TY - CONF A1 - Kromm, Arne T1 - Kombinierter Einsatz von Dilatometrie und Diffraktion zur Analyse umwandlungsbedingter Spannungen beim Schweißen T2 - Herbstsitzung 2014 des AWT Fachausschusses Eigenspannung CY - Kassel, Germany DA - 2014-10-28 PY - 2014 AN - OPUS4-32018 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Boateng, Francis Twumasi A1 - Ewert, Uwe A1 - Kannengießer, Thomas A1 - Zscherpel, Uwe A1 - Griesche, Axel A1 - Kromm, Arne A1 - Hohendorf, Stephan A1 - Redmer, Bernard T1 - Real-time radiography for observation of crack growth during GTA (Gas Tungsten Arc) welding N2 - In situ crack detection in the mushy zone and the solid weld of a gas tungsten arc (GTA) weld using X-ray imaging during welding is a new research area for NDT inspection. Usually, NDT flaw detection is done after the complete solidification of the weld seam. In this paper, we present the use of real-time radiography with a minifocus X-ray source (YXLON X-ray tube Y.TU 225-D04) and a 75μm pixel size digital detector array (Dexela 1512) for the acquisition of 2D radiographic images by a sequence of exposures with time intervals of 80 ms for hot crack detection during single pass bead-on-plate GTA welding of 3 mm thick plates of aluminium alloy AlMgSi (6060). An analysis of the crack distribution in the weld sample is conducted from the acquired 2D radiographs and its corresponding 3D volumetric reconstruction achieved by linear coplanar digital laminography. This in situ approach opens new possibilities in the field of hot crack research by having the direct information of both the crack initiation and growth and its correlation to the welding parameters. KW - Hot cracking KW - Radiography KW - GTA welding KW - Aluminium alloys KW - Real-time operation PY - 2016 DO - https://doi.org/10.1007/s40194-016-0351-7 SN - 0043-2288 SN - 1878-6669 VL - 60 IS - 5 SP - 931 EP - 937 AN - OPUS4-37128 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Materials Research in Welding using modern Visualization Techniques T2 - Fabtech 2015 Professional Program CY - Chicago, USA DA - 2015-11-09 PY - 2015 AN - OPUS4-34874 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schröpfer, Dirk A1 - Kromm, Arne A1 - Kannengießer, Thomas T1 - Improving welding stresses by filler metal and heat control selection in component-related butt joints of high-strength steel N2 - The application of high-strength fine-grained structural steels with yield strengths greater than or equal to 690 MPa expands because of present light weight design trends. The requirements regarding the welded components safety increased due to high loading capacity. This determines a sustainable and economic application as well. However, high welding residual stresses could diminish the components safety, especially due to high restraint conditions in component or repair welds. Therefore, this work is concerned with global and local welding stresses, especially crack-critical welding stresses in the HAZ and while root welding due to the restraint conditions. Restraint intensities of real components were analysed and realised with two different weld tests, alongside two different plate dimensions and steel grades. A comparison of the test results showed several significant effects for heat control and restraint intensity regarding restraint forces and local welding stresses. Among these effects, substantial influences were found for the filler metal selection with partially altered results for root and filler beads. Local stresses of weld seam and HAZ were affected differently. KW - Residual stresses KW - MAG welding KW - Restraint KW - High-strength steels KW - Process parameters PY - 2015 DO - https://doi.org/10.1007/s40194-014-0219-7 SN - 0043-2288 SN - 1878-6669 VL - 59 IS - 3 SP - 455 EP - 464 PB - Springer CY - Oxford AN - OPUS4-32546 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Influence of weld repair by gouging on the residual stresses in high strength steels N2 - Carbon arc-air gouging is a common technology when repairing defects in welded structures. Often this technique is applied in repeated cycles even on the same location of the joint. Due to the multiple heat input by gouging and subsequent re-welding, the residual stresses are strongly influenced. This can become crucial when microstructure and mechanical properties are adversely affected by multiple weld reparations. Knowledge about the relation of gouging and residual stresses is scarce but important when high strength steels, which are sensitive to residual stresses, are processed. The present study shows the effect of repair welding on a high strength steel structural element. The weld and the heat affected zone were subjected to multiple thermal cycles by gouging and subsequent repair welding. The residual stresses were determined by X-ray diffraction at different positions along the joint. The results showed that the residual stress level has increased by the repair cycles. This is most pronounced for the heat affected zone. Adapted welding procedures may prevent detrimental residual stress distributions. T2 - International Conference on Residual Stresses 10 CY - Sydney, Australia DA - 03.07.2016 KW - Repair welding KW - Residual stress KW - Carbon arc-air gouging PY - 2016 AN - OPUS4-36886 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Residuel Stress Engineering by Low Transformation Temperature Alloys - State of the Art and Recent Developments T2 - IIW Intermediate Meeting 2013 CY - Graz, Austria DA - 2013-03-11 PY - 2013 AN - OPUS4-27984 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kromm, Arne A1 - Brauser, Stephan A1 - Kannengießer, Thomas A1 - Rethmeier, Michael T1 - High-energy synchrotron diffraction study of a transformation induced plasticity steel during tensile deformation N2 - Energy-dispersive x-ray diffraction offers the possibility for measurement and evaluation of diffraction spectra containing information of various diffraction lines of all contributing crystalline phases of a material. Combined strain imaging and diffraction analysis was conducted during the tensile test of a low alloyed transformation-induced plasticity (TRIP) steel in order to investigate the transformation induced plasticity, strain hardening, and load partitioning effects. Optical strain imaging allowed for determination of localized true strains from three-dimensional deformations measured in situ. High-energy synchrotron radiation has permitted diffraction analysis in transmission mode to gather information from the material interior. Phase-specific stress evolution during loading could be observed applying the sin2ψ technique during certain load steps. The strains of the individual lattice planes were determined in different locations under varying angles between loading and perpendicular direction. Using energy-dispersive methods it was also possible to determine the transformation behaviour during elastic and plastic regime taking into account a large number of diffraction lines. The results show that the approach practised here enables one to pull together macroscopic and phase-specific microscopic material behaviour in order to improve existing models for prediction of complex load situations. KW - EDXRD KW - Transformation-induced plasticity (TRIP) KW - Residual stress KW - Synchrotron KW - Martensite transformation PY - 2011 DO - https://doi.org/10.1177/0309324711403969 SN - 0309-3247 SN - 2041-3130 VL - 46 IS - 7 SP - 581 EP - 591 PB - Sage CY - London AN - OPUS4-24604 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Kromm, Arne A1 - Kannengießer, Thomas A1 - Altenkirch, J. A1 - Gibmeier, J. T1 - Residual stresses in multilayer welds with different martensitic transformation temperatures analyzed by high-energy synchrotron diffraction N2 - Low Transformation Temperature (LTT) alloys were developed in order to control the residual stress development by the martensitic phase transformation already during cooling of the weld metal. The positive effect of such LTT alloys on the mitigation of detrimental tensile residual stresses during welding has already been confirmed on the basis of individual laboratory tests. Within the current project it was experimentally investigated whether the phase transformation mechanisms are effective under increased restraint due to multi-pass welding of thicker specimens. The local residual stress depth distribution was analyzed non-destructively for V-type welds processed by arc welding using energy dispersive synchrotron X-ray diffraction (EDXRD). The use of high energy (20 keV to 150 keV) EDXRD allowed for the evaluation of diffraction spectra containing information of all contributing phases. As the investigated LTT alloy contains retained austenite after welding, this phase was also considered for stress analysis. The results show in particular how the constraining effect of increased thickness of the welded plates and additional deposited weld metal influences the level of the residual stresses in near weld surface areas. While the longitudinal residual stresses were reduced in general, in the transition zone from the weld to the heat-affected zone (HAZ) compressive residual stresses were found. KW - Low Transformation Temperature KW - Phase Transformation KW - Residual Stress KW - Synchrotron Diffraction PY - 2011 DO - https://doi.org/10.4028/www.scientific.net/MSF.681.37 SN - 0255-5476 VL - 681 SP - 37 EP - 42 PB - Trans Tech Publications CY - Aedermannsdorf, Switzerland AN - OPUS4-23470 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Altenkirch, J. A1 - Gibmeier, J. A1 - Kromm, Arne A1 - Kannengießer, Thomas A1 - Nitschke-Pagel, T. A1 - Hofmann, M. T1 - In situ study of structural integrity of low transformation temperature (LTT)-welds N2 - We discuss the stability of weld residual strain under static and quasi cyclic transverse tensile loading in the elastic and elastic–plastic region. The test welds were joined with low transformation temperature weld filler materials with 10 wt% Cr and varying Ni-content from 8 to 12 wt%. Using neutron diffraction the residual lattice strain in the martensitic α'- and austenitic γ-phase in the fusion zone as well as the ferritic α-phase in the heat affected zone and base metal as induced by welding, superimposed by stepwise tensile loading and after unloading was measured. The amount of retained austenite in the fusion zone increases with increasing Ni-content, but it decreases with increasing load level due to stress induced martensite formation. In the as-welded condition the transverse macroscopic residual lattice strain was found to be in low compression in the fusion zone in each weld, while the heat affected zone was in tension. Local plastic deformation of the γ-phase as a result of yielding during tensile loading in combination with the change in phase fraction resulted in increased macroscopic compression in the fusion zone. The reduced yield strength in the heat affected zone resulted in plastic deformation and a considerable shift into compression. Comparison with the cross weld distribution of the hardness and FWHM of the neutron diffraction interference lines supported the assumption of plastic deformation of the γ- and α-phase in the fusion and heat affected zone, respectively, while the α'-phase in the fusion zone was stressed within the elastic regime only. Microstructural observations as well as measurement of the local γ-phase fraction by means of laboratory X-ray diffraction in the fusion zone strengthen these observations. KW - Low transformation temperature KW - Residual stress KW - Neutron diffraction PY - 2011 DO - https://doi.org/10.1016/j.msea.2011.03.091 SN - 0921-5093 SN - 1873-4936 VL - 528 IS - 16-17 SP - 5566 EP - 5575 PB - Elsevier CY - Amsterdam AN - OPUS4-24359 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kannengießer, Thomas A1 - Kromm, Arne T1 - Design-specific influences on local weld displacement and hot cracking N2 - The action of thermomechanical effects and of external geometrical restraint conditions on hot crack formation was to be investigated. Autogenous GTA welds have been made on Aluminium 6083 plate under the conditions of free shrinkage as well as varied restraint intensity. Local deformation associated with the moving weld pool was monitored using extensometers placed at opposite ends of the joint. Linear interpolation was used to approximate displacement between the extensometers. External structural restraint and defined variation of the restraint intensity, respectively, have a major impact on the transverse displacement mechanism of the weld edges during welding and are directly linked to solidification cracking. Crack initiation and growth is believed associated with the rapid outward displacement of the material behind the moving weld pool, experienced at the weld start. Outward displacement makes it more difficult to feed solidification shrinkage, the root cause of solidification cracking. As welding proceeds, the rate of outward movement gradually decreases and crack growth eventually stops when local base material begins moving inward (i.e. helping to feed solidification shrinkage). The direction, magnitude, and rate of local deformation (inward vs outward) depends upon a complex interaction between thermal expansion and restraining forces, affected by the restraint intensity. T2 - II. International Conference on Welding and Joining of Materials (ICWJM 2007) CY - Cusco, Peru DA - 2007-04-16 KW - Hot cracking KW - Local weld displacement KW - Restraint intensity KW - Aluminium alloy PY - 2007 SP - 1 EP - 9 PB - Pontificia Universidad Católica del Perú CY - Lima AN - OPUS4-14770 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Kromm, Arne A1 - Kannengießer, Thomas A1 - Gibmeier, J. A1 - Genzel, C. A1 - Mee, V. van der T1 - Determination of Residual Stresses in Low Transformation Temperature (LTT-) Weld Metals using X-ray and High Energy Synchrotron Radiation KW - Filler material KW - Low transformation temperature KW - Synchrotron radiation KW - Phase specific residual stresses KW - Energy dispersive diffraction PY - 2007 IS - II-1658r1-07 SP - 1 EP - 17 PB - International Institute of Welding CY - Paris AN - OPUS4-15716 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Kromm, Arne A1 - Kannengießer, Thomas T1 - Stress build up in low transformation temperature filler material under defined restraint conditions T2 - JOM 15 - 15th International Conference on the Joining of Materials / 6th International Conference on Education in Welding ICEW-6 CY - Helsingor, Denmark DA - 2009-05-03 PY - 2009 SN - 87-89582-17-9 SP - 1 EP - 12(?) AN - OPUS4-19433 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - New Low Transformation Temperature Filler Material for Optimizing the Welding-Specific Residual Stresses T2 - Euromat 2007 CY - Nuremberg, Germany DA - 2007-09-10 PY - 2007 AN - OPUS4-20446 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Interaction of Phase Transformation and Residual Stresses during Welding Characterized by Synchrotron Diffraction T2 - Workshop VULCAN at the SNS: Scientific Opportunities, Industrial Applications and Challenges CY - Oak Ridge, TN, USA DA - 2010-01-21 PY - 2010 AN - OPUS4-20852 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Umwandlungsbedingte Eigenspannungen beim Schweißen mit neuartigen Schweißzusatzwerkstoffen - Ergebnisse oberflächennaher Messungen mittels Synchrotronbeugung T2 - Arbeitsgemeinschaft Wärmebehandlung und Werkstofftechnik e. V., AWT Fachausschuss 13 Eigenspannungen CY - Hamburg, Germany DA - 2010-05-03 PY - 2010 AN - OPUS4-21286 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Residual Stresses in Multilayer Welds with Different Martensitic Transformation Temperatures Analyzed by High-Energy Synchrotron Diffraction T2 - 8th European Conference on Residual Stresses CY - Riva del Garda, Italy DA - 2010-06-26 PY - 2010 AN - OPUS4-21660 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Einsatz neuartiger LTT-Zusatzwerkstoffe zur metallurgischen Abstimmung und schweißtechnologischen Verarbeitung höherfester Stähle für die Windenergie N2 - Beim Schweißen höherfester Stähle mit LTT-Zusatzwerkstoffen im Wurzelbereich der Schweißverbindung wird eine Erhöhung der Kaltrisssicherheit durch die Erzeugung von Druckeigenspannungen erreicht. Es sind mechanische Gütewerte und Eigenspannungen in Abhängigkeit der Randbedingungen, insbesondere der Wärmeführung und des Nahtaufbaus im Wurzelbereich, systematisch zu ermitteln. Durch das Ableiten von Verarbeitungsempfehlungen wird eine sichere und optimale Handhabung der LTT-Zusätze ermöglicht. Ziel ist die Entwicklung eines Maßnahmenkatalogs für die schweißtechnische Verarbeitung von LTT-Zusatzwerkstoffen zur Kaltrissvermeidung im Wurzelbereich höherfester Schweißverbindungen speziell für den Offshore-Bereich. T2 - Sitzung des Arbeitskreises „Fügetechnik für die Windenergie" des DVS e.V. CY - Duisburg, Germany DA - 14.02.2018 KW - Eigenspannungen KW - Schweißen KW - Kaltriss KW - Windenergie PY - 2018 AN - OPUS4-44247 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Combining sectioning method and x-ray diffraction for evaluation of residual stresses in welded high strength steel components N2 - Residual stresses and distortions in welded I-girders for steel construction are relevant when evaluating the stability of steel beams and column members. The application of high strength steels allows smaller wall thicknesses compared to conventional steels. Therefore, the risk of buckling has to be considered carefully. Due to the lack of knowledge concerning the residual stresses present after welding in high strength steel components conservative assumptions of their level and distribution is typically applied. In this study I-girders made of steels showing strengths of 355 MPa and 690 MPa were welded with varying heat input. Due to the dimension of the I-girders and the complex geometry the accessibility for residual stress measurement using X-ray diffraction was limited. Therefore, saw cutting accompanied by strain gauge measurement has been used to produce smaller sections appropriate to apply X-ray diffraction. The stress relaxation measured by strain gauges has been added to residual stresses determined by X-ray diffraction to obtain the original stress level and distribution before sectioning. The combination of both techniques can produce robust residual stress values. From practical point of view afford for strain gauge application can be limited to a number of measuring positions solely to record the global amount of stress relaxation. X-ray diffraction can be applied after sectioning to determine the residual stresses with sufficient spatial resolution. T2 - International Conference on Residual Stresses 10 CY - Sydney, Australia DA - 03.07.2016 KW - Residual stress KW - Sectioning method KW - X-ray diffraction PY - 2016 AN - OPUS4-36887 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kromm, Arne T1 - Large scale hydrogen assisted cracking test for thick walled SAW joints for offshore applications N2 - Offshore wind turbines continuously increase in size and weight and demand adequate offshore foundations concepts like monopiles, tripods or jackets. These components are typically submerged arc welded (SAW) high-strength thick steel plates like the S420ML. During welding, the occurrence of delayed hydrogen assisted cracking (HAC) must be anticipated. HAC is a critical combination of the local hydrogen concentration within a susceptible microstructure under certain mechanical load, i.e., the occurring (welding) residual stresses. The welding sequence of the thick-walled plates complicate the residual stress distribution due to the necessary repeated thermal cycling, i.e., welding seam / layer deposition to fill the joint. For that purpose, SAW with two-wire-technique was used to weld a specially designed and prototype-like mock-up of a real component with a thickness of 50 mm, filled more than 20 passes and a seam length of 1,000 mm. Additional welded stiffeners simulated the effect of a high restraint, to stimulate critical HAC conditions. The necessity of a minimum waiting time (MWT) before the NDT can be conducted (to exclude HAC) was critically verified by the application of ultrasonic testing of the welded joint at different time-steps of the NDT of 48 h after welding. The residual stresses were determined by a robot XRD goniometer. Tensile residual stresses up to the yield limit are found both in the weld metal and in the heat-affected zone. Numerical modelling allowed the qualitative estimation of the hydrogen diffusion in the weld. A remarkable HAC occurrence was not identified and proves both, a certain resistance of the weld joint to HAC and the (questionable) duration of the MWT. T2 - IIW Intermediate Meeting of Commission II-A CY - Garching, Germany DA - 06.03.2023 KW - Hydrogen assisted cracking KW - Submerged arc welding KW - Offshore wind turbine KW - High-strength steel KW - Component test PY - 2023 AN - OPUS4-57100 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schröpfer, Dirk A1 - Kromm, Arne A1 - Lausch, Thomas A1 - Rhode, Michael A1 - Wimpory, R. C. A1 - Kannengießer, Thomas T1 - Influence of welding stresses on relief cracking during heat treatment of a creep-resistant 13CrMoV steel: Part III - Assessment of residual stresses from small-scale to real component welds N2 - For higher operational temperatures and pressures required in petrochemical plants, the modified 13CrMoV9-10 steel was developed providing high resistance against creep and compressed hydrogen. Extreme care during the welding procedure is necessary for this steel, attributed to low toughness, high strength in as-welded state, and increased susceptibility to stress relief cracking (SRC) during post-weld heat treatment (PWHT). Previous research of SRC in creep-resistant steels discussed mainly thermal and metallurgical factors. Few previous findings addressed the influences of welding procedure on crack formation during PWHT considering real-life manufacturing conditions. These investigations focus on effects of welding heat control on stresses during welding and subsequent PWHT operations close to realistic restraint and heat dissipation conditions using a special 3D testing facility, which was presented in parts I and II of this contribution. Part III addresses investigations on residual stress evolution affecting crack formation and discusses the transferability of results from large-scale testing to laboratory-scale. Experiments with test set-ups at different scales under diverse rigidity conditions and an assessment of the residual stresses of the weld-specimens using X-ray (surface near) and neutron diffraction analysis (bulk) were performed. This study aims to provide a way of investigating the SRC behaviour considering component-specific residual stresses via small-scale testing concepts instead of expensive weld mock-ups. KW - Welding KW - Creep-resistant steel KW - Residual stresses KW - Post-weld heat treatment KW - Stress relief cracking PY - 2021 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-524403 DO - https://doi.org/10.1007/s40194-021-01101-7 SN - 1878-6669 VL - 65 SP - 1671 EP - 1685 PB - Springer CY - Berlin AN - OPUS4-52440 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Schröpfer, Dirk A1 - Scharf-Wildenhain, R. A1 - Hälsig, A. A1 - Wandtke, Karsten A1 - Kromm, Arne A1 - Kannengießer, Thomas T1 - Process-related influences and correlations in wire arc additive manufacturing of high-strength steels N2 - High-strength fine-grained structural steels have great potential for weight-optimized, efficient structures in many modern steel applications. Further advances in efficiency can be achieved through additive manufacturing and bionic design. Commercial high-strength filler materials for wire arc additive manufacturing (WAAM) are already provided by the consumable producers. Today, application would be strictly limited due to absence of quantitative findings or any guidelines for the industry regarding welding-related stresses and component safety during manufacturing and service. Hence, process- and material-related influences and design-related restraint conditions associated with formation of residual stresses and cold cracking risk are investigated. The aim is the accessibility of special WAAM self-restraining cold cracking tests and easy applicable processing recommendations, enabling an economical, fit-for-purpose and crack-safe WAAM of high-strength steels. This first study focuses on determination of interactions between WAAM process parameters, resulting layer geometry, microstructure and residual stresses, analyzed via X-ray diffraction. Defined reference specimens are automated welded using a special WAAM solid wire (yield strength >820 MPa). Geometric properties can be specifically adjusted by wire feed and welding speed, but cannot be varied arbitrarily, since a high heat input causes local overheating, inadmissible changes of microstructure and mechanical properties, defects and comparable high tensile residual stresses. T2 - 22. Werkstofftechnischen Kolloquium der TU Chemnitz CY - Online meeting DA - 24.03.2021 KW - Residual stresses KW - Additive Manufacturing KW - High-strength steel PY - 2021 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-533300 DO - https://doi.org/10.1088/1757-899X/1147/1/012002 VL - 1147 SP - 012002 PB - IOP Publishing Ltd AN - OPUS4-53330 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -