TY - CONF A1 - Zoёga, Andreas A1 - Kurz, J. H. A1 - Oelschlägel, T. A1 - Rohrschneider, A. A1 - Müller, Christina A1 - Pavlovic, Mato A1 - Hintze, H. A1 - Kanzler, D. T1 - Investigations to introduce the probability of detection method for ultrasonic inspection of hollow axles at Deutsche Bahn N2 - Currently at Deutsche Bahn (DB) ultrasonic inspections in maintenance procedures for wheelset axles with a bore hole are, to the greatest possible extent, carried out using automated ultrasonic inspection system. Although the acceptance levels are in accordance with DIN 27201 part 7, the testing results have shown in recent years that in the case of true indications, the effective defect sizes were far below the level of acceptance. Due to this experience it can be assumed that the automated ultrasonic inspection systems are testing substantially more sensitively than required. This increased sensitivity leads to an increase in false indications, generally resulting in the unnecessary demounting of wheelsets. In Research cooperation between Federal Institute for Materials Research and Testing (BAM) and DB the effective flaw detection sensitivity of existing automated ultrasonic inspection system will be determined and the true/false indication ratio optimised. Through systematic investigations with the Probability of Detection method on the existing automated ultrasonic inspection system the results could be directly applied to the optimisation of existing ultrasonic inspections of wheelset axles with a bore hole in maintenance procedures and the level of reliability can be considerably increased. T2 - 19th World Conference on Non-Destructive Testing CY - München, Germany DA - 13.06.2016 KW - NDT KW - Reliability KW - POD KW - Railway KW - Axles KW - UT PY - 2016 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-375813 UR - http://www.ndt.net/article/wcndt2016/papers/we2g4.pdf SP - id 19515, 1 EP - 8 AN - OPUS4-37581 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Weigert, Florian A1 - Müller, A. A1 - Häusler, I. A1 - Geißler, Daniel A1 - Skroblin, D. A1 - Unger, Wolfgang A1 - Radnik, Jörg A1 - Resch-Genger, Ute T1 - Combining HR‑TEM and XPS to elucidate the core–shell structure of ultrabright CdSe/CdS semiconductor quantum dots N2 - Controlling thickness and tightness of surface passivation shells is crucial for many applications of core–shell nanoparticles (NP). Usually, to determine shell thickness, core and core/shell particle are measured individually requiring the availability of both nanoobjects. This is often not fulfilled for functional nanomaterials such as many photoluminescent semiconductor quantum dots (QD) used for bioimaging, solid state lighting, and display technologies as the core does not show the applicationrelevant functionality like a high photoluminescence (PL) quantum yield, calling for a whole nanoobject approach. By combining high-resolution transmission electron microscopy (HR-TEM) and X-ray photoelectron spectroscopy (XPS), a novel whole nanoobject approach is developed representatively for an ultrabright oleic acid-stabilized, thick shell CdSe/CdS QD with a PL quantum yield close to unity. The size of this spectroscopically assessed QD, is in the range of the information depth of usual laboratory XPS. Information on particle size and monodispersity were validated with dynamic light scattering (DLS) and small angle X-ray scattering (SAXS) and compared to data derived from optical measurements. In addition to demonstrating the potential of this novel whole nanoobject approach for determining architectures of small nanoparticles, the presented results also highlight challenges faced by different sizing and structural analysis methods and method-inherent uncertainties. KW - Photoluminescence KW - Single particle KW - Microscopy KW - Particle architecture KW - Thickness KW - SAXS KW - Shell KW - XPS KW - TEM KW - Semiconductor KW - Quantum dot KW - Photophysics KW - Quantum yield PY - 2020 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-517911 DO - https://doi.org/10.1038/s41598-020-77530-z VL - 10 IS - 1 SP - 20712 PB - Springer Nature AN - OPUS4-51791 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Weh, Lothar A1 - Müller, Ralf A1 - Moseler, D. A1 - Heide, G. A1 - Frischat, G. T1 - Topographische Untersuchungen von Glasoberflächen mit Vickers-Eindrücken T2 - 74. Glastechnische Tagung CY - Ulm, Deutschland DA - 2000-05-29 PY - 2000 SP - 237 EP - 240 PB - DGG, Dt. Glastechn. Ges. CY - Frankfurt/M. AN - OPUS4-934 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wang, Y. A1 - Ulbricht, Alexander A1 - Schmidt, F. A1 - Müller, Bernd R. A1 - Kupsch, Andreas A1 - Schwitalla, A.D. T1 - Micro-CT analysis and mechanical properties of low dimensional CFR-PEEK specimens additively manufactured by material extrusion N2 - Material extrusion of thermoplastic polymers enables the realization of complex specific designs with high performance composites. The present study aims at evaluating the mechanical properties of carbon fiberreinforced semi-crystalline thermoplastic polymer polyether ether ketone (CFR-PEEK) manufactured by material extrusion and correlating them with results obtained by micro-CT. Samples in the shape of small bars were provided by Kumovis (Munich, Germany). The determination of surface roughness and density was followed by three-point bending tests. To reveal the pore distribution as well as the fusion quality of CFR PEEK when applied with external forces, micro-CT scans were performed with an X-ray microscope before and after the mechanical test to localize the sites where the fracture is generated. The density of CFR-PEEK bars indicated that they had superior mechanical properties compared with our previous study on unfilled 3D printed PEEK (bending modulus: (5.4 ± 0.5) GPa vs. (1.05 ± 0.05) GPa to (1.48 ± 0.10) GPa; bending strength: (167 ± 11) MPa vs. (51 ± 15) to (193 ± 7) MPa). Micro-CT analyses revealed the local 3D-distribution of voids. Voids of 30 μm diameter are nearly spherical and make up the main part of the total porosity. The larger the voids, the more they deviate from a spherical shape. Significant lack-of-fusion voids are located between the deposited filaments. By growing and merging, they act as seeds for the forming fracture line in the region of the flexural specimens where the maximum local tensile stresses occurred under bending load. Our work provides a detailed analysis of printed PEEK with fiber additive and relates this with mechanical properties. KW - CFR-PEEK KW - Material extrusion (MEX) KW - FFF KW - Surface topography KW - Bending property KW - Micro-CT PY - 2023 DO - https://doi.org/10.1016/j.jmbbm.2023.106085 SN - 1751-6161 VL - 146 SP - 1 EP - 9 PB - Elsevier Ltd. AN - OPUS4-58112 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Voss, Heike A1 - Knigge, Xenia A1 - Knapic, D. A1 - Weise, Matthias A1 - Sahre, Mario A1 - Hertwig, Andreas A1 - Sacco, A. A1 - Rossi, A. M. A1 - Radnik, Jörg A1 - Müller, Kai A1 - Wasmuth, Karsten A1 - Krüger, Jörg A1 - Hassel, A. W. A1 - Hodoroaba, Vasile-Dan A1 - Bonse, Jörn T1 - Picosecond laser processing of hierarchical micro–nanostructures on titanium alloy upon pre- and postanodization: morphological, structural, and chemical effects N2 - Recent publications indicate that the order of electrochemical anodization (before or after the laser processing step) plays an important role for the response of bone-forming osteoblasts—an effect that can be utilized for improving permanent dental or removable bone implants. For exploring these different surface functionalities, multimethod morphological, structural, and chemical characterizations are performed in combination with electrochemical pre- and postanodization for two different characteristic microspikes covered by nanometric laser-induced periodic surface structures on Ti–6Al–4V upon irradiation with near-infrared ps-laser pulses (1030 nm wavelength, ≈1 ps pulse duration, 67 and 80 kHz pulse repetition frequency) at two distinct sets of laser fluence and beam scanning parameters. This work involves morphological and topographical investigations by scanning electron microscopy and white light interference microscopy, structural material examinations via X-ray diffraction, and micro-Raman spectroscopy, as well as near-surface chemical analyses by X-ray photoelectron spectroscopy and hard X-ray photoelectron spectroscopy. The results allow to qualify the mean laser ablation depth, assess the spike geometry and surface roughness parameters, and provide new detailed insights into the near-surface oxidation that may affect the different cell growth behavior for pre- or postanodized medical implants. T2 - 2023 E-MRS Spring Meeting, Symposium L "Making light matter: lasers in material sciences and photonics" CY - Strasbourg, France DA - 29.05.2023 KW - Hierarchical micro-nanostructures KW - Laser-induced periodic surface structures (LIPSS) KW - Ultrashort laser pulses KW - Ti-6Al-4V alloy KW - X-ray photoelectron spectroscopy PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-601962 DO - https://doi.org/10.1002/pssa.202300920 SN - 1862-6319 SP - 1 EP - 11 PB - Wiley-VCH GmbH CY - Weinheim AN - OPUS4-60196 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Tscharntke, D. A1 - Boehm, Rainer A1 - Müller, Christina A1 - Ronneteg, U. A1 - Rydén, H. T1 - Ultrasonic Investigations on Copper Canister Welds in Preparation for the Storage of Spent Nuclear Fuel in a Deep Repository T2 - 9th European Conference on NDT CY - Berlin, Germany DA - 2006-09-25 KW - Ultrasonic measurement and modelling KW - Copper canister weld KW - Spent nuclear fuel KW - Encapsulation KW - Deep repository PY - 2006 SN - 3-931381-86-2 SP - 1(?) EP - 7(?) PB - European Federation for Non-Destructive Testing CY - Berlin AN - OPUS4-14056 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Thieme-Hack, M. A1 - Berghaus, U. A1 - Brümmer, F. A1 - Elsner, U. A1 - Färber, C. A1 - Frank, D. A1 - Illgas, M. A1 - Kalbe, Ute A1 - Kathage, J. A1 - Leers, A. A1 - Müller, B. A1 - Röger-Göpfert, C. A1 - Russland, H.-J. A1 - Schnabel, B. A1 - Schneider, O. A1 - Schockmann, D. A1 - Schomakers, H. A1 - Schwalbe, D. A1 - Stegemann, D. A1 - van den Berg, T. A1 - Kramps, S. T1 - Fachbericht Kunststoffsportböden - Nachhaltige Kunststoffbelagsauswahl für Sportfreianlagen N2 - Kunststoff- und Kunststoffrasenflächen kommt bei intensiv genutzten Flächen als Allwetterbeläge eine große Bedeutung zu. Sie leisten einen wichtigen Beitrag zur Absicherung eines ganzjähriger Sportangebote. Gerade Kunststoffrasen ist aber in den letzten Jahren häufig in die Kritik geraten, insbesondere durch gefährliche Inhaltsstoffe und andere negative Einflüsse auf die Umwelt. Dies hat bei Bauherren zu einer Verunsicherung geführt und Fragen aufgeworfen, die erst teilweise beantwortet sind. Die Diskussionen rund um diesen Allwetterbelag haben bereits dazu geführt, dass von Seiten der Industrie viel verändert wurde und neue innovative Lösungen gefunden werden. Der Fachbericht stellt eine Handreichung für Fachleute und interessierte Laien dar, um mehr Klarheit besonders hinsichtlich der Umweltanforderungen zu erzielen. KW - Kunststoffsportbeläge KW - Kunstrasen KW - Umweltverträglichkeit KW - Schadstofftransfer KW - Mikroplastik PY - 2022 UR - https://shop.fll.de/de/fachbericht-kunststoffsportboeden-broschuere.html SP - 1 EP - 70 PB - Forschungsgesellschaft Landschaftsentwicklung Landschaftsbau (FLL) CY - Bonn AN - OPUS4-54390 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Strangfeld, Christoph A1 - Müller-Vahl, H. A1 - Nayeri, C. N. A1 - Paschereit, C. O. A1 - Greenblatt, D. T1 - Airfoil in a high amplitude oscillating stream N2 - A combined theoretical and experimental investigation was carried out with the objective of evaluating theoretical predictions relating to a two-dimensional airfoil subjected to high amplitude harmonic oscillation of the free stream at constant angle of attack. Current theoretical approaches were reviewed and extended for the purposes of quantifying the bound, unsteady vortex sheet strength along the airfoil chord. This resulted in a closed form solution that is valid for arbitrary reduced frequencies and amplitudes. In the experiments, the bound, unsteady vortex strength of a symmetric 18 % thick airfoil at low angles of attack was measured in a dedicated unsteady wind tunnel at maximum reduced frequencies of 0.1 and at velocity oscillations less than or equal to 50 %. With the boundary layer tripped near the leading edge and mid-chord, the phase and amplitude variations of the lift coefficient corresponded reasonably well with the theory. Near the maximum lift coefficient overshoot, the data exhibited an additional high-frequency oscillation. Comparisons of the measured and predicted vortex sheet indicated the existence of a recirculation bubble upstream of the trailing edge which sheds into the wake and modifies the Kutta condition. Without boundary layer tripping, a mid-chord bubble is present that strengthens during flow deceleration and its shedding produces a dramatically different effect. Instead of a lift coefficient overshoot, as per the theory, the data exhibit a significant undershoot. This undershoot is also accompanied by high-frequency oscillations that are characterized by the bubble shedding. In summary, the location of bubble and ist subsequent shedding play decisive roles in the resulting temporal aerodynamic loads. KW - vortex shedding KW - aerodynamics KW - general fluid mechanics PY - 2016 DO - https://doi.org/10.1017/jfm.2016.126 SN - 0022-1120 VL - 2016 IS - 793 SP - 79 EP - 108 AN - OPUS4-35594 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Strangfeld, Christoph A1 - Müller-Vahl, H. F. A1 - Nayeri, C. N. A1 - Paschereit, C. O. A1 - Greenblatt, D. T1 - Airfoil synchronous surging and pitching N2 - Combined surging and pitching of an airfoil at the identical frequency (i.e. synchronously), at four different phase differences, was investigated theoretically and experimentally. The most general unsteady theoretical formulation was adopted to calculate the lift coefficient, and then extended to explicitly compute the unsteady bound vortex sheet. This was used for comparison with experiments and facilitated the computation of both Joukowsky and impulsive-pressure lift contributions. Experiments were performed using a symmetric 18 % thick airfoil in an unsteady wind tunnel at an average Reynolds number of 3.0*10^5 , with a free-stream oscillation amplitude of 51 %, an angle-of-attack range of 2° +- 2° and a reduced frequency of 0.097. In general, excellent correspondence was observed between theory and experiment, representing the first direct experimental validation of the general theory. It was shown, both theoretically and experimentally, that the lift coefficient was not accurately represented by independent superposition of surging and pitching effects, due to variations in the instantaneous effective reduced frequency not accounted for during pure pitching. Deviations from theory, observed at angle-of-attack phase leads of 90° and 180°, were attributed to bursting of separation bubbles during the early stages of the acceleration phase. The largest deviations occurred when the impulsive-pressure lift contribution was small relative to the Joukowsky contribution, because the latter was most affected by bubble bursting. Bubble bursting resulted in large form-drag oscillations that occurred at identical phase angles within the oscillation cycle, irrespective of the phase difference between surging and pitching, as well as in the absence of pitching. KW - Unsteady aerodynamics KW - Dynamic stall KW - Separation bubble KW - Bubble bursting PY - 2025 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-630068 DO - https://doi.org/10.1017/jfm.2025.220 SN - 1469-7645 VL - 1009 SP - 1 EP - 33 PB - Cambridge University Press (CUP) AN - OPUS4-63006 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Stephan, H. A1 - Gloe, K. A1 - Kraus, Werner A1 - Spies, H. A1 - Johannsen, B. A1 - Wichmann, K. A1 - Reck, Günter A1 - Chand, D. K. A1 - Bharadwaj, P. K. A1 - Müller, U. A1 - Müller, W. M. A1 - Vögtle, F. ED - Moyer, B. A. T1 - Binding and extraction of pertechnetate and perrhenate by azacages T2 - Symposium Fundamentals and Applications of Anion Separations ; American Chemical Society national meeting CY - Chicago, IL, USA DA - 2001-08-25 PY - 2004 SN - 0-306-47911-7 SP - 151 EP - 168 PB - Kluwer Acad./Plenum Publ. CY - New York, NY AN - OPUS4-3667 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -