PY - 2015 DO - https://doi.org/10.1002/adem.201500088 SN - 1438-1656 VL - 17 IS - 6 SP - 755 EP - 760 PB - Wiley-VCH Verl. CY - Weinheim AN - OPUS4-34474 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Chyrkin, A. A1 - Epishin, A. A1 - Pillai, R. A1 - Link, T. A1 - Nolze, Gert A1 - Quaddaker, W. J. T1 - Modeling interdiffusion processes in CMSX-10/Ni diffusion couple N2 - A diffusion couple between directionally solidified nickel and the single crystal Ni-base superalloy CMSX-10 was produced by hot pressing in vacuum. The diffusion couples were heat treated at temperatures between 1050 and 1250 °C. The exposed samples were characterized by SEM/EBSD/EPMA. The interdiffusion results in dissolution of the c¢-Ni3 Al in the superalloy and in growth of nickel grains towards CMSX-10. Rapid diffusion of aluminum from the superalloy into pure nickel leads to a significant formation of pores in the superalloy. The interdiffusion processes were modelled using the finite-element simulation software DICTRA with the databases TCNi5 and MobNi2, tailored specially for Ni-base superalloys. The effect of alloying elements on the interdiffusion profiles is discussed in terms of alloy thermodynamics. The calculated element concentration profiles are in good agreement with the EPMA measurements. The interdiffusion modeling correctly predicts the shapes of the concentration profiles, e.g. kinks on the Al and Ti profiles in the vicinity of the original interface in the joint. The calculation predicts with reasonable accuracy the extent and the location of the Kirkendall porosity. KW - Chemical potential KW - Diffusion KW - EBSD KW - Composition profiles KW - DICTRA modeling KW - Electron probe microanalysis KW - EPMA PY - 2016 DO - https://doi.org/10.1007/s11669-015-0444-9 SN - 1547-7037 VL - 37 IS - 2 SP - 201 EP - 211 PB - Springer AN - OPUS4-35776 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Klingelhöffer, Hellmuth A1 - Epishin, A. A1 - Link, T. A1 - Portella, Pedro Dolabella ED - Portella, Pedro Dolabella ED - T. Beck, ED - M. Okazaki, T1 - Low cycle fatigue of the single crystal nickel-base superalloy CMSX-4: anisotropy and effect of creep damage T2 - 6th International Conference on Low Cycle Fatigue (LCF 6) CY - Berlin, Germany DA - 2008-09-08 KW - Anisotropy of mechanical properties KW - Effect of creep damage on LCF KW - Single-crystal nickel-base superalloys PY - 2008 SP - 403 EP - 408 AN - OPUS4-17914 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Klingelhöffer, Hellmuth A1 - Epishin, Alexander A1 - Link, T. T1 - Low cycle fatigue of the single-crystal nickel-base superalloy CMSX-4 - Anistropy and effect of creep damage KW - Single crystal nickel-base superalloys KW - CMSX-4 KW - Creep KW - Low cycle fatigue PY - 2009 SN - 0025-5300 VL - 51 IS - 5 SP - 291 EP - 294 PB - Hanser CY - München AN - OPUS4-19430 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Epishin, Alexander A1 - Link, T. T1 - Mechanisms of high-temperature creep of nickel-based superalloys under low applied stresses KW - Superalloys KW - Creep PY - 2004 SN - 1478-6435 SN - 0031-8086 VL - 84 IS - 19 SP - 1979 EP - 2000 PB - Taylor & Francis CY - London AN - OPUS4-7144 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Epishin, Alexander A1 - Brückner, Udo A1 - Link, T. A1 - Portella, Pedro Dolabella ED - Dias, A. T1 - Investigation of stresses in superalloys by analysis of y/y'-Microstructure T2 - 6th European Conference on Residual Stresses CY - Coimbra, Portugal DA - 2002-07-10 KW - Superalloys KW - Stress KW - Misfit KW - Rafting PY - 2002 SN - 0-87849-900-8 SN - 0255-5476 N1 - Serientitel: Materials science forum – Series title: Materials science forum IS - 404/407 SP - 287 EP - 292 PB - Trans Tech Publ. CY - Uetikon-Zuerich AN - OPUS4-7147 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Epishin, Alexander A1 - Link, T. ED - Green, K. T1 - Mechanisms of high temperature creep of nickel-base superalloys under low applied stress T2 - Superalloys 2004 / 10th International Symposium on Superalloys 2004 CY - Seven Springs, PA, USA DA - 2004-09-19 KW - Superalloys KW - Creep KW - Porosity KW - Dislocations KW - Diffusion PY - 2004 SN - 0-87339-576-X SP - 137 EP - 143 PB - TMS CY - Warrendale AN - OPUS4-7149 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Brückner, Udo A1 - Epishin, Alexander A1 - Link, T. A1 - Portella, Pedro Dolabella ED - Böttger, A. T1 - Creep induced evolution of internal stresses and structure in a single crystal nickel-base superalloy N2 - Changes in the structure of single-crystal (SC) superalloy SRR99 during creep at 980 °C and 200 MPa were investigated. Geometrical parameters of the y/y'-microstructure, y/y'-misfit, stresses in the phases and local misorientation of the structure were determined at defined points of the dendritic structure by use of X-ray diffraction (XRD), wavelength dispersive X-ray spectroscopy (WDXS), scanning (SEM) and transmission (TEM) electron microscopy. Correlation of the microstructural period and local misorientation of the structure with creep strain were found. T2 - 5th European Conference on Residual Stresses CY - Delft-Noordwijkerhout, the Netherlands DA - 1999-10-28 KW - Creep KW - Dendrite KW - Misfit KW - Segregation KW - Superalloys PY - 2000 UR - http://cat.inist.fr/?aModele=afficheN&cpsidt=1381837 SN - 0-87849-855-9 SN - 0255-5476 N1 - Serientitel: Materials science forum – Series title: Materials science forum IS - 347/349 SP - 363 EP - 367 PB - Trans Tech Publ. CY - Uetikon-Zürich AN - OPUS4-7151 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Epishin, Alexander A1 - Link, T. A1 - Portella, Pedro Dolabella A1 - Brückner, Udo T1 - Evolution of the gamma/gamma'-microstructure during high-temperature creep of a nickel-base superalloy KW - Nickel alloys KW - Creep KW - Mesostructure KW - Scanning electron microscopy (SEM) KW - Image analysis PY - 2000 SN - 1359-6454 SN - 1873-2453 VL - 48 SP - 4169 EP - 4177 PB - Elsevier Science CY - Kidlington AN - OPUS4-7152 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Epishin, Alexander A1 - Brückner, Udo A1 - Portella, Pedro Dolabella A1 - Link, T. T1 - Influence of small rhenium additions on the lattice spacing of nickel solid solution N2 - The influence of small rhenium additions on the lattice spacing of a nickel solid solution was investigated using a nickel–rhenium single crystal with an axial macrosegregation of rhenium. The effect of rhenium on the lattice spacing of the nickel solid solution was found to be similar to that of tungsten. KW - Nickel alloys KW - Crystallography PY - 2003 DO - https://doi.org/10.1016/S1359-6462(02)00436-0 SN - 1359-6462 SN - 1872-8456 VL - 48 IS - 4 SP - 455 EP - 459 PB - Elsevier CY - Oxford AN - OPUS4-2278 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Link, T. A1 - Epishin, Alexander A1 - Klaus, M. A1 - Brückner, Udo A1 - Reznicek, A. T1 - (100) Dislocations in nickel-base superalloys: Formation and role in creep deformation N2 - α(1 0 0) Dislocations are observed in nickel-base superalloys after creep deformation at high temperatures and low stresses. They are formed in the γ/γ´ interfaces by a three step mechanism. First, primary dislocations with Burgers vector α/2(1 0 1) and 60° character are left behind in the interfaces when dislocation loops glide through the γ channels. The 60° dislocations move into edge orientation and react forming secondary dislocations α/2(1 1 0). In the third step, new primary dislocations are knit into the already existing meshes of primary and secondary dislocations, which results in hexagonal misfit dislocation networks consisting of secondary dislocations α/2(1 1 0) and tertiary dislocations α(1 0 0), both of edge type. This self-organisation process is explained by dislocation theory and crystallography. Creep deformation accelerates when the α(1 0 0) interfacial dislocations enter the γ´ phase. During their climb towards the opposite interface, they attain a characteristic rectangular shape. This shape and the importance of the α(1 0 0) super dislocations for creep deformation are discussed. KW - Superalloys KW - Creep KW - Dislocation reactions KW - Dislocation theory KW - Deformation mechanisms PY - 2005 SN - 0921-5093 SN - 1873-4936 VL - 405 IS - 1-2 SP - 254 EP - 265 PB - Elsevier CY - Amsterdam AN - OPUS4-11968 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Link, T. T1 - High resolution synchrotron topography of Nickelbase superalloys T2 - 69. DPG Physikertagung CY - Berlin, Germany DA - 2006-03-07 PY - 2006 AN - OPUS4-12176 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Link, T. T1 - High resolution synchrotron topography of Nickelbase superalloys T2 - European Congress on Advanced Materials and Processes, EUROMAT 2005 CY - Prague, Czech Republic DA - 2005-09-05 PY - 2005 AN - OPUS4-12177 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Epishin, Alexander A1 - Link, T. A1 - Brückner, Udo A1 - Klingelhöffer, Hellmuth A1 - Portella, Pedro Dolabella T1 - The effect of high temperature creep damage on low cycle fatigue of CMSX-4 T2 - 8th Liège Conference "Materials for Advanced Power Engineering 2006" CY - Liege, Belgium DA - 2006-01-01 KW - Superalloys KW - CMSX-4 KW - Single crystal KW - Creep KW - Fatigue PY - 2006 SN - 3-89336-436-6 N1 - Serientitel: Schriften des Forschungszentrums Jülich - Reihe Energietechnik / Energy Technology – Series title: Schriften des Forschungszentrums Jülich - Reihe Energietechnik / Energy Technology IS - 53 SP - 317 EP - 325 PB - Forschungszentrum Jülich CY - Jülich AN - OPUS4-13701 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Epishin, Alexander A1 - Link, T. A1 - Brückner, Udo T1 - Microstructural stability of CMSX-4 and CMSX-10 under high temperature creep conditions T2 - 8th Liège Conference "Materials for Advanced Power Engineering 2006" CY - Liege, Belgien DA - 2006-01-01 KW - Superalloys KW - CMSX-4 KW - Creep KW - Microstructure KW - CMSX-10 PY - 2006 SN - 3-89336-436-6 N1 - Serientitel: Schriften des Forschungszentrums Jülich - Reihe Energietechnik / Energy Technology – Series title: Schriften des Forschungszentrums Jülich - Reihe Energietechnik / Energy Technology IS - 53 SP - 507 EP - 520 PB - Forschungszentrum Jülich CY - Jülich AN - OPUS4-13702 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Epishin, Alexander A1 - Link, T. A1 - Nolze, Gert T1 - SEM investigation of interfacial dislocations in nickel-base superalloys N2 - A new technique for investigation of interfacial dislocations in nickel-base superalloys by scanning electron microscopy is presented. At high temperatures the pressure of interfacial dislocations against the γ/γ'-interface causes grooves. This 'fingerprint of the dislocation network' is visualized by deep selective etching, which removes the γ'-phase down to the γ/γ'-interface. Compared with transmission electron microscopy, the proposed method has important advantages: observation of large sample areas, no superposition of dislocations lying in different specimen depths, possibility of three-dimensional view of dislocation configurations, information about the dislocation mobility, reduced time for preparation and visualization. The method can be applied for multiphase materials where the interface is grooved by interfacial dislocations. KW - Dislocation structure KW - Interfaces KW - Nickel alloys KW - Scanning electron microscopy PY - 2007 SN - 0022-2720 SN - 1365-2818 VL - 228 IS - 2 SP - 110 EP - 117 PB - Blackwell CY - London AN - OPUS4-16039 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -