TY - JOUR A1 - Haist, M. A1 - Link, J. A1 - Nicia, D. A1 - Leinitz, Sarah A1 - Baumert, C. A1 - von Bronk, T. A1 - Cotardo, D. A1 - Eslami Pirharati, M. A1 - Fataei, S. A1 - Garrecht, H. A1 - Gehlen, C. A1 - Hauschildt, I. A1 - Ivanova, I. A1 - Jesinghausen, S. A1 - Klein, C. A1 - Krauss, H.-W. A1 - Lohaus, L. A1 - Lowke, D. A1 - Mazanec, O. A1 - Pawelczyk, S. A1 - Pott, U. A1 - Radebe, N. W. A1 - Riedmiller, J. J. A1 - Schmid, H.-J. A1 - Schmidt, Wolfram A1 - Secrieru, E. A1 - Stephan, D. A1 - Thiedeitz, M. A1 - Wilhelm, M. A1 - Mechtcherine, V. T1 - Interlaboratory study on rheological properties of cement pastes and reference substances: comparability of measurements performed with different rheometers and measurement geometries JF - Materials and Structures N2 - This paper presents the results of an interlaboratory study of the rheological properties of cement paste and ultrasound gel as reference substance. The goal was to quantify the comparability and reproducibility of measurements of the Bingham parameters yield stress and plastic viscosity when measured on one specific paste composition and one particular ultrasound gel in different laboratories using different rheometers and measurement geometries. The procedures for both in preparing the cement paste and carrying out the rheological measurements on cement paste and ultrasound gel were carefully defined for all of the study’s participants. Different conversion schemes for comparing the results obtained with the different measurement setups are presented here and critically discussed. The procedure proposed in this paper ensured a reasonable comparability of the results with a coefficient of variation for the yield stress of 27% and for the plastic viscosity of 24%, despite the individual measurement series’ having been performed in different labs with different rheometers and measurement geometries. KW - Rheometry KW - Rheology KW - Interlaboratory test KW - Test setup KW - Testing procedure KW - Cement paste KW - Ultrasound gel PY - 2020 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-511220 DO - https://doi.org/10.1617/s11527-020-01477-w SN - 1871-6873 VL - 53 IS - 4 SP - 92 PB - Rilem AN - OPUS4-51122 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Burgbacher, G. A1 - Kafka, P. A1 - Klein, G. A1 - Konersmann, Rainer A1 - Loock, J. A1 - Rupp, M. A1 - Scholz, A. A1 - Seel, H. A1 - Spitzer, C. T1 - Risikoabschätzung Chlorlagerung/Chlortransport unter Einbeziehung der Seveso II-Richtlinie und der Störfallverordnung (2000) N2 - Die BAM, Berlin, die Gesellschaft für Anlagen- und Reaktorsicherheit (GRS), Köln, und der TÜV Süd, München, erarbeiteten eine vergleichende Untersuchung (Risikostudie) an einer realen Anlage zur Lagerung - einschließlich des Transports - von Chlor als für die Studie geeigneten gefährlichen Stoff. T3 - BAM Forschungsberichtreihe - 269 PY - 2005 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-1820 SN - 978-3-86509-319-1 SN - 0938-5533 VL - 269 SP - 1 EP - 240 PB - Wirtschaftsverlag NW CY - Bremerhaven AN - OPUS4-182 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kelm, Jürgen A1 - Kühn, H. A1 - Klein, M. A1 - Wiesmath, A. A1 - Demco, D.E. A1 - Blümich, B. A1 - Gold, P.W. T1 - The NMR-MOUSE: quality control of elastomers JF - Journal of magnetic resonance KW - NMR-MOUSE KW - Double-quantum NMR KW - Quality control KW - Elastomers PY - 2001 SN - 1090-7807 SN - 0022-2364 VL - 19 SP - 497 EP - 499 PB - Elsevier CY - San Diego, Calif. AN - OPUS4-1034 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Ressel, P. A1 - Österle, Werner A1 - Urban, Ingrid A1 - Dörfel, Ilona A1 - Klein, A. A1 - Vogel, K. A1 - Kräutle, H. T1 - Transmission electron microscopy study of rapid thermally annealed Pd/Ge contacts on IN0.53Ga0.47As JF - Journal of applied physics PY - 1996 SN - 0021-8979 SN - 1089-7550 VL - 88 SP - 3910 EP - 3914 PB - American Institute of Physics CY - Melville, NY AN - OPUS4-2514 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Bahlmann, Stefanie A1 - Rübner, Katrin A1 - Meng, Birgit A1 - Hauer, B. A1 - Klein, H. A1 - Müller, C. A1 - Ruppert, J. A1 - Schäfer, S. A1 - Spanka, G. A1 - Wassing, W. A1 - Zunzer, U. T1 - Potenziale des Sekundärstoffeinsatzes im Betonbau - Teilprojekt B1 T2 - Schlussberichte zur ersten Phase des DAfStb/BMBF-Verbundforschungsvorhabens "Nachhaltig Bauen mit Beton" KW - Nachhaltigkeit KW - Sekundäre Gesteinskörnung KW - Rezyklierte Gesteinskörnung KW - Betonbrechsand KW - Müllverbrennungsasche PY - 2007 SN - 978-3-410-65772-9 SN - 0171-7197 N1 - Geburtsname von Bahlmann, Stefanie: Ramolla, S. - Birth name of Bahlmann, Stefanie: Ramolla, S. IS - 572 SP - 131 EP - 222 PB - Beuth AN - OPUS4-16361 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Eichler, Thorsten A1 - Isecke, Bernd A1 - Klein, H.-H. A1 - Schade, A. A1 - Pruckner, F. A1 - Michel, S. T1 - Kathodischer Korrosionsschutz von Stahl in Beton - Instandsetzung des Parkhauses "Am Gericht" in Frankfurt am Main JF - Beton- und Stahlbetonbau N2 - Die Instandsetzung von Stahlbetonbauteilen bzw.-werken, welche durch chloridinduzierte Korrosion der Bewehrung gefährdet oder bereits geschädigt sind, hat in den letzten Jahrzehnten weltweit an Bedeutung gewonnen. Der kathodische Korrosionsschutz, als elektrochemisches Instandsetzungsverfahren, bildet in diesem Fall eine zuverlässige und oftmals kostengünstige Methode zur Instandsetzung. Am Beispiel des Parkhauses Am Gericht in Frankfurt am Main werden die Durchführung solch einer Maßnahme sowie die Besonderheiten des Verfahrens beschrieben. Es werden die theoretischen Hintergründe erläutert und die praktische Umsetzung sowie zu klärende Detailfragen beschrieben. Die Daten der ersten Depolarisationsmessungen zeigen den aktuellen Zustand der Anlage sowie des Schutzobjektes. KW - Stahlbeton KW - Kathodischer Korrosionsschutz KW - Korrosion KW - Lochkorrosion KW - Instandsetzung KW - Elektrochemische Verfahren PY - 2007 SN - 0005-9900 SN - 1437-1006 VL - 102 IS - 5 SP - 310 EP - 320 PB - Ernst CY - Berlin AN - OPUS4-14769 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Klein, H.-H. A1 - Schade, A. A1 - Eichler, Thorsten A1 - Pruckner, F. T1 - Parkhaus "Am Gericht" in Frankfurt am Main - Eine Sanierung mit kathodischem Korrosionsschutz JF - Bautechnik N2 - Parkhäuser haben nach mehreren Jahrzehnten der Nutzung häufig Sanierungsbedarf in Bezug auf die tragende Stahlbetonkonstruktion, die durch eingedrungene Chloride aus eingeschlepptem Tausalz und die hierdurch hervorgerufene Korrosion der Bewehrung in der Tragfähigkeit erheblich beeinträchtigt sein kann. Das Verfahren des kathodischen Korrosionsschutzes kann hier als elektrochemisches Instandsetzungsverfahren eine wirtschaftliche und zuverlässige Alternative zu herkömmlichen Sanierungsverfahren bieten. Voraussetzungen sind intensive Voruntersuchungen, die Kenntnis der sinnvollen Anwendungsgrenzen des Systems, eine qualitativ hochwertige bauliche Umsetzung des Systems und die Nutzung der Möglichkeiten der Überwachung des Instandsetzungserfolges durch Monitoring, was am Beispiel des Parkhauses Am Gericht in Frankfurt am Main erläutert wird. Parking garage Am Gericht in Frankfurt am Main - a refurbishment with cathodic corrosion protection. After several decades in use a refurbishment is often necessary for the bearing structure of reinforced concrete parking garages due to chlorides, which have been brought into concrete by road salt, and the resulting corrosion of the reinforcement, which may lead to a serious decrease of the bearing capacity. With the system of the cathodic protection of the reinforcement exists a cost-effective and reliable technique as an alternative to common solutions. An intensive investigation of the structure, the knowledge of the reasonable limits of the system, excellent design and execution of the construction work and the monitoring of the working system are nevertheless required, which is illustrated by the example of the parking garage Am Gericht in Frankfurt am Main. KW - Stahlbeton KW - Kathodischer Korrosionsschutz KW - Korrosion KW - Lochkorrosion KW - Instandsetzung KW - Elektrochemische Verfahren PY - 2007 DO - https://doi.org/10.1002/bate.200710040 SN - 0932-8351 SN - 1437-0999 SN - 0005-6820 SN - 0341-1052 SN - 0932-6359 SN - 0932-8351 VL - 84 IS - 7 SP - 465 EP - 476 PB - Ernst & Sohn CY - Berlin AN - OPUS4-17871 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Eichler, Thorsten A1 - Isecke, Bernd A1 - Klein, H.-H. T1 - Application of thermal sprayed zinc anode for CP of a multi-storey-car-park T2 - EUROCORR 2009 - Corrosion from the nanoscale to the plant T2 - EUROCORR 2009 CY - Nice, France DA - 2009-09-06 KW - Cathodic protection KW - Thermal sprayed zinc KW - Multi-storey-car-park KW - Service life PY - 2009 IS - Paper 7862 SP - 1 EP - 14 AN - OPUS4-20237 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Enderlein, M. A1 - Kuna, M. A1 - Ricoeur, A. A1 - Baer, Wolfram A1 - Müller, Karsten A1 - Klein, K. A1 - Winkler, H. P. T1 - Numerische Analyse des Stoßbiegeversuchs zur Ermittlung der dynamischen Bruchzähigkeit T2 - 35. Tagung des DVM-Arbeitskreises Bruchvorgänge - Fortschritte der Bruch- und Schädigungsmechanik - Simulationsmethoden der Bruchmechanik (DVM-Bericht 235) KW - Bruchmechanik KW - Finite-Elemente-Methode KW - Dynamisches J-Integral KW - 3-Punkt-Biege-Großprobe PY - 2003 SN - 0943-3473 SN - 1616-4687 IS - 235 SP - 251 EP - 260 PB - DVM CY - Berlin AN - OPUS4-32709 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Ressel, P. A1 - Österle, Werner A1 - Urban, Ingrid A1 - Klein, A. A1 - Vogel, K. A1 - Kräutle, H. T1 - Transmission electron microscopy study of rapid thermally annealed Pd/Ge contacts on In0.53Ga0.47As JF - Journal of Applied Physics N2 - Phase formation in rapid thermally annealed Pd/Ge contacts on In0.53Ga0.47As has been investigated by means of cross-sectional transmission electron microscopy, convergent-beam electron diffraction, and energy-dispersive x-ray analysis. Solid-phase regrowth is observed to occur similarly as in Pd/Ge contacts on GaAs or InP. The reaction starts at low temperatures with the formation of an amorphous Pd–In–Ga–As layer, which crystallizes at elevated temperatures yielding hexagonal Pd4In0.53Ga0.47As being first described in this work. At temperatures .250 °C, this phase decomposes due to epitaxial solid-phase regrowth of In0.53Ga0.47As and formation of Pd–Ge phases. The stable composition is reached at temperatures .350 °C with excess Ge diffused through top Pd–Ge to the contact interface and growing epitaxially on the semiconductor. KW - Semiconductor KW - Thin film contact layer KW - Electron microscopy KW - Intermetallic phases PY - 1996 DO - https://doi.org/10.1063/1.363348 SN - 0021-8979 VL - 80 IS - 7 SP - 3910 EP - 3914 AN - OPUS4-38537 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kuhmann, J. F. A1 - Chiang, C. H. A1 - Harde, P. A1 - Reier, F. A1 - Österle, Werner A1 - Urban, Ingrid A1 - Klein, A. T1 - Pt thin-film metallization for FC-bonding using SnPb60/40 solder bump metallurgy JF - Materials Science and Engineering N2 - Platinum does not form any adherent oxides and can be easily wetted by tin-based solders. Platinum is also an available metallization in semiconductor laboratories. Therefore we investigated the diffusion of platinum thin-film metallizations into eutectic tin–lead solder by using a high-resolution secondary ion mass spectroscopy (SIMS) profiling from the back side. It is shown that an intermetallic phase (PtSn4) is formed during soldering, which controls the consumption of platinum during soldering and in operation. The consumption of platinum follows the well-known parabolic diffusion law. The activation energy of this process is 0.63 eV. Even at extended heating cycles of 2 min at 250°C, 190 nm from the original 300 nm of the platinum film remain undissolved. This high stability makes platinum a very attractive thin-film metallization for flip-chip (FC) bonding of new microsystems. KW - Pt thin film metallization KW - FC solder bonding KW - Diffusion KW - SIMS PY - 1998 SN - 0921-5093 VL - A242 SP - 22 EP - 25 PB - Elsevier AN - OPUS4-38540 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Thinnes, A. A1 - Westenberger, M. A1 - Piechotta, Christian A1 - Letho, L. A1 - Wirth, F. A1 - Lau, H. A1 - Klein, J. T1 - Cholinergic and metabolic effects of metformin in mouse brain JF - Brain Research Bulletin N2 - Metformin is widely used as a first-line treatment for type 2 diabetes, but central effects of metformin have received little attention. When metformin (200 mg/kg i.p.) was administered to C57Bl6 mice, metformin concentration in cerebrospinal fluid peaked at 29 μM after 30 min but dropped quickly and was low at 90 min. In mouse hypothalamus sampled by microdialysis, systemically administered metformin caused minor and transient increases of acetylcholine, glucose and lactate while choline levels decreased. When metformin (0.2−10 mM) was locally infused via retrodialysis, there was a short-lasting increase of acetylcholine in the hypothalamus. Extracellular lactate levels in hypothalamus showed a massive increase upon metformin infusion while glucose levels decreased. In isolated mitochondria of mouse brain, metformin inhibited oxygen consumption and the activity of complex I. Inhibition of mitochondrial respiration likely explains lactate formation in the brain during metformin infusion which may cause lactic acidosis during metformin intoxication. The changes of cholinergic activity in the hypothalamus may be associated with appetite suppression observed during metformin treatment. KW - Metformin KW - Blood-brain barrier KW - Lactate KW - Glucose KW - Microdialysis KW - Hypothalamus PY - 2021 DO - https://doi.org/10.1016/j.brainresbull.2021.02.018 SN - 0361-9230 VL - 170 SP - 211 EP - 217 PB - Elsevier CY - Amsterdam, Niederlande AN - OPUS4-52189 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Feltin, N. A1 - Crouzier, L. A1 - Delvallée, A. A1 - Pellegrino, F A1 - Maurino, V. A1 - Bartczak, D. A1 - Goenaga-Infante, H. A1 - Taché, O. A1 - Marguet, S. A1 - Testard, F. A1 - Artous, S. A1 - Saint-Antonin, F. A1 - Salzmann, Christoph A1 - Deumer, J. A1 - Gollwitzer, C. A1 - Koops, R. A1 - Sebaïhi, N. A1 - Fontanges, R. A1 - Neuwirth, M. A1 - Bergmann, D. A1 - Hüser, D. A1 - Klein, T. A1 - Hodoroaba, Vasile-Dan T1 - Metrological Protocols for Reaching Reliable and SI-Traceable Size Results for Multi-Modal and Complexly Shaped Reference Nanoparticles JF - Nanomaterials N2 - The study described in this paper was conducted in the framework of the European nPSize project (EMPIR program) with the main objective of proposing new reference certified nanomaterials for the market in order to improve the reliability and traceability of nanoparticle size measurements. For this purpose, bimodal populations as well as complexly shaped nanoparticles (bipyramids, cubes, and rods) were synthesized. An inter-laboratory comparison was organized for comparing the size measurements of the selected nanoparticle samples performed with electron microscopy (TEM, SEM, and TSEM), scanning probe microscopy (AFM), or small-angle X-ray scattering (SAXS). The results demonstrate good consistency of the measured size by the different techniques in cases where special care was taken for sample preparation, instrument calibration, and the clear definition of the measurand. For each characterization method, the calibration process is described and a semi-quantitative table grouping the main error sources is proposed for estimating the uncertainties associated with the measurements. Regarding microscopy-based techniques applied to complexly shaped nanoparticles, data dispersion can be observed when the size measurements are affected by the orientation of the nanoparticles on the substrate. For the most complex materials, hybrid approaches combining several complementary techniques were tested, with the outcome being that the reliability of the size results was improved. KW - Certified reference nanomaterials KW - Traceable nanoparticle size measurements; KW - Hybrid metrology KW - Scanning probe microscopy KW - Small-angle X-ray scattering KW - Electron microscopy PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-571902 DO - https://doi.org/10.3390/nano13060993 SN - 2079-4991 VL - 13 IS - 6 - Special Issue "Identification and Quantification of Nanomaterials" SP - 1 EP - 25 PB - MDPI CY - Basel, CH AN - OPUS4-57190 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -