TY - JOUR A1 - Sonntag, Nadja A1 - Jürgens, Maria A1 - Skrotzki, Birgit A1 - Olbricht, Jürgen T1 - Creep-fatigue of P92 in service-like tests with combined stress- and strain-controlled dwell times N2 - Complex service-like relaxation- and creep-fatigue tests with strain- and stress-controlled dwells and fatigue cycle durations of approx. 2200 s were performed exemplarily on a grade P92 steel at 620 ◦C in this study. The results indicate deviations in the prevailing creep mechanisms of long-term relaxation and creep dwells, affecting subsequent dwells, load shifts, and the macroscopic softening behavior quite differently. In addition, fracture surfaces and longitudinal metallographic sections reveal intergranular crack growth for complex loading with stress-controlled dwells, whereas complex strain-controlled tests enhance oxidation and transgranular crack propagation. These findings substantiate the limited transferability of relaxation-fatigue to creep-fatigue conditions. KW - Tempered martensite-ferritic steel KW - P92 KW - Dwell periods KW - Creep-fatigue interaction KW - Stress relaxation PY - 2023 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-564239 DO - https://doi.org/10.1016/j.ijfatigue.2022.107381 SN - 0142-1123 VL - 168 SP - 1 EP - 12 PB - Elsevier Ltd. AN - OPUS4-56423 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kling e Silva, Lucas A1 - Pereira, Gabriela Ribeiro A1 - Jardim, Paula Mendes A1 - Sonntag, Nadja A1 - Skrotzki, Birgit T1 - CARACTERIZAÇÃO MAGNÉTICA DOS EFEITOS DE DEFORMAÇÃO EM AÇOS ESTRUTURAIS ATRAVÉS DA TÉCNICA BITTER MODIFICADA N2 - The plastic deformation results in irreversible microstructure changes in the steel, which can be considered as the initial stage of the fracture process. However, detecting, monitoring and evaluating, damage states and small defects non-destructively in advance still proves challenging. It was reported in literature the phenomenon of the spontaneous emergence of weak magnetic fields in structural steels and pipelines, which originates due to heterogeneous mechanical and / or thermal stresses. This observation is not associated with induced phase transformations by deformation and appears to be a promising tool for the prior characterization of damage in ferromagnetic steels. To provide a better understanding of the physical bases of the process, the magnetic microstructure of such materials and the change of magnetic domains after undergoing plastic deformation were studied. For this purpose, a colloidal solution with paramagnetic particles in the nanometer scale (ferrofluid) was used, through the Bitter technique, in order to, not only observe a change in size of the magnetic domains of the material, but also changes in their morphology. Ferritic steels with different carbon contents (0.08%; 0.22% and 0.45%) were studied in this work. T2 - ABM Week 2017 CY - Sao Paulo, Brazil DA - 02.10.2017 KW - Magnetic domains KW - Steels KW - Ferrofluid KW - Plastic deformation PY - 2017 DO - https://doi.org/10.5151/1516-392X-30810 SN - 2594-5327 VL - 72 IS - 1 SP - 3003 EP - 3013 PB - Blucher Preceeding CY - Brasilien AN - OPUS4-48876 LA - por AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kling e Silva, Lucas A1 - Sonntag, Nadja A1 - Skrotzki, Birgit T1 - CARACTERIZAÇÃO MAGNÉTICA PRÉ E PÓS DEFORMAÇÃO DE AÇOS DE CONSTRUÇÃO NÃO LIGADOS ATRAVÉS DA TÉCNICA BITTER (FERROFLUIDO) T1 - Magnetic characterization before and after deformation of non-alloyed contruction steels using bitter technic N2 - The plastic deformation results in irreversible microstructure changes in the steel, which can be considered as the initial stage of the fracture process. However, detecting, monitoring and evaluating, damage states and small defects non-destructively in advance still proves challenging. Dubov reported the phenomenon of the spontaneous emergence of weak magnetic fields in ferritic structural steel and pipelines, which originate due to heterogeneous mechanical and / or thermal stresses. This observation is not associated with induced phase transformations by deformation and appears to be a promising tool for the prior characterization of damage in ferromagnetic steels. To provide a better understanding of the physical bases of the process, the magnetic microstructure of such materials and a change of magnetic domains after undergoing plastic deformation were studied. A colloidal solution with paramagnetic particles in the nanometer range (ferrofluid), which allowed, through the Bitter technique, not only to observe a change in size of the magnetic domains of the material, but also changes in their morphology. Ferritic steels with their concentrations of carbon in its composition (0.12%; 0.17% and 0.45%) were studied in this work. T2 - 15° ENEMET - ABM Week 2015 CY - Rio de Janeiro, Brazil DA - 17.08.2015 KW - Magnetic Domains KW - Bitter Technique KW - Steels KW - Ferrofluid PY - 2015 DO - https://doi.org/10.5151/1516-392X-26931 SN - 2594-4711 VL - 15 IS - 15 SP - 2942 EP - 2950 PB - Blucher Preceedings CY - Rio de Janeiro, Brazil AN - OPUS4-48875 LA - mul AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Sonntag, Nadja A1 - Jürgens, M. A1 - Uhlemann, Patrick A1 - Skrotzki, Birgit A1 - Olbricht, Jürgen T1 - Datasets for Service-Like Creep-Fatigue Experiments on Grade P92 Steel N2 - The dataset contains experimental mechanical data from complex service-like creep-fatigue experiments performed isothermally at 620 °C and a low strain amplitude of 0.2 % on tempered martensite-ferritic grade P92 steel. The data sets in text file format provide cyclic deformation (min. and max. stresses) and the total (hysteresis) data of all recorded fatigue cycles for three different creep-fatigue experiments: 1) a standard relaxation fatigue (RF) test with symmetrical dwell times of three minutes introduced at minimum and maximum strain, 2) a fully strain-controlled service-like relaxation (SLR) test combining these three-minute peak strain dwells with a 30-minute dwell in between at zero strain, and 3) a partly stress-controlled service-like creep (SLC) test combining the three-minute peak strain dwells with 30-minute dwells at constant stress. Further information on data and data acquisition, analysis, and experimental details are given in “Experimental Data from Service-Like Creep-Fatigue Experiments on Grade P92 Steel”, submitted to Data in Brief. Additional analyses of these datasets, as well as experimental findings and discussions are presented in “Creep-Fatigue of P92 in Service-Like Tests with Combined Stress- and Strain-Controlled Dwell Times”, submitted to International Journal of Fatigue. KW - Creep-fatigue KW - Stress relaxation KW - Dwell-Fatigue KW - Tempered martensite-ferritic steel PY - 2022 DO - https://doi.org/10.5281/zenodo.7198218 PB - Zenodo CY - Geneva AN - OPUS4-55995 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Sonntag, Nadja A1 - Piesker, Benjamin A1 - Ávila Calderón, Luis Alexander A1 - Mohr, Gunther A1 - Rehmer, Birgit A1 - Agudo Jácome, Leonardo A1 - Hilgenberg, Kai A1 - Evans, Alexander A1 - Skrotzki, Birgit T1 - Tensile and Low‐Cycle Fatigue Behavior of Laser Powder Bed Fused Inconel 718 at Room and High Temperature N2 - This study investigates the room‐ and high‐temperature (650 °C) tensile and low‐cycle‐fatigue behavior of Inconel 718 produced by laser powder bed fusion (PBF‐LB/M) with a four‐step heat treatment and compares the results to the conventional wrought material. The microstructure after heat treatment is characterized on different length scales. Compared to the wrought variant, the elastic and yield properties are comparable at both test temperatures while tensile strength, ductility, and strain hardening capacity are lower. The fatigue life of the PBF‐LB/M variant at room temperature is slightly lower than that of the wrought material, while at 650 °C, it is vice versa. The cyclic stress response for both material variants is characterized by cyclic softening, which is more pronounced at the higher test temperature. High strain amplitudes (≥0.7%) at room temperature and especially a high testing temperature result in the formation of multiple secondary cracks at the transitions of regions comprising predominantly elongated grain morphology and columns of stacked grains with ripple patterns in the PBF‐LB/M material. This observation and pronounced crack branching and deflection indicate that the cracks are controlled by sharp micromechanical gradients and local crystallite clusters. KW - Additive manufacturing KW - Fatigue damage KW - Heat treatment KW - Inconel 718 KW - Laser powder bed fusion KW - Low-cycle fatigue KW - Tensile strength PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-599316 DO - https://doi.org/10.1002/adem.202302122 SN - 1527-2648 SP - 1 EP - 17 PB - Wiley AN - OPUS4-59931 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Stegemann, Robert A1 - Sonntag, Nadja A1 - Kreutzbruck, Marc A1 - Skrotzki, Birgit ED - Brune, M. ED - Buffière, J.Y. ED - Morel, F. ED - Nadot, Y. T1 - Self-magnetic-leakage field detection using magneto-optical sensor technique N2 - Measurement of spontaneous magnetic stray field signals has been reported to be a promising tool for capturing macro-scale information of deformation states, defects and stress concentration zones in a material structure. This paper offers a new method for self-magnetic leakage field detection using a magneto-optical (MO) hand-held microscope. Its sensor has a dynamic field range between ±0.05 and ±2 kA/m and a lateral optical resolution of approx. 10 µm. We examined flat tensile test specimens of metastable austenitic steel AISI 304. Static tensile tests were repeatedly interrupted at various predetermined states of strain and the magnetic information was measured by the MO system. Comparative measurements using a high-precision magnetic field GMR-sensor, verify the outstanding capability of the MO microscope regarding spatial resolution of magnetic fields. T2 - FDMDII-JIP 2014 - 14th International spring meeting CY - Paris, France DA - 06.11.2014 KW - Magneto-optical sensor KW - Metal magnetic memory KW - GMR KW - NDT PY - 2014 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-326911 SN - 978-2-7598-1274-5 DO - https://doi.org/10.1051/matecconf/20141204010 N1 - Serientitel: Materials science, Engineering and Chemistry – Series title: Materials science, Engineering and Chemistry VL - 12 SP - 04010-1 EP - 04010-3 PB - EDP Sciences AN - OPUS4-32691 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Sonntag, Nadja A1 - Skrotzki, Birgit A1 - Stegemann, Robert A1 - Löwe, Peter A1 - Kreutzbruck, M. T1 - The role of surface topography on deformation-induced magnetization under inhomogeneous elastic-plastic deformation N2 - It is widely accepted that the magnetic state of a ferromagnetic material may be irreversibly altered by mechanical loading due to magnetoelastic effects. A novel standardized nondestructive testing (NDT) technique uses weak magnetic stray fields, which are assumed to arise from inhomogeneous deformation, for structural health monitoring (i.e., for detection and assessment of damage). However, the mechanical and microstructural complexity of damage has hitherto only been insufficiently considered. The aim of this study is to discuss the phenomenon of inhomogeneous “self-magnetization” of a polycrystalline ferromagnetic material under inhomogeneous deformation experimentally and with stronger material-mechanical focus. To this end, notched specimens were elastically and plastically deformed. Surface magnetic states were measured by a three-axis giant magnetoresistant (GMR) sensor and were compared with strain field (digital image correlation) and optical topography measurements. It is demonstrated that the stray fields do not solely form due to magnetoelastic effects. Instead, inhomogeneous plastic deformation causes topography, which is one of the main origins for the magnetic stray field formation. Additionally, if not considered, topography may falsify the magnetic signals due to variable lift-off values. The correlation of magnetic vector components with mechanical tensors, particularly for multiaxial stress/strain states and inhomogeneous elastic-plastic deformations remains an issue. KW - Magnetic stray fields KW - Magnetomechanical effect KW - Damage KW - Topography KW - Multiaxial deformation KW - Notch KW - Plastic deformation KW - Metal magnetic memory KW - Digital image correlation KW - Structural steel PY - 2018 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-457878 DO - https://doi.org/10.3390/ma11091518 SN - 1996-1944 VL - 11 IS - 9 SP - 1518, 1 EP - 26 PB - MDPI CY - Basel, Switzerland AN - OPUS4-45787 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - GEN A1 - Beygi Nasrabadi, Hossein A1 - Skrotzki, Birgit A1 - Hanke, Thomas A1 - Eisenbart, Miriam T1 - Mechanical testing ontology (MTO) N2 - The materials mechanical testing ontology (MTO) was developed by collecting the mechanical testing vocabulary from ISO 23718 standard, as well as the standardized testing processes described for various mechanical testing of materials like tensile testing, Brinell hardness test, Vickers hardness test, stress relaxation test, and fatigue testing. Versions info: V2 developed using BFO+CCO top-level ontologies. V3 developed using PROVO+PMDco top-level ontologies. V4 developed using BFO+IOF top-level ontologies. Repositories: GitLab: https://gitlab.com/kupferdigital/ontologies/mechanical-testing-ontology GitHub: https://github.com/HosseinBeygiNasrabadi/Mechanical-Testing-Ontology MatPortal: https://matportal.org/ontologies/MTO IndustryPortal: https://industryportal.enit.fr/ontologies/MTO KW - Ontology KW - Mechanical testing KW - FAIR data PY - 2023 UR - https://gitlab.com/kupferdigital/ontologies/mechanical-testing-ontology/ PB - GitLab CY - San Francisco, CA, USA AN - OPUS4-58271 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Beygi Nasrabadi, Hossein A1 - Hanke, Thomas A1 - Skrotzki, Birgit T1 - Semantic Representation of Low‐Cycle‐Fatigue Testing Data Using a Fatigue Test Ontology and ckan.kupferdigital Data Management System N2 - Addressing a strategy for publishing open and digital research data, this article presents the approach for streamlining and automating the process of storage and conversion of research data to those of semantically queryable data on the web. As the use case for demonstrating and evaluating the digitalization process, the primary datasets from low‐cycle‐fatigue testing of several copper alloys are prepared. The fatigue test ontology (FTO) and ckan.kupferdigital data management system are developed as two main prerequisites of the data digitalization process. FTO has been modeled according to the content of the fatigue testing standard and by reusing the basic formal ontology, industrial ontology foundry core ontology, and material science and engineering ontology. The ckan.kupferdigital data management system is also constructed in such a way that enables the users to prepare the protocols for mapping the datasets into the knowledge graph and automatically convert all the primary datasets to those machine‐readable data which are represented by the web ontology language. The retrievability of the converted digital data is also evaluated by querying the example competency questions, confirming that ckan.kupferdigital enables publishing open data that can be highly reused in the semantic web. KW - Accessible KW - CKAN KW - Interoperable KW - Digitalizations KW - Ontologies KW - Reusable data KW - Fatigue testing PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-604991 UR - https://onlinelibrary.wiley.com/doi/10.1002/adem.202400675 DO - https://doi.org/10.1002/adem.202400675 SN - 1527-2648 SP - 1 EP - 11 PB - Wiley AN - OPUS4-60499 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Beygi Nasrabadi, Hossein A1 - Bauer, Felix A1 - Uhlemann, Patrick A1 - Thärig, Steffen A1 - Rehmer, Birgit A1 - Skrotzki, Birgit T1 - Mechanical testing dataset of cast copper alloys for the purpose of digitalization N2 - This data article presents a set of primary, analyzed, and digitalized mechanical testing datasets for nine copper alloys. The mechanical testing methods including the Brinell and Vickers hardness, tensile, stress relaxation, and low-cycle fatigue (LCF) testing were performed according to the DIN/ISO standards. The obtained primary testing data (84 files) mainly contain the raw measured data along with the testing metadata of the processes, materials, and testing machines. Five secondary datasets were also provided for each testing method by collecting the main meta- and measurement data from the primary data and the outputs of data analyses. These datasets give materials scientists beneficial data for comparative material selection analyses by clarifying the wide range of mechanical properties of copper alloys, including Brinell and Vickers hardness, yield and tensile strengths, elongation, reduction of area, relaxed and residual stresses, and LCF fatigue life. Furthermore, both the primary and secondary datasets were digitalized by the approach introduced in the research article entitled “Toward a digital materials mechanical testing lab” [1]. The resulting open-linked data are the machine-processable semantic descriptions of data and their generation processes and can be easily queried by semantic searches to enable advanced data-driven materials research. KW - FAIR principles KW - Hardness KW - Low-Cycle Fatigue (LCF) KW - Tensile testing KW - Stress relaxation PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-605005 DO - https://doi.org/10.1016/j.dib.2024.110687 SN - 2352-3409 SP - 1 EP - 15 PB - Elsevier BV AN - OPUS4-60500 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -