TY - RPRT A1 - Wäsche, Rolf A1 - Köse, Fatma T1 - Einfluß der Verfahrensparameter beim Gelcasting auf die Entstehung bruchauslösender Gefügefehler in hochreinen Aluminiumoxidkeramiken N2 - Es wird die Untersuchung des Entlüftungsvorgangs in Keramikschlickern beschrieben, die Teil des Gelcastingprozesses zur Herstellung hochfester Aluminiumoxidkeramiken sind. Ziel der Untersuchung war es, den Einfluss von Viskosität und Entlüftungszeit als prozessvariablen auf die Entstehung von bruchauslösenden Fehlern im Gefüge zu verdeutlichen. T3 - BAM Forschungsberichtreihe - 221 PY - 1997 U6 - http://nbn-resolving.de/urn/resolver.pl?urn:nbn:de:kobv:b43-2294 SN - 978-3-89429-036-4 SN - 0938-5533 VL - 221 SP - 1 EP - 54 PB - Wirtschaftsverlag NW CY - Bremerhaven AN - OPUS4-229 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - RPRT A1 - Wäsche, Rolf A1 - Habig, Karl-Heinz T1 - Physikalisch-chemische Grundlagen der Feststoffschmierung - Literaturübersicht - N2 - Die für einen erfolgreichen Einsatz von Festschmierstoffen zur Minderung von Reibung und Verschleiß systembestimmender Parameter wie Last, Geschwindigkeit, Temperatur, umgebende Atmosphäre, Filmbildung und -haltung sowie die Anwendungstechnologien werden dargestellt, ferner Modellvorstellungen zum Verschleißverhalten von Festschmierstoffen im Hinblick auf konkrete Anwendungsfälle diskutiert. T3 - BAM Forschungsberichtreihe - 158 KW - Festschmierstoff KW - Transferschmierung KW - Hohe Temperaturen KW - Graphit KW - Reibung KW - Verschleißmodelle KW - gebundene Filme KW - Synergieeffekte PY - 1989 U6 - http://nbn-resolving.de/urn/resolver.pl?urn:nbn:de:kobv:b43-2921 SN - 978-3-88314-889-X SN - 0938-5533 VL - 158 SP - 1 EP - 112 PB - Wirtschaftsverlag NW CY - Bremerhaven AN - OPUS4-292 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Dörfel, Ilona A1 - Wäsche, Rolf A1 - Rabe, Torsten A1 - Steinborn, Gabriele T1 - Tribological Induced Microstructural Changes in Subsurface Layers of Si3N4-Based Materials KW - Tribologie PY - 1994 SN - 1013-9826 VL - 89-91 SP - 763 EP - 767 PB - Trans Tech Publ. CY - Aedermannsdorf AN - OPUS4-577 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Klaffke, Dieter T1 - Wear of multiphase SiC based ceramic composites containing free carbon N2 - Ceramics are of increasing interest for application in many branches of technique. In order to improve the tribological performance of ceramic materials, composites on the basis of silicon carbide with different amounts of titanium carbide, boron carbide, titanium diboride and free carbon in the form of graphite were manufactured by a reaction sintering process. The friction and wear behaviour of these composites was investigated with oscillating sliding motion in unlubricated tests at room temperature on different levels of relative humidity. Additional tests were performed under water lubrication, revealing the superior behaviour of composites for special test conditions. A major influence of the free carbon on friction or wear behaviour was not observed. The tribological behaviour in air as well as under water is mainly dependant on the amount of titanium phases. KW - Siliziumkarbid KW - Verbundwerkstoffe KW - Tribooxidation KW - Silicon carbide KW - Ceramic composites KW - Humidity water KW - Lubrication PY - 2001 U6 - https://doi.org/10.1016/S0043-1648(01)00566-X SN - 0043-1648 VL - 249 SP - 220 EP - 228 PB - Elsevier CY - Amsterdam AN - OPUS4-900 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf A1 - Naito, M. A1 - Jahanmir, S. T1 - TWA 27 Characterization Methods for Ceramic Powders and Green Bodies KW - Standardisierung KW - Keramische Pulver KW - Grünkörper PY - 2000 SN - 1016-2178 IS - 23 SP - 21 EP - 27 PB - National Institute of Standards and Technology AN - OPUS4-979 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kautek, Wolfgang A1 - Rudolph, Pascale A1 - Brzezinka, Klaus-Werner A1 - Wäsche, Rolf ED - Meunier, M. T1 - Physical chemistry of the femtosecond and nanosecond laser-material-interaction with SiC and a SiC-TiC-TiB2 composite ceramic compound N2 - The interaction of nanosecond laser pulses in the ultraviolet wavelength range and femtosecond laser pulses in the near-infrared region with the direct semiconductor SiC and the composite compound SiC-TiC-TiB2 was investigated in respect to resulting physicochemical processes. Surface analytical techniques, such as XPS, µ-Raman, and EDX were used to identify the chemical changes between untreated and laser-treated areas. Single-pulse irradiation led to material modifications in the condensed state in most instances. Multi-pulse results differed depending on the pulse duration. In the nanosecond case, melting of the surface and redeposited material (debris) were observed. With femtosecond pulses instead, only negligible melting and few debris could be detected. Additionally, periodic structures (ripples) appeared, with parallel orientation and in most cases two different periodicities for a particular material. Laser ablation of all the studied compound materials exhibited preferential ablation of the lighter component elements. Crystal structure changes of the irradiated surface were observed as a consequence of laser-induced melting and resolidification. An oxidation process interfered with all this processes so that unstoichiometric oxides were formed. T2 - Symposium D - European Materials Research Society CY - Strasbourg, France DA - 2002-06-18 PY - 2002 UR - http://www.emrs-strasbourg.com/files/pdf/2002_SPRING/02_Prog_Dv2.pdf N1 - Serientitel: Applied surface science – Series title: Applied surface science VL - 208/209.2003,1 IS - 1 SP - 1 PB - Elsevier CY - Amsterdam AN - OPUS4-1732 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Rudolph, Pascale A1 - Brzezinka, Klaus-Werner A1 - Wäsche, Rolf A1 - Kautek, Wolfgang T1 - Physical chemistry of the femtosecond and nanosecond laser-material interaction with SiC and a SiC-TiC-TiB2 composite ceramic compound N2 - The interaction of nanosecond laser pulses in the ultraviolet wavelength range and femtosecond laser pulses in the near-infrared region with the semiconductor SiC and the composite compound SiC–TiC–TiB2 was investigated. Surface analytical techniques, such as XPS, depth profile (DP), and micro-Raman spectroscopy (?-RS) were used to identify the chemical changes between untreated and laser-treated areas. Single-pulse irradiation led to material modifications in the condensed state in most instances. Multi-pulse results differed depending on the pulse duration. Crystal structure changes were observed as a consequence of laser-induced melting and resolidification. In air contact all components underwent oxidation reactions according to thermodynamic expectations. Exceptions were observed under exclusion of oxygen, SiC was reduced to elemental Si. KW - Femtosecond techniques KW - Nanosecond techniques KW - Ceramics KW - Raman spectra/condensed matter KW - XPS/surface analysis PY - 2003 U6 - https://doi.org/10.1016/S0169-4332(02)01356-9 SN - 0169-4332 SN - 1873-5584 VL - 208-209 SP - 285 EP - 291 PB - North-Holland CY - Amsterdam AN - OPUS4-2791 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Wäsche, Rolf A1 - Suchantke, Christian A1 - Yarim, Rasim ED - Schulte, K. ED - Kainer, K. T1 - Sintern von Verbundwerkstoffen im System SiC-TiC-TiB2 T2 - 12. Tagung "Verbundwerkstoffe und Werkstoffverbunde" CY - Hamburg, Deutschland DA - 1999-10-05 KW - Sintern KW - Verbundwerkstoffe KW - Thermochemische Analyse PY - 1999 SN - 3-527-29967-X SP - 189 EP - 194 PB - Wiley-VCH CY - Weinheim AN - OPUS4-720 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Klaffke, Dieter A1 - Hartelt, Manfred A1 - Wäsche, Rolf ED - Bartz, Wilfried J. T1 - Non-Oxide Ceramics as Tribo Materials - Analysis of Wear Mechanisms under Oscillating Sliding Conditions in Various Atmospheres T2 - 12th International Colloquium Tribology CY - Esslingen, Germany DA - 2000-01-11 KW - Tribologie PY - 2000 SN - 3-924813-44-2 VL - 3 SP - 1755 EP - 1763 PB - Techn. Akad. Esslingen CY - Ostfildern AN - OPUS4-848 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Wäsche, Rolf T1 - Feste Schmierstoffe für hohe Temperaturen - Eine Literaturübersicht PY - 1989 SN - 0724-3472 VL - 36 IS - 3 SP - 145 EP - 151 PB - Expert Verlag CY - Renningen AN - OPUS4-1432 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -