TY - GEN A1 - Weber, Gert A1 - Bschorr, T. A1 - Cramer, H. A1 - Hahn, Oliver A1 - Rethmeier, Michael A1 - Thommes, H. ED - da Silva, L.F.M. ED - Altenbach, H. T1 - Hybrid bonding of advanced high strength steels in the lightweight body shell design for the automobile manufacturing N2 - In the lightweight body shell mass production of automobiles, the application of hybrid bonding techniques becomes more and more important. Especially the combination of adhesive bonding and resistance spot welding called weldbonding is of great importance. The target of this contribution is to show the influence of medium-viscosity and low-viscosity structural adhesives on the process reliability of the weldbonding process and the mechanical properties of the hybrid bonded joints. The given results are based on the application of an epoxy PUR-based, an epoxy resin-based and a rubber-based adhesive system for joining a mild and some different advanced high strength steels (AHSS). It will be shown that both the process reliability of the weldbonding process and the mechanical behaviour of the weldbonded joints are influenced by the combinations of the base metals, the applied adhesive systems and the choice of the joining parameters. The behaviour of the weldbonded joints will be studied under quasi-static and impact loads. The discussion of the metallurgical structure of the weldbonded joints depending on the joining parameters will be given, too. Furthermore, the fatigue behaviour of the weldbonded joints will be studied. KW - Advanced high strength steels KW - Hybrid bonding KW - Lightweight body shell design KW - Weldbonding process reliability KW - Weldbonded joint behaviour PY - 2010 SN - 978-3-642-12666-6 DO - https://doi.org/10.1007/978-3-642-12667-3_22 N1 - Serientitel: Advanced Structured Materials – Series title: Advanced Structured Materials VL - 3 SP - 343 EP - 372 PB - Springer AN - OPUS4-23150 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Weber, Gert A1 - Thommes, H. A1 - Gaul, H. A1 - Hahn, O. A1 - Rethmeier, Michael T1 - Mechanical properties of weldbonded joints of advanced high strength steels N2 - In lightweight car body shell mass production, due to requirements on vehicle weight reduction and carbon dioxide emissions, joining of advanced high strength steels (AHSS) with different joining procedures and especially hybrid bonding techniques is becoming more and more important. One of these hybrid bonding techniques is the combination of resistance spot welding and adhesive bonding called weldbonding. One of the important advantages of weldbonded joints in comparison to resistance spot welded joints are the enhanced mechanical properties. To guarantee sufficiently high quality conditions regarding the strength of the weldbonded joints, the influences of the applied adhesive systems and of different base metal combinations are studied. This is carried out for both non-corrosive and corrosive environments and for the choice of different joining parameters settings. In particular, the mechanical behaviour of the weldbonded joints is investigated under quasi-static, impact and fatigue loads. Furthermore, the energy absorption of the weldbonded joints for both non-corrosive and corrosive environments is studied. It is shown that the weldbonded joints possess higher mechanical strengths in all load cases (quasi-static, impact and fatigue). Corrosive attack affects weldbonded joints, and the quasi-static strength is reduced. Resistance spot welded joints are not affected by the corrosive attack, but even after several weeks of corrosive attack, the quasi-static strength of weldbonded joints remains higher than that of resistance spot welded joints. KW - Weldbonded joints KW - Corrosion KW - Mechanical strength KW - Fracture behaviour KW - Fatigue KW - Crash behaviour PY - 2011 DO - https://doi.org/10.1163/016942411X580090 SN - 0169-4243 SN - 1568-5616 VL - 25 IS - 18 SP - 2369 EP - 2389 PB - VNU Science Press CY - Utrecht AN - OPUS4-24513 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Neumaier, P. A1 - Weber, H. P. A1 - Wittig, Günther T1 - Durchführung der Wirbelstromprüfung von Rohren - Hinweise für die Prüfpraxis und Angabe allgemeingültiger Regeln PY - 1985 SN - 0025-5300 VL - 27 IS - 7 SP - 187 EP - 190 PB - Carl Hanser Verlag CY - München AN - OPUS4-34223 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Maaß, K.-E. A1 - Weber, P.-M. A1 - Geipel, H. A1 - Hübner, Heinz W. A1 - Weymann, J. T1 - Transport Analyses for Determination of Man-Rem Dose Rates with Regard to Different Modes of Transport, Routing and Packaging T2 - 7th International symposium Packaging and Transportation of Radioactive Materials CY - New Orleans, La., USA DA - 15.05.1983 PY - 1983 VL - 1 SP - 343 EP - 349 AN - OPUS4-36401 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wolff, M. A1 - Wonneberger, R. A1 - Freiberg, K.E. A1 - Hertwig, Andreas A1 - Bonse, Jörn A1 - Giebeler, L. A1 - Koitzsch, A. A1 - Kunz, C. A1 - Weber, H. A1 - Hufenbach, J.K. A1 - Müller, F.A. A1 - Gräf, S. T1 - Formation of laser-induced periodic surface structures on Zr-based bulk metallic glasses with different chemical composition N2 - Bulk metallic glasses (BMG) are amorphous metal alloys known for their unique physical and mechanical properties. In the present study, the formation of femtosecond (fs) laser-induced periodic surface structures (LIPSS) on the Zr-based BMGs Zr46Cu46Al8, Zr61Cu25Al12Ti2, Zr52.5Cu17.9Al10Ni14.6Ti5 (Vit105) and Zr57Cu15.4Al10Ni12.6Nb5 (Vit106) was investigated as a function of their different chemical composition. For this purpose, LIPSS were generated on the sample surfaces in an air environment by fs-laser irradiation (λ = 1025 nm, τ = 300 fs, frep = 100 kHz). The surface topography was characterized by scanning electron microscopy and atomic force microscopy. Moreover, the impact of LIPSS formation on the structure and chemical surface composition was analyzed before and after fs-laser irradiation by X-ray diffraction and X-ray photoelectron spectroscopy as well as by transmission electron microscopy in combination with energy dispersive X-ray spectroscopy. Despite the different chemical composition of the investigated BMGs, the fs-laser irradiation resulted in almost similar properties of the generated LIPSS patterns. In the case of Zr61Cu25Al12Ti2, Vit105 and Vit106, the surface analysis revealed the preservation of the amorphous state of the materials during fs-laser irradiation. The study demonstrated the presence of a native oxide layer on all pristine BMGs. In addition, fs-laser irradiation results in the formation of laser-induced oxide layers of larger thickness consisting of an amorphous ZrAlCu-oxide. The precise laser-structuring of BMG surfaces on the nanoscale provides a versatile alternative to thermoplastic forming of BMG surfaces and is of particular interest for the engineering of functional material surfaces. KW - Bulk metallic glasses KW - Femtosecond laser KW - Laser-induced periodic surface structures (LIPSS) KW - Chemical analysis KW - Oxidation PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-581799 DO - https://doi.org/10.1016/j.surfin.2023.103305 SN - 2468-0230 VL - 42 SP - 1 EP - 11 PB - Elsevier B.V. AN - OPUS4-58179 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Altenburg, Simon A1 - Weber, H. A1 - Krankenhagen, Rainer T1 - Thickness determination of semitransparent solids using flash thermography and an analytical model N2 - As groundwork for thickness determination of polymeric surface protection systems for concrete, we present a method for measuring the thickness of isolated semitransparent solids using flash thermography both in transmission and reflection configuration. Since standard models do not capture semitransparency, an advanced analytical model by Salazar et al. is applied. Physical material parameters are deduced by fitting experimental data from samples of well-known thickness. Using those, the thickness of samples of the material can be obtained by fitting, as demonstrated for different semitransparent polymer materials. KW - Analytical model KW - Concrete KW - Semitransparency KW - Surface protection KW - Thermography KW - Thickness PY - 2017 DO - https://doi.org/10.1080/17686733.2017.1331655 SN - 1768-6733 SN - 2116-7176 VL - 15 IS - 1 SP - 95 EP - 105 PB - Taylor and Francis CY - Abingdon, UK AN - OPUS4-40468 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Altenburg, Simon A1 - Krankenhagen, Rainer A1 - Weber, H. T1 - Thickness determination of semitransparent isolated solids using the flash method and an analytical model N2 - As groundwork for thickness determination of polymeric surface protection systems for concrete, we present a method for measuring the thickness of isolated semitransparent solids using pulse thermography both in Transmission and reflection geometry. Since standard models do not capture semitransparency, an advanced analytical model by Salazar et al. is applied. Physical material parameters are deduced by fitting experimental data from samples of well-known thickness. Using those, the thickness of samples of the material can be obtained by fitting, as demonstrated for different semitransparent polymer materials. T2 - QIRT 2016 CY - Gdańsk, Poland DA - 04.07.2016 KW - Analytical model KW - Concrete KW - Flash thermography KW - Semitransparency KW - Surface protection KW - Thermography KW - Thickness PY - 2016 DO - https://doi.org/10.21611/qirt.2016.001 SN - 2371-4085 VL - 2016 SP - 71 EP - 78 AN - OPUS4-37200 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Wittig, Günther A1 - Beller, M. A1 - Leider, A. A1 - Stumm, W. A1 - Weber, H. P. T1 - Application of Reference Standards for Control of Eddy-Current Test Equipment T2 - Symposium on Eddy-Current Characterization of Materials and Structures CY - Gaithersburg, MD, USA DA - 1979-09-05 PY - 1981 N1 - Serientitel: ASTM special technical publication – Series title: ASTM special technical publication IS - 722 SP - 79 EP - 85 PB - ASTM CY - Philadelphia, PA, USA AN - OPUS4-33329 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Weber, Gert A1 - Thommes, H. A1 - Gaul, Holger A1 - Hahn, O. A1 - Rethmeier, Michael T1 - Resistance spot welding and weldbonding of advanced high strength steels KW - Resistance spot welding KW - High strength steel KW - Weldbonding KW - Widerstandspunktschweißen KW - Hochfester Stahl KW - Punktschweißkleben PY - 2010 DO - https://doi.org/10.1002/mawe.201000687 SN - 0933-5137 SN - 1521-4052 VL - 41 IS - 11 SP - 931 EP - 939 PB - Wiley-VCH Verl. CY - Weinheim AN - OPUS4-22948 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Erhard, Anton A1 - Völzke, Holger A1 - Noack, Volker A1 - Weber, Wolfgang A1 - Wolff, Dietmar A1 - Rittscher, D. A1 - Schmidt, H. T1 - Construction of long term interim storage facility for nuclear reactor compartments of submarines: German support for utilisation of nuclear submarines in Russia KW - Interim storage facility KW - Nuclear reactor compartments of submarines KW - Building of the storage facility KW - Transportation of heavy compartments PY - 2008 SN - 1746-5095 SN - 1746-5109 SN - 0957-476X VL - 19 IS - 2 SP - 117 EP - 121 PB - Ramtrans Publ. CY - Ashford AN - OPUS4-17708 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Erhard, Anton A1 - Völzke, Holger A1 - Noack, Volker A1 - Weber, Wolfgang A1 - Wolff, Dietmar A1 - Rittscher, D. A1 - Schmidt, H. T1 - Long term interim storage facility for nuclear reactor compartments of submarines - German support for utilization of nuclear submarines in Russia T2 - PATRAM 2007, 15th International Symposium on the Packaging and Transportation of Radioactive Materials CY - Miami, Florida, USA DA - 2007-10-21 PY - 2007 SP - 155 PB - Institute of Nuclear Materials Management AN - OPUS4-16157 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Rethmeier, Michael A1 - Weber, Gert A1 - Gaul, H. A1 - Brauser, Stephan T1 - Untersuchungen zur Ermüdungsfestigkeit von Widerstandspunktschweißverbindungen aus hochfesten Mehrphasenstählen unter Berücksichtigung fertigungsspezifischer Einflüsse N2 - Unter den rauen Bedingungen in der Automobilrohkarosseriefertigung lassen sich schweißbedingte Imperfektionen wie Risse beim Widerstandspunktschweißen von hochfesten Stählen nicht immer vermeiden. Für die sichere Auslegung ist die Kenntnis über den Einfluss solcher Risse von erheblicher Bedeutung. PY - 2011 SN - 978-3-942541-04-6 VL - P 802 SP - 1 EP - 86 PB - Verlag und Vertriebsgesellschaft mbH CY - Düsseldorf AN - OPUS4-25450 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Hoebbel, D. A1 - Weber, Ch. A1 - Schmidt, H. A1 - Krüger, Ralph-Peter T1 - Synthesis and Properties of Perfluoroalkyl Groups Containing Double Four-Ring Spherosilicate (Siloxysilsesquioxane) Precursors N2 - Organically modified cage-like double four-ring spherosilicates have received considerable interest in the construction of nanosized hybrid materials, as well as building units for structural well-defined polymers. This group is extended by perfluoroalkyl ligands containing spherosilicates, synthesized by addition reaction of the octahydridodimethylsiloxyoctasilsesquioxane [H(CH3)2Si]8Si8O20 and heptadecafluorodecyl methacrylate. The resultant liquid spherosilicate substituted with eight terminal perfluoroalkyl groups was characterized by 29Si and 13C NMR spectroscopies and MALDI Time-of-Flight mass spectrometry. Partial substitution of perfluoroalkyl ligands by trimethoxysilyl containing groups provides condensable precursors for the synthesis of hydrophobic and oleophobic materials via the sol-gel process. This new spherosilicate, carrying on average four perfluoroalkyl groups and four trimethoxysilyl groups shows better hydrophobic and oleophobic properties compared with commonly used perfluoroalkyltrialkoxysilanes under identical concentration of perfluoroalkyl chains. In addition a comprehensive literature survey is given on structural well characterized, organically modified cage-like double four-ring spherosilicates. KW - Spherosilicate KW - Siloxysilsesquioxane KW - Perfluoralkylalkoxysilane KW - 29Si NMR KW - Coatings KW - Hydrophobicity PY - 2002 DO - https://doi.org/10.1023/A:1015239707783 SN - 0928-0707 SN - 1573-4846 VL - 24 SP - 121 EP - 129 PB - Kluwer Academic Publ. CY - Dordrecht AN - OPUS4-1658 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Bekemeier, Simon A1 - Caldeira Rêgo, C. R. A1 - Mai, H. L. A1 - Sikia, Ujjal A1 - Waseda, O. A1 - Apel, M. A1 - Arendt, F. A1 - Aschemann, A. A1 - Bayerlein, Bernd A1 - Courant, R. A1 - Dziwis, G. A1 - Fuchs, F. A1 - Giese, U. A1 - Junghanns, K. A1 - Kamal, M. A1 - Koschmieder, L. A1 - Leineweber, S. A1 - Luger, M. A1 - Lukas, M. A1 - Maas, J. A1 - Mertens, J. A1 - Mieller, Björn A1 - Overmeyer, L. A1 - Pirch, N. A1 - Reimann, J. A1 - Schröck, S. A1 - Schulze, P. A1 - Schuster, J. A1 - Seidel, A. A1 - Shchyglo, O. A1 - Sierka, M. A1 - Silze, F. A1 - Stier, S. A1 - Tegeler, M. A1 - Unger, Jörg F. A1 - Weber, M. A1 - Hickel, Tilmann A1 - Schaarschmidt, J. T1 - Advancing Digital Transformation in Material Science: The Role of Workflows Within the MaterialDigital Initiative N2 - The MaterialDigital initiative represents a major driver toward the digitalization of material science. Next to providing a prototypical infrastructure required for building a shared data space and working on semantic interoperability of data, a core focus area of the Platform MaterialDigital (PMD) is the utilization of workflows to encapsulate data processing and simulation steps in accordance with findable, accessible, interoperable, and reusable principles. In collaboration with the funded projects of the initiative, the workflow working group strives to establish shared standards, enhancing the interoperability and reusability of scientific data processing steps. Central to this effort is the Workflow Store, a pivotal tool for disseminating workflows with the community, facilitating the exchange and replication of scientific methodologies. This article discusses the inherent challenges of adapting workflow concepts, providing the perspective on developing and using workflows in the respective domain of the various funded projects. Additionally, it introduces the Workflow Store’s role within the initiative and outlines a future roadmap for the PMD workflow group, aiming to further refine and expand the role of scientific workflows as a means to advance digital transformation and foster collaborative research within material science. KW - Digitalisation KW - FAIR principles KW - MaterialDigital KW - Scientific workflows KW - Semantic interoperability PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-624088 DO - https://doi.org/10.1002/adem.202402149 SN - 1527-2648 IS - 2402149 SP - 1 EP - 25 PB - Wiley-VCH GmbH AN - OPUS4-62408 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Villatoro, J. A1 - Zühlke, M. A1 - Riebe, D. A1 - Beitz, T. A1 - Weber, M. A1 - Riedel, Jens A1 - Löhmannsröben, H.-G. T1 - IR-MALDI ion mobility spectrometry: physical source characterization and application as HPLC detector N2 - Infraredmatrix-assisted laser dispersion and ionization(IR-MALDI) in combination with on mobility (IM) spectrometry enables the direct Analysis of biomolecules in aqueous solution. The release of ions directly from an aqueous solution is based on a phase explosion, induced by the Absorption of an IR laser pulse, which disperses the liquid as vapor, nano- and micro-droplets. The ionization process is characterized initially by a broad spatial distribution of the ions, which is a result of complex fluid dynamics and desolvation kinetics. These processes have a profound effect on the shape and width of the peaks in the IM spectra. In this work, the Transport of ions by the phase explosion-induced shockwave could be studied independently from the transport by the electric field. The shockwave-induced mean velocities of the ions at different time scales were determined through IM spectrometry and shadowgraphy. The results show a deceleration of the Ions from 118m∙s−1 at a distance of 400 μm from the liquid surface to 7.1 m∙s−1 at a distance of 10 mm, which is caused by a pileup effect. Furthermore, the desolvation kinetics were investigated and a first-order desolvation constant of 325 ± 50 s−1 was obtained. In the second part, the IR-MALDI-IM spectrometer is used as an HPLC detector for the twodimensional separation of a pesticide mixture. KW - Ion mobility spectrometry KW - IR-MALDI KW - Shadowgraphy KW - Laser PY - 2016 DO - https://doi.org/10.1007/s12127-016-0208-1 VL - 2016 IS - 4 SP - 197 EP - 207 PB - Springer-Verlag Berlin CY - Heidelberg AN - OPUS4-38467 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Debatin, F. A1 - Behrens, K. A1 - Weber, J. A1 - Baburin, I. A. A1 - Thomas, A. A1 - Schmidt, J. A1 - Senkovska, I. A1 - Kaskel, S. A1 - Kelling, A. A1 - Hedin, N. A1 - Bacsik, Z. A1 - Leoni, S. A1 - Seifert, G. A1 - Jäger, Christian A1 - Günter, C. A1 - Schilde, U. A1 - Friedrich, A. A1 - Holdt, H.-J. T1 - An isoreticular family of microporous metal-organic frameworks based on zinc and 2-substituted imidazolate-4-amide-5-imidate: syntheses, structures and properties N2 - We report on a new series of isoreticular frameworks based on zinc and 2-substituted imidazolate-4-amide-5-imidate (IFP-1–4, IFP=imidazolate framework Potsdam) that form one-dimensional, microporous hexagonal channels. Varying R in the 2-substitued linker (R=Me (IFP-1), Cl (IFP-2), Br (IFP-3), Et (IFP-4)) allowed the channel diameter (4.0–1.7 Å), the polarisability and functionality of the channel walls to be tuned. Frameworks IFP-2, IFP-3 and IFP-4 are isostructural to previously reported IFP-1. The structures of IFP-2 and IFP-3 were solved by X-ray crystallographic analyses. The structure of IFP-4 was determined by a combination of PXRD and structure modelling and was confirmed by IR spectroscopy and 1H MAS and 13C CP-MAS NMR spectroscopy. All IFPs showed high thermal stability (345–400°C); IFP-1 and IFP-4 were stable in boiling water for 7 d. A detailed porosity analysis was performed on the basis of adsorption measurements by using various gases. The potential of the materials to undergo specific interactions with CO2 was investigated by measuring the isosteric heats of adsorption. The capacity to adsorb CH4 (at 298 K), CO2 (at 298 K) and H2 (at 77 K) at high pressure were also investigated. In situ IR spectroscopy showed that CO2 is physisorbed on IFP-1–4 under dry conditions and that both CO2 and H2O are physisorbed on IFP-1 under moist conditions. KW - Adsorption KW - Metal-organic frameworks KW - Microporous materials KW - N,O ligands KW - Zinc PY - 2012 DO - https://doi.org/10.1002/chem.201200889 SN - 0947-6539 SN - 1521-3765 VL - 18 IS - 37 SP - 11630 EP - 11640 PB - Wiley-VCH Verl. CY - Weinheim AN - OPUS4-27725 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -