63803 2025 eng poster 0 -- -- -- Mechanochemistry is an environmentally friendly synthetic approach that enables the sustainable production of a wide range of chemicals while reducing or eliminating the need for solvents. Reactive extrusion aims to move mechanochemistry from its conventional gram-scale batch reactions, typically performed in laboratory ball mills, to a continuous, large-scale process. Meeting this challenge requires in situ monitoring techniques to gain insights into reactive extrusion and its underlying processes. While the effectiveness of in situ Raman spectroscopy in providing molecular-level information has been demonstrated, our study uses energy-dispersive X-ray diffraction to monitor reactive extrusion in real time at the crystalline level. Our results provide previously unavailable control over thereactiveextrusion process, promoting its perception as an industrially feasible green alternative to traditional solventbased syntheses. #RSCPoster 2025 Online meeting 04.03.2025 04.03.2025 publish false true Nikita Gugin eng uncontrolled Mechanochemistry Ingenieurwissenschaften und zugeordnete Tätigkeiten 1 Analytische Chemie; Referenzmaterialien 1.4 Non-Target-Analytik 6 Materialchemie 6.3 Strukturanalytik Material Datei im Netzwerk der BAM verfügbar ("Closed Access") Präsentation Advanced Materials