TY - JOUR A1 - Dixneit, J. A1 - Gibmeier, J. A1 - Kromm, Arne A1 - Schubnell, J. A1 - Lang, F. A1 - Loebich, F. A1 - Carl, E.-R. A1 - Ya, W. T1 - Residual stress distribution of a large component manufactured by AM-DED-Arc from high-strength weld filler material X90 N2 - Currently, DED-Arc manufactured components are not covered by design guidelines, and design factors such as residual stress factors are not defined for such components. This hinders industrial use, especially for components with a remaining surface waviness required by industry. For the first time the stress state of a high-strength, low-alloy, large-scale DED-Arc component was characterised in the as-built state and after cutting off the component from the substrate plate. Complementary methods of residual stress analyses were applied to gain a holistic insight into the residual stress distributions of a thick-walled part. In the as-built state, direction-dependent and position-dependent tensile residual stresses were found for the component at the level of the yield strength of the part. The additive manufacturing strategy continuous spiral deposition has no significant influence on the residual stresses in bead threshold area compared to the residual stresses of the remaining component. For this case, bead threshold is no structural imperfection. By removing the part from the substrate plate, the residual stresses are significantly redistributed. Tensile residual stresses are then present at a moderate level. Compressive residual stresses were determined in the volume of the deposited material. The general consideration of ‘‘high’’ tensile residual stresses in such thick-walled components is rather conservative. Therefore, design guidelines should take the manufacturing condition into account. KW - AM-DED-Arc KW - Residual stress KW - High strength steel PY - 2026 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-655239 DO - https://doi.org/10.1177/03093247251406876 SN - 2041-3130 SP - 1 EP - 18 PB - SAGE AN - OPUS4-65523 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Vollert, F. A1 - Gibmeier, J. A1 - Rebelo-Kornmeier, J. A1 - Dixneit, Jonny A1 - Pirling, T. ED - Neu, R. W. ED - Totten, G. E. T1 - Two-dimensional residual stress mapping of multilayer LTT weld joints using the contour method N2 - Low transformation temperature (LTT) weld filler materials offer an attractive alternative to cost intensive postweld treatments as they can mitigate detrimental welding residual stresses during the welding process. Compared to conventional weld filler materials, LTT alloys are characterized by a delayed martensite transformation at low temperatures, which can result in compressive residual stresses in the weld. The high strength of these filler materials makes them potentially applicable to high-strength steels as well as for a large amount of requested repair works in steel structures. The focus of the study is on the confirmation of the LTT idea with regard to the residual stress state for multipass weld lines processed by metal active gas welding. It is demonstrated that the contour method is a well-suited technique for measuring the residual stress in the weld joint as it gives an entire two-dimensional map of the residual stress state in the weld line, heat affected zone (HAZ), and base material. The technique was applied at different LTT alloys with varying chemical compositions. Additionally, the results are compared to residual stress maps that were determined by Neutron diffraction using the Strain Analyzer for Large Scale Engineering Applications, an instrument referred to as SALSA, at the Institut Laue-Langevin in Grenoble. For all investigated specimens, compressive residual stress distributions were determined in the area of the weld joint and the HAZ. They are balanced by tensile residual stresses in the surrounding base material. However, it is shown that the size of theregion exhibiting compressive residual stresses and the absolute values of the compressive residual stresses depend on the chemical composition of the weld filler material. KW - LTT Weld Filler Materials KW - contour method KW - neutron diffraction KW - Welding KW - residual stress analysis PY - 2018 DO - https://doi.org/10.1520/MPC20170110 SN - 2379-1365 VL - 7 IS - 4 SP - 545 EP - 558 PB - ASTM International CY - West Conshohocken, PA, USA AN - OPUS4-46694 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Gibmeier, J. A1 - Obelode, E. A1 - Altenkirch, J. A1 - Kromm, Arne A1 - Kannengießer, Thomas T1 - Residual stress in steel fusion welds joined using low transformation temperature (LTT) filler material N2 - Welding residual stress is of major concern for structural integrity assessment in industrial components. Shear and volume strains resulting from the austenite-martensite-transformation affect the development of residual stress during welding. Controlling the phase transformation allows adjustment of the welding residual stress. Low transformation temperature (LTT) weld filler materials exhibiting reduced MS-temperatures allow postponing the phase transformation. The associated strain arising from the delayed transformation compensates for the thermal contraction strains and as such may reduce tensile or even introduce compressive residual stress. In this article we discuss the tri-axial residual stress distribution in 15 mm S690Q steel plates joined with LTT filler materials with 10 wt% Cr and a Ni-content that varies from 8 to 12 wt%. Using complementary synchrotron X-ray and neutron diffraction stress analysis the macroscopic residual stress was derived from the phase specific lattice strain and phase fraction of martensite and retained austenite, respectively. The local phase specific unstrained lattice parameters were determined using stress relieved combs. The investigation revealed increasing phase fraction of retained austenite with increasing Ni-content. Further, independent of the Ni-content in each weld in the fusion zone, significant compressive residual stresses were found in the longitudinal direction, which are balanced by tensile residual stresses in the heat affected zone (HAZ). In the weld transverse and normal direction the stress distribution is qualitatively similar but less in magnitude. The increased amount of retained austenite reduces the compressive stress arising from shear and volume strains during the delayed phase transformation and therefore no significant increase in compression was observed for decreasing MS-temperatures. KW - Welding residual stresses KW - Neutron diffraction KW - LTT filler materials PY - 2014 DO - https://doi.org/10.4028/www.scientific.net/MSF.768-769.620 SN - 0255-5476 VL - 768-769 SP - 620 EP - 627 PB - Trans Tech Publications CY - Aedermannsdorf, Switzerland AN - OPUS4-29706 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Gibmeier, J. A1 - Held, A. A1 - Altenkirch, J. A1 - Kromm, Arne A1 - Kannengießer, Thomas A1 - Buslaps, T. T1 - Real time monitoring of phase transformation and strain evolution in LTT weld filler material using EDXRD N2 - For a newly developed 10% Cr and 10% Ni low transformation temperature (LTT) weld filler material, the local phase transformation kinetics and the strain evolution during gas tungsten arc welding (GTAW) under real welding conditions was studied. An experimental set-up and a measuring and evaluation strategy are presented to gain a real time insight into the welding process. The experiments were carried out at the beam line ID15@ESRF using a two detector EDXRD (energy dispersive X-ray diffraction) set-up and high energy synchrotron X-rays. The time-resolved diffraction analysis during welding was carried out locally throughout the weld in longitudinal as well as in transverse direction to the weld line to examine the interdependence of the strain state and the transformation kinetics. This comprehension is crucial for the optimization of the weld process, and thus for the tailoring of the resulting residual stress states, which is one of the main issues for the application of LTT alloys. Using the herein proposed approach EDXRD diffraction pattern can be monitored during real welding with a counting rate of 5 Hz. By means of the time resolved diffraction data the local transformation temperatures and times were determined and the local phasespecific strain evolutions are discussed with respect to the transformation rates and the time-delayed phase transformations. KW - In situ synchrotron X-ray diffraction KW - Low transformation temperature KW - Welding PY - 2014 DO - https://doi.org/10.1016/j.jmatprotec.2014.06.008 SN - 0924-0136 SN - 1873-4774 VL - 214 IS - 11 SP - 2739 EP - 2747 PB - Elsevier CY - Amsterdam AN - OPUS4-30955 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kromm, Arne A1 - Kannengießer, Thomas A1 - Altenkirch, J. A1 - Gibmeier, J. T1 - Residual stresses in multilayer welds with different martensitic transformation temperatures analyzed by high-energy synchrotron diffraction N2 - Low Transformation Temperature (LTT) alloys were developed in order to control the residual stress development by the martensitic phase transformation already during cooling of the weld metal. The positive effect of such LTT alloys on the mitigation of detrimental tensile residual stresses during welding has already been confirmed on the basis of individual laboratory tests. Within the current project it was experimentally investigated whether the phase transformation mechanisms are effective under increased restraint due to multi-pass welding of thicker specimens. The local residual stress depth distribution was analyzed non-destructively for V-type welds processed by arc welding using energy dispersive synchrotron X-ray diffraction (EDXRD). The use of high energy (20 keV to 150 keV) EDXRD allowed for the evaluation of diffraction spectra containing information of all contributing phases. As the investigated LTT alloy contains retained austenite after welding, this phase was also considered for stress analysis. The results show in particular how the constraining effect of increased thickness of the welded plates and additional deposited weld metal influences the level of the residual stresses in near weld surface areas. While the longitudinal residual stresses were reduced in general, in the transition zone from the weld to the heat-affected zone (HAZ) compressive residual stresses were found. KW - Low Transformation Temperature KW - Phase Transformation KW - Residual Stress KW - Synchrotron Diffraction PY - 2011 DO - https://doi.org/10.4028/www.scientific.net/MSF.681.37 SN - 0255-5476 VL - 681 SP - 37 EP - 42 PB - Trans Tech Publications CY - Aedermannsdorf, Switzerland AN - OPUS4-23470 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Altenkirch, J. A1 - Gibmeier, J. A1 - Kromm, Arne A1 - Kannengießer, Thomas A1 - Nitschke-Pagel, T. A1 - Hofmann, M. T1 - In situ study of structural integrity of low transformation temperature (LTT)-welds N2 - We discuss the stability of weld residual strain under static and quasi cyclic transverse tensile loading in the elastic and elastic–plastic region. The test welds were joined with low transformation temperature weld filler materials with 10 wt% Cr and varying Ni-content from 8 to 12 wt%. Using neutron diffraction the residual lattice strain in the martensitic α'- and austenitic γ-phase in the fusion zone as well as the ferritic α-phase in the heat affected zone and base metal as induced by welding, superimposed by stepwise tensile loading and after unloading was measured. The amount of retained austenite in the fusion zone increases with increasing Ni-content, but it decreases with increasing load level due to stress induced martensite formation. In the as-welded condition the transverse macroscopic residual lattice strain was found to be in low compression in the fusion zone in each weld, while the heat affected zone was in tension. Local plastic deformation of the γ-phase as a result of yielding during tensile loading in combination with the change in phase fraction resulted in increased macroscopic compression in the fusion zone. The reduced yield strength in the heat affected zone resulted in plastic deformation and a considerable shift into compression. Comparison with the cross weld distribution of the hardness and FWHM of the neutron diffraction interference lines supported the assumption of plastic deformation of the γ- and α-phase in the fusion and heat affected zone, respectively, while the α'-phase in the fusion zone was stressed within the elastic regime only. Microstructural observations as well as measurement of the local γ-phase fraction by means of laboratory X-ray diffraction in the fusion zone strengthen these observations. KW - Low transformation temperature KW - Residual stress KW - Neutron diffraction PY - 2011 DO - https://doi.org/10.1016/j.msea.2011.03.091 SN - 0921-5093 SN - 1873-4936 VL - 528 IS - 16-17 SP - 5566 EP - 5575 PB - Elsevier CY - Amsterdam AN - OPUS4-24359 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Altenkirch, J. A1 - Gibmeier, J. A1 - Kostov, V. A1 - Kromm, Arne A1 - Kannengießer, Thomas A1 - Doyle, S. A1 - Wanner, A. T1 - Time- and temperature-resolved synchrotron X-ray diffraction: observation of phase transformation and strain evolution in novel low temperature transformation weld filler materials N2 - Solid-state phase transformations and the evolution of thermal and elastic strains in novel low temperature transformation (LTT) weld filler materials in the near surface region are monitored in real time by means of an innovative experimental set-up at the PDIFF (powder diffraction) beamline at the synchrotron light source ANKA (Angströmquelle Karlsruhe) at the KIT (Karlsruhe Institute for Technology). The key components of the diffraction set-up are two fast microstrip line detectors, which enables the strain evolution to be followed as a function of time and temperature for a 0.5?s counting time. During controlled heating and cooling cycles, as well as during near welding cycles, the martensite–austenite–martensite phase transitions are analysed. The transformation kinetics are monitored during resistance heating of small chips of the pure LTT alloys and during gas tungsten arc welding of simplified LTT welds using a specially designed welding rig for in-situ studies on the diffraction instruments. Under the mechanically unconstrained condition allowing free thermal expansion and shrinkage, the LTT alloys are found to exhibit decreasing transformation temperatures Ac and MS and increasing phase fraction of retained austenite for increasing Ni content. The strain evolution during welding reveals increased compressive stresses upon welding, which is attributed to the martensite formation upon cooling, which counteracts the thermal contraction strains. Comparison of the transformation temperatures reveals higher values than in the pure LTT alloys, but no variation between the different alloys. On the one hand, this is attributed to preferred grain orientation affecting the diffraction measurements and the determination of the transformation temperatures. On the other hand, it is possible that with the different chemical compositions of the LTT alloys and the mechanical constraints during welding, the evolution of the residual strain and stress may vary and result in counteracting affects with respect to lowered martensite start temperatures. KW - In-situ synchrotron X-ray diffraction KW - Low temperature transformation KW - Welding PY - 2011 DO - https://doi.org/10.1177/0309324711413190 SN - 0309-3247 SN - 2041-3130 VL - 46 IS - 7 SP - 563 EP - 579 PB - Sage CY - London AN - OPUS4-24683 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Vollert, F. A1 - Thomas, Maximilian A1 - Kromm, Arne A1 - Gibmeier, J. T1 - Solidification Cracking Assessment of LTT Filler Materials by Means of Varestraint Testing and μCT N2 - Investigations of the weldability of metals often deal with hot cracking, as one of the most dreaded imperfections during weld fabrication. The hot cracking investigations presented in this paper were carried out as part of a study on the development of low transformation temperature (LTT) weld filler materials. These alloys allow to mitigate tensile residual stresses that usually arise during welding using conventional weld filler materials. By this means, higher fatigue strength and higher lifetimes of the weld can be achieved. However, LTT weld filler materials are for example, high-alloyed Cr/Ni steels that are susceptible to the formation of hot cracks. To assess hot cracking, we applied the standardized modified varestraint transvarestraint hot cracking test (MVT), which is well appropriate to evaluate different base or filler materials with regard to their hot cracking susceptibility. In order to consider the complete material volume for the assessment of hot cracking, we additionally applied microfocus X-ray computer tomography (μCT). It is shown that by a suitable selection of welding and MVT parameter the analysis of the complete 3D hot crack network can provide additional information with regard to the hot cracking model following Prokhorov. It is now possible to determine easy accessible substitute values (e.g., maximum crack depth) for the extent of the Brittleness Temperature Range (BTR) and the minimum critical strain Pmin. KW - LTT weld filler materials KW - μCT-analysis KW - Hot cracking KW - Varestraint test PY - 2020 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-509126 DO - https://doi.org/10.3390/ma13122726 VL - 13 IS - 12 SP - 2726 PB - MDPI AN - OPUS4-50912 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Vollert, F. A1 - Thomas, Maximilian A1 - Kromm, Arne A1 - Gibmeier, J. T1 - Hot crack assessment of LTT welds using μCT N2 - Investigations on weldability often deal with hot cracking, as one of the most popular failure during weld fabrication. The modified varestraint transvarestraint hot cracking test (MVT) is well known for the assessment of the hot cracking susceptibility of materials. The shortcoming of this approach is that the information is only from the very near surface region, which inhibits access to the characteristic of the hot crack network in the bulk. Here, we report about a new approach, illustrated in the example of low transformation temperature (LTT) weld filler materials, to monitor the entire 3D hot crack network after welding by means of microfocus X-ray computer tomography (μCT). T2 - 10th Conference on Industrial Computed Tomography (iCT 2020) CY - Wels, Austria DA - 04.02.2020 KW - Varestraint testing KW - LTT weld filler materials KW - Hot cracking KW - Welding KW - μCT-analysis PY - 2020 DO - https://doi.org/https://doi.org/10.58286/25121 SN - 1435-4934 VL - 25 IS - 2 SP - 1 EP - 7 PB - NDT.net CY - Kirchwald AN - OPUS4-50341 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Abou-Ras, D. A1 - Gibmeier, J. A1 - Nolze, Gert A1 - Gholinia, A. A1 - Konijnenberg, P. T1 - On the capability of revealing the pseudosymmetry of the chalcopyrite-type crystal structure N2 - The tetragonal crystal- structure type of chalcopyrites (chemical formula AIBIIICVI2) is a superstructure of sphalerite type. The c/a ratio differs generally from the ideal value 2, i.e., the crystal structure is pseudocubically distorted. For CuInSe2 and CuGaSe2 thin films, simulations demonstrate that it is theoretically possible to reveal the tetragonality in electron backscatter-diffraction (EBSD) patterns for CuGaSe2, whereas it may not be possible for CuInSe2. EBSD experiments on CuGaSe2 thin films using the ”Advanced Fit” band-detection method show that it is possible to extract accurate misorientation-angle distributions from the CuGaSe2 thin film. Pole figures revealing the texture of the CuGaSe2 thin film are shown, which agree well with X-ray texture measurements from the same layer. KW - Pseudosymmetry KW - Chalcopyrite KW - Electron backscatter diffraction KW - Pattern simulation KW - Pattern matching KW - Sphalerite PY - 2008 DO - https://doi.org/10.1002/crat.200711082 VL - 43 IS - 3 SP - 234 EP - 239 PB - WILEY-VCH AN - OPUS4-38003 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Dixneit, Jonny A1 - Vollert, F. A1 - Kromm, Arne A1 - Gibmeier, J. A1 - Hannemann, Andreas A1 - Fischer, Tobias A1 - Kannengießer, Thomas T1 - In situ analysis of the strain evolution during welding using low transformation temperature filler materials N2 - Compared to conventional welding consumables using low transformation temperature (LTT) filler materials is an innovative method to mitigate tensile residual stresses due to delayed martensite transformation of the weld. For the effective usage of LTT filler materials, a deeper understanding of the complex processes that lead to the final residual stress state during multipass welding is necessary. Transformation kinetics and the strain evolution of multi-pass welds during welding were investigated in situ at the beamline HEMS@PETRAIII, Germany. Compared to conventional welds, the total strain was reduced and compression strain was achieved when using LTT filler materials. For an optimal use of the LTT effect in the root of multi-pass welds, the alloying concept must be adapted taking care of dilution. KW - Low transformation temperature filler materials KW - Synchrotron diffraction KW - Phase transformation KW - Multi-pass welding KW - ADXRD PY - 2018 DO - https://doi.org/10.1080/13621718.2018.1525150 SN - 1362-1718 SN - 1743-2936 VL - 24 IS - 3 SP - 243 EP - 255 PB - Taylor & Francis AN - OPUS4-46039 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Dixneit, Jonny A1 - Kromm, Arne A1 - Hannemann, Andreas A1 - Friedersdorf, Peter A1 - Kannengießer, Thomas A1 - Gibmeier, J. T1 - In-situ load analysis in multi-run welding using LTT filler materials N2 - Modifying the level of mostly detrimental welding residual stresses already during the welding process would be highly attractive as time- and cost-consuming post processing may be prevented. The nature of stress buildup during welding-associated cooling is highly affected by phase transformations. Up to now, it is not clear in which way this is applicable to real component welding exhibiting high shrinkage restraint and complex heat input. In this study, two different low transformation temperature (LTT) alloys have been investigated concerning the stress development in restrained multi-run butt welding in order to evaluate the potential of stress reduction. Pulsed gas metal arc welding (P-GMAW) welding was executed on a testing facility designed to simulate real lifelike restraint conditions of component weldments. The effect of reducedMS-temperatures and the heat control on the globally acting stresses was monitored by in-situ measurement of the reaction forces during welding fabrication. Additional local residual stress measurements allowed analyzing global as well as local loading of the welded construction. Although phase transformation has a significant influence on unloading the joint during each weld pass, the reaction stress upon cooling to room temperature seems to be determined mainly by the heat input. On the surface, low longitudinal residual stresses were observed in case of LTT whereas transverse residual stresses are less affected. T2 - 69th IIW Annual Assembly and International Conference CY - Melbourne, Australia DA - 10.07.2016 KW - Phase transformation temperature KW - Residual stress KW - Welding KW - Dilution KW - Restraint PY - 2016 DO - https://doi.org/10.1007/s40194-016-0373-1 SN - 0043-2288 VL - 60 IS - 6 SP - 1159 EP - 1168 PB - Springer CY - Heidelberg AN - OPUS4-37892 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Gibmeier, J. A1 - Weidemann, Jens A1 - Dixneit, Jonny A1 - Kannengießer, Thomas A1 - Kromm, Arne T1 - Influence of structural stiffness on the residual stresses during welding of low transformation temperature alloys N2 - Low Transformation Temperature (LTT) alloys are high alloyed filler materials, which exhibit a martensitic phase transformation at comparatively low temperatures in order to prevent high tensile residual stresses. A number of publications have already shown that even compressive residual stresses can be observed when using LTT filler materials. Up to know it is not clear in which way this it applicable to multi-run welding exhibiting high shrinkage restraint and complex heat input. In this study the potential for stress reduction during welding of LTT alloys was studied by numerical simulation. This allows for evaluation of the stress development in every single weid run. Additionally, the impact of the structural stiffness was incorporated by modelling a special sample geometry exhibiting a high intensity of restraint. The results show that the stress formation in weid longitudinal direction is determined by the phase transformation as high compressive residual stresses were found here independent from the weid run. On the other hand the transformation induced stresses in weid transverse direction are superimposed by tensile stresses originated from shrinkage restraint. With increasing number of runs the tensile residual stress level is raised. The results were confirmed by residual stress measurements using diffraction methods. T2 - 11th International Seminar - Numerical Analysis of Weldability CY - Graz, Austria DA - 27.09.2015 KW - Influence KW - Structural stiffness KW - Residual stresses KW - Low transformation KW - Temperature alloys KW - Welding PY - 2016 SN - 978-3-85125-490-7 SN - 2410-0544 SP - 259 EP - 276 PB - Verlag der Technischen Universität Graz CY - Graz AN - OPUS4-38998 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Held, E. A1 - Ohl, H. A1 - Gibmeier, J. A1 - Dixneit, Jonny A1 - Kromm, Arne A1 - Kannengießer, Thomas ED - Petzow, G. T1 - Mikrostruktur- und Härteentwicklung in Schweißnähten mit neuartigen LTT-Schweißzusatzwerkstoffen N2 - Das Schweißen von hochfesten Stahlstrukturen ist Gegenstand aktueller Forschungsbestrebungen wobei unter anderem der Eigenspannungsausbildung eine entscheidende Rolle zugeordnet wird. Neuartige LTT (Low Transformation Temperature) Schweißzusatzwerkstoffe mit deutlich abgesenkten Martensitstarttemperaturen wurden entwickelt, um die Eigenspannungsentwicklung in der Schweißnaht durch die späte Martensitumformung während des Abkühlens des Schweißguts kontrollieren zu können. Auf diese Weise können in den Schweißnähten nicht nur Zugeigenspannungen reduziert sondern sogar gezielt Druckeigenspannungen eingebracht werden. Dies konnte bereits in verschiedenen Arbeiten zu diesem Themenkomplex gezeigt werden. Durch das gezielte Einbringen von Druckeigenspannungen in die Schweißnaht kann die Lebensdauer und die mechanische Integrität von hochfesten Schweißverbindungen ohne aufwändige mechanische oder thermische Nachbehandlungsverfahren deutlich erhöht w erden. Einen großen Einfluss auf die Eigenspannungsausbildung in Schweißnähten haben die Umwandlungstemperatur und die Schrumpfungsbehinderung bei der Abkühlung. In der vorliegenden Arbeit wird nun untersucht, wie der Grad der Einspannung sich auf die Mikrostruktur- und Härteentwicklung in Schweißnähten mit LTT -Zusatzwerkstoffen auswirkt. Der in dieser Arbeit untersuchte neuartige LTT-Schweißzusatzstoff wurde nach dem 10%Ni - 10%Cr-Konzept nach 111 ausgewählt. Die Schweißeignung des untersuchten Werkstoffes sowie die Beeinflussung der Mikrostrukturausbildung durch eine Variation des Nickelgehalt wurden bereits in vorangehenden Arbeiten eingehend untersucht. Hierbei zeigte sich, dass der Nickelgehalt einen signifikanten Einfluss auf die Martensitstarttemperatur und damit auf die lokale Mikrostrukturausbildung hat. Eine Erhöhung des Nickelgehaltes von S auf 12 Ma-% führt zu einer Verminderung der Martensitstarttemperatur von 16()°C auf etwa 60°C (bestimmt mittels in-situ Röntgenbeugungsanalysen im reinen Schweißgut). T2 - 47. Metallographie-Tagung CY - Friedrichshafen, Germany DA - 18.09.2013 PY - 2013 SN - 978-3-88355-398-6 VL - 45 SP - 297 EP - 302 AN - OPUS4-29710 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kannengießer, Thomas A1 - Kromm, Arne A1 - Gibmeier, J. A1 - Rethmeier, Michael T1 - In-situ-Analyse der Phasenumwandlungskinetik während des Schweißens N2 - Zugeigenspannungen, wie sie beim Schweißprozess durch inhomogene Temperaturverteilungen und Schrumpfungen hervorgerufen werden, können die Lebensdauer geschweißter Verbindungen signifikant herabsetzen. Eine neue und außerordentlich attraktive Methode, um Druckeigenspannungen bereits während des Schweißens gezielt einzustellen, gelingt mit sogenannten LTT (Low Transformation Temperature)-Legierungen. LTT-Legierungen weisen eine martensitische Phasenumwandlung bei relativ niedrigen Temperaturen auf, wobei die damit verbundene Volumenexpansion zu einer Reduktion der Schrumpfeigenspannungen bzw. Erzeugung von Druckeigenspannungen führt. Zum direkten Nachweis der Phasenumwandlungen und der damit verbundenen resultierenden Schweißeigenspannungen wurden erstmals In-situ-Schweißexperimente unter Nutzung hoch energetischer, polychromatischer Synchrotronstrahlung (Weißstrahl) realisiert, um die Umwandlungskinetik während eines realen Schweißprozesses und die daraus resultierenden Schweißeigenspannungen zu analysieren. Es wird gezeigt, dass mit LTT-Legierungen signifikante Druckeigenspannungen in der Schweißnaht erreicht werden. PY - 2010 SN - 0025-5300 VL - 52 IS - 4 SP - 204 EP - 210 PB - Hanser CY - München AN - OPUS4-21219 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kannengießer, Thomas A1 - Kromm, Arne A1 - Rethmeier, Michael A1 - Gibmeier, J. A1 - Genzel, C. T1 - Residual stresses and in-situ measurement of phase transformation in low transformation temperature (LTT) welding materials PY - 2009 SN - 1097-0002 SN - 0069-8490 SN - 0376-0308 VL - 52 SP - 755 EP - 762 CY - Newtown Square, Pa., USA AN - OPUS4-19817 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Kromm, Arne A1 - Kannengießer, Thomas A1 - Gibmeier, J. A1 - Genzel, C. A1 - Mee, V. van der T1 - Determination of Residual Stresses in Low Transformation Temperature (LTT-) Weld Metals using X-ray and High Energy Synchrotron Radiation KW - Filler material KW - Low transformation temperature KW - Synchrotron radiation KW - Phase specific residual stresses KW - Energy dispersive diffraction PY - 2007 IS - II-1658r1-07 SP - 1 EP - 17 PB - International Institute of Welding CY - Paris AN - OPUS4-15716 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kromm, Arne A1 - Thomas, Maximilian A1 - Kannengießer, Thomas A1 - Gibmeier, J. A1 - Vollert, F. T1 - Assessment of the Solidification Cracking Susceptibility of Welding Consumables in the Varestraint Test by Means of an Extended Evaluation Methodology N2 - Various test methods are available for assessing the susceptibility of materials to solidification cracking during welding. In the widely used Varestraint test, the crack length is selected as a criterion as a function of the applied bending strain. Unfortunately, the crack length does not characterize the material behavior alone but depends to varying degrees on the individual test parameters used, which makes the interpretation of the results difficult. In addition, the crack length is not comparable under different test conditions. To overcome these disadvantages, we have developed a novel evaluation methodology that decouples the machine influence from the material behavior. The measured crack length is related to the maximum possible value specified by welding speed and deformation time. This relative crack length is calculated numerically, considering the orientation of the cracks. Experiments on two high-alloy martensitic welding consumables show that, in contrast to the conventional evaluation, a comparison of different welding parameters becomes possible. Furthermore, the strain rate proved to be a suitable crack criterion in agreement with Prokhorov's hot cracking model. KW - Welding KW - Solidification cracking KW - Varestraint test PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-545780 DO - https://doi.org/10.1002/adem.202101650 SN - 1438-1656 SP - 2101650 PB - Wiley online library AN - OPUS4-54578 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Dixneit, Jonny A1 - Kromm, Arne A1 - Boin, M. A1 - Kannengießer, Thomas A1 - Gibmeier, J. ED - Olden, T.-M. ED - Muransky, O. Muransky ED - Edwards, L. T1 - Influence of heat control on residual stresses in low transformation temperature (LTT) large scale welds N2 - The current paper presents residual stress analyses of large scale LTT (Low Transformation Temperature) welds. LTT filler materials are specially designed for residual stress engineering by means of an adjusted martensite phase transformation. Controlling the level of mostly detrimental residual stresses already during the welding process would be highly attractive as time and cost consuming post processing may be prevented. In large scale welds the residual stress state is influenced by the heat control (e.g. interpass temperature) during welding. Therefore, welding residual stresses are studied here putting the focus on the influence of welding process parameters while joining heavy steel sections with a thickness of 25 mm. The residual stress state was determined at the top surface using X-ray diffraction as well as in the bulk by neutron diffraction. The results show that control of the interpass temperature is vital for the residual stresses present in the joints. This accounts for the top surface but is most pronounced for the bulk of the welds. While high interpass temperatures are appropriate to induce compressive residual stresses in the weld metal, low interpass temperatures favor unwanted tensile residual stresses instead. T2 - ICRS 2016 - 10th International Conference on Residual Stresses CY - Sydney, Australia DA - 03.07.2016 KW - LTT KW - Welding residual stress KW - Phase transformation KW - Interpass temperature PY - 2016 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-389628 SN - 978-1-94529117-3 SN - 978-1-94529116-6 DO - https://doi.org/10.21741/9781945291173-38 SN - 2474-395X VL - 2 SP - 223 EP - 228 PB - Materials Research Forum LLC CY - Millersville (PA), USA AN - OPUS4-38962 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Thomas, Maximilian A1 - Vollert, F. A1 - Weidemann, Jens A1 - Gibmeier, J. A1 - Kromm, Arne A1 - Kannengießer, Thomas T1 - Surface- and volume-based investigation on influences of different Varestraint testing parameters and chemical compositions on solidification cracking in LTT filler metals N2 - The subject of this study is how, and to what extent, Varestraint/Transvarestraint test results are influenced by both testing parameters and characteristics of evaluation methods. Several different high-alloyed martensitic LTT (low Transformation temperature) filler materials, CrNi and CrMn type, were selected for examination due to their rather distinctive solidification cracking behaviour, which aroused interest after previous studies. First, the effects of different process parameter sets on the solidification cracking response were measured using standard approaches. Subsequently, microfocus X-ray computer tomography (μCT) scans were performed on the specimens. The results consistently show sub-surface cracking to significant yet varying extents. Different primary solidification types were found using wavelength dispersive X-ray (WDX) analysis conducted on filler metals with varying Cr/Ni equivalent ratios. This aspect is regarded as the main difference between the CrNiand CrMn-type materials in matters of cracking characteristics. Results show that when it comes to testing of modern highperformance alloys, one set of standard Varestraint testing parameters might not be equally suitable for all materials. Also, to properly accommodate different solidification types, sub-surface cracking has to be taken into account. KW - Solidification cracking KW - Varestraint testing KW - MVT KW - LTT filler metal KW - Microfocus X-ray computer tomography (μCT) PY - 2020 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-506039 DO - https://doi.org/10.1007/s40194-020-00895-2 VL - 64 SP - 913 EP - 923 PB - Springer Nature CY - Heidelberg, New York AN - OPUS4-50603 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Dixneit, Jonny A1 - Kromm, Arne A1 - Boin, M. A1 - Wimpory, Robert A1 - Kannengießer, Thomas A1 - Gibmeier, J. A1 - Schröpfer, Dirk T1 - Residual stresses of LTT welds in large-scale components N2 - Residual stresses of welds become more and more important influencing cold cracking as well as the fatigue life of welded components. Low transformation temperature (LTT) filler materials offer the opportunity to alter the residual stresses already during the welding process by means of ad- justed martensite phase transformation temperature (MS). In the current paper, welding residual stresses are studied putting the focus on MS while joining heavy steel sections with a thickness of 20 and 25 mm, respectively. The residual stress state was determined at the top surface using X-ray diffraction as well as in the bulk by neutron diffraction. The results com- pare the residual stresses present in a conventional weld and LTT welds when multi-pass welding of large-scale compo- nents was applied. Repeated phase transformation in the case of the LTT weld is more vital for the residual stresses present in the real-life-like joints. This accounts for the top surface in longitudinal direction but is most pronounced for the bulk of the welds. Detrimental tensile residual stresses are mainly re- duced in the bulk in comparison to a conventional filler wire even in multi-pass welds of thick steel sections. T2 - IIW AA 2016 CY - Melbourne, Australia DA - 10.07.2016 KW - LTT KW - Welding residual stress KW - Phase transformation KW - Interpass temperature PY - 2017 DO - https://doi.org/10.1007/s40194-017-0502-5 SN - 0043-2288 SN - 1878-6669 VL - 61 IS - 6 SP - 1089 EP - 1097 PB - Springer CY - Heidelberg AN - OPUS4-41169 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kromm, Arne A1 - Kannengießer, Thomas A1 - Gibmeier, J. A1 - Genzel, C. A1 - Van der Mee, V. T1 - Determination of residual stresses in low transformation temperature (LTT -) welds metals using X-rayand high energy synchrotron radiation N2 - Crack and fatigue resistance are relevant evaluation criteria for welded joints and are decreased by tensile residual stresses resulting from the welding and cooling process, while compressive residual stresses can have a positive influence on the characteristics mentioned. In order to generate compressive residual stresses, a set of post weld treatment procedures is available, like shot peening, hammering, etc. These procedures have the disadvantage that they are time and cost extensive and have to be applied after welding. As another point, such technologies can only produce compressive stresses at the top surface, i.e. can only contribute to the reduction of the risk of cracks initiated at the surface, like fatigue cracks. A chance to generate compressive stresses over the complete weld joint during the welding procedure is offered by the so-called Low Transformation Temperature (LTT -) filler wires. Compared to conventional wires, these materials show lower phase transformation temperatures, which can work against coolingrelated tensile stresses, resulting from respective shrinkage restraint. In consequence, distinct compressive residual stresses can be observed within the weld and adjacent areas. The strength of these fillers makes them potentially applicable to high-strength steel welding. Welds produced with different LTT – filler wires have shown different levels and distributions of the resulting residual stresses depending on the specific transformation temperature. The transformation temperatures are determined by temperature measurement. Classical X-ray diffraction as well as diffraction methods using high energy synchrotron radiation have been used for residual stress analysis. By means of high energy synchrotron diffraction in reflection mode residual stress depth gradients can be determined nondestructively. The phase selective nature of the diffraction measurements enables the simultaneous determination of the phase specific residual stresses of all contributing crystalline phases within one experiment. The application of white beam diffraction implies recording of a multitude of diffraction lines within the energy range of the provided energy spectrum of the white beam. By this means phase specific residual stress depth distributions up to distances of 150 ìm below the surface can be analysed for steel using the energy dispersive set-up of the HMI-beamline EDDI at the Bessy site, Berlin, providing an energy range between 20-150 keV. As a side effect quantitative phase analysis can be carried out using white energy dispersive diffraction e.g. the determination of the content of retained austenite in the weld. KW - Filler materials KW - Low temperature KW - Reference lists KW - Residual stresses KW - Temperature KW - Transformation KW - Synchrotron radiation KW - Phase specific residual stresses KW - Energy dispersive diffraction PY - 2009 SN - 0043-2288 SN - 1878-6669 VL - 53 IS - 1/2 SP - 3 EP - 16 PB - Springer CY - Oxford AN - OPUS4-19214 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kromm, Arne A1 - Kannengießer, Thomas A1 - Gibmeier, J. T1 - In-situ observation of phase transformations during welding of low transformation temperature filler material KW - LTT filler material KW - In-situ observation KW - Energy dispersive diffraction KW - Transformation temperature KW - Residual stress PY - 2010 DO - https://doi.org/10.4028/www.scientific.net/MSF.638-642.3769 SN - 0255-5476 VL - 638-642 SP - 3769 EP - 3774 PB - Trans Tech Publications CY - Aedermannsdorf, Switzerland AN - OPUS4-20725 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Gibmeier, J. T1 - Residual stress in steel fusion welds joined using low tranfsformation temperature (LTT) filler material T2 - Mecasens CY - Hamburg, Germany DA - 2011-09-07 PY - 2011 AN - OPUS4-24324 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Vollert, F. A1 - Dixneit, Jonny A1 - Gibmeier, J. ED - Marais, D. ED - Holden, T.M. ED - Venter, A.M. T1 - Effect of Residual Stress Relaxation due to Sample Extraction on the Detectability of Hot Crack Networks in LTT Welds by means of µCT N2 - Investigations on weldability often deal with hot cracking as one of the most prevalent failure mechanisms during weld fabrication. The modified varestraint transvarestraint hot cracking test (MVT) is well known to assess the hot cracking susceptibility of materials. The shortcoming of this approach is that the information is only from the very near surface region which inhibits access to the characteristic of the hot crack network in the bulk. Here, we report about an alternative approach to monitor the entire 3D hot crack network after welding by means of microfocus X-ray computer tomography (µCT). However, to provide sufficient high spatial resolution small samples must be sectioned from the MVT-welded joint. The sampling is accompanied by local relaxation of the residual stress distributions that are induced by welding, which can have an impact on the crack volumes prior to the sampling. The studies were carried out to investigate the hot cracking susceptibility of low transformation temperature filler materials (LTT). As high compression residual stresses up to -600 MPa in the area of the crack networks were determined by means of the contour method, stress relaxation caused by sectioning for µCT sample extraction can affect the detectability of the cracks later on. X-ray diffraction studies revealed surface residual stress relaxations up to about 400 MPa due to cutting. To investigate this effect, the specimens with hot cracks were subjected to a load test with known stress states. The results clearly show that local stress relaxations will have a strong impact on the volume images reconstructed from tomography analysis. This effect must be considered during hot crack assessment on basis of µCT data. T2 - 9th International Conference on Mechanical Stress Evaluation by Neutron and Synchrotron Radiation (MECA SENS 2017) CY - Skukuza Rest Camp, South Africa DA - 19.09.2017 KW - LTT Weld Filler Materials KW - µCT-analysis KW - Hot Cracks KW - Welding PY - 2018 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-456765 SN - 978-1-945291-66-1 DO - https://doi.org/10.21741/9781945291678-13 SN - 2474-395X VL - 4 SP - 85 EP - 90 AN - OPUS4-45676 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -