TY - THES A1 - Nagelschmidt, Sven T1 - Ein Beitrag zur Zusammenführung von Zeit-Temperatur-Äquivalenz-Methoden: Entwicklung und Anwendung am Beispiel ausgewählter Materialverhalten für Zeit-Temperatur-Parameter und Zeit-Temperatur-Superpositionsprinzip N2 - In der Wissenschaft und Technik gibt es verschiedene Gründe, um auf Basis geeigneter Modelle in die Zukunft schauen zu wollen, beispielsweise um zu bewerten, ob ein Bauteil auch noch deutlich länger verwendet werden kann als eigentlich einmal vorgesehen. Eine Methode dieses zu tun, basiert auf dem Zeit-Temperatur-Äquivalenz-Prinzip, welches besagt, dass ein Zustand oder eine Materialeigenschaft gleichwertig bei verschiedenen Zeit-Temperatur-Kombinationen auftritt oder erreicht werden kann. Höhere Temperaturen verkürzen in der Regel die Dauer und umgekehrt. In den letzten Jahrzehnten hat sich ein umfangreiches Methodenspektrum für unterschiedliche Werkstoffe und Anwendungsgebiete entwickelt, sodass die Identifikation einer geeigneten Methode für einen konkreten Anwendungsfall oder neue Materialien eine Herausforderung darstellt. These: „Fortschrittlich wäre, existierende Methoden zusammenzuführen, methodenspezifische Vorteile zu kombinieren, um mit geringerem Aufwand ein geeignetes Prognosemodell zu entwickeln.“ Für metallische Werkstoffe und Polymere verläuft die Entwicklung von Prognosemodellen mit Zeit-Temperatur-Korrelation seit ca. 1940 parallel und unabhängig voneinander. In diesem Zusammenhang bekannte Methoden sind das Zeit-Temperatur-Superpositionsprinzip und Zeit-Temperatur-Parameter, wie der LARSON-MILLER-Parameter. Die jeweiligen methodischen Ansätze sind in der Regel anwendungs- und materialspezifisch und nur einzelnen Fachartikeln zu entnehmen. Eine zusammenführende thematische Übersicht und Untersuchung existierender Methoden wurden bislang nicht publiziert. Diese Forschungsarbeit verfolgt dahingehend einen neuartigen methodischen Ansatz und zeigt untersuchte Gemeinsamkeiten und Unterschiede als auch Analogien für das Zeit-Temperatur-Superpositionsprinzip und Zeit-Temperatur-Parameter anhand bestimmter Merkmale auf. Dafür wurden verschiedene analytische und grafische Ansätze verwendet. Ferner wird eine zusammenführende Untersuchung anhand eines rheologischen Materialmodells sowie anhand eines praktischen Anwendungsbeispiels gezeigt. Hergeleitet wurde u. a., dass das Prinzip der Zeit-Temperatur-Superposition für sogenanntes thermorheologisch einfaches und komplexes Verhalten konkreten Zeit-Temperatur-Parametern zugeordnet werden können. Und dadurch Verschiebefunktionen nicht nur in Abhängigkeit der Temperatur, sondern auch abhängig vom Zustand untersucht und definiert werden können. Ferner ermöglicht eine Skalierung der Zeit-Temperatur-Parameter auf eine Referenztemperatur physikalisch anschaulichere Auswertungen analog zum Zeit-Temperatur-Superpositionsprinzip. Untersuchungen zeigen, dass sich für einen konkreten Anwendungsfall die geeignetste Zeit-Temperatur-Äquivalenz-Methode aus einer gegenseitigen Abhängigkeit bzw. Kompatibilität einzelner Elemente, wie zugrunde gelegte Daten, Koordinatenachsenskalierung, ermittelte Zeit-Temperatur-Äquivalenz, Masterfunktionsansatz und der geforderten Interpolationsgüte herleitet. Der gewählte Forschungsansatz und die erzielten Ergebnisse bieten eine Plattform für die weitere Entwicklung von Prognosemodellen auf Basis des Zeit-Temperatur-Äquivalenz-Prinzips, insbesondere im Hinblick auf eine Zusammenführung und Kombination existierender Methoden. KW - Zeit-Temperatur-Äquivalenz KW - Zeit-Temperatur-Korrelation KW - Zeit-Temperatur-Superposition KW - Extrapolation PY - 2024 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-601530 DO - https://doi.org/10.14279/depositonce-20439 SP - 1 EP - 145 CY - TU Bibliothek online AN - OPUS4-60153 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Nagelschmidt, Sven A1 - Herbrich, Uwe A1 - Qiao, Linan T1 - Applicability of developed calculation models to predict long-term behavior of metal seals – Necessary scope of tests T2 - Waste Management Symposia - WM2019 Conference N2 - The long-term sealing behavior of metal seals, assembled in the lid system of casks for transportation and storage of radioactive materials, has been investigated. For that purpose, phenomenological models describing the time- and temperature dependent behavior have been introduced by BAM since 2016, e.g. by using the time-temperature superposition principle. Results have shown that these models describe the relaxation behavior adequately and are suitable for extrapolations. In this work, the applicability of these models is checked by analyzing the necessary scope of tests, which must be carried out to get sufficient information about the long-term behavior of metal seals based on short-term tests. T2 - Waste Management Conference CY - Phoenix, Arizona, USA DA - 03.03.2019 KW - Metal seal KW - Time-temperature superposition principle KW - Transportation and storage cask KW - Long-term interim storage PY - 2019 SP - 19311, 1 EP - 6 AN - OPUS4-48353 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Qiao, Linan A1 - Nagelschmidt, Sven A1 - Herbrich, Uwe T1 - Application of a Modified Arrhenius Equation to Describe the Time-Temperature Equivalence in Relaxation Analysis of Metal Seals JF - Journal of Civil Engineering and Architecture N2 - For the application of the time-temperature superposition principle a suitable relation is needed to describe the time-temperature shift factor α. Therefore, the Arrhenius equation is widely used due to its simple form and often leads to suitable results. Where, the Arrhenius equation presents a linear relation for the temperature-dependent shift factor in logarithmic scale ln(α) with the absolute inverse temperature (1/ϑ). However, in cases with a large temperature range which eventually include more complex reaction processes, the functional relation between ln(α) and (1/ϑ) is nonlinear in the ‘Arrhenius plot’. In those cases, the monotone change of the nonlinear range in the ‘Arrhenius plot’ can be interpreted as a transient range between two approximately linear or constant regions. An extended application of the modified Arrhenius equation from Nakamura (1989) is presented in this study for this transient range. The introduced method was applied to describe the time-temperature equivalence in the relaxation analysis of restoring seal force of metal seals, which are used in lid-systems of transport and interim storage casks for radioactive materials. But, the method is widely valid and can be used for different objectives which are characterized by thermorheologically simple behavior with nonlinear sensitivity to inverse temperature. KW - Metal seals KW - TTS principle KW - Arrhenius equation KW - Non-linear Arrhenius behavior KW - Relaxation analysis KW - Seal force PY - 2017 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-446759 UR - http://www.davidpublisher.org/index.php/Home/Article/index?id=33931.html DO - https://doi.org/10.17265/1934-7359/2017.09.004 SN - 1934-7359 VL - 11 IS - 9 SP - 853 EP - 861 PB - David Publishing Company CY - USA, NY 10989, Valley Cottage AN - OPUS4-44675 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Nagelschmidt, Sven A1 - Herbrich, Uwe A1 - Probst, Ulrich A1 - Wolff, Dietmar T1 - Evaluation of test results with regard to ageing mechanisms of metal seals in casks for dry storage of spent nuclear fuel T2 - Ageing of Materials & Structures 2014 T2 - Ageing of Materials & Structures 2014 CY - Delft, Netherlands DA - 2014-05-26 PY - 2014 AN - OPUS4-30675 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Nagelschmidt, Sven A1 - Probst, Ulrich A1 - Herbrich, Uwe A1 - Wolff, Dietmar T1 - Evaluation of test results with regard to ageing mechanisms of metal seals used in casks for spen nuclear fuel T2 - CEA Workshop 2014 - Predictive approach of sealing T2 - CEA Workshop 2014 - Predictive approach of sealing CY - Paris, Frankreich DA - 2014-10-13 PY - 2014 AN - OPUS4-31792 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Nagelschmidt, Sven A1 - Herbrich, Uwe A1 - Probst, Ulrich A1 - Wolff, Dietmar ED - Van Breugel, K. ED - Koenders, E.A.B. T1 - Evaluation of test results with regard to ageing mechanisms of metal seals in casks for dry storage of spent nuclear fuel T2 - AMS 14 - Ageing of materials & structures - Proceedings of the 1st ageing of materials & structures 2014 conference N2 - Metal seals are widely used for extreme applications, e.g. in dual-purpose casks for dry interim storage of spent nuclear fuel in Germany. Due to the fact that interim storage must be safe at least for the approved period of 40 years there is a major interest to investigate the long-term behaviour and ageing mechanisms of metal seals. Experimental analyses indicate a time and temperature dependency of seal characteristics. This dependency was researched with a time- and temperature parameterization based up on Larson-Miller. The paper describes the derivation of the material parameter C from test results and the applicability of the Larson-Miller-Relationship for those metal seals in principle. Overall a constant material parameter C was not. Nevertheless, an approach comparable to the Larson-Miller-Parameter was developed. T2 - 1st Ageing of materials & structures 2014 conference CY - Delft, The Netherlands DA - 26.05.2014 KW - Metal seal KW - Ageing KW - Larson-Miller-Parameter KW - Aluminium KW - Silver KW - Larson and Miller relationship KW - Casks KW - Spent fuel PY - 2014 SN - 978-94-6186-313-3 SP - 126 EP - 133 AN - OPUS4-30821 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Weber, Mike A1 - Zencker, Uwe A1 - Wolff, Dietmar A1 - Völzke, Holger A1 - Herbrich, Uwe A1 - Nagelschmidt, Sven T1 - Numerical analysis of cask accident scenarios in storage facilities T2 - WM2014 Conference (Proceedings) N2 - Mechanical drop test scenarios for Type B (U) packages according to the IAEA regulations have to be carried out onto the so-called “unyielding target” (usually with cask impact limiters) and onto the puncture bar respectively. They are predefined and do not require any further investigation of scenarios that really could happen on transportation routes. Cask accident scenarios in the framework of approval procedures for interim storage sites are derived from a detailed analysis of the handling procedures necessary from arrival of cask at the site to its storing position. In that case, casks are usually handled without impact limiters. Dependent on possible drop heights, drop positions and floor properties, conservative cask accident scenarios are derived for further safety proofs. According to the mechanical assessment concept of the considered approval procedure numerical calculations have to be provided by the applicant to demonstrate mechanical cask safety. Stresses and strains in the cask body as well as in the lid System have to be identified and assessed. Using the example of a 3-mvertical-drop of a transport and storage cask for spent fuel elements onto the floor construction made of damping concrete covered by screed, BAM developed a finite element model. The finite element code ABAQUS/Explicit™ was used. Results of experimental investigations are not available. Therefore parameter studies are necessary to identify the sensitivity of the finite element model to significant Parameters and to verify the finite element models according to the requirements of the Guidelines for the Numerical Safety Analyses for the Approval of Transport and Storage Casks for Radioactive Materials (BAM GGR-008). The paper describes the modeling of the material behavior and attachment of bottom side cask components. Questions concerning the modeling of a crack length limiting reinforcement in the screed layer are discussed. The influence of the mesh density of the screed layer and its strength is considered as well. Finally, the developed finite element model can be used for a numerical safety assessment. It can help to understand the complex mechanisms of the interaction between the cask components and floor construction. T2 - WM2014 Conference CY - Phoenix, Arizona, USA DA - 02.03.2014 KW - Numerical analysis KW - Interim storage KW - Cask accident scenario PY - 2014 SN - 978-0-9836186-3-8 SP - Paper 14541, 1 EP - 12 AN - OPUS4-31516 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - JOUR A1 - Völzke, Holger A1 - Wolff, Dietmar A1 - Probst, Ulrich A1 - Nagelschmidt, Sven A1 - Schulz, Sebastian T1 - Long term performance of metal seals for transport and storage casks JF - Packaging, transport, storage & security of radioactive materials (RAMTRANS) N2 - Dual purpose casks for the transportation and storage of spent nuclear fuel and other radioactive materials require very high leak tightness of lid closure systems under accident conditions as well as in the long term to prevent activity release. For that purpose metal seals of specific types with an inner helical spring and outer metal liners are widely used and have shown their excellent performance if certain quality assurance requirements for fabrication and assembling are satisfied. Well defined surface roughness, clean and dry inert conditions are therefore essential. No seal failure in a loaded cask happened under these conditions until today. Nevertheless, the considered and licensed operation period is limited and all safety assessments have been performed and approved for this period of time which is 40 years in Germany so far. However, in the meantime longer storage periods might be necessary for the future and therefore additional material data will be required. BAM is involved in the qualification and evaluation procedures of those seals from the early beginning. Because long term tests are always time consuming BAM has early decided to perform additional tests with specific test seal configurations to gain a better understanding of the long term behaviour with regard to seal pressure force, leakage rate and useable resilience which is safety relevant mainly in case of accidental mechanical loads inside a storage facility or during a subsequent transport. Main test parameters are the material of the outer seal jacket (silver or aluminium) and the temperature. This paper presents the BAM test program including an innovative test mock-up and most recent test results. Based on these data extrapolation models to extended time periods are discussed, and also future plans to continue tests and to investigate seal behaviour for additional test parameters are explained. KW - Metal Seal KW - Spent Fuel KW - Storage KW - Ageing KW - Cask KW - Leak tightness PY - 2014 DO - https://doi.org/10.1179/1746510914Y.0000000057 SN - 1746-5095 SN - 1746-5109 SN - 0957-476X VL - 25 IS - 1 SP - 8 EP - 15 PB - Ramtrans Publ. CY - Ashford AN - OPUS4-32327 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Nagelschmidt, Sven A1 - Herbrich, Uwe A1 - Probst, Ulrich A1 - Wolff, Dietmar A1 - Völzke, Holger T1 - The Results and Analyses in Terms of Aging Mechanisms of Metal Seals in Casks for Dry Storage of SNF - 14255 T2 - Waste Management Conference 2014 T2 - Waste Management Conference 2014 CY - Phoenix, AZ, USA DA - 2014-03-02 PY - 2014 AN - OPUS4-30676 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Herbrich, Uwe A1 - Nagelschmidt, Sven A1 - Weber, Wolfgang A1 - Wolff, Dietmar A1 - Völzke, Holger T1 - Die sicherheitstechnische Behälterbegutachtung für die trockene Zwischenlagerung bestrahlter Brennelemente aus Sicht der BAM T2 - Jahrestagung Kerntechnik 2013 (Proceedings) T2 - Jahrestagung Kerntechnik 2013 CY - Berlin, Germany DA - 2013-05-14 PY - 2013 SP - 1 EP - 6(?) AN - OPUS4-28585 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -