TY - CONF A1 - Madia, Mauro A1 - Werner, Tiago A1 - Sprengel, Maximilian A1 - Evans, Alexander A1 - Serrano Munoz, Itziar A1 - Zerbst, Uwe T1 - Effect of residual stresses on crack propagation in Laser Beam Melted (LBM) additively manufactured 316L N2 - Residual stresses count among the most limiting factors in the application of additively manufactured materials in safety relevant components subject to cyclic loading. The source of such stresses is inherent in the manufacturing Laser Beam Melted (LBM) process due to rapid cooling and solidification and their distribution in the specimen or component is not homogeneous, but it is usually characterized by high gradients. Moreover, the magnitude of the residual stress field depends very much on the orientation, being higher in the build direction. Many works in the literature advise to carry out a post-LBM treatment to relieve residual stresses, even though particular attention should be paid in choosing the parameters for the thermal treatment in order to avoid microstructural/phase transformations, which would affect greatly the mechanical properties of the material. Particularly in the case of the austenitic stainless steel 316L, it has been shown that annealing at high temperatures (above 900°C), besides relieving the residual stresses, may cause recrystallization, grain growth and even phase transformation. In contrast, if a too low annealing temperature is chosen in order to preserve the microstructure, the residual stresses cannot be completely relieved. This work aims to address the effect of residual stresses on short and long crack propagation for SEN(B) specimens made of 316L fabricated by LBM, in which notches have been machined by electro-discharge machining (EDM) on the mid-plane, perpendicular to the build direction. The specimens underwent different annealing treatments in inert atmosphere, in which the maximum temperature has been varied up to 900°C. The amount of residual stresses and their distribution has been measured by X-ray and neutron diffraction and the specimens have been subject to cyclic loading in a resonant testing machine. The tests show a massive influence of the residual stresses in the build direction on the resistance to fatigue crack propagation of additively manufactured 316L. Finally, a comparison with conventionally manufactured 316L is presented. T2 - Fourth Symposium on Structural Integrity of Additive Manufactured Materials and Parts CY - Gaylord National Resort And Convention Center; National Harbor, MD, USA DA - 07.10.2019 KW - Fatigue Crack Propagation KW - Additive Manufacturing KW - Residual Stresses PY - 2019 AN - OPUS4-49415 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Werner, Tiago A1 - Madia, Mauro A1 - Zerbst, Uwe A1 - Sprengel, Maximilian A1 - Ulbricht, Alexander A1 - Evans, Alexander T1 - Experimental investigation on cyclic R-curves for additively manufactured 316L steel N2 - The present study deals with the experimental characterization of short crack propagation in SLM (selective-laser-melting) manufactured stainless steel. More specifically, the determination of cyclic R-curves is discussed. This describes the dependency of the crack propagation threshold on crack growth during the short crack propagation stage. For metals, the threshold, starting at a material-intrinsic value, increases until it reaches a value independent of the crack length due to crack closure phenomena which build up at that stage. The cyclic R-curve, when used in the frame of a cyclic R curve analysis, characterizes the resistance of a material to fatigue crack growth and the ability to arrest a physically short crack. Thus, it is the link between classical fatigue and fracture mechanics. In the high-cycle-fatigue range, the short crack propagation stage dominates the overall lifetime, i.e., the number of cycles until failure. Below the fatigue limit crack arrest of hitherto propagable micro-cracks will occur. The effort for the experimental characterization of the short fatigue crack propagation behavior and the cyclic R-curve is very high compared to experiments on long crack propagation. A very exact measurement of crack extension is required, since small increments need to be depicted. Pre-cracking must leave a closure free initial crack, since closure must be build up only by the cyclic R-curve. The closure-free status is achieved by compression pre-cracking. The aim of the present study is an insight into the influence of an AM process on the short crack propagation threshold. Cyclic R-curves are experimentally determined at different load-ratios for 316L austenitic steel specimens produced by SLM and conventional manufacturing. Residual stresses are measured in the crack plane and their influence on the cyclic R-curve is discussed. T2 - ESIAM19 CY - Trondheim, Norway DA - 09.09.2019 KW - fatigue crack growth KW - Additive Manufacturing KW - 316L KW - Cyclic R-curve KW - Laser Powder Bed Fusion KW - AM KW - L-PBF PY - 2019 AN - OPUS4-49412 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Lugovtsova, Yevgeniya A1 - Mesnil, Olivier A1 - Bulling, Jannis A1 - Prager, Jens A1 - Boller, Christian T1 - Erstellung von Wellenzahlkarten zur Schadensquantifizierung auf Basis von geführten Ultraschallwellen N2 - Die Verwendung von Verbundwerkstoffen ist nicht nur mit den Vorteilen einer Gewichtsreduzierung und einer verbesserten strukturellen Leistung verbunden, sondern auch mit der Gefahr von kaum sichtbaren Impakt- oder Herstellungsschäden. Eine der vielversprechenden Methoden zur Erkennung und Charakterisierung solcher Schäden basiert auf der Ausbreitung und Analyse geführter Ultraschallwellen. Der multimodale und dispersive Charakter dieser Wellen erschweren jedoch die Analyse. Verschiedene Signalverarbeitungsmethoden wurden vorgeschlagen, um die Interpretation von Signalen und die Extraktion der notwendigen Informationen über den Schaden zu erleichtern. Eine davon ist die Erstellung einer Wellenzahlkarte. Die Wellenzahlkarte erlaubt es jeden Punkt in einer hochaufgelöste Wellenfeldaufnahme eine Wellenzahl zuzuordnen. Diese Methode ermöglicht sowohl die Quantifizierung der Größe als auch der Tiefe des Schadens. In diesem Beitrag wird diese Bildgebungsmethode auf delaminierte Aluminium-CFK-Verbundstrukturen angewendet. Solche Strukturen entsprechen den umwickelten Druckbehältern, die zur Speicherung von Gasen in der Luft- und Raumfahrt sowie in der Automobilindustrie verwendet werden. Zunächst werden die numerischen Untersuchungen zur einfachen Delamination in unterschiedlicher Tiefe vorgestellt. Als nächstes wird die Analyse von experimentellen Ergebnissen von einer geschädigten Aluminium-CFK-Platte präsentiert. Das Ergebnis der Bildgebung ist eine dreidimensionale Darstellung, die sowohl die Größe als auch die Tiefe des Impakt-Schadens liefert. T2 - Doktorandenseminar "Geführte Wellen" CY - Delbrück, Germany DA - 21.10.2019 KW - Schaden Quantifizierung KW - Faserverbundwerkstoffe KW - Geführte Wellen KW - Ultraschall KW - Impakt-Schaden PY - 2019 AN - OPUS4-49392 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mohr, Gunther A1 - Altenburg, Simon A1 - Ulbricht, Alexander A1 - Hilgenberg, Kai T1 - In-situ defect detection in Laser Powder Bed Fusion (L-PBF) by using thermography and optical tomography N2 - Laser powder bed fusion (L-PBF) is one of the most promising additive manufacturing (AM) technologies for the production of complex metallic real part components. Due to the multitude of factors influencing process conditions and part quality and due to the layer-wise characteristic of the process, monitoring of process signatures seems to be mandatory in case of the production of safety critical components. Here, the iterative process nature enables unique access for in-situ monitoring during part manufacture. In this talk, the successful test of the synchronous use of a high-frequency infrared camera and a camera for long time exposure, working in the visible spectrum (VIS) and equipped with a near infrared filter (NIR), will be introduced as a machine manufacturer independent thermal detection monitoring set-up. Thereby, the synchronous use of an infrared camera and a VIS NIR camera combines the advantages of high framerate and high spatial resolution. The manufacture of a 316L stainless steel specimen, containing purposely seeded defects and volumes with forced changes of energy inputs, was monitored during the build. The measured thermal responses are analysed and compared with a defect mapping obtained by micro X-ray computed tomography (CT). The first results regarding methods for data analysis, derived correlations between measured signals and detected defects as well as sources of possible data misinterpretation are presented in this talk. T2 - 45. MPA Seminar - Fit for Future – Advanced Manufacturing Technologies, Materials and Lifetime CY - Stuttgart, Germany DA - 01.10.2019 KW - Data fusion KW - Laser Powder Bed Fusion (L-PBF) KW - Selective Laser Melting (SLM) KW - Additive Manufacturing (AM) KW - Process monitoring KW - Infrared thermography KW - Optical tomography KW - Computed tomography (CT) KW - Lack-of-fusion PY - 2019 AN - OPUS4-49386 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Evans, Alexander A1 - Bruno, Giovanni A1 - Sprengel, Maximilian A1 - Madia, Mauro A1 - Kromm, Arne T1 - Residual stresses in Laser Beam Melting (LBM) – Critical Review and outlook of activities at BAM N2 - Additive manufacturing (AM) technologies have experienced an exceedingly rapid growth, which is coupled with the knowledge about the resulting material properties and performance. In particular, residual stress (RS) was soon recognized as an important issue in AM parts, such that parts are usually subjected to a post build-heat-treated. Significant effort has been spent on simulations of RS in AM, especially using finite element methods. As a consequence, the experimental determination of RS has thereby become increasingly important as a validation tool for simulations, as well as a method for assessing the influence of process parameters. In particular, diffraction methods, which are fundamentally non-destructive, offer enormous possibilities to gain knowledge on the residual stress state in real components, since synchrotron radiation and neutrons can penetrate even heavy metals up to several millimeters or centimeters, respectively. Indeed, significant progress has been achieved, in the understanding of the origins of the RS fields as a function of process parameters, as well as their stability under thermal and/or mechanical exposure. In this paper, a few success stories will be outlined. It will be shown how the determination of RS in metallic parts (with the focus on those produced by laser powder bed fusion) has even revealed that process parameters that were previously considered unimportant (e.g. the position and orientation on the base plate) play a major role in the onset of residual stress accumulation. However, while RS characterization is starting to be considered in the component design, deposition strategy (e.g. build plate temperature), and even in the definition of the relevant metric to assess the quality of a part, much is still to be investigates about the hypotheses underlying its experimental determination. Therefore, some aspects to be aware of, or even those which to date are unclear, will also be discussed. These include the determination of the stress-free reference and of the principal axes of stress. All of these aspects will lead towards a comprehensive understanding of the process-structure-performance relationships in AM materials and parts. T2 - Fourth ASTM Symposium on Structural Integrity of Additive Manufactured Materials and Parts CY - Gaylord National Resort And Convention Center; National Harbor, MD DA - 07.10.2019 KW - Diffraction KW - Additive Manufacturing KW - Residual stress PY - 2019 AN - OPUS4-49367 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Strangfeld, Christoph T1 - Correlation between the electric impedance and the water layer thickness in partially saturated screed samples N2 - Discussion of material moisture in liquid and vapour phase. Prediction of the pore saturation in partially saturated pores in building materials. Correlation between the electric impedance and the water layer thickness in partially saturated screed samples. T2 - 10. CMM Tagung CY - Ettlingen, Germany DA - 10.10.2019 KW - Embedded sensors KW - Corresponding relative humidity KW - Electrical impedance KW - Material moisture KW - Building materials KW - Partiallly saturated pores PY - 2019 AN - OPUS4-49261 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Strangfeld, Christoph A1 - Munsch, Sarah Mandy A1 - Kruschwitz, Sabine T1 - Water content in construction materials N2 - Discussion of material moisture and moisture transport in liquid and vapour phase. Prediction of the pore saturation in partially saturated pores in building materials. T2 - 5. Herbstschule Competence Center for Material Moisture CY - Ettlingen, Germany DA - 08.10.2019 KW - Material moisture KW - Building materials KW - Embedded sensors KW - Partially saturated pores PY - 2019 N1 - Geburtsname von Munsch, Sarah Mandy: Nagel, S. M. - Birth name of Munsch, Sarah Mandy: Nagel, S. M. AN - OPUS4-49260 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Müller, I. A1 - Moll, J. A1 - Kexel, C. A1 - Schubert, L. A1 - Tschöke, K. A1 - Prager, Jens A1 - Lugovtsova, Yevgeniya A1 - Bach, M. A1 - Vogt, T. T1 - SHM using Guided Waves – Recent Activities and Advances in Germany N2 - Issues that prevent Structural Health Monitoring (SHM) based on Guided Waves (GW) from being a part of today’s monitoring solutions in industry are not all obvious to the scientific community. To uncover and overcome these issues, scientists working on SHM and GW problems joined in an expert committee under the patronage of the German Society for Non-Destructive Testing. An initiated online survey among more than 700 experts and users reveals the hurdles hindering the practical application of GWbased SHM. Firstly, methods for proof of reliability of SHM approaches are missing. Secondly, detailed understanding of phenomenological described wave-damage interactions is needed. Additionally, there are significant unsolved implementation issues and unsolved problems of signal processing including handling of environmental influences. To enable substantial proof of reliability without unaffordable experimental effort also efficient simulation tools including realistic damage interaction are needed, enabling the joint use of experimental and simulated data to predict the capabilities of the Monitoring system. Considering these issues, the committee focusses on simulation, signal processing, as well as probability of detection and standardization. In the presented work, recent activities of the expert committee starting with survey results are summarized. An open access data basis of life-like measurements is presented to allow testing and comparison of signal processing and simulation algorithms. Finally, a strategy for efficient proof of reliability increasing the acceptance of SHM in industry and for successful Integration of SHM into real-world engineering structures is proposed. T2 - The 12th International Workshop on Structural Health Monitoring (IWSHM) CY - Stanford, California, USA DA - 10.09.2019 KW - Structural Health Monitoring KW - Ultrasonic Guided Waves KW - Non-Destructive Testing KW - Survey KW - Probability of Detection KW - Reliability PY - 2019 AN - OPUS4-49231 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bernard, D. A1 - Léonard, Fabien A1 - Plougonven, E. A1 - Bruno, Giovanni T1 - On the use of autocorrelation functions, permeability tensors, and computed tomography to characterize the anisotropy of Diesel particulate filter materials N2 - 3D images such as those produces by X-ray tomography can provide a wealth of information on the internal structure of materials, but quantification of specific geometrical or topological characteristics linked to some bulk physical property is far from being straightforward. This study focuses on methods to quantify the differences in physical properties as a function of direction, i.e. their anisotropy, and how it can be linked to measures of anisotropy of the internal structure of the material. The auto-correlation function gives a similarity measure in the volume as a function of distance and direction. This is a cross-correlation of the image with itself fast to compute and relatively insensitive to noise. It is why we focus on this method to compare with the physical property of our DPF material. Diesel Particulate Filter (DPF) materials are porous ceramics that; a) can be used at very high temperatures; b) have very good thermal shock resistance; c) are inert; d) can be manufactured with tailored porosity. Their usual way of production consists of the extrusion of a slurry into the desired filter shape, with successive ceramming at high temperature. This process causes anisotropy at both microscopic and macroscopic levels. T2 - ICTMS 2019 CY - Cairns, Australia DA - 22.07.2019 KW - Structure-property relationship KW - Anisotropy estimate KW - Porous ceramics KW - Autocorrelation PY - 2019 AN - OPUS4-49226 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Krankenhagen, Rainer T1 - Entwicklung einer reproduzierbaren und quantifizierbaren Heißluftquelle für thermografische Untersuchungen N2 - Der Beitrag beschreibt den Aufbau und die Entwicklung einer Heißluftquelle als Wärmequelle für die aktive Thermografie. Als Ausgangspunkt wird zunächst die Quellenlage betrachtet. In der Literatur über Thermografie spielt Heißluft als Wärmequelle nur in weniger als 0,1% eine Rolle, die Ursache dafür ist nicht bekannt. Es wird vermutet, dass dieser Erwärmungsmethode unterstellt wird, sie hätte Nachteile bezüglich Homogenität der Erwärmung sowie Leistungseintrag. In einer der raren Publikationen über einen Verfahrensvergleich schnitt die Heißluft-Thermografie jedoch nicht schlechter als die Vergleichsverfahren mit optischer Anregung ab, bei gleichzeitig deutlichem Zeitgewinn und geringerem technischen Aufwand. Danach wird der fertige Versuchsaufbau mit seinen wesentlichen Komponenten dargestellt. Der Einfluss der Geometrie der Luftaustrittsdüse auf die erreichbare Wärmeverteilung an einem flachen Blech wurde an mehreren Düsen untersucht. Hierbei erwies sich eine langgestreckte Umlenkdüse mit einer Strahlumlenkung von etwa 20° als optimal zur Erzeugung einer möglichst homogenen Erwärmung. Ein weiterer zu optimierender Parameter war die erreichbare Schaltdynamik des Heißgasstromes. Beim schnellen Schalten großer Volumenströme treten Druckstöße mit entsprechenden Temperaturänderungen auf. Hinzu kommt, dass der verwendete MFC (mass flow controller) bei großen Volumenströmen zum Einschwingen bei Schaltprozessen neigt. Daher enthält der Aufbau einen offenen Bypass zur Stabilisierung des Volumenstroms. Mit dem so realisierten Messplatz wurde die Reproduzierbarkeit der erzielten Erwärmung durch mehrfache Wiederholungsmessungen über einen längeren Zeitraum untersucht. Hierzu wurde ein auch zu Validierungszwecken genutzter PVC-Block mit 13 mm Dicke jeweils für 60 s erwärmt und die Oberflächentemperatur des PVC-Blocks mit einer IR-Kamera aufgezeichnet. Bei jeweiligem Neuaufbau ohne Justierhilfe ergab sich eine Reproduzierbarkeit von etwa 22% bei 5 Versuchen. Unter Nutzung einer Justierhilfe (Schablone für Abstand in der Kamerasoftware) ließ sich die Reproduzierbarkeit auf 5% bei 7 Versuchen reduzieren. Ein weiterer zu klärender Punkt war der erzielbare Wärmeeintrag im Vergleich zu einer Anregung mit Blitzlampen. Hierzu wurde eine Messung mit 60 s Heißluftheizung direkt mit einer Evaluierungsmessung mit Blitzlampen am gleichen PVC-Probekörper mit 4 FBB an der Rückseite verglichen. Die Inhomogenität der Erwärmung wurde durch eine Phasenauswertung unterdrückt. Die Phasenauswertung gestattete den Nachweis aller 4 FBB, wobei das Signal zu Rausch-Verhältnis bei der Heißlufterwärmung deutlich besser war. Der direkte Vergleich der Temperaturkurven zeigt, dass bei 60 s Heizlufterwärmung ca. 4,5 mal mehr Energie als bei der Blitzanregung vom Probekörper absorbiert wurde. Hieraus lässt sich die eingekoppelte Heizleistung mit 100 mW/cm² abschätzen. Das entspricht in etwa dem Niveau, wie es auch mit bewegten Halogenstrahlern, bewegten IR-Strahlern oder der Sonne erreicht wird. Diese Ergebnisse belegen, dass eventuell vorhandene Vorbehalte gegenüber einer Heißluft als Wärmequelle für die aktive Thermografie zumindest für thermisch langsame Materialien wie Kunststoffe oder mineralische Baustoffe unbegründet sind. Die Einsatzgrenzen bei der Untersuchung thermisch schnellerer Materialien wie Metalle steht noch aus, hier ist mit Abstrichen zu rechnen. Auf der anderen Seite lässt eine mögliche Düsenoptimierung noch deutliche Verbesserungen erwarten. T2 - Thermografiekolloquium der DGZfP 2019 CY - Halle, Germany DA - 19.09.2019 KW - Thermografie KW - Zerstörungsfreie Prüfung KW - Heißluftquelle PY - 2019 AN - OPUS4-49217 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bernegger, Raphael A1 - Altenburg, Simon A1 - Maierhofer, Christiane T1 - Pulsed thermography on semitransparent materials - what has to be considered? N2 - Pulsed thermography is a well-known non-destructive testing technique and has proven to be a valuable tool for examination of material defects, to determine thermal material parameters, and the thickness of test specimens through calibration or mathematical models. However, the application to semitransparent materials is quite new and demanding, especially for semitransparent materials like epoxy, polyamide 12, or glass fiber reinforced polymers with epoxy or polyamide matrix. In order to describe the temporal temperature evolution in such materials, which are recorded with an infrared camera during pulse thermography experiments, much more influences have to be considered, compared to opaque materials: - The wavelength of the excitation source and the spectral range of the infrared camera - The angles between the specimen, the excitation source and the infrared camera - The area behind the specimen - The roughness of the material surface - The scattering mechanism within the material Here, we will consider all these influences and describe how they can be treated mathematically in analytical or numerical models (using COMSOL Multiphysics software). These models describe the temperature development during the pulse thermography experiment in reflection and transmission configuration. By fitting the results of the mathematical models to experimental data it is possible to determine the thickness or the optical and thermal properties of the specimen. T2 - 20-th International Conference on Photoacoustic and Photothermal Phenomena CY - Moscow, Russia DA - 07.07.2019 KW - Numerical simulation KW - Pulsed thermography KW - Semitransparent KW - Analytical model KW - Delamination KW - GFRP PY - 2019 AN - OPUS4-49215 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Vössing, Konrad A1 - Gaal, Mate A1 - Niederleithinger, Ernst T1 - Contactless testing of wood-based materials with novel air-coupled ultrasonic transducers N2 - The detection of delamination, rot and cracks causing a decrease of strength in wooden construction elements is a key task for nondestructive testing (NDT). Air-coupled ultrasound (ACU) is used to detect flaws without having to provide contact to the surface or otherwise affect the object. Novel ferroelectric transducers with a high signal-to-noise ratio enable an accurate flaw detection. Transducers made of cellular polypropylene (PP) are suitable for characterizing wood-based materials (WBM) because their extremely low Young’s modulus and low density mean a favorable acoustic impedance for the transmission of ultrasonic waves between the transducer and air. The transducers can be applied during the production of WBM and during its service life. The device enables a fast in-situ recognition of defects with frequencies between 90 kHz and 250 kHz. Measurements can be performed in through transmission for a high resolution or in pulse-echo technique in case of one-sided access at the expense of reduced signal strength. Ultrasonic quality assurance for wood is an important attempt to increase the acceptance of wooden structures and towards sustainability in civil engineering in general. T2 - 21. International Nondestructive Testing and evaluation of Wood Symposium CY - Freiburg, Germany DA - 24.09.2019 KW - Air-coupled ultrasound KW - Defect detection KW - Nondestructive Testing KW - Timber PY - 2019 AN - OPUS4-49170 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Müller, Jan P. A1 - Krankenhagen, Rainer T1 - Ein Blick unter die Oberfläche von Windkraftanlagen durch Thermografie N2 - Rotorblätter von Windkraftanlagen sind hohen Belastungen ausgesetzt. Nach Jahren der Nutzung können Klebeverbindungen unter der Oberfläche versagen. Thermografie soll die Zustandsüberwachung während der gesamten Lebensdauer verbessern. N2 - Rotor blades of wind power generators are subject to high strains. After years of use, adhesive bonds under the surface may fail. Thermography is intended to improve condition monitoring during the entire service life. T2 - Hannover Messe 2019 CY - Hanover, Germany DA - 1.4.2019 KW - Wiederkehrende Prüfung KW - Thermografie KW - Klebeverbindungen KW - Rotorblatt KW - GFK PY - 2019 AN - OPUS4-49160 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Stelzner, Ludwig A1 - Weise, Frank A1 - Oesch, Tyler A1 - Dlugosch, R. A1 - Powierza, Bartosz T1 - Transport and reconfiguration of moisture in HPC due to unilateral heating N2 - Explosive spalling is caused by, among others, the thermohydraulic spalling mechanism. During this process, vaporization, dehydration, moisture-transport and condensation processes interact. As a result, a drying and dehydration zone as well as a saturated zone, known as a moisture clog, are observed inside the unilaterally-heated concrete. The presented research is focused on the experimental investigation of the underlying thermohydraulic processes. To investigate these, a test methodology based on X-ray computed tomography (CT) and nuclear magnetic resonance (NMR) was developed. Thereby, the X-ray CT scans are carried out simultaneously during the application of a defined unilateral-heating regime on a specially-constructed specimen. This miniaturized specimen, equipped with a double-layer casing, reproduces the condition within a planar, unilaterally-heated building component. A preliminary test methodology and the first experimental results were presented at the 5th International Workshop on Concrete Spalling in Borås, Sweden (2017). The contribution for the upcoming workshop presents an improved version of this test methodology and new results for a high-performance concrete (HPC) mixture exposed to temperatures up to 500 °C. Regarding the CT measurements, a higher time-resolution of 15 min was achieved and a quantification of the moisture changes was implemented. Due to an increase in signal quality of the NMR measurements, a pore-size specific moisture distribution can now be resolved. This allows to conclude about the moisture reconfiguration between small gel pores and larger interhydrate pores. Additionally, the NMR measurement are no longer limited to first 2.5 cm below the heated surface but a one-dimensional moisture distribution can now be estimated over the whole 10 cm long specimen. The presented results demonstrate that the combination of X-ray CT and NMR measurements enables to image and quantify the thermally-induced moisture transport and reconfiguration from small gel pores up to macro pores. This provides important insights into the thermohydraulic damage mechanism and leads to a better understanding of spalling avoidance strategies, like the addition of polypropylene fibres. T2 - 6th International Workshop on Concrete Spalling due to fire exposure CY - Sheffield, UK DA - 19.09.2019 KW - Moisture clog KW - X-ray CT KW - NMR KW - Moisture transport KW - HPC PY - 2019 AN - OPUS4-49159 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Müller, Jan P. A1 - Dell'Avvocato, G. A1 - Krankenhagen, Rainer T1 - Applying a two-layer quadrupole model for quantitative thermography at overload-induced delaminations in GFRP N2 - The applicability of 1D-quadrupole-model on the depth estimation of overload-induced delaminations is tested in this contribution. While classical 1D-methods like Pulsed Phase Transformation and Thermographic Signal Reconstruction determine the depth of a defect by one parameter, a two-layer quadrupole model provides two parameters: depth and thermal resistance. In addition, the convectional losses at the surfaces may be considered. The defect investigated is a large-scale delamination in glass fibre reinforced polymer generated by tension overload. T2 - Advanced Infrared Technology & Applications (AITA) CY - Florenz, Italy DA - 16.9.2019 KW - Aktive Thermographie KW - Nicht-lineare Regression KW - 1D-Simulation KW - GFK PY - 2019 AN - OPUS4-49133 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Scheuschner, Nils A1 - Altenburg, Simon A1 - Straße, Anne A1 - Gumenyuk, Andrey A1 - Maierhofer, Christiane T1 - In-situ Thermografie in der additiven Fertigung mittels Laser-Pulver-Auftragsschweißen N2 - Im Rahmen des Themenfeld Projektes „Process Monitoring of AM“ (ProMoAM) evaluiert die BAM gegenwärtig die Anwendbarkeit verschiedenster ZfP-Verfahren, darunter die Thermografie, zur Prozessüberwachung in der additiven Fertigung von Metallen in Hinblick auf die Qualitätssicherung. In diesem Beitrag werden SWIR-Thermografiemessungen während des Bauprozesses mittels Laser Pulver Auftragsschweißen (LPA) vorgestellt. Eine Herausforderung im Rahmen dieser Messungen liegt in der Positionierung der Kamera, welche entweder fixiert am Schweißarm, also mitbewegt, oder fixiert in der Baukammer, also stationär, erfolgen kann, wobei beide Varianten mit individuellen Vor- und Nachteilen verbunden sind. Eine stationäre Befestigung der Kamera ermöglicht zwar eine einfachere Zuordnung der Messdaten zu der jeweiligen Position im Bauteil, führt jedoch bei komplexeren Geometrien zwangsläufig zu Problemen durch Abschattungen und zu defokussierten Bereichen. Zur Auswertung von Thermogrammen, welche durch eine mit dem Schweißarm mitbewegte Kamera aufgenommen wurden, sind hingegen für jedes Bild akkurate Positionsdaten der Kamera nötig um die Messdaten einer Position im Bauteil zuzuordnen. Da die Positionsdaten des Schweißarmes im allgemeinen Fall durch die Anlagensoftware nicht zur Verfügung gestellt werden, muss diese Information durch zusätzliche Messungen aufgezeichnet werden. Hierzu verwenden wir einen an der Kamera befestigten Beschleunigungssensor. Dieser ermöglicht einen zeitlichen Abgleich mit dem vorprogrammierten Verfahrweg des Schweißarmes, welcher im Allgemeinen noch Unsicherheiten bezüglich genauer Geschwindigkeiten und Beschleunigungen offenlässt. Weiterhin untersuchen wir den Einfluss des empfindlichen Spektralbereiches der IR-Kamera durch den Vergleich von Messungen mit verschiedenen schmalbandigen Bandpassfiltern (25 nm FWHM) in einem Bereich von 1150 nm bis 1550 nm. T2 - Thermographie-Kolloquium 2019 CY - Halle (Saale), Germany DA - 19.09.2019 KW - Additive manufacturing KW - 3D printing KW - Thermography KW - Direct energy deposition KW - Laser Metal Deposition KW - 3D Druck KW - Laser Pulver Auftragsschweißen KW - Additive Fertigung KW - Thermografie PY - 2019 AN - OPUS4-49078 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Scheuschner, Nils A1 - Altenburg, Simon A1 - Straße, Anne A1 - Gumenyuk, Andrey A1 - Maierhofer, Christiane T1 - In-situ thermographic monitoring of the laser metal deposition process N2 - By allowing economic on demand manufacturing of highly customized and complex workpieces, metal based additive manufacturing (AM) has the prospect to revolutionize many industrial areas. Since AM is prone to the formation of defects during the building process, a fundamental requirement for AM to become applicable in most fields is the ability to guarantee the adherence to strict quality and safety standards. A possible solution for this problem lies in the deployment of various in-situ monitoring techniques. For most of these techniques, the application to AM is still very poorly understood. Therefore, the BAM in its mission to provide safety in technology has initiated the project “Process Monitoring of AM” (ProMoAM). In this project, a wide range of in-situ process monitoring techniques, including active and passive thermography, optical tomography, optical emission and absorption spectroscopy, eddy current testing, laminography, X-ray backscattering and photoacoustic methods, are applied to laser metal deposition (LMD), laser powder bed fusion and wire arc AM. Since it is still unclear which measured quantities are relevant for the detection of defects, these measurements are performed very thoroughly. In successive steps, the data acquired by all these methods is fused and compared to the results of reference methods such as computer tomography and ultrasonic immersion testing. The goal is to find reliable methods to detect the formation of defects during the building process. The detailed acquired data sets may also be used for comparison with simulations. Here, we show first results of high speed (> 300 Hz) thermographic measurements of the LMD process in the SWIR range using 316L as building material. For these experiments, the camera was mounted fixed to the welding arm of the LMD machine to keep the molten pool in focus, regardless of the shape of the specimen. As the thermograms do not contain any information about the current spatial position during the building process, we use an acceleration sensor to track the movement and synchronize the measured data with the predefined welding path. This allows us to reconstruct the geometry of the workpieces and assign the thermographic data to spatial positions. Furthermore, we investigate the influence of the acquisition wavelength on the thermographic data by comparing measurements acquired with different narrow bandpass filters (50 nm FWHM) in a spectral range from 1150 nm to 1550 nm. This research was funded by BAM within the Focus Area Materials. T2 - Sim-AM 2019 - 2. International Conference on Simulation for Additive Manufacturing CY - Pavia, Italy DA - 11.09.2019 KW - Additive manufacturing KW - 3D printing KW - Thermography KW - Direct energy deposition KW - Laser Metal Deposition KW - 3D Druck KW - Laser Pulver Auftragsschweißen KW - Additive Fertigung KW - Thermografie PY - 2019 AN - OPUS4-49070 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Jonietz, Florian A1 - Krankenhagen, Rainer A1 - Altenburg, Simon A1 - Eisenkrein-Kreksch, H. T1 - Standardisierung eines thermografischen Verfahrens zur Schichtdickenbestimmung von Beton-Oberflächenschutzsystemen N2 - Polymerbeschichtungen auf Beton bieten einerseits mechanischen Schutz vor Beschädigungen und verhindern das Eindringen von Wasser, gelösten Salzen und CO2 und können andererseits der Oberfläche ein gewünschtes Aussehen geben. Daher werden sie in der Bauindustrie insbesondere bei Brücken und Parkhäusern häufig verwendet. Für die beabsichtigte Wirkung der Beschichtung ist deren Schichtdicke ein entscheidender Faktor und muss daher nach Aufbringung der Schicht und im Betrieb regelmäßig überprüft werden. Üblich sind hier zerstörende Verfahren mit nachträglich erforderlicher Ausbesserung. Im Rahmen eines Vorgängerprojektes wurde an der BAM in Kooperation mit der IBOS GmbH ein zerstörungsfreies Verfahren entwickelt, welches auf aktiver Thermografie basiert. Ein Prototyp mit Halogenlampe und Infrarot-Kamera wurde erprobt. Das hier beschriebene Folgeprojekt hat das Ziel, dieses Verfahren zu standardisieren, damit es sich in der Industrie als zerstörungsfreies Alternativverfahren zur Schichtdickenbestimmung durchsetzt. Im ersten Schritt wird gezeigt, bei welchen Oberflächenschutzsystemen das Verfahren bereits zuverlässige Schichtdickenmessungen ermöglicht und praxistauglich ist. Anschließend werden weitere Forschungsthemen definiert und bearbeitet, die eine Anwendung für alle Oberflächenschutzsysteme ermöglichen sollen. Besondere Herausforderungen stellen etwa Sandeinstreuungen in der Polymerschicht dar. Auch muss der Frage nach der Anwendbarkeit auf Mehrschichtsysteme nachgegangen werden. Des Weiteren stellt sich die Frage nach dem Einfluss der Beschaffenheit des Betonuntergrunds auf die Anwendbarkeit des Verfahrens. Im zu erarbeitenden Normentwurf sollen diese Untersuchungen die Möglichkeiten, aber auch die Grenzen der aktiven Thermografie zur Schichtdickenmessung von Oberflächenschutzsystemen aufzeigen. Im Beitrag werden die systematischen Untersuchungen bezüglich dieser Fragestellungen dargelegt. T2 - DACH-Jahrestagung 2019 CY - Friedrichshafen, Germany DA - 27.05.2019 KW - thermografisches Verfahren KW - Standardisierung KW - Schichtdickenbestimmung KW - Beton-Oberflächenschutzsysteme KW - Polymerbeschichtungen auf Beton PY - 2019 AN - OPUS4-49008 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Küttenbaum, Stefan A1 - Braml, T. A1 - Maack, Stefan T1 - Refining stochastic models for the reassessment of bridges using NDT-methods N2 - Increasing requirements on the infrastructure caused by more and heavier traffic coincide with both the aging and the progressive degradation of bridge constructions. These exemplary issues lead to a non-negligible need for reassessments of existing bridges. Compared to the new building design, safety reserves can be used in the evaluation of such existing structures, since uncertainties that may arise during the design, construction and previous Service time are better known or no longer present. Uncertainties can be evaiuated more precisely by measurements. In the meantime, the application of advanced NDT-methods on concrete structures have become so capable, that crucial structure Parameters like certain material properties or geometrical dimensions can be quantified without significant destructive interventions. The measured data can be explicitly incorporated into the probabilistic computation models used for the bridge reassessment in form of random variables. Therewith, a previously insufficient model can be refined to achieve a higher level of approximation. This contribution emphasises two fundamental steps of the measured data based probabilistic reassessment: The sensitivity analyses to identify the cruciai Parameters and the needed accuracy of the related information as well as the comparison with expected uncertainties of non-destructively measured Parameters. T2 - 17th International Probabilistic Workshop CY - Edinburgh, UK DA - 11.09.2019 KW - Measurement KW - Reassessment KW - Structural safety KW - Concrete bridges KW - NDT PY - 2019 AN - OPUS4-48999 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bertovic, Marija A1 - Ronneteg, U. T1 - Usability of the written procedures: an eye tracking study N2 - Usability of the written procedures: an eye tracking study Non-destructive evaluation (NDE) is regarded as one of the key elements in ensuring quality of engineering systems and their safe use. A failure of NDE to detect critical defects in safety-relevant components, such as those in the nuclear industry, may lead to catastrophic consequences for the environment and the people. NDE inspection procedure is one of the most important tools in the everyday life of an NDE inspector. Experience and research studies have shown that NDE procedures are not always used as foreseen and may need to be optimized. Both the content and format play an important role in producing reliable procedures. Whereas the content aids in the understanding of the task and in its subsequent correct execution, the format determines the efficiency and frequency of the procedure’s use. For the purposes of this study, an inspection procedure - designed to be used in the inspection of components used in the final disposal of spent nuclear fuel - was further developed by adopting a user-centered design. This was achieved by following the eye movements during a data evaluation task whilst using the procedure, by interviews and group discussions, accompanied by a review from a human factors’ perspective, the suggestions from relevant literature and by reiterating the entire process once again. This process resulted in identifying shortcomings and in suggesting alterations to the existing procedure. The newly created procedure was empirically tested for its usability using eye tracking. By comparing the old instruction format to the newly developed one, the results showed that appropriately highlighting warnings, exceptions, or reminders, and placing them at a logical position assures that they will be read and identified with ease rather than overlooked. The presentation of the information in a stepwise manner, with one action per step, allows the user to follow more easily the steps that must be carried out to save time and effort. This study - the first of its kind in the field of non-destructive evaluation - showed that the procedure can be improved by applying human factors principles to the design and by involving the users into the process of procedure development and quality assurance. Introduction of the speaker – Marija Bertovic Marija Bertovic has a degree in psychology and a PhD in human factors. Since 2006 she has been working on topics related to human factors in non-destructive testing at the BAM Federal Institute for Materials Research and Testing, German Society for Non-Destructive Testing and as an independent consultant. The focus of her research has been on identifying and studying human factors’ related risks during NDT inspections and suggesting ways of optimizing the inspections and inspection procedures. She is currently a research staff member at BAM responsible for probabilistic safety and reliability analyses AND human factors analyses. She is the chairwoman of the German Society for Non-Destructive Testing’s (DGZfP) subcommittee on human machine interaction and the winner of the DGZfP Science Award in 2018. T2 - AHFE International, 10th International Conference on Applied Human Factors and Ergonomics CY - Washington Hilton, Washington D.C., USA DA - 24.07.2019 KW - Human Factors KW - ZfP KW - NDE PY - 2019 AN - OPUS4-48851 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -