TY - CONF A1 - Lay, Vera A1 - Baensch, Franziska A1 - Sturm, Patrick A1 - Prabhakara, Prathik A1 - Mielentz, Frank A1 - Hofmann, Detlef A1 - Johann, Sergej A1 - Kühne, Hans-Carsten A1 - Niederleithinger, Ernst T1 - Sichere Verschlussbauwerke mittels innovativer Materialien, multisensorischem Monitoring und Ultraschall-Prüfung zur Qualitätssicherung N2 - Verschlussbauwerke sind für die untertägige Endlagerung im Salzgestein als eine wichtige technische Barriere vorgesehen. Diese Bauwerke müssen hohen Anforderungen an Sicherheit und Integrität genügen, weshalb im Projekt SealWasteSafe Werkstofftechnik, Prüfverfahren und Überwachungsmethoden für sichere Verschlussbauwerke verbessert werden. Dabei zeigen die untersuchten alkaliaktivierten Materialien (AAM) langsamere Reaktionskinetik bei der Erhärtung im Vergleich zu Salzbeton, was potenziell geringere Rissbildung erwarten lässt. Die Erhärtung wird an Probekörpern (100-300 l) multisensorisch über einen Zeitraum von mindestens 28 Tagen überwacht. Die Parameter Temperatur und Feuchtigkeit werden einerseits kabelgebunden, andererseits mittels drahtloser Radio Frequency Identification (RFID)-Technik aufgezeichnet. Zusätzlich kommen Schallemissionsmessungen sowie Dehnungsmessungen mittels verteilter faseroptischer Sensorik (FOS) zum Einsatz. Die Überwachung zeigt verschiedene Charakteristika beim Erhärten der Materialien mit geringerer Temperaturentwicklung des AAM. Zusätzlich werden Ultraschallmessungen genutzt, um Einbauteile und Störstellen wie Risse und Delaminationen im Rahmen der Qualitätssicherung am Probekörper und am Verschlussbauwerk zu detektieren. Dafür werden sowohl ein Ultraschallmesssystem mit großer Apertur (LAUS) als auch eine Ultraschall-Bohrlochsonde eingesetzt. Durch Erhöhung des Schalldrucks und Schallfeldbündelung im Beton wird die Aussagekraft der von der Bohrlochsonde aufgezeichneten Messsignale verbessert, was in Modellierungen und ersten Labortests gezeigt werden kann. Die Auswertung der Ultraschallmessungen zeigt das große Potenzial der Methode mit Eindringtiefen bis zu 9 m, wobei anspruchsvolle Abbildungsverfahren zu einer verbesserten Abbildung der internen Strukturen führen. Insgesamt verbessern die im Projekt SealWasteSafe entwickelten Materialien und Methoden die Möglichkeiten für sichere Verschlussbauwerke nuklearer Endlager. Obwohl die Konzepte speziell für Bauwerke im Salzgestein entwickelt werden, sind sie partiell gut auf andere Wirtsgesteine übertragbar. T2 - 3. Tage der Standortauswahl CY - Aachen, Germany DA - 08.06.2022 KW - SealWasteSafe KW - Salzbeton KW - Verschlussbauwerke KW - Monitoring KW - Ultraschall KW - Inspektion PY - 2022 AN - OPUS4-55093 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera T1 - Das Themenfeldprojekt SealWasteSafe im Überblick N2 - Das Projekt SealWasteSafe verbessert Werkstofftechnik, Prüfverfahren und Überwachungsmethoden für sichere Verschlussbauwerke in Endlagern. Dieser Überblick fasst die laufenden Arbeiten in folgenden Bereichen zusammen: 1) Materialentwicklung und Dauerhaftigkeit; 2) Überwachung; 3) Inspektion. T2 - Online-Workshop „Dauerhafte Verschlussbauwerke für Endlager“ CY - Online meeting DA - 14.02.2022 KW - SealWasteSafe KW - Salzbeton KW - Verschlussbauwerke KW - Monitoring KW - Inspektion KW - Ultraschall PY - 2022 AN - OPUS4-55089 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Johann, Sergej A1 - Baensch, Franziska A1 - Sturm, Patrick A1 - Tiebe, Carlo A1 - Pötschke, Samuel A1 - Lay, Vera ED - Holl, H. T1 - HF RFID-based measurement comparison for method optimization in M2 concrete and alkali-activated mortars N2 - Monitoring of repositories for radioactive waste requires techniques which can be applied long-term under harsh conditions. In this work, the reliability and suitability of materials and a capacitive sensor for measuring relative humidity are investigated, which are to be embedded in the special concrete components for the closure structures of underground repository. Preliminary tests with accelerated aging of the materials used, validation of the sensors under difficult conditions, investigations of the surfaces after aging by pH 14 solution, defined exposure of the sensors in a climatic chamber and the microscope images are discussed. The results will be used for further development and optimization of the RFID based sensor systems which can be applied to monitor the condition of different building structures without cabling. T2 - 37th Danubia - Adria Symposium on Advances in Experimental Mechanics CY - Linz, Austria DA - 21.09.2021 KW - Alkali-activated mortars KW - Passive sensor interface KW - RFID KW - Structural health monitoring KW - Smart structures PY - 2022 U6 - https://doi.org/10.1016/j.matpr.2022.03.465 SN - 2214-7853 VL - 62 IS - 5 SP - 2571 EP - 2576 PB - Elsevier CY - Amsterdam AN - OPUS4-54697 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Fulawka, K. A1 - Kwietniak, A. A1 - Lay, Vera A1 - Jaskiewicz-Proc, I. T1 - Importance of seismic wave frequency in FEM-based dynamic stress and displacement calculations of the earth slope N2 - Reliable assessment of earthen dams’ stability and tailing storage facilities widely used in the mining industry is challenging, particularly under seismic load conditions. In this paper, we propose to take into account the effect of the dominant frequency of seismic load on the stability assessment of tailing/earthen dams. The calculations are performed by finite element modelling (FEM) with the Mohr–Coulomb failure criteria. To separate the frequency content from other dynamic parameters describing the seismic wave, synthetic waveforms with identical amplitude and attenuation characteristics, but differing spectral characteristics have been used. The analysis has been performed for three different slope angles and two scenarios of seismic wave propagation. Consequently, the changes of total displacement and shear stresses depending on the frequencies have been determined and clearly show that lower frequencies cause higher stress levels and displacement. Finally, the response surface methodology has been applied to determine how different parameters affect the slope stability under dynamic load conditions. Overall, this study is a first step to improve the existing methods to assess slope stability when considering seismic load. KW - Slope stability KW - Numerical analysis KW - Seismic load KW - Frequency analysis PY - 2022 U6 - http://nbn-resolving.de/urn/resolver.pl?urn:nbn:de:kobv:b43-544047 SN - 2083-831X VL - 44 IS - 1 SP - 82 EP - 96 PB - De Gruyter CY - Berlin AN - OPUS4-54404 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Lay, Vera A1 - Buske, S. A1 - Townend, J. A1 - Kellett, R. A1 - Savage, M. A1 - Schmitt, D. R. A1 - Constantinou, A. A1 - Eccles, J. D. A1 - Gorman, A. A1 - Bertram, M. A1 - Hall, K. A1 - Lawton, D. A1 - Kofman, R. T1 - 3D Active Source Seismic Imaging of the Alpine Fault Zone and the Whataroa Glacial Valley in New Zealand N2 - The Alpine Fault zone in New Zealand marks a major transpressional plate boundary that is late in its typical earthquake cycle. Understanding the subsurface structures is crucial to understand the tectonic processes taking place. A unique seismic survey including 2D lines, a 3D array, and borehole recordings, has been performed in the Whataroa Valley and provides new insights into the Alpine Fault zone down to ∼2 km depth at the location of the Deep Fault Drilling Project (DFDP)-2 drill site. Seismic images are obtained by focusing prestack depth migration approaches. Despite the challenging conditions for seismic imaging within a sediment filled glacial valley and steeply dipping valley flanks, several structures related to the valley itself as well as the tectonic fault system are imaged. A set of several reflectors dipping 40°–56° to the southeast are identified in a ∼600 m wide zone that is interpreted to be the minimum extent of the damage zone. Different approaches image one distinct reflector dipping at ∼40°, which is interpreted to be the main Alpine Fault reflector located only ∼100 m beneath the maximum drilled depth of the DFDP-2B borehole. At shallower depths (z < 0.5 km), additional reflectors are identified as fault segments with generally steeper dips up to 56°. Additionally, a glacially over-deepened trough with nearly horizontally layered sediments and a major fault (z < 0.5 km) are identified 0.5–1 km south of the DFDP-2B borehole. Thus, a complex structural environment is seismically imaged and shows the complexity of the Alpine Fault at Whataroa. KW - Imaging KW - Signal processing KW - Seismic KW - Borehole KW - DAS PY - 2021 U6 - http://nbn-resolving.de/urn/resolver.pl?urn:nbn:de:kobv:b43-539163 VL - 126 IS - 12 SP - 1 EP - 21 PB - American Geophysical Union AN - OPUS4-53916 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera A1 - Baensch, Franziska A1 - Johann, Sergej A1 - Sturm, Patrick A1 - Mielentz, Frank A1 - Prabhakara, Prathik A1 - Hofmann, Detlef A1 - Niederleithinger, Ernst A1 - Kühne, Hans-Carsten T1 - SealWasteSafe: materials technology, monitoring techniques, and quality assurance for safe sealing structures in underground repositories N2 - Within the project SealWasteSafe, we advance construction materials and monitoring concepts of sealing structures applied for underground disposal of nuclear or toxic waste. As these engineered barriers have high demands concerning integrity, an innovative alkali-activated material (AAM) is improved and tested on various laboratory scales. This AAM has low reaction kinetics related to a preferential slow release of the heat of reaction in comparison to alternative salt concretes based on Portland cement or magnesium oxychloride cements. Hence, crack formation due to thermally induced strain is reduced. After successful laboratory scale analysis (Sturm et al., 2021), the AAM is characterised on a larger scale by manufacturing test specimens (100–300 L). Conventional salt concrete (DBE, 2004) and the newly developed AAM are compared using two specimen geometries, i.e. cylindrical and cuboid. A comprehensive multisensor monitoring scheme is developed to compare the setting process of AAM and salt concrete for these manufactured specimens. The analysed parameters include temperature and humidity of the material, acoustic emissions, and strain variations. Passive sensor systems based on radiofrequency identification technology (RFID) embedded in the concrete, enable wireless access to temperature and humidity measurements and are compared to conventional cabled systems. Additionally, fibre-optic sensors (FOS) are embedded to record strain, but also have potential to record temperature and moisture conditions. Part of this project aims at demonstrating the high reliability of sensors and also their resistance to highly alkaline environments and to water intrusion along cables or at sensor locations. Further technical improvements were implemented so that first results clearly show the scalability of the setting process from previous small-scale AAM experiments and particularly the high potential of the newly developed approaches. Furthermore, ultrasonic methods are used for quality assurance to detect obstacles, potential cracks and delamination. On the one hand, both active and passive ultrasonic measurements complement the results obtained from the multisensor monitoring scheme for the produced specimens. On the other hand, the unique large aperture ultrasonic system (LAUS) provides great depth penetration (up to nearly 10 m) and can thus be applied at in situ sealing structures built as a test site in Morsleben by the Federal Company for Radioactive Waste Disposal (Bundesgesellschaft für Endlagerung, BGE) as shown by Effner et al. (2021). An optimised field lay-out identified from forward modelling studies and advanced imaging techniques applied to the measured data will further improve the obtained results. To characterise the inside of the test engineered barrier and achieve a proof-of-concept, an ultrasonic borehole probe is developed to enable phased arrays that can further improve the detection of potential cracks. Modelling results and first analysis of semispherical specimens confirmed the reliability of the directional response caused by the phased arrays of the newly constructed ultrasonic borehole probe. Overall, the project SealWasteSafe improves the construction material, multisensor monitoring concepts and ultrasonics for quality assurance. This will help to develop safe sealing structures for nuclear waste disposal. The outcomes are particularly valuable for salt as a host rock but partly also transferrable to alternative conditions. T2 - Safe ND Interdisciplinary research symposium on the safety of nuclear disposal practices CY - Berlin, Germany DA - 10.11.2021 KW - Borehole probe KW - SealWasteSafe KW - Engineered barrier KW - Materials technology KW - AAM KW - Monitoring KW - Ultrasound PY - 2021 AN - OPUS4-53919 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Johann, Sergej A1 - Baensch, Franziska A1 - Strurm, Patrick A1 - Tiebe, Carlo A1 - Pötschke, Samuel A1 - Lay, Vera ED - Hall, H. T1 - HF RFID-based Measurement Comparison for Method Optimization in M2 Concrete and Alkali-Activated Mortars N2 - The internal project "SealWasteSafe" of the Federal Institute for Materials Research and Testing is dedicated to the further improvement in the construction of sealing systems for underground repositories of radioactive waste. Particularly, a multi-sensory concept is developed to ensure quality assurance and continuous long-term monitoring on the engineered barriers. Therefore, beside other measures, the temperature and equilibrium moisture of the construction shall be monitored and respective multi-sensoric monitoring concepts are tested first on the laboratory scale. One focus in this project is on embedded application in alkali-activated mortars (AAM), which results in special requirements for the resistance of the sensors to strongly alkaline environments with up to pH 14. In addition, the ingress of water along cables or at sensor positions is critical for sensors embedded in concrete, as the cable access of the sensor housing is a major weak point. It is therefore advisable to equip wireless high frequent radio frequency identification-based sensors, so called HF RFID sensors (short: RFID), that do not require cable access and thus have a stable and leak-proof sensor housing for long-term monitoring. In this contribution, the results from temperature, moisture and transmitted power monitoring of a AAM and a M2 specimens by means of HF RFID sensor systems are presented. T2 - 35th Danubia - Adria Symposium on Advances in Experimental Mechanics CY - Linz, Österreich DA - 21.09.2021 KW - Passive sensor interface KW - RFID KW - Structural Health Monitoring KW - Alkali-Activated Mortars PY - 2021 SN - 978-3-9504997-0-4 SP - 116 EP - 117 AN - OPUS4-53397 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera A1 - Buske, S. A1 - Kleine, F. A1 - Townend, J. A1 - Kellett, R. A1 - Savage, M. A1 - Schmitt, D. R. A1 - Constantinou, A. A1 - Eccles, J. A1 - Lawton, D. A1 - Bertram, M. A1 - Hall, K. A1 - Kofman, R. A1 - Gorman, A. T1 - 3D seismic imaging of the Alpine Fault and the glacial valley at Whataroa, New Zealand N2 - The Alpine Fault at the West Coast of the South Island (New Zealand) is a major plate boundary that is expected to rupture in the next 50 years, likely as a magnitude 8 earthquake. The Deep Fault Drilling Project (DFDP) aimed to deliver insight into the geological structure of this fault zone and its evolution by drilling and sampling the Alpine Fault at depth. Here we present results from a seismic survey around the DFDP-2 drill site in the Whataroa Valley where the drillhole almost reached the fault plane. This unique 3D seismic survey includes several 2D lines and a 3D array at the surface as well as borehole recordings. Within the borehole, the unique option to compare two measurement systems is used: conventional three-component borehole geophones and a fibre optic cable (heterodyne Distributed Vibration Sensing system (hDVS)). Both systems show coherent signals but only the hDVS system allowed a recording along the complete length of the borehole. Despite the challenging conditions for seismic imaging within a glacial valley filled with sediments and steeply dipping valley flanks, several structures related to the valley itself as well as the tectonic fault system are imaged. The pre-processing of the seismic data also includes wavefield separation for the zero-offset borehole data. Seismic images are obtained by prestack depth migration approaches. Within the glacial valley, particularly steep valley flanks are imaged directly and correlate well with results from the P-wave velocity model obtained by first arrival travel-time tomography. Additionally, a glacially over-deepened trough with nearly horizontally layered sediments is identified about 0.5 km south of the DFDP-2B borehole. With regard to the expected Alpine fault zone, a set of several reflectors dipping 40-56° to the southeast are identified in a ~600 m wide zone between depths of 0.2 and 1.2 km that is interpreted to be the minimum extent of the damage zone. Different approaches image one distinct reflector dipping at 40°, which is interpreted to be the main Alpine Fault reflector. This reflector is only ~100 m ahead from the lower end of the borehole. At shallower depths (z<0.5 km), additional reflectors are identified as fault segments and generally have steeper dips up to 56°. About 1 km south of the drill site, a major fault is identified at a depth of 0.1-0.5 km that might be caused by the regional tectonics interacting with local valley structures. A good correlation is observed among the separate seismic data sets and with geological results such as the borehole stratigraphy and the expected surface trace of the fault. In conclusion, several structural details of the fault zone and its environment are seismically imaged and show the complexity of the Alpine Fault at the Whataroa Valley. Thus, a detailed seismic characterization clarifies the subsurface structures, which is crucial to understand the transpressive fault’s tectonic processes. T2 - EGU 2021 General Assembly CY - Online meeting DA - 19.04.2021 KW - Imaging KW - Signal processing KW - Seismic KW - Borehole KW - DAS PY - 2021 AN - OPUS4-52614 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera A1 - Effner, Ute A1 - Niederleithinger, Ernst A1 - Arendt, J. A1 - Kudla, W. T1 - Ultrasonic quality assurance for underground salt shotcrete sealing structures in Teutschenthal mine, Germany N2 - Underground sealing structures are necessary to seal radioactive or toxic waste in underground repositories. A special version of MgO concrete is used in the mine in Teutschenthal and applied at a large-scale test with the aim to provide a low permeability barrier. The test structures (up to 10 m long) were created by shotcreting. Besides destructive tests, non-destructive ultrasonic measurements have been evaluated for quality assurance to monitor potential anomalies such as cracks, concrete inhomogeneities, and delamination. We show results of ultrasonic measurements with a multi-transducer system used at the front and from the side of the concrete structure. Images are obtained by synthetic aperture focusing techniques. The boundaries between concreting sections are not visible in the ultrasonic images systematically so that a successful concreting is assumed, which is confirmed by the low permeabilities observed. Several reflectors up to a depth of 1.2 m are identified and interpreted as potential damages in the concrete. Phase analysis of prominent reflectors reveal a negative impedance contrast thus indicating air filled voids, cracks or delamination. Boreholes through some of the identified reflectors are used to verify the results from ultrasonic measurements. Additionally, an experiment with incorporated artificial defects was undertaken to analyse the reliability of the applied methods. Overall, the conducted tests show the potential of ultrasonic measurements to detect critical anomalies. Despite challenges at small-scale structures (cm-order), large-scale anomalies can be identified. Consequently, implementing ultrasonic monitoring during and after the construction of concrete sealing structures has shown its potential as a tool for quality assurance, but needs further development and validation. T2 - NDT-CE 2022 CY - Zurich, Switzerland DA - 16.08.2022 KW - Ultrasound KW - Ultrasonic imaging KW - Magnesia shotcrete KW - Underground KW - Engineered barrier systems PY - 2022 UR - https://www.ndt.net/events/proceedings/topic.php?eventID=292&TopicID=27209 SP - 1 EP - 4 PB - NDT.net AN - OPUS4-55824 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera T1 - Geophysikalische Methoden für die Zerstörungsfreie Prüfung im Bauwesen N2 - Im Rahmen des Seminars "Angewandte Forschungsthemen (SAFT)" am Institut für Geowissenschaften der Christian-Albrechts-Universität zu Kiel werden verschiedene geophysikalische Methoden vorgestellt, die bei der zerstörungsfreien Prüfung im Bauwesen zum Einsatz kommen. Neben einem Überblick der Arbeiten an der BAM im Allgemeinen und dem Fachbereich im Besonderen geht es vor allem um den Einsatz von Ultraschallmethoden. Drei wesentliche Schwerpunkte werden dabei beleuchtet: 1) (Geophysikalische) Antworten auf Herausforderungen bei Ultraschall-Anwendungen 2) Material research and multi-sensory monitoring for concrete sealing structures in rock salt unterground repositories (Projekt SealWasteSafe) und 3) Untersuchung von Spritzbeton-Probekörpern unter Tage mit Ultraschall zur Qualitätssicherung von Verschlussbauwerken. Insgesamt werden diverse Möglichkeiten für die Geophysik für Forschung und Studierende im Bereich der zerstörungsfreien Prüfung im Bauwesen aufgezeigt. T2 - Seminar Angewandte Forschungsthemen CY - Kiel, Germany DA - 14.06.2023 KW - SealWasteSafe KW - Ultraschall KW - Verschlussbauwerke KW - Abbildungsverfahren PY - 2023 AN - OPUS4-57828 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera T1 - Innovations in cemented waste handling and pre-disposal storage (WP7 project PREDIS) N2 - During the webinar "Dismantling and waste management: a playground for innovation" the innovative aspects of the PREDIS work package "innovations in cemented waste handling and pre-disposal storage" are presented. The webinar is jointly organised by Women in Nuclear Decommissioning (WINDI) and Women in Nuclear Innovation (WINI). The shown innovations include quality assurance (mainly NDE) and monitoring technologies with associated sensor systems, digital twin technology, and appropriate data handling including a decision framework. An overview of the on-going research in the field of pre-disposal waste management in the project Predis (WP7) is summarised. T2 - Webinar "Dismantling and waste management: a great playground for innovation" CY - Online meeting DA - 13.10.2022 KW - Predis KW - Waste management KW - Concrete PY - 2022 AN - OPUS4-56926 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera A1 - Mielentz, Frank A1 - Prabhakara, Prathik A1 - Baensch, Franziska A1 - Johann, Sergej A1 - Hofmann, Detlef A1 - Sturm, Patrick A1 - Stamm, Michael A1 - Niederleithinger, Ernst T1 - Multi-sensory monitoring and ultrasound for quality assurance at underground sealing structures N2 - Within the safety concepts of underground disposal sites of nuclear waste, engineered barriers play an important role. As these sealing structures have high demands concerning integrity, we aim at advancing the available construction materials, monitoring and inspection techniques within the project SealWasteSafe. After successful laboratory analysis on the cm-scale, cylindrical and cuboid specimens on the m-scale are produced from classical salt concrete and a specifically developed alkali-activated material. A comprehensive multi-sensory monitoring scheme is applied to compare the setting process of both materials and to demonstrate the sensors’ resistance to highly alkaline environments. Besides temperature and humidity of the materials, strain variations using fibre optic sensors and acoustic emissions are recorded over periods of at least 28 days, partly for more than 8 months. Passive sensor systems based on radiofrequency identification technology (RFID) embedded in the concrete allow for wireless access to temperature and humidity measurements and are compared to conventional cabled systems. After hardening and removal of the outer casings of the specimens, further non-destructive evaluations using ultrasonic echo and thermographic measurements are conducted. Preliminary results clearly highlight differences between the tested materials, particularly showing lower acoustic emission activity for the newly developed alkali-activated material potentially indicating less phase changes or cracks. Complementary, ultrasonic methods are improved to be used for quality assurance to detect obstacles, potential cracks and delamination at in-situ sealing structure scale. A unique large aperture ultrasonic system (LAUS) with depth penetration as large as 9 m has already successfully been applied at the test site in Morsleben, Germany, of the federal company for radioactive waste disposal (BGE). Modelling studies help to further optimize the measurement layout. Advanced imaging techniques applied to the modelled and measured data will further improve the obtained images of internal structures. Additionally, an ultrasonic borehole probe is developed and constructed using phased arrays to further enhance the detection of potential cracks. Modelling and preliminary results from laboratory specimens prove the feasibility and potential of the directional response even in heterogeneous material such as concrete. Final investigations under in-situ conditions at the test site of the sealing structure are planned. Overall, the project SealWasteSafe improves the construction material, multi-sensory monitoring, and ultrasound for quality assurance to allow for the development of safe nuclear sealing structures. Although the techniques are tailored for sealing structures within salt as a host rock, they are transferrable to a wider field of applications and alternative disposal conditions. T2 - NDE NucCon CY - Espoo, Finland DA - 25.01.2023 KW - SealWasteSafe KW - Engineered barriers KW - Monitoring KW - Embedded sensors KW - Ultrasonic imaging PY - 2023 AN - OPUS4-56927 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Lay, Vera A1 - Effner, Ute A1 - Niederleithinger, Ernst A1 - Arendt, J. A1 - Hofmann, M. A1 - Kudla, W. T1 - Correction: Lay et al. Ultrasonic quality assurance at magnesia shotcrete sealing structures. Sensors 2022, 22, 8717 N2 - The authors wish to correct the following errors in the original paper Lay, V.; Effner, U.; Niederleithinger, E.; Arendt, J.; Hofmann, M.; Kudla, W. Ultrasonic Quality Assurance at Magnesia Shotcrete Sealing Structures. Sensors 2022, 22, 8717, https://doi.org/10.3390/s22228717. PY - 2023 U6 - http://nbn-resolving.de/urn/resolver.pl?urn:nbn:de:kobv:b43-584969 SN - 1424-8220 VL - 23 IS - 18 SP - 1 EP - 3 PB - MDPI CY - Basel AN - OPUS4-58496 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera A1 - Prabhakara, Prathik A1 - Mielentz, Frank A1 - Baensch, Franziska A1 - Johann, Sergej A1 - Hofmann, Detlef A1 - Sturm, Patrick A1 - Effner, Ute A1 - Niederleithinger, Ernst T1 - Zerstörungsfreie Prüfmethoden für Verschlussbauwerke nuklearer Endlager im Projekt SealWasteSafe N2 - Für die sichere Einlagerung von radioaktiven oder toxischen Abfällen kommen im Salzgestein technische Barrieren in Form von untertägigen Verschlussbauwerken zum Einsatz. Aufgrund der hohen Anforderungen an Sicherheit und Integrität dieser Verschlussbauwerke werden umfangreiche zerstörungsfreie Prüfmethoden zur Überwachung und Qualitätssicherung verwendet. Im BAM-Projekt SealWasteSafe werden Werkstofftechnik, Prüfverfahren und Überwachungsmethoden für sichere Verschlussbauwerke in Endlagern verbessert. Dabei wird der bisherige Salzbeton mit dem innovativen alkaliaktivierten Material (AAM) mit langsamerer Reaktionskinetik bei der Erhärtung und somit potenziell geringerer Rissbildung verglichen. Im Labormaßstab werden Probekörper mit Volumina von 100-300 l multisensorisch ausgestattet und somit die Zuverlässigkeit und Widerstandsfähigkeit der Sensoren gegenüber der hochalkalischen Umgebung nachgewiesen. Durch das Monitoring wird der Abbindevorgang des Betons überwacht und die Materialien über einen Zeitraum von mehreren Wochen charakterisiert. Dabei werden die Parameter Temperatur und Feuchtigkeit einerseits verkabelt als auch mittels drahtloser Radio Frequency Identification (RFID)-Technik aufgezeichnet. Zusätzlich kommen Schallemissionsmessungen sowie Dehnungsmessung mittels verteilter faseroptischer Sensorik (FOS) zum Einsatz. Das multisensorische Überwachungssystem wird durch aktive Ultraschallmessungen ergänzt, die durch die Detektion von Rissen, Delaminationen oder anderen Störstellen eine Qualitätssicherung der Verschlussbauwerke ermöglichen. Dafür werden sowohl ein Ultraschallsystem mit großer Apertur (LAUS) als auch eine Ultraschall-Bohrlochsonde eingesetzt. Durch Erhöhung des Schalldrucks und Bündelung der Schallsignale im Beton wird die Aussagekraft der von der Bohrlochsonde aufgezeichneten Messsignale verbessert, was in Modellierungen und ersten Labortests gezeigt werden kann. Die Auswertung der Ultraschallmessungen erfolgt mit auf Diffraktionssummation beruhenden Migrationsverfahren wie Kirchhoff-Tiefenmigration und Synthetic Aperture Focusing Technique (SAFT), die Abbildungen vom Inneren der Probekörper erzeugen. Insgesamt verbessert das Projekt SealWasteSafe mithilfe innovativer Multisensorik und Ultraschallmethodik die Überwachungs- und Qualitätssicherungskonzepte für sichere Verschlussbauwerke nuklearer Endlager. T2 - 82. Jahrestagung der Deutschen Geophysikalischen Gesellschaft CY - Online meeting DA - 07.03.2022 KW - SealWasteSafe KW - Ultraschall KW - Verschlussbauwerke KW - Abbildungsverfahren PY - 2022 AN - OPUS4-54533 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera A1 - Effner, Ute A1 - Niederleithinger, Ernst A1 - Arendt, J. A1 - Kudla, W. T1 - Ultrasonic quality assurance for underground salt shotcrete sealing structures in Teutschenthal mine, Germany N2 - Underground sealing structures are necessary to seal radioactive or toxic waste in underground repositories. Particularly developed MgO concrete is used in the mine in Teutschenthal and applied at a large-scale test with the aim to provide concrete with low permeabilities. The test structures (up to 10 m long) were created with the help of a shotcrete procedure. Besides destructive tests, non-destructive ultrasonic measurements are used for quality assurance to monitor potential anomalies such as cracks, concrete inhomogeneities, and delamination. We show results of ultrasonic measurements with a multi-transducer system used at the front site of the concrete structure. Images are obtained by synthetic aperture focusing techniques. Concreting sections are not systematically imaged so that a successful concreting is assumed as also indicated by observed low permeabilities. Several reflectors up to a depth of 1.2 m are identified and interpreted as potential damages in the concrete. Phase analysis of prominent reflectors reveal a negative impedance contrast thus indicating air filled voids, cracks or delamination. Boreholes through some of the identified reflectors are used to verify the results from ultrasonic measurements. Additionally, an experiment with incorporated defects is undertaken to analyse the reliability of the applied methods. Overall, the conducted tests show the great potential of ultrasonic measurements to detect critical anomalies. Despite challenges at small-scale structures (cm-order), large-scale anomalies can be identified. Implementing ultrasonic monitoring during and after the construction of concrete sealing structures is recommended as a tool for quality assurance. T2 - NDT-CE 2022 CY - Zurich, Switzerland DA - 16.08.2022 KW - Ultrasound KW - Ultrasonic imaging KW - Magnesia shotcrete KW - Underground KW - Engineered barrier systems PY - 2022 AN - OPUS4-55825 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Baensch, Franziska A1 - Hofmann, Detlef A1 - Johann, Sergej A1 - Tiebe, Carlo A1 - Basedau, Frank A1 - Sturm, Patrick A1 - Lay, Vera A1 - Niederleithinger, Ernst T1 - Multi-sensor conception for safe sealing structures in underground repositories N2 - The project "SealWasteSafe" of the Bundesanstalt für Materialforschung und -prüfung (BAM, Berlin) deals with sealing structures applied for underground disposal of nuclear waste from two perspectives: (1) material improvement for application in sealing constructions and (2) feasibility study regarding multi-sensor approaches to ensure quality assurance and long-term monitoring. One specimen of 150 l made of alkali-activated material, which was found innovative and suitable for sealing constructions based on preliminary laboratory studies, and, for comparison purpose, another one made of salt concrete, are manufactured with an integrated multi-sensory setup for quality assurance and long-term-monitoring. The specimens were left in their cast form and additionally thermally insulated to simulate the situation in the repository. The multi-sensory concept comprises RFID technology embedded in the specimens suppling material temperature and moisture measurements, integrated fibre optic sensing allowing strain measurement and acoustic emission testing for monitoring possible crack formation. Overall, the suitability and the functionality of the sensors embedded into and attached to strongly alkaline (pH > 13 for the AAM) and salt corrosive (NaCl) environment was proven for the first 672 h. First temperature measurement based on RFID succeeded after 626 h for the alkali-activated material and after 192 h for the conventional salt concrete. Strain measurement based on distributed fibre optic sensing turned out the alkali-activated material with > 1 mm m-1 undergoing approximately twice the compression strain as the salt concrete with strains < 0.5 mm m-1. In contrast, the acoustic emission first and single hits representing crack formation in numbers, was found for alkali-activated material half of that detected at the salt concrete. T2 - SMIRT 26 CY - Berlin/Potsdam, Germany DA - 10.07.2022 KW - SealWasteSafe KW - Monitoring KW - Acoustic emission KW - Fibre optic sensing KW - RFID technology KW - alkali-activated material PY - 2022 SP - 1 EP - 10 AN - OPUS4-55371 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Prabhakara, Prathik A1 - Lay, Vera A1 - Mielentz, Frank A1 - Niederleithinger, Ernst A1 - Behrens, Matthias T1 - Enhancing the Performance of a Large Aperture Ultrasound System (LAUS): A Combined Approach of Simulation and Measurement for Transmitter–Receiver Optimization N2 - The Large Aperture Ultrasound System (LAUS) developed at BAM is known for its ability to penetrate thick objects, especially concrete structures commonly used in nuclear waste storage and other applications in civil engineering. Although the current system effectively penetrates up to ~9 m, further optimization is imperative to enhance the safety and integrity of disposal structures for radioactive or toxic waste. This study focuses on enhancing the system’s efficiency by optimizing the transducer spacing, ensuring that resolution is not compromised. An array of twelve horizontal shear wave transducers was used to find a balance between penetration depth and resolution. Systematic adjustments of the spacing between transmitter and receiver units were undertaken based on target depth ranges of known reflectors at depth ranges from 5 m to 10 m. The trade-offs between resolution and artifact generation were meticulously assessed. This comprehensive study employs a dual approach using both simulations and measurements to investigate the performance of transducer units spaced at 10 cm, 20 cm, 30 cm, and 40 cm. We found that for depths up to 5 m, a spacing of 10 cm for LAUS transducer units provided the best resolution as confirmed by both simulations and measurements. This optimal distance is particularly effective in achieving clear reflections and a satisfactory signal-to-noise ratio (SNR) in imaging scenarios with materials such as thick concrete structures. However, when targeting depths greater than 10 m, we recommend increasing the distance between the transducers to 20 cm. This increased spacing improves the SNR in comparison to other spacings, as seen in the simulation of a 10 m deep backwall. Our results emphasize the critical role of transducer spacing in achieving the desired SNR and resolution, especially in the context of depth imaging requirements for LAUS applications. In addition to the transducer spacing, different distances between individual sets of measurement positions were tested. Overall, keeping the minimal possible distance between measurement position offsets provides the best imaging results at greater depths. The proposed optimizations for the LAUS in this study are primarily relevant to applications on massive nuclear structures for nuclear waste management. This research highlights the need for better LAUS efficiency in applications such as sealing structures, laying the foundation for future technological advances in this field. KW - Engineered barrier system KW - Phased array technique KW - Ultrasonic testing KW - Non-destructive testing in civil engineering KW - Seismic migration PY - 2024 U6 - http://nbn-resolving.de/urn/resolver.pl?urn:nbn:de:kobv:b43-592426 VL - 24 IS - 1 SP - 1 EP - 23 PB - MDPI CY - Basel, Switzerland AN - OPUS4-59242 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Prabhakara, Prathik A1 - Mielentz, Frank A1 - Stolpe, Heiko A1 - Behrens, Matthias A1 - Lay, Vera A1 - Niederleithinger, Ernst T1 - Validation of novel ultrasonic phased array borehole probe by using simulation and measurement N2 - Low-frequency ultrasonic testing is a well-established non-destructive testing (NDT) method in civil engineering for material characterization and the localization of cracks, reinforcing bars and delamination. A novel ultrasonic borehole probe is developed for in situ quality assurance of sealing structures in radioactive waste repositories using existing research boreholes. The aim is to examine the sealing structures made of salt concrete for any possible cracks and delamination and to localize built-in components. A prototype has been developed using 12 individual horizontal dry point contact (DPC) shear wave transducers separated by equidistant transmitter/receiver arrays. The probe is equipped with a commercially available portable ultrasonic flaw detector used in the NDT civil engineering industry. To increase the sound pressure generated, the number of transducers in the novel probe is increased to 32 transducers. In addition, the timed excitation of each transducer directs a focused beam of sound to a specific angle and distance based on the previously calculated delay time. This narrows the sensitivity of test volume and improves the signal-to-noise ratio of the received signals. In this paper, the newly designed phased array borehole probe is validated by beam computation in the CIVA software and experimental investigations on a half-cylindrical test specimen to investigate the directional characteristics. In combination with geophysical reconstruction methods, it is expected that an optimised radiation pattern of the probe will improve the signal quality and thus increase the reliability of the imaging results. This is an important consideration for the construction of safe sealing structures for the safe disposal of radioactive or toxic waste. KW - Ultrasound KW - Phased array KW - Concrete KW - Borehole PY - 2022 U6 - http://nbn-resolving.de/urn/resolver.pl?urn:nbn:de:kobv:b43-565722 SN - 1424-8220 VL - 22 IS - 24 SP - 1 EP - 16 PB - MDPI CY - Basel AN - OPUS4-56572 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Prabhakara, Prathik A1 - Mielentz, Frank A1 - Stolpe, Heiko A1 - Behrens, Matthias A1 - Lay, Vera A1 - Niederleithinger, Ernst T1 - Construction and validation of a novel phased array borehole probe for ultrasonic investigations at sealing structures in radioactive repositories N2 - A new type of ultrasonic borehole probe is currently under development for the quality assurance of sealing structures in radioactive waste repositories using existing research boreholes. The goal is to examine the sealing structures made of salt concrete for possible cracks, delamination, and embedded objects. Earlier prototype probes use 12 or 16 individual dry point contact (DPC) horizontal shear wave transducers grouped into a transmitter and a receiver array, each made up of six or eight individual transducers. They are operated with a commercially available portable ultrasonic flaw detector used in the civil engineering industry. To increase the generated sound pressure of the borehole probe, the number of transducers in the novel probe is increased to 32. In addition, timed excitation of each probe is used to direct a focused sound beam to a specific angle and distance based on calculated time delays. Hence, the sensitive test volume is limited, and the signal-to-noise ratio of the received signals is improved. This paper presents the validation of the newly developed phased array borehole probe by beam computation in CIVA software and experimental investigations on a semi-cylindrical test specimen to investigate the directional characteristics. In combination with geophysical reconstruction techniques, an optimised radiation pattern of the probe is expected to improve the signal quality and thus increase the reliability of the imaging results. This is of great importance for the construction of safe sealing structures needed for the disposal of radioactive or toxic waste. T2 - NDT-CE 2022 CY - Zurich, Switzerland DA - 16.08.2022 KW - Borehole probe KW - Phased array technique KW - SealWasteSafe KW - Monitoring KW - Engineered barrier; PY - 2022 U6 - http://nbn-resolving.de/urn/resolver.pl?urn:nbn:de:kobv:b43-568016 SN - 1435-4934 SP - 1 EP - 4 PB - NDT.net AN - OPUS4-56801 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Prabhakara, Prathik A1 - Mielentz, Frank A1 - Stolpe, Heiko A1 - Behrens, Matthias A1 - Lay, Vera A1 - Niederleithinger, Ernst T1 - Ultrasonic Investigation for the Quality Assurance of Sealing Structures in Radioactive Waste Repositories N2 - The structural integrity of sealing structures in underground repositories for radioactive waste is a major concern regarding safe disposal. Non-destructive testing plays a very important role in the safety of this sealing structures. Ultrasonic pulse echo technology has been established in the construction industry as a non-destructive testing method for locating potential defects and material characterization of concrete structures. A borehole probe is an ultrasonic pulse-echo device used to investigate the internal structures of salt concrete. A prototype borehole probe is successfully demonstrated with the existing research borehole in the test site using a commercially available flaw detector. A novel phased array borehole probe that allows the beam to be focused based on the delay law was constructed and tested. The directivity measurements on the semi-cylindrical concrete sample agree well with the simulation results for the different focusing angles. In combination with geophysical reconstruction methods, the optimized radiation pattern of the probe is expected to improve the signal quality and thus increase the reliability of the imaging results. In addition, a unique large aperture ultrasound system (LAUS) is expected to provide enhanced images of possible cracks and embedded objects in in-situ structures. LAUS will be optimized to reliably detect objects at depths greater than 9 m and, at the same time, provide good resolution. Modeling studies show the potential to increase the distance between the transducer arrays further, and the same configuration has been successfully tested on a thick concrete wall. Overall, the paper shows that quality assurance using ultrasonic testing is crucial for constructing safe sealing structures to dispose of radioactive or toxic waste. T2 - NDE 2022 CY - Gandhinagar, India DA - 24.12.2022 KW - Ultrasonic Testing KW - Engineered barrier KW - Phased array technique KW - Non-destructive testing civil engineering KW - Quality assurance PY - 2022 AN - OPUS4-56802 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Lay, Vera A1 - Effner, Ute A1 - Niederleithinger, Ernst A1 - Arendt, J. A1 - Hofmann, M. A1 - Kudla, W. T1 - Ultrasonic quality assurance at magnesia shotcrete sealing structures N2 - Engineered barriers are a key element to enable safe nuclear waste disposal. One method currently under research for their construction is magnesia concrete applied in a shotcrete procedure. In this study, the ultrasonic echo method is evaluated as a means for quality assurance. Imaging of internal structures (backwall, boreholes) and defects, such as delamination, has successfully been achieved in the shotcrete. Additionally, detailed information about the potential cause of selected reflectors are obtained by phase analysis. In several test blocks of various sizes, no consistent concrete section boundaries have been found by ultrasonic imaging, which was verified by subsequent drilling and complementary tests. An experiment with artificial defects imitating cracks, air-filled voids, and material with lower density has been challenging and shows the limitations of the current methods. Although significant defects, such as a large delamination, are reliably identified, several smaller defects are not identified. Generally, ultrasonic imaging provides a suitable base as a mean for quality assurance during and after the construction of sealing structures. However, further developments are required to enhance the reliability of the method and a full validation is still pending. Still, the method has potential to increase the safety of nuclear waste repositories. KW - Ultrasound KW - Imaging KW - Engineered barrier systems KW - Underground KW - Shotcrete PY - 2022 U6 - http://nbn-resolving.de/urn/resolver.pl?urn:nbn:de:kobv:b43-563170 SN - 1424-8220 VL - 22 IS - 22 SP - 1 EP - 16 PB - MDPI CY - Basel AN - OPUS4-56317 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera A1 - Mielentz, Frank A1 - Prabhakara, Prathik A1 - Baensch, Franziska A1 - Johann, Sergej A1 - Hofmann, Detlef A1 - Sturm, Patrick A1 - Stamm, Michael A1 - Niederleithinger, Ernst T1 - Multi-sensory monitoring and ultrasound for quality assurance at underground sealing structures N2 - Within the safety concepts of underground disposal sites of nuclear waste, engineered barriers play an important role. As these sealing structures have high demands concerning integrity, we aim at advancing the available construction materials, monitoring, and inspection techniques within the project SealWasteSafe. A specifically developed alkali-activated material is compared to classical salt concrete. A comprehensive multi-sensory monitoring scheme is used at 150-340 l specimens to monitor setting and hardening of both materials. All sensors are demonstrated to resist the highly alkaline environments. Besides cabled and wireless temperature and humidity of the materials, strain variations using fibre optic sensors and acoustic emissions are recorded over periods of at least 28 days, partly for more than eight months. After hardening of the specimens, further nondestructive evaluations using ultrasonic echo and thermographic measurements are conducted. Preliminary results proof the suitability of the tested sensors and clearly highlight differences between the tested materials. Particularly, the newly developed alkali-activated material shows lower acoustic emission activity indicating less cracking activity. Additionally, unique ultrasonic methods will enable better images of potential internal objects and cracks at in-situ sealing structures. A largescale ultrasonic system is optimised to reliably detect objects at a depth exceeding 9 m while still obtaining a good resolution. Modelling studies show the potential of further increasing the distance between individual transducer arrays. Additionally, a new ultrasonic borehole probe using phased arrays allowing for beam focussing is constructed and tested. Laboratory measurements at a halfcylindrical concrete specimen coincide well with the previous modelling. In total, the presented safe materials, detailed monitoring approaches and ultrasonic quality assurance methods will help to obtain safe sealing structures within salt as a host rock. The concepts can partly be transferred to sealing structures in alternative host rocks and will also be valuable for non-nuclear waste repositories. T2 - NDE NucCon CY - Espoo, Finland DA - 25.01.2023 KW - SealWasteSafe KW - Engineered barriers KW - Monitoring KW - Embedded sensors KW - Ultrasonic imaging PY - 2023 SP - 2 EP - 10 AN - OPUS4-56928 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera A1 - Prabhakara, Prathik A1 - Mielentz, Frank A1 - Johann, Sergej A1 - Fritsch, Tobias A1 - Stamm, Michael A1 - Kühne, Hans-Carsten A1 - Niederleithinger, Ernst T1 - Material research and multi-sensory monitoring for concrete sealing structure in rock salt underground repositories N2 - Within the project SealWasteSafe, we advance construction materials and non-destructive monitoring concepts of sealing structures applied for underground disposal of nuclear waste. As these engineered barriers have high demands regarding structural integrity, an innovative alkali-activated material (AAM) that is highly suitable for the application in salt as a host rock is improved and tested on two laboratory scales. This AAM has a low heat evolution due to the reaction mechanism in comparison to common salt concretes based on Portland cement or magnesium oxychloride binders. Hence, crack formation due to thermally induced stress during the hardening process is reduced. After successful laboratory tests with small specimens (height ~5 cm), comparably manufactured large cubic (edge length 70 cm) and cylindrical specimens (height 120 cm, diameter 40 cm) are equipped with sensing technologies to demonstrate the sensors´ technical capabilities. A comprehensive multi-sensory monitoring scheme is developed and investigated to characterize and compare the different material behaviour during the setting and hardening process of two materials: (1) the newly developed AAM-based mortars with salt aggregate, and (2) a blended Portland cement-based salt concrete as reference. The analysed parameters include temperature and humidity of the material, acoustic emissions, and strain variations recorded by fiber optic cables. Passive sensor systems based on radiofrequency identification technology (RFID) embedded in the concrete provide an interface for the wireless readout of various sensors. In parallel to the embedded RFID sensors, conventional cabled systems to read out the temperature and humidity measurements are installed for comparison. Additionally, a detailed inspection of the two large cubic specimens after a monitoring period of more than six months has been undertaken. Active thermography and ultrasonic echo measurements are used to reveal potentially occurring inner cracks from the surface. To verify the non-invasive results, a core sample (diameter 2 cm) was extracted from each of the investigated cubic specimens and analysed in detail with X-ray computed tomography. Furthermore, ultrasonic methods are used for quality assurance to detect obstacles, cracks, and delamination at in-situ scale sealing structures. Experimental layout and applied imaging techniques are optimised to enhance the image quality for measurements from the front side of the engineered barrier. To characterize the inside of the test sealing structure and to improve the detection of potentially existing cracks, an ultrasonic borehole probe using the phased array technique is developed. First analyses at a half-spherical specimen coincide with modelling results and prove the reliability of the directional response caused by the phased array technique of the newly constructed ultrasonic borehole probe. Overall, the project SealWasteSafe helps to characterize construction materials and improves multi-sensory monitoring concepts and ultrasonic equipment for the sake of quality assurance. Particularly for salt as a host rock, this will help to design safe sealing structures for nuclear waste disposal. T2 - EGU General Assembly 2023 CY - Vienna, Austria DA - 23.04.2023 KW - SealWasteSafe KW - Engineered barriers KW - Salt concrete KW - Quality assurance KW - Ultrasound KW - CT KW - Thermography PY - 2023 U6 - https://doi.org/10.5194/egusphere-egu23-11582 AN - OPUS4-57500 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera A1 - Effner, Ute A1 - Niederleithinger, Ernst T1 - Untersuchung eines Spritzbeton-Probekörpers unter Tage mit Ultraschall N2 - Für die sichere Endlagerung nuklearer Abfälle sind im Salzgestein Verschlussbauwerke aus Salzbeton als geotechnischen Barrieren vorgesehen. Um die Integrität der Bauwerke im Rahmen einer Qualitätssicherung nachzuweisen, eignet sich eine zerstörungsfreie Prüfung (ZfP) mit Ultraschall-Verfahren. Potenziell auftretende Risse oder Ablösungen sowie Einbauteile können detektiert werden. Um die Möglichkeiten und Grenzen der Ultraschall-Echo-Messungen sowie der Auswertemethoden zu untersuchen, wurden in einem aus Spritzbeton hergestellten Testbauwerk in der Grube Teutschenthal (bei Halle, Deutschland) verschiedene Störkörper während der Betonage eingebettet. Die Störkörper (Breite 3 cm bis ~8 cm) liegen in Tiefen von etwa 30 cm bis 80 cm und repräsentieren Hohlräume, Risse oder Inhomogenitäten des Betons. Von der Oberfläche führten wir Ultraschall-Echo-Messungen auf einer Fläche von etwa 100x150 cm² in einem 3D Modus durch. Die Auswertung erfolgte zunächst mithilfe der in der ZfP etablierten Synthetic-Aperture-Focusing Technique (SAFT), die der Kirchhoff Migration ähnelt. Insgesamt wird eine Vielzahl von Reflektoren im Bauwerk abgebildet, die jedoch nur in wenigen Fällen den eingebauten Störkörpern zugeordnet werden konnten, so dass auch die Grenzen des Verfahrens bei dieser Bauweise deutlich werden. Allerdings konnte eine ungeplante großflächige (>30 cm) Ablösung nachgewiesen und durch anschließende Bohrungen verifiziert werden. Um das strukturelle Abbild des Bauwerksinneren trotz des stark streuenden Spritzbetons zu verbessern, wenden wir fokussierende Migrationsverfahren an. Erste Ergebnisse zeigen, dass eine klarere Abbildung einzelner Reflektoren erreicht werden kann. Dies erleichtert die Detektion einzelner Objekte. Das hier präsentierte Experiment mit bekannten Reflektoren unter realen Bedingungen mit Spritzbeton unter Tage bietet hervorragende Möglichkeiten zur Überprüfung von methodischen Weiterentwicklungen im Bereich der Ultraschallanalyse. Durch die Verbesserung der Auswertemethodik und der darauf basierenden ultraschallbasierten Qualitätssicherungskonzepte werden insgesamt sicherere Verschlussbauwerke für nukleare Endlager ermöglicht. T2 - 83. Jahrestagung der Deutschen Geophysikalischen Gesellschaft (DGG) CY - Bremen, Germany DA - 06.03.2023 KW - Ultraschall KW - Spritzbeton KW - Qualitätssicherung KW - Abbildungsverfahren PY - 2023 AN - OPUS4-57136 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera A1 - Büttner, Christoph A1 - Buske, Stefan A1 - Niederleithinger, Ernst T1 - Advanced analysis of ultrasonic investigations at sealing structures N2 - Engineering barrier systems are a crucial part of the safe underground disposal of radioactive waste, particularly in salt as a host rock. Sealing structures made of tailored concrete are under test at various sites in Germany. To characterise the material properties of the concrete and potentially also the bonding to the host rock as part of the necessary subsurface structures, we apply non-destructive testing making use of advanced geophysical imaging methods. Ultrasonic investigations have been carried out at underground concrete structures in the Teutschenthal mine in Germany. Here, we show results from two distinct constructions produced in a shotcrete procedure. Our goal is to analyse the performance of ultrasonics to be used as quality assurance for sealing structures made from shotcrete. First, a ~10 m long shotcrete structure is investigated with the help of a unique Large Aperture Ultrasonic System (LAUS) allowing for depth penetration of > 9 m. We perform measurements at the front and from the side of the construction. Second, we obtain results from a 1 m thick shotcrete body containing several artificial defects (width up to 8 cm). Ultrasonic testing data were acquired using a commercial multi-static device. Additionally, a new device measuring with 3D mode instead of line mode is applied and preliminary results will be shown. Generally, the acquired ultrasonic data are analysed by the Synthetic Aperture Focusing Technique that is commonly applied in non-destructive testing. As a result, reflectors in the analysed shotcrete structures are imaged. Individual reflections from internal features and particularly the opposite wall are identified. An unexpected delamination wider than 30 cm is clearly imaged and later verified by boreholes. Thus, the method is – in general – suitable to serve as a quality measure. However, particularly the small and deep artificial defects can hardly be identified in the resulting images. Thus, we use advanced geophysical imaging methods to further enhance the quality of the obtained images. The recorded ultrasonic energy is focused to the physically reflective origin in the analysed volume. First results clearly show that we successfully improve the image quality regarding noise level and artifacts and hence facilitate the detection of objects. In total, we present a valuable experiment under realistic conditions for underground sealing structures made from shotcrete, where the locations of artificial reflectors are partly known. This experiment serves as a unique basis to analyse the performance of advanced analysis methods to obtain high-quality images of the structure’s interior. Hence, the developed ultrasonic testing and analysis schemes can serve as a part of quality assurance that will help to enable safe sealing structures for nuclear waste disposal. T2 - SafeND2023: Interdisciplinary research symposium on the safety of nuclear disposal practices CY - Berlin, Germany DA - 13.09.2023 KW - Ultrasound KW - Imaging KW - Engineered barrier systems KW - Shotcrete PY - 2023 U6 - https://doi.org/10.5194/sand-2-67-2023 AN - OPUS4-58497 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera A1 - Büttner, Christoph A1 - Roumia, Nzeeh A1 - Niederleithinger, Ernst T1 - Potential of 3D matrix ultrasonic measurements to image complex concrete structures N2 - Ultrasonic echo testing is a well-established non-destructive testing technique used to investigate the interior of concrete structures in civil engineering. For the reconstruction of internal features, methods similar to seismic imaging are applied. To improve the ultrasonic imaging capabilities, we investigate the potential of a newly available 3D matrix mode measurement device in combination with advanced imaging techniques. Commonly used ultrasonic array measurement devices rely on several ultrasonic transducers coupled to act as one transducer that transmits or receives transversal ultrasound waves. Although this approach is well suited to detect elongated structures such as pipes and rebars, it has limitations if 3D embedded objects are present. Hence, the ultrasonic device MiraA1040Pro used here is designed to measure the ultrasonic wavefield on a 4 by 16 matrix of individual transducers. For testing, we used laboratory specimens with linear and spheric embedded structures first. Both linear and matrix mode measurements were conducted and analysed using the Synthetic Aperture Focusing Technique (SAFT) which is similar to Kirchhoff migration. Second, we used a data set from Teutschenthal mine at a shotcrete specimen constructed to simulate engineered barriers tailored for nuclear waste repositories. Ultrasonic measurements were investigated as a tool for quality assurance of these structures. The specimen contains both artificial 3D artifacts as well as naturally occurring defects such as a delamination. To make use of the advanced data acquisition, focusing 3D imaging techniques are applied to further improve the imaging quality. Generally, the reconstructed images from the 3D matrix mode data have a lower level of Signal-to-Noise-Ratio than the 2D linear mode because the source signal is weaker compared to the linear mode. Moreover, complex wave conversions of the SH-transversal wave occur that are reduced in the 2D linear scenario. However, clearer images can be achieved at non-linear features, particularly with focusing imaging methods. Thus, combining 3D data acquisition techniques with advanced imaging methods improves the success in imaging complex concrete structures. This is of particular interest for thick concrete structures in nuclear barrier systems or foundations. Additionally, we demonstrate opportunities to use well-constrained test laboratory scenarios from non-destructive testing as a practical test case for geophysical methods. T2 - Jahrestagung der Deutschen Geophysikalischen Gesellschaft (DGG) CY - Jena, Germany DA - 11.03.2024 KW - Ultrasound KW - Imaging KW - Quality assurance PY - 2024 AN - OPUS4-59729 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera A1 - Baensch, Franziska A1 - Johann, Sergej A1 - Sturm, Patrick A1 - Mielentz, Frank A1 - Prabhakara, Prathik A1 - Hofmann, Detlef A1 - Niederleithinger, Ernst A1 - Kühne, Hans-Carsten T1 - SealWasteSafe: materials technology, monitoring techniques, and quality assurance for safe sealing structures in underground repositories N2 - Within the project SealWasteSafe, we advance construction materials and monitoring concepts of sealing structures applied for underground disposal of nuclear or toxic waste. As these engineered barriers have high demands concerning integrity, an innovative alkali-activated material (AAM) is improved and tested on various laboratory scales. This AAM has low reaction kinetics related to a preferential slow release of the heat of reaction in comparison to alternative salt concretes based on Portland cement or magnesium oxychloride cements. Hence, crack formation due to thermally induced strain is reduced. After successful laboratory scale analysis (Sturm et al., 2021), the AAM is characterised on a larger scale by manufacturing test specimens (100–300 L). Conventional salt concrete (DBE, 2004) and the newly developed AAM are compared using two specimen geometries, i.e. cylindrical and cuboid. A comprehensive multisensor monitoring scheme is developed to compare the setting process of AAM and salt concrete for these manufactured specimens. The analysed parameters include temperature and humidity of the material, acoustic emissions, and strain variations. Passive sensor systems based on radiofrequency identification technology (RFID) embedded in the concrete, enable wireless access to temperature and humidity measurements and are compared to conventional cabled systems. Additionally, fibre-optic sensors (FOS) are embedded to record strain, but also have potential to record temperature and moisture conditions. Part of this project aims at demonstrating the high reliability of sensors and also their resistance to highly alkaline environments and to water intrusion along cables or at sensor locations. Further technical improvements were implemented so that first results clearly show the scalability of the setting process from previous small-scale AAM experiments and particularly the high potential of the newly developed approaches. Furthermore, ultrasonic methods are used for quality assurance to detect obstacles, potential cracks and delamination. On the one hand, both active and passive ultrasonic measurements complement the results obtained from the multisensor monitoring scheme for the produced specimens. On the other hand, the unique large aperture ultrasonic system (LAUS) provides great depth penetration (up to nearly 10 m) and can thus be applied at in situ sealing structures built as a test site in Morsleben by the Federal Company for Radioactive Waste Disposal (Bundesgesellschaft für Endlagerung, BGE) as shown by Effner et al. (2021). An optimised field lay-out identified from forward modelling studies and advanced imaging techniques applied to the measured data will further improve the obtained results. To characterise the inside of the test engineered barrier and achieve a proof-of-concept, an ultrasonic borehole probe is developed to enable phased arrays that can further improve the detection of potential cracks. Modelling results and first analysis of semispherical specimens confirmed the reliability of the directional response caused by the phased arrays of the newly constructed ultrasonic borehole probe. Overall, the project SealWasteSafe improves the construction material, multisensor monitoring concepts and ultrasonics for quality assurance. This will help to develop safe sealing structures for nuclear waste disposal. The outcomes are particularly valuable for salt as a host rock but partly also transferrable to alternative conditions. T2 - Safe ND Interdisciplinary research symposium on the safety of nuclear disposal practices CY - Berlin, Germany DA - 10.11.2021 KW - Borehole probe KW - SealWasteSafe KW - Engineered barrier KW - Materials technology KW - Monitoring KW - AAM KW - Ultrasound PY - 2021 U6 - http://nbn-resolving.de/urn/resolver.pl?urn:nbn:de:kobv:b43-539172 VL - 1 SP - 127 EP - 128 PB - Copernicus AN - OPUS4-53917 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera A1 - Baensch, Franziska A1 - Hofmann, Detlef A1 - Johann, Sergej A1 - Tiebe, Carlo A1 - Basedau, Frank A1 - Sturm, Patrick A1 - Niederleithinger, Ernst T1 - Multi-sensor conception for safe sealing structures in underground repositories N2 - The project "SealWasteSafe" of the Bundesanstalt für Materialforschung und -prüfung (Berlin) deals with sealing structures applied for underground disposal of nuclear waste from two perspectives: material improvement for application in sealing constructions and feasibility study regarding multi-sensor approaches to ensure quality assurance and long-term monitoring. One specimen of 150 l made of alkali-activated material, which was found innovative and suitable for sealing constructions based on preliminary laboratory studies, and another one made of conventional salt concrete, are manufactured with an integrated multi-sensory setup for quality assurance and long-term-monitoring. The specimens were left in their cast form and additionally thermally insulated to simulate the situation in the repository. The multi-sensory concept comprises RFID technology embedded in the specimens suppling material temperature and moisture measurements, integrated distributed fibre optic sensing allowing strain measurement and acoustic emission testing for monitoring crack formation. Overall, the suitability and the functionality of the sensors embedded into and attached to strongly alkaline (pH > 13 for the AAM) and salt corrosive (NaCl) environment was proven for the first 672 h. First RFID measurement succeeded after 626 h for the alkali-activated material and after 192 h for the conventional salt concrete. Strain measurement based on fibre optic sensing turned out the alkali-activated material (> 1 mm/m) undergoing approximately twice the compression strain as the salt concrete (< 0.5 mm/m). In contrast, the acoustic emission first and single hits representing crack formation in numbers, was found for alkali-activated material half of that detected at the salt concrete. T2 - SMIRT 26 CY - Berlin, Germany DA - 10.07.2022 KW - SealWasteSafe KW - Monitoring KW - Acoustic emission KW - Fibre optic sensing KW - RFID technology KW - Alkali-activated material PY - 2022 AN - OPUS4-55372 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera A1 - Baensch, Franziska A1 - Hofmann, Detlef A1 - Mielentz, Frank A1 - Sturm, Patrick A1 - Prabhakara, Prathik A1 - Johann, Sergej A1 - Kühne, Hans-Carsten A1 - Niederleithinger, Ernst T1 - New materials and innovative monitoring for safe sealing structures in underground repositories N2 - Within the project SealWasteSafe, we advance construction materials and monitoring concepts of sealing structures applied for underground disposal of nuclear waste. As these engineered barriers have high demands concerning integrity, an innovative alkali-activated material (AAM) is improved and tested on various laboratory scales that is highly suitable for the application in salt as a host rock. This AAM has a low reaction kinetics related to a preferential slow release of the heat of reaction in comparison to alternative salt concretes based on Portland cement or magnesium oxychloride cements. Hence, crack formation due to thermally induced strain is reduced. A comprehensive multi-sensory monitoring scheme is developed and investigated to compare the setting process of AAM and salt concrete for manufactured specimens (100-300 l). The analysed parameters include temperature and humidity of the material, acoustic emissions, and strain variations recorded by fiber optic cables. Passive sensor systems based on radiofrequency identification technology (RFID) embedded in the concrete allow for wireless access and are compared to conventional cabled systems for temperature and humidity measurements. Furthermore, ultrasonic methods are used for quality assurance to detect obstacles, potential cracks and delamination. Field layout and applied imaging techniques are optimised to enhance the image quality. To characterise the inside of the test engineered barrier and achieve a proof-of-concept, an ultrasonic borehole probe is developed to allow for phased arrays that can further improve the detection of potential cracks. Modelling results and first analysis of half-spherical specimen prove the reliability of the directional response caused by the phased arrays of the newly constructed ultrasonic borehole probe. Overall, the project SealWasteSafe improves the construction material, multi-sensory monitoring concepts and ultrasonics for quality assurance. Particularly for salt as a host rock, this will help to develop safe sealing structures for nuclear waste disposal. T2 - 9th IGD-TP Symposium CY - Zurich, Switzerland DA - 20.09.2022 KW - SealWasteSafe KW - Monitoring KW - Engineered barrier systems KW - Alkali-activated material KW - Ultrasonic inspection PY - 2022 AN - OPUS4-55826 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lay, Vera A1 - Niederleithinger, Ernst A1 - Köpp, Christan T1 - Monitoring and digital tools for pre-disposal handling of cemented wastes N2 - Multifaceted developments for pre-disposal management of low and intermediate level radioactive waste are undertaken in the EC funded project PREDIS. In work package 7, innovations in cemented waste handling and pre-disposal storage are advanced by testing and evaluating. To provide better means for safe and effective monitoring of cemented waste packages including prediction tools to assess the future integrity development during pre-disposal activities, several monitoring and digital tools are evaluated and improved. Both safety enhancement (e. g. less exposure of testing personnel) and cost effectiveness are part of the intended impact. Current methods to pack, store, and monitor cemented wastes are identified, analysed and improved. Innovative integrity testing and monitoring techniques applied to evaluate and demonstrate package and storage quality assurance are further developed. The work includes but is not limited to inspection methods such as muon imaging, wireless sensors integrated into waste packages as well as external package and facility monitoring such as remote fiber optical sensors. The sensors applied will go beyond radiation monitoring and include proxy parameters important for long term integrity assessment (e. g. internal pressure). The measured data will be used in digital twins of the packages for specific simulations (geochemical, integrity) providing a prediction of future behaviour. Machine Learning techniques trained by the characterization of older packages will help to connect the models to the actual data. As data handling, processing and fusion are crucial for both the monitoring and the digital twin model, all data (measured and simulated) will be collected in a joint data base and connected to a decision framework. Finally, the implementation of the improved techniques will be tested at actual facilities. An overview about various relevant tools, their interconnections, and first research results will be shown. T2 - 9th IGD-TP Symposium CY - Zurich, Switzerland DA - 20.09.2022 KW - Predis KW - Monitoring KW - Sensors KW - Simulation KW - Digital twin PY - 2022 AN - OPUS4-55827 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -