TY - CONF A1 - Trappe, Volker A1 - Sachs, Patrick ED - Vassilopoulos, A. P. ED - Michaud, V. T1 - Dynamic mechanical analysis of epoxy-matrix cross linking measured in-situ using an elastomer container N2 - A new patented dynamic mechanical analysis (DMA) is presented, where the tensile, bending- or torsional stiffness of a media can be characterized in-situ during the phase transition from liquid to solid. An epoxy system, e.g. Hexion L285/H287, is filled into an elastomer container, such as a silicone tube. This can be mounted into a conventional OMA and, based on a linear viscoelastic approach, the storage modulus (E';G'), the loss modulus (E'';G'') and the loss angle tan(δ) can be measured at constant temperature as a function of time in order to investigate the liquid to sol-gel to solid transition. With this new method, the stiffness increase as a result of the cure process can be directly measured more precisely than with a rheometer in a shear plate set-up, because using an elastomer container gives a defined cross section for calculating the Young's modulus. T2 - 20th European Conference on Composite Materials CY - Lausanne, Switzerland DA - 26.06.2022 KW - Cross linking KW - Dynamic mechanical analysis (DMA) KW - Thermoset polymers KW - Cure process PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-569651 UR - https://infoscience.epfl.ch/record/298799 SN - 978-2-9701614-0-0 VL - Vol. 5 - Applications and structures SP - 181 EP - 186 PB - Composite Construction Laboratory (CCLab) CY - Lausanne AN - OPUS4-56965 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Bhadeliya, Ashok A1 - Rehmer, Birgit A1 - Fedelich, Bernard A1 - Olbricht, Jürgen A1 - Skrotzki, Birgit A1 - Jokisch, T. ED - Zimmermann, M. T1 - Rissfortschrittsuntersuchungen an gefügten Nickelbasiswerkstoffen bei hoher Temperatur N2 - In nickelbasierten Superlegierungen, die für Gasturbinenschaufeln verwendet werden, sind bei hohen Betriebstemperaturen und -belastungen Kriechschäden, Ermüdung, Korrosion und Oxi-dation zu beobachten. Die betroffenen Turbinenschaufeln müssen ersetzt oder repariert werden, um Effizienzverluste und ein eventuelles Bauteilversagen zu vermeiden. In letzter Zeit wurden additive Fertigungs- und Lötverfahren für die Reparatur und das Fügen von Nickelbasiswerk-stoffen entwickelt, um die Einschränkungen der traditionellen Reparaturverfahren zu überwinden. Für eine auslegungsrelevante Bewertung des Risswachstumsverhaltens in den Fügezonen, die durch diese neuen Technologien erzeugt werden, sind Rissfortschrittsuntersuchungen erfor-derlich. Entsprechende Untersuchungen an gefügten Proben werden in diesem Beitrag vorge-stellt. Die Rissfortschrittsversuche werden an gefügten SEN-Proben (Single Edge Notch) bei einem Spannungsverhältnis von 0,1 und einer Temperatur von 950 °C durchgeführt. Das Riss-wachstum wird mit der DCPD-Methode (Direct Current Potential Drop) überwacht, und die ge-messenen Potenzialsignale werden anhand der optisch vermessenen Risslänge und einer Finite-Elemente-Analyse kalibriert. Der Spannungsintensitätsfaktor (SIF) für die gefügte SEN-Geometrie wird mit Hilfe von Finite-Elemente-Analysen berechnet. Auf diese Weise können Rissfortschrittskurven aus den experimentellen Daten abgeleitet werden. T2 - Tagung „Werkstoffprüfung 2022“ CY - Dresden, Germany DA - 27.10.2022 KW - Lötverbindung KW - Rissfortschritt KW - SEN-Probe KW - Gefügte Nickelbasislegierungen PY - 2022 SN - 978-3-88355-430-3 VL - 2022 SP - 67 EP - 72 AN - OPUS4-57090 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Memmolo, V. A1 - Lugovtsova, Yevgeniya A1 - Olino, M. A1 - Prager, Jens ED - Kundu, T. ED - Reis, H. ED - Ihn, J.-B. T1 - Application of Temperature Compensation Strategies for Ultrasonic Guided Waves to Distributed Sensor Networks N2 - Temperature compensation strategies play a key role in the implementation of guided wave based structural health monitoring approaches. The varying temperature influences the performance of the inspection system inducing false alarms or missed detection, with a consequent reduction of reliability. This paper quantitatively assesses two temperature compensation methods, namely the optimal baseline selection (OBS) and the baseline signal stretch (BSS), with the aim to extend their use to the case of distributed sensor networks (DSN). The effect of temperature separation between baseline time-traces in OBS and BSS are investigated considering multiple couples of sensors employed in the DSN. A decision strategy that uses frequent value warning to define the optimal baseline or stretching parameter is found to be effective analyzing data from two several experiments, which use different frequency analysis with either predominantly A0 mode or S0 mode data or both. The focus is given on the fact that different paths are available in a sensor network and several possible combinations of results are available. Nonetheless, introducing a frequent value warning it is possible to increase the efficiency of the OBS and BSS approach making use of fewer signal processing algorithms. In addition, the effectiveness of those approach is quantified using damage indicators as metric, which confirms that the performance of OBS and BSS quantitatively agree with predictions and also demonstrate that the use of compensation strategies improve detectability of damage with a higher reliability of the system. T2 - 2022 49th Annual Review of Progress in Quantitative Nondestructive Evaluation (QNDE 2022) CY - San Diego, CA, USA DA - 25.07.2022 KW - Ultrasound KW - Elastic waves KW - Structural Health Monitoring KW - Environmental Effects KW - Damage Detection PY - 2022 SN - 978-0-7918-8659-5 DO - https://doi.org/10.1115/QNDE2022-98534 SP - 1 PB - The American Society of Mechanical Engineers (ASME) CY - 2 Park Avenue, New York, NY 10016, USA AN - OPUS4-57074 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Appel, S. A1 - Schepers, Winfried T1 - Tieffrequente Schwingungsimmissionen durch den Betrieb einer Rohzementmühle N2 - Der Beitrag berichtet von einer aufwändigen Messkampagne vor Ort, mit der die Emissionen direkt an einer Rohzementmühle, die Transmissionen im Baugrund und die Immissionen in benachbarten Bebauungen genauer untersucht wurden. Im Ergebnis der ausgewerteten Messungen sowie strukturdynamischer Berechnungen zeigte sich, dass der Baugrund zwar aus statischer Sicht sehr gut tragfähig, aber dynamisch als eher ungünstig zu beurteilen ist. Weiterhin wurde festgestellt, dass in dynamischer Hinsicht ein vorgenommener Bodenaustausch tendenziell eine Verschlechterung der Aufstellbedingungen darstellte. Für das betroffene Bürogebäude konnte nachgewiesen werden, dass durch den Betrieb der Zementmühle die Anregung der Deckeneigenfrequenzen zu deutlich spürbaren Resonanzschwingungen führte. Aufgrund der tieffrequenten Anregung durch den Mühlenbetrieb sind Maßnahmen zur Minderung der Schwingungsemissionen generell und insbesondere nach erfolgter Aufstellung der Mühle schwer bzw. gar nicht zu realisieren. Im Beitrag wird daher darauf eingegangen, auf welche Aspekte bei der Planung zur Aufstellung derart großer Mühlen zwingend zu achten ist. T2 - 7. VDI-Fachtagung Baudynamik CY - Würzburg, Germany DA - 27.04.2022 KW - Erschütterungen KW - Maschinenbetrieb KW - Minderungsmaßnahmen PY - 2022 SN - 978-3-18-092379-6 SP - 385 EP - 397 PB - VDI-Verlag CY - Düsseldorf AN - OPUS4-58584 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zhang, K. A1 - Schmidt, Wolfram A1 - Mezhov, Alexander T1 - Influence of the hydroxypropylation of starch on its performance as viscosity modifying agent N2 - Synopsis: Starch is a commonly used viscosity modifying agent (VMA). The performance of starch as VMA depends on its origin (e.g. potato, corn, cassava, etc.) and corresponding molecular properties, such as molecular weight, ratio between amylose and amylopectin etc. Depending upon the application, the efficiency of starch can be enhanced by hydroxypropylation. The maximum degree of substitution (DoS) cannot be greater than 3.0, which is the number of hydroxy groups per glucose monomer in the polymer. In the current research three potato starches exhibiting the DoS of 0.4, 0.6 and 0.8 were utilised. The influence of the modified starch on the rheological properties and hydration of cement paste, as well as the viscosity of the pore solution were investigated. Our findings show that the starch with the highest DoS increases the dynamic yield stress the most, while the plastic viscosity is less dependent on the DoS. Additionally, starch with the highest DoS retards hydration to lower degree than other starches. T2 - 13th International Conference on Superplasticizers and Other Chemical Admixtures in Concrete CY - Milan, Italy DA - 10.07.2022 KW - Potato starch KW - Rheological KW - Cement hydration KW - Pore solutions PY - 2022 DO - https://doi.org/10.14359/51736074 VL - 354 SP - 209 EP - 218 PB - ACI Special Publications AN - OPUS4-58320 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Mezhov, Alexander A1 - Schmidt, Wolfram A1 - Zhang, H. A1 - Diesendruck, Ch. E. T1 - The effect of the charge density of a comb polyphosphate superplasticizer on the structural build-up of cement paste N2 - Synopsis: Lately, there has been rising attention to superplasticizers (SP) based on polyphosphate esters. However, the influence of the molecular structure of the polyphosphate polymers on time-dependent properties such as structural build-up has not been examined yet intensively. To investigate this effect, three comb polyphosphate superplasticizers with different charge densities were synthesised by free radical polymerisation. Our findings indicate that SP with the lowest and medium charge densities extend the induction period more strongly than the SP with the highest charge density. The reduction of the structural build-up rate is linearly dependent on the dosage and concentration of the functional group of polyphosphate SP in the cementitious system. This study proposes a mathematical equation expressing the relationship between the structural build-up rate during the induction period and the molecular structure of the polyphosphate SP. T2 - 13th International Conference on Superplasticizers and Other Chemical Admixtures in Concrete CY - Milan, Italien DA - 10.07.2022 KW - Admixture KW - Superplasticizer KW - Polyphosphate KW - Structural build-up PY - 2022 DO - https://doi.org/10.14359/51736079 VL - 354 SP - 255 EP - 262 PB - ACI Special Publications AN - OPUS4-58321 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Zhang, K. A1 - Mezhov, Alexander A1 - Schmidt, Wolfram T1 - Thixotropic and chemical structural build-up of cement pastes with superplasticizer under different storage conditions N2 - Synopsis: The paper presents the results of a study on the influence of agitation on the structural build-up of fresh cement pastes using a penetration test. It first presents results about the influence of the penetrating shape’s geometry on the influence on the cement paste specimen. Then, results are shown for the load-deflection curves depending upon time and agitation before testing. Based on the observation of the force required to penetrate the sample, conclusions on the structural build-up can be made. The observations were made over the course of time with samples that were left at rest and partly agitated before testing at different time steps. The setup allows to identify the contribution of the chemical reaction to the structural build-up process. The presence of superplasticizer obviously reduces the load that cement paste can withstand, while the loss of thixotropy is found notably lower than that of neat cement pates T2 - 13th International Conference on Superplasticizers and Other Chemical Admixtures in Concrete CY - Milan, Italy DA - 10.07.2022 KW - Thixotropy KW - Superplasticizer KW - Structural build-up KW - Texture analyzer KW - Penetration test PY - 2022 DO - https://doi.org/10.14359/51736058 VL - 354 SP - 13 EP - 24 PB - ACI Special Publications AN - OPUS4-58324 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Munsch, Sarah A1 - Bintz, Thilo A1 - Heyn, R. A1 - Hirsch, H. A1 - Grunewald, J. A1 - Kruschwitz, Sabine T1 - Detailed investigation of capillary active insulation materials by 1H nuclear magnetic resonance (NMR) and thermogravimetric drying N2 - Capillary active interior insulation materials are an important approach to minimize energy losses of historical buildings. A key factor for their performance is a high liquid conductivity, which enables redistribution of liquid moisture within the material. We set up an experiment to investigate the development of moisture profiles within two different interior insulation materials, calcium-silicate (CaSi) and expanded perlite (EP), under constant boundary conditions. The moisture profiles were determined by two different methods: simple destructive sample slicing with subsequent thermogravimetric drying as well as non-destructive NMR measurements with high spatial resolution. The moisture profiles obtained from both methods show good agreement, when compared at the low spatial resolution of sample slicing, which demonstrates the reliability of this method. Moreover, the measured T2-relaxation-time distributions across the sample depth were measured, which may give further insight into the saturation degree of the different pore sizes. In order to explain differences in the moisture profiles between CaSi and EP, we determined their pore-size distribution with different methods: conversion of the NMR T2 relaxationtime distribution at full saturation, mercury intrusion porosimetry and indirect determination from pressure plate measurements. CaSi shows a unimodal distribution at small pore diameters, while in EP, a bi-modal or wider distribution was found. We assume that the smaller pore diameters of CaSi lead to a higher capillary conductivity, which causes a more distributed moisture profile in comparison with that of EP. T2 - NDT-CE CY - Zurich, Switzerland DA - 16.08.2022 KW - Insulation material KW - Nuclear magnetic resonance KW - Capillary conductivity KW - Pore-size distribution PY - 2022 UR - https://nbn-resolving.org/urn:nbn:de:kobv:b43-579172 DO - https://doi.org/10.58286/27205 SN - 1435-4934 VL - 27 IS - 9 SP - 1 EP - 11 AN - OPUS4-57917 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kluge, Martin A1 - Habib, Abdel Karim A1 - van Wingerden, Kees ED - Beyer, Michael ED - Lucassen, Arnas T1 - Large-scale tests to investigate the consequences of exposing cryogenic storage vessels containing liquid hydrogen to a fire load N2 - Large Scale Experiments have been performed to determine whether a storage vessel containing liquid hydrogen (LH2) and caught in a fire engulfing the vessel can result in a BLEVE (Boiling Liquid Expanding Vapour Explosion) and if so its consequences. The tests were performed at the Test Site Technical Safety of the Bundesanstalt für Materialforschung und –prüfung (BAM) in Germany at the Hydrogen Test Area (H2TA) within a research cooperation between BAM and Gexcon as part of the SH2IFT program. Three tests were performed using double-walled vacuum insulated vessels of 1 m3 volume. The cylindrical Vessels differed in orientation (horizontal or vertical) and the insulation material used (perlite or multi-layer insulation (MLI)). The degree of filling of the vessels was approximately 35-40 % in each of the tests performed. The fire load was provided by a propane fed burner-system positioned under the storage vessel and designed to give a homogeneous fire load. The conditions in the vessel (temperatures and pressure) as well as external effects (heat radiation, blast waves, flame ball development and fragmentation) were measured. All vessels were equipped with K-type thermocouples at several locations at the inner and outer vessel shell. The pressure inside the inner vessel and in the space between the inner and outer vessels (vacuum pressure) was measured. Bolometers were used to measure the heat radiation generated by both the propane fire and that generated by a possible fireball/BLEVE. To measure blast generated by the vessel burst/BLEVEs blast pencils were positioned at up to three locations. Further several cameras were used to monitor the events: normal cameras, infrared (IR)-cameras, high-speed cameras also on board of an UAV. Two of these vessels, a horizontal and a vertical vessel both insulated with perlite withstood the fire loading for 1 hour 20 minutes and 4 hours respectively without catastrophic failure. A horizontal vessel insulated with MLI failed by bursting after 1 hour and 6 minutes resulting in a fireball, fragments, and blast wave. T2 - 14th International Symposium on Hazards, Prevention and Mitigation of Industrial Explosions CY - Braunschweig, Germany DA - 11.07.2022 KW - Prevention KW - Industrial explosions KW - BLEVE KW - LH2 KW - Fire ball KW - Fragments PY - 2022 DO - https://doi.org/10.7795/810.20221124 SP - 168 EP - 181 AN - OPUS4-59440 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Habib, Abdel Karim A1 - Kluge, Martin A1 - van Wingerden, Kees ED - Beyer, Michael ED - Lucassen, Arnas T1 - Experimental investigation into the consequences of release of liquified hydrogen onto and under water N2 - Large-scale experiments have been performed to investigate the possible consequences of realistic amounts of liquified hydrogen (LH2) encountering water. The experiments aimed at simulating an accidental release of LH2 during especially the fuelling of a ship. For liquified natural gas (LNG) it has been demonstrated that when spilled onto water the evaporation rate can be that high that physical explosions occur which are referred as rapid phase transitions (RPTs). It cannot be excluded that RPTs are also possible in the case of LH2. The tests were performed in a 10 m x 10 m x 1.5 m basin filled with water, at the Test Site Technical Safety of the Bundesanstalt für Materialforschung und –prüfung (BAM) in Horstwalde, Germany within a research cooperation between BAM and Gexcon as part of the SH2IFT program. LH2 releases were established releasing directly from a trailer carrying LH2 through a long flexible double vacuum insulated transfer line. The releases occurred from a height of 50 cm above and 30 cm under the water surface both pointing downwards and 30 cm under the water surface pointing along the water surface too. The release rate was determined based on the weight loss rate of the road tanker which was placed onto load cells. Special blast pressure sensors were used to measure the shock waves generated by the release processes both in the water and in the air. At several locations the gas concentration was measured. Heat radiation was measured at 3 distances from the point of release. High speed, Infrared (IR) and normal cameras were used to record events and to follow the gas cloud behaviour in time. This includes cameras mounted on a UAV and underwater cameras. Two weather stations were used to measure wind speed, wind direction, temperature and humidity during all tests performed. All investigated release configurations resulted in a very chaotic LH2-water mixing zone, causing considerable evaporation but only minor over pressures. The main phenomenon observed was an ignition of the released gas cloud, resulting in significant blast wave overpressures and heat radiation to the surroundings. The location of the ignition occurred in free air at some distance from the instrumentation and release location. T2 - 14th International Symposium on Hazards, Prevention and Mitigation of Industrial Explosions (ISHPMIE 2022) CY - Braunschweig, Germany DA - 11.07.2022 KW - LH2 KW - RPT KW - Release KW - Gas cloud explosion KW - Heat radiation PY - 2022 SP - 182 EP - 196 AN - OPUS4-59441 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Linnemann, Konrad A1 - Quercetti, Thomas A1 - Sterthaus, Jens A1 - Ballheimer, Viktor T1 - Experimental and numerical investigation of prestressed bolt connections under lateral displacements N2 - The containment system of transport packages for spent nuclear fuel and high-level waste usually includes bolted lids with metal gaskets. The packages are assessed to specific transport conditions which are specified in the IAEA safety standards SSR-6 (IAEA 2018). These transport conditions, especially the so-called accident conditions of transport, imply high dynamic loading on the lids and the bolt connections of the package. The response of the lid systems on the mechanical accident conditions is generally investigated by experimental drop tests or numerically, e.g., by finite element analyses. The interpretation of the drop test results for the verification of the numerical models is often not obvious due to the complex superposition of different effects in the real tests. BAM has started a research project to get a better understanding about the behavior of prestressed bolt connections under loadings typical for these drop tests. In this context an experimental test set-up was developed to investigate the response of a single bolt connection under a prescribed lateral displacement of clamped parts. The bolt is instrumented by strain gauges to get the pretensional, the torsional and the bending stress in the bolt shank. Furthermore, the lateral movement and the tilt of the bolt head is measured during the test. A finite element model of the test set-up has been created in Abaqus FEA (Simulia 2021). The very detailed instrumentation of the test set-up shall give the opportunity to investigate and validate the numerical model. The aim of this paper is to give an overview about the proposed research project and to present first results. T2 - SMIRT 26 (26th conference on Structural Mechanics in Reactor Technology) CY - Potsdam, Germany DA - 10.07.2022 KW - Bolt connections KW - Finite element anaylsis KW - Experimental testing KW - Transport package for radioactive materials PY - 2022 UR - https://www.lib.ncsu.edu/resolver/1840.20/40614 SP - 1 EP - 7 PB - IASMiRT AN - OPUS4-59378 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Krankenhagen, Rainer A1 - Dell'Avvocato, Giuseppe A1 - Gohlke, Dirk A1 - Palumbo, Davide A1 - Galietti, Umberto T1 - Quantitative evaluation of the welded area in Resistance Projection Welded (RPW) thin joints by pulsed laser thermography N2 - A semi-automatic thermographic procedure for the assessment of the welded area of resistance projection welded joints has been developed. Currently, to assess the quality of RPW joints destructive tests are used and the more commonly used non-destructive technique is the ultrasonic one. The possibility for a quantitative evaluation of the welded area by thermographic technique has been proved by means of an innovative procedure applied on steel RPW joints with ‘as it’ surface conditions. Measurements obtained by thermography and ultrasound have been compared, to verify the developed procedure. T2 - Thermosense: Thermal Infrared Applications XLIV, CY - Orlando, USA DA - 03.04.2022 KW - Nondestructive evaluation KW - Ultrasonics KW - Contact area PY - 2022 DO - https://doi.org/10.1117/12.2618806 VL - 12109 SP - 1 EP - 14 PB - SPIE AN - OPUS4-59380 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Giese, Marcel A1 - Schröpfer, Dirk A1 - Kannengießer, Thomas A1 - Müller, Thomas A1 - Treutler, Kai A1 - Wesling, Volker T1 - Legierungsmodifikation und Einsatz hybrider Fräsprozesse zur Optimierung der Zerspanungssituation Ni-basierter Verschleißschutzauftragschweißungen mit definierten Oberflächen N2 - Die Bestrebungen zur Verringerung der CO2-Emissionen erfordern hochbelastbare und effiziente Komponenten aus Stahl in der Anlagen-, Verfahrens- und Kraftwerkstechnik. Hierfür sind in zunehmendem Maße auf den Anwendungsfall und Stahlwerkstoff abgestimmte Verschleißschutzschich-ten und definierte, zerspante Oberflächen notwendig. Die hohen Härten dieser Schichten und der Einsatz konventioneller Co-basierter Verschleißwerkstoffe führen oftmals zu unwirtschaftlichen Bauteilen, gerade aufgrund hohen Werkzeugverschleißes bei der Zerspanung mit geometrisch bestimmter Schneide. Er-kenntnisse über den Einsatz Ni-basierter Verschleißwerkstoffe und die Optimierung der Zerspanbarkeit mittels Legierungsmodifikationen und moderner hybrider Fräsprozesse ohne Verschlechterung der Ver-schleißschutzeigenschaften sind deshalb für die Anwender und Verarbeiter zur wirtschaftlichen Fertigung hochbelasteter Stahlbauteile wesentlich. Der vorliegende Beitrag stellt die Untersuchungsmethodik eines aktuell laufenden Vorhabens der TU Clausthal und BAM, Berlin, vor. Fokus liegt hierbei auf den hochin-strumentierten Fräsexperimenten, die eine reproduzierbare Analyse und Korrelation zwischen den mik-rostrukturellen Eigenschaften der auftraggeschweißten Legierungen, dem Zerspanprozess und der Zer-spanbarkeit, insbesondere der resultierenden Oberflächenintegrität, ermöglichen sollen. T2 - Tagung Werkstoffprüfung 2022 CY - Dresden, Germany DA - 27.10.2022 KW - Werkzeugverschleiß KW - Oberflächenintegrität KW - Ultraschallunterstütztes Fräsen KW - Zerspankräfte PY - 2022 SP - 368 EP - 374 AN - OPUS4-59211 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Shaheen, Sabahat A1 - Hicke, Konstantin T1 - Measurement of Geometric Phase using a φ-OTDR setup N2 - Geometric phase showing sensitivity to changes in polarisation state and intensity of backscattered light is measured using a novel φ-OTDR setup based on coherent heterodyne detection. Principle is demonstrated using a polarisation scrambler inline a fiber-under-test. T2 - Optical Fiber Sensors 2022 CY - Alexandria, Virginia, United States DA - 29.08.2022 KW - Coherent Heterodyne KW - Geometric Phase KW - Distributed Fiber Optic Sensor PY - 2022 SN - 978-1-957171-14-2 SP - W4.72 AN - OPUS4-56116 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Weise, Frank A1 - Fladt, Matthias A1 - Wieland, M. T1 - Internal water-repellent treatment - a novel strategy for mitigating alkali-aggregate reaction in concrete pavements N2 - To prevent future alkali-aggregate reaction (AAR) damage, which has occurred frequently in the Germanhighway network in recent years, a new regulation has been drafted. This regulation severely limits the use of alkali-sensitive aggregates by requiring that their suitability be verified by certified inspectors using newly developed AAR concrete tests that involve the external supply of alkali. This has led to a significant limitation in the number of aggregates usable for concrete pavements. A novel AAR avoidance strategy is now being pursued, which aims to enable the use of borderline alkali-sensitive aggregates through the application of an internal water-repellent treatment. The addition of water repellents during concrete production should significantly reduce the ingress of water and external de-icing salts into the concrete pavement, thus reducing the potential for AAR damage. This paper presents the results of laboratory tests to assess the suitability of this new AAR prevention strategy. Representative, highly AAR-susceptible road paving concrete made with an alkali- sensitive greywacke and various water repellents were used as the basis for these experiments. The tests for concrete suitability included determining the conventional fresh and hardened concrete properties as well as concrete prism tests with external alkaline supply. Building on these results, laser-induced breakdown spectroscopy (LIBS) analyses of de-icing-salt intrusion as well as microscopic examinations for verification of the AAR characteristics were carried out. The results of the AAR concrete tests with external alkaline supply support the conclusion that, when hydrophobic agents containing a suitable active ingredient are used, the AAR damage process in road paving concrete can be sufficiently prevented. T2 - 16th International Conference on Alkali-Aggregate Reaction in Concrete CY - Lisboa, Portugal DA - 31.05.2022 KW - Concrete pavements KW - Internal water-repellent treatment KW - Preventive measures KW - Testing for potential AAR PY - 2021 SN - 978-972-49-2315-4 VL - 1 SP - 511 EP - 524 AN - OPUS4-54551 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Kositz, M. A1 - Hünger, K.-J. A1 - Weise, Frank T1 - Regression analysis of ASR expansions and silica dissolution in the presence of NaCl N2 - The durability of concrete structures due to alkali-silica-reaction (ASR) is usually been assessed by ASR concrete prism tests (CPT). Therefore, the expansion of concrete specimens indicates an alkalisensitivity. In Germany these tests are performed at 40°C or accelerated 60°C. Nevertheless, ASR prism tests are expensive, power and time-consuming. For these reasons, an alternative chemical test (“mod. BTU-test”) was developed in the past. The “mod. BTU-test” was correlated with German standard CPT. In this test, the solubility of silica and alumina in the liquid phase is measured by ICP-OES. For special requirements in concrete road construction, stricter test procedures are necessary. The specimens are repeatedly subjected to cyclic alternating storage in NaCl. On the one hand, the presence of NaCl increases the ASR expansion, on the other hand NaCl also changes the dissolution behaviour of silica and alumina. For now is not possible to correlate the solubilities of “mod. BTU-test” and ASR expansions influenced by NaCl. Therefore, four aggregates with different ASR sensitivities were chosen and ASR concrete prism tests (in addition with NaCl) have been performed. According to the “mod. BTU-test” the solubilities of silica and alumina in presence of different NaCl concentrations were measured. This paper is about the regression analysis of silica and alumina dissolution and ASR expansion tests in presence of NaCl. The regression analysis shows the influence of a quasi-continuous and an interrupted cyclic alternating storage. Additionally the effects of temperature and NaCl concentration are investigated. In the end, a suitable NaCl concentration of the “mod. BTU-test” for dissolution experiments is recommended. The “mod. BTU-Test” with NaCl might be a serious and reliable test method for ASR classification for concrete road construction. T2 - 16th International Conference on Alkali-Aggregate Reaction in Concrete CY - Lisboa, Portugal DA - 31.05.2022 KW - Alkali silica reaction KW - Alkaline solution KW - Alumina & silica dissolution KW - NaCl KW - Regression analysis PY - 2021 SN - 978-972-49-2315-4 VL - 1 SP - 711 EP - 723 AN - OPUS4-54552 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Krütt, Enno A1 - Pirskawetz, Stephan A1 - Wallau, Wilma A1 - Meng, Birgit T1 - Development of an automated 60 °C Concrete Prism Test N2 - ln most of the ASR-test procedures, the expansion of concrete or mortar specimens is used as an indicator to assess the ASR-potential of an aggregate or a specific concrete mix. For these tests, the specimens are stored in an ASR-provoking environment, where the reaction is accelerated by elevated temperature and humidity. To measure the length change, the storage must be interrupted for at least a few minutes. Düring the 60 °C Concrete Prism Test (60 °C-CPT), the specimens are cooled down to 20 °C for 24 hours, to ensure the same hygrothermal conditions for every measurement. This limits the number of measurements during the test period and may lead to additional effects, that probably influence the expansion development. With a recently developed device, it is possible to continuously monitor the expansion ofprisms without interrupting the ASR-provoking storage. Due to the dense database of this automated test, the results can contribute to a better understanding of the ASR-process. This study compares results of the automated and conventional 60 °C-CPT. Tests of different aggregates showed, that the results of the automated and conventional test are consistent, but the expansions during the conventional test are generally higher. Preliminary results led to the conclusion, that the cooling for the measurements leads to additional expansions. Therefore, a modified threshold should be discussed for the automated 60 °C-CPT. T2 - 16th International Conference on Alkali-Aggregate Reaction in Concrete CY - Lisboa, Portugal DA - 31.05.2022 KW - 60 °C-CPT KW - ASR expansion monitoring KW - Automated testing PY - 2021 SN - 978-972-49-2315-4 VL - 1 SP - 789 EP - 799 AN - OPUS4-54553 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Pirskawetz, Stephan A1 - Weise, Frank A1 - Rieffel, Y. A1 - Gorbushina, Anna T1 - Die Schlossbrücke Berlin - Schutz der Göttinnen N2 - Vielleicht nannten es die Berliner „Puppen putzen“, wenn in den 1880er Jahren die Marmorstatuen auf der Schlossbrücke vor dem Berliner Stadtschloss mit Bürste, Wasser und Seife von Staub, Ruß und Taubendreck befreit wurden. Soviel Pflege wurde diesen Göttinnen aus der griechischen Mythologie nicht immer zuteil. So haben Klima, Luftverschmutzung und der 2. Weltkrieg, wie bei anderen Kunstwerken auch, tiefe Spuren hinterlassen. Der Erhalt dieser zwischen 1847 und 1857 aufgestellten Skulpturen und vieler vergleichbarer Objekte im Stadtbild ist durch die auch heute weiter fortschreitende Schädigung des Marmors gefährdet. In den Jahren 2006 bis 2010 förderte die Deutsche Bundesstiftung Umwelt (DBU) ein Projekt zur „Entwicklung und Überprüfung von Einhausungssystemen zur Reduzierung umweltbedingter Schädigungen von außenexponierten Marmorobjekten mit dem Ziel des langfristigen Erhalts in situ an einem national bedeutenden Objektkomplex, den Schlossbrückenfiguren unter den Linden, Berlin“. Geleitet und restauratorisch betreut wurde das Projekt durch das Landesdenkmalamt (LDA) Berlin. Durch die Abteilung Strukturgeologie und Geodynamik (GZG) der Georg-August Universität Göttinnen wurden die Verwitterungsmechanismen des Marmors untersucht und auf dieser Basis Anforderungen an das Schutzsystem formuliert. Anhand von numerischen Simulationen des Instituts für Bauklimatik der Technischen Universität Dresden (TUD) wurde das bauphysikalische Konzept des Einhausungssystems optimiert. Die konstruktive Gestaltung eines Prototyps und des finalen Entwurfs erfolgte durch das Fachgebiet Konstruktives Entwerfen und Tragwerkslehre der Universität der Künste Berlin. Durch den Fachbereich Baustoffe der BAM erfolgten die Realisierung des Prototyps der Einhausung sowie ein umfangreiches Klimamonitoring an den Skulpturen. Anhand dieses interdisziplinären Projektes und ergänzt durch weitere Messungen wird gezeigt, mit welchen Methoden die für die Degradation von Marmor relevanten Mechanismen untersucht werden können. Die Erkenntnisse aus dem Projekt sind die Grundlage für die Entwicklung nachhaltiger Pflege- und Schutzkonzepte für die kulturhistorisch wertvollen Skulpturen. Nur mit solchen modernen konservatorischen Programmen können die Originalskulpturen im Berliner Stadtraum erlebbar bleiben. T2 - Workshop Kulturerhaltung - Vom Dampfkessel zu Nanomaterialien CY - Berlin, Germany DA - 17.11.2021 KW - Baustoffe KW - Marmor KW - Verwitterung KW - Kulturelles Erbe KW - Wintereinhausungen KW - Klima KW - Zerstörungsfreie Prüfung KW - Building materials KW - Marble KW - Degradation KW - Cultural heritage KW - Winter shelters KW - Climate KW - Nondestructive testing PY - 2021 SN - 2567-1251 VL - 3 SP - 87 EP - 96 PB - Druckerei G. Bohm CY - Berlin AN - OPUS4-54637 LA - deu AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Rabin, Ira ED - Ciner, P. ED - Nunez, A. T1 - Writing Materials of the Dead See Scrolls N2 - The first manuscripts from the Qumran caves were found in 1947. Within the following 10 years, clandestine and legal excavations revealed some 900 highly fragmented manuscripts from the late Second Temple period. This collection is generally known as Scrolls of the Judea Desert or Dead Sea Scrolls (DSS). For many years after their discovery, text analysis and fragmeents attribution were the main concern of the scholars dealing with the scrolls. The uncertain archaeological provenance of the larger part of the collection added an additional difficulty to the formidable task of sorting some 19000 fragments. After 60 years of scholar research the question of origin, archaeological provenance and correct attribution of the fragmenst are still hotly debated. To dtermine a possible contribution to the debate from the point of view of writing materials, we used otpical and electron microscopy, various X-ray based techniques as well as vibratiional sprectroscopy. We validated our approach with SY - based studies using the advantages of the synchroton radiation source with respect to the benchtop devices. Our laboratory studies showed that often production and storage locality could be distinguished thenks to the specific residues ("fingerprint") they left on the material. Moreover, we have diescovered that diferrent parchment production processses coexisted in the antiquity, and the resulting writing materials can readily be distinguished. T2 - 2nd International Conference on Patristic Studies CY - San Juan, Argentina DA - 28.03.2017 KW - Dead Sea Scrolls KW - Text analysis KW - Fragmented manuscripts KW - X-ray based techniques KW - Archaeological provenance PY - 2021 SN - 978-2-503-59149-0 DO - https://doi.org/10.1484/M.STR-EB.5.1211558 SN - 2566-073X VL - 0095/ 19 SP - 325 EP - 331 PB - Brepols CY - Turnhout, Belgium AN - OPUS4-54593 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER - TY - CONF A1 - Brandt, S. A1 - Brozowski, F. A1 - Plehn, W. A1 - Horn, Wolfgang A1 - Müller, B. T1 - Further Development of Odour Testing of Building Products – Sample Presentation and Evaluation of Perceived Intensity N2 - Indoor air quality is affected by the emission of volatile organic compounds (VOC) or the odour from building products. Odours can be measured by applying the standard ISO 16000-28:2020. In the study presented here proposals for further technical development of the ISO method are presented. The sampling procedure and evaluation method of the perceived intensity are investigated in particular because they have a major influence on reproducibility of measurement results. T2 - 17th International Conference HEALTHY BUILDINGS EUROPE 2021 CY - Online meeting DA - 21.06.2021 KW - Geruchsmessung KW - Emissionen KW - Bauprodukte KW - VOC KW - Perceived Intensity PY - 2021 SN - 978-82-536-1728-2 VL - 2021 SP - 1 EP - 4 PB - SINTEF Books CY - Oslo, Norwegen AN - OPUS4-54574 LA - eng AD - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany ER -