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    <id>65148</id>
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    <publishedYear>2025</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst>1</pageFirst>
    <pageLast>24</pageLast>
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    <type>preprint</type>
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    <title language="eng">Understanding the Activity Trade-Off between Tetrapyrrolic Fe-NCs and Co-NCs in the Alkaline Oxygen Reduction Reaction</title>
    <abstract language="eng">A water-free ionothermal synthesis of porous magnesium-imprinted nitrogen-doped carbon (Mg–NC) materials is introduced to prepare a platform material to investigate electrocatalytic structure-performance relations. Atomically dispersed Co- and Fe-NCs isomorphic to the pristine Mg-NCs are prepared by ion-exchange reactions. The current Mg-templating strategy enables relatively high pyrolysis product yields of up to 50 wt% and resultant Fe-NC and Co-NC catalysts contain high and comparable active metal loading of up to 2.52 wt% Fe and 2.29 wt% Co, respectively. A combination of X-ray spectroscopies with DFT studies reveals a tetrapyrrolic structure of the coordination sites, originating from a pyrolytic magnesium template ion reaction within the ionothermal synthesis. Two sets of highly active isomorphic tetrapyrrolic Fe-NCs and Co-NCs are utilized to understand the differences in intrinsic electrocatalytic performance of Co-NCs and Fe-NCs towards the alkaline oxygen reduction reaction (ORR). Despite their superior valence electronic properties to facilitate the initial outer-sphere electron transfer to O2, Co-NCs show significantly lower performance than Fe-NC with comparable loading. Although the generally discussed weaker binding of peroxide intermediates to CoN4 sites compared to FeN4 sites is evident, experimental and theoretical investigation reveal that it is the underlying peroxide oxidation activity that suppresses the oxygen reduction activity of M-NCs. The high peroxide oxidation activity of Co-NCs explains their reduced alkaline ORR relative to Fe-NCs, shedding light on the understated significance of controlling peroxide chemistry for the optimizing cathodic performance.</abstract>
    <parentTitle language="eng">Understanding the Activity Trade-Off between Tetrapyrrolic Fe-NCs and Co-NCs in the Alkaline Oxygen Reduction Reaction</parentTitle>
    <identifier type="doi">10.26434/chemrxiv-2025-s59s5</identifier>
    <identifier type="urn">urn:nbn:de:kobv:b43-651487</identifier>
    <enrichment key="opus.source">publish</enrichment>
    <licence>Creative Commons - CC BY - Namensnennung 4.0 International</licence>
    <author>Arielle Rieck</author>
    <author>Jian Liang Low</author>
    <author>Simon Dietzmann</author>
    <author>Jörg Radnik</author>
    <author>Zahra Teimouri</author>
    <author>Drew Higgins</author>
    <author>Vasile-Dan Hodoroaba</author>
    <author>Asad Mehmood</author>
    <author>Tim-Patrick Fellinger</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Magnesium Imprinting</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Tetrapyrrolic Sites</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Metal- and nitrogen-doped carbon (M-N-C)</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Oxygen Reduction Reaction (ORR)</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Nitrogen doped Carbon</value>
    </subject>
    <collection role="ddc" number="621">Angewandte Physik</collection>
    <collection role="institutes" number="">3 Gefahrgutumschließungen; Energiespeicher</collection>
    <collection role="institutes" number="">6 Materialchemie</collection>
    <collection role="institutes" number="">6.1 Oberflächen- und Dünnschichtanalyse</collection>
    <collection role="themenfelder" number="">Energie</collection>
    <collection role="themenfelder" number="">Elektrische Energiespeicher und -umwandlung</collection>
    <collection role="fulltextaccess" number="">Datei für die Öffentlichkeit verfügbar ("Open Access")</collection>
    <collection role="literaturgattung" number="">Graue Literatur</collection>
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    <thesisPublisher>Bundesanstalt für Materialforschung und -prüfung (BAM)</thesisPublisher>
    <file>https://opus4.kobv.de/opus4-bam/files/65148/Rieck_Low_ChemRxiv.pdf</file>
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  <doc>
    <id>61757</id>
    <completedYear/>
    <publishedYear>2024</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst/>
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    <title language="eng">Commercially Available Sodium-Ion Cells: Multi-Scale Analysis and Material Characterisation</title>
    <abstract language="eng">As the first commercial sodium-ion-batteries (SIBs) are available for purchase, it is possible to investigate material composition. Gaining an insight into the material composition of these SIBs is of interest not only for the classification of possible safety risks and hazards, but also in regards to recycling. Herein we report the preliminary investigations of the chemical and structural composition of first commercial SIB-cells. Two different SIB-cells with different specification were compared regarding electrode size, thickness and further parameters. Furthermore, the composition of the active materials and electrolyte was investigated and compared.</abstract>
    <enrichment key="eventName">Adlershofer Forschungsforum 2024</enrichment>
    <enrichment key="eventPlace">Berlin, Germany</enrichment>
    <enrichment key="eventStart">11.11.2024</enrichment>
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    <author>Luise Sander</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Sodium-Ion</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Multi-Scale Analysis</value>
    </subject>
    <collection role="ddc" number="621">Angewandte Physik</collection>
    <collection role="institutes" number="">1 Analytische Chemie; Referenzmaterialien</collection>
    <collection role="institutes" number="">1.7 Organische Spuren- und Lebensmittelanalytik</collection>
    <collection role="institutes" number="">3 Gefahrgutumschließungen; Energiespeicher</collection>
    <collection role="institutes" number="">6 Materialchemie</collection>
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    <collection role="themenfelder" number="">Elektrische Energiespeicher und -umwandlung</collection>
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  <doc>
    <id>62921</id>
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    <publishedYear>2025</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
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    <title language="eng">Comparison of Commercially Available SIBs: Linking Material and Electrode Properties to Cell Performance</title>
    <abstract language="eng">As the first commercial sodium-ion-batteries (SIBs) are available for purchase, it is possible to investigate material composition. Gaining an insight into the material composition of these SIBs is of interest not only for the classification of possible safety risks and hazards, but also in regards to recycling. Herein we report the preliminary investigations of the chemical and structural composition of first commercial SIB-cells. Two different SIB-cell types were compared in terms of electrode size, thickness, loading etc. Furthermore, the composition of the active materials and electrolyte was investigated and compared. Finally, the gained results were linked to the different data sheet performance of the two cell types.</abstract>
    <enrichment key="eventName">Batterieforum 2025</enrichment>
    <enrichment key="eventPlace">Berlin, Germany</enrichment>
    <enrichment key="eventStart">21.01.2025</enrichment>
    <enrichment key="eventEnd">23.01.2025</enrichment>
    <enrichment key="opus.source">publish</enrichment>
    <author>Luise Sander</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Battery</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Sodium-Ion-Battery</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Electrochemical Energy Storage</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Energy Storage</value>
    </subject>
    <collection role="ddc" number="621">Angewandte Physik</collection>
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    <collection role="institutes" number="">3.1 Sicherheit von Gefahrgutverpackungen und Batterien</collection>
    <collection role="institutes" number="">6 Materialchemie</collection>
    <collection role="institutes" number="">6.1 Oberflächen- und Dünnschichtanalyse</collection>
    <collection role="institutes" number="">6.3 Strukturanalytik</collection>
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    <collection role="themenfelder" number="">Elektrische Energiespeicher und -umwandlung</collection>
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  </doc>
  <doc>
    <id>61998</id>
    <completedYear/>
    <publishedYear>2024</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst/>
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    <completedDate>--</completedDate>
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    <title language="eng">Synthetic Carbon Anodes for SIBs</title>
    <abstract language="eng">Hard carbon (HC) is currently one of the most promising anode materials for sodium-ion batteries (SIBs). However, the Na storage mechanism remains controversial, leaving the theoretical limits carbon anodes unclear. To deconvolute the specific capacity from irreversible capacity losses resulting from the formation of solid electrolyte interphase (SEI), core-shell carbon materials with tailored pore structure and defined surface functionalities are synthesized. Meanwhile, these synthetic designer carbons could achieve more competitive capacities for use as better anodes for SIBs.</abstract>
    <enrichment key="eventName">Adlershofer Forschungsforum (AFF)</enrichment>
    <enrichment key="eventPlace">Berlin, Germany</enrichment>
    <enrichment key="eventStart">11.11.2024</enrichment>
    <enrichment key="eventEnd">11.11.2024</enrichment>
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    <author>Shu-Han Wu</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Na-ion Battery</value>
    </subject>
    <collection role="ddc" number="621">Angewandte Physik</collection>
    <collection role="institutes" number="">3 Gefahrgutumschließungen; Energiespeicher</collection>
    <collection role="institutes" number="">6 Materialchemie</collection>
    <collection role="institutes" number="">6.1 Oberflächen- und Dünnschichtanalyse</collection>
    <collection role="institutes" number="">6.5 Synthese und Streuverfahren nanostrukturierter Materialien</collection>
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  <doc>
    <id>64037</id>
    <completedYear/>
    <publishedYear>2025</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst/>
    <pageLast/>
    <pageNumber/>
    <edition/>
    <issue/>
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    <type>lecture</type>
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    <title language="eng">Coupling Single Atom Electrocatalysts with a Bioreactor for CO2 to C2+ Conversion</title>
    <abstract language="eng">To alleviate CO2 emissions impact on climate change, and close the carbon cycle, converting carbon dioxide into valuable products such as multi-carbon organic chemicals is of great importance. Each approach offers distinct merits but also certain challenges in terms of process efficiency, product selectivity and implementation at scale. Developing coupled CO2 conversion systems, for instance bio-electrochemical reactors, can address some of the challenges.[1] Precious-metal free biocompatible single atoms in N-doped C (M-N-C, where M = Fe, Ni, Co) electrocatalysts, based on Mg active site imprinting of bioinspired MN4 sites,[2][3] have shown state-of-the-art activity and selectivity for conversion of CO2 to CO.[4] Pyrolysis of Mg-N-C is carried out in a salt-melt at high temperatures (≥ 800 oC) and followed by an exchange with stoichiometric amounts of Ni or Co at low temperatures. N2-sorption of the materials reveal a micro-mesoporous structure with high surface areas (&gt; 1000 m2 g-1) and a mass-transport enabling pore system. Extended X-ray absorption fine structure reveal the existence of atomically dispersed single atom active sites with defined active site structure. These catalysts were implemented in a home-made bio-electrocatalytic system (BES) consisting of a bioreactor coupled to a CO2 electrolysis cell.[5] Here, CO2 is first electrochemically converted to CO in the electrolysis cell which is then directly fed to bacteria (Clostridium ragsdalei) in the bioreactor which further metabolize it to valuable carbon compounds, such as acetate. An acetate formation rate of 1.8 mg L-1 h-1 was achieved and an acetate concentration of 0.103 g L-1, corresponding to acetate formation rate of 0.73 mmol d-1. We have successfully demonstrated the validity of a coupled bio-electrocatalytic system operating with resource efficient single atom Co- and Ni-N-C electrocatalysts for CO2 conversion.</abstract>
    <enrichment key="eventName">Electrifying Organic Synthesis</enrichment>
    <enrichment key="eventPlace">Mülheim an der Ruhr, Germany</enrichment>
    <enrichment key="eventStart">03.09.2025</enrichment>
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    <author>Angus Pedersen</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Single atom</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Electrochemical CO2 conversion</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Bioelectrolysis</value>
    </subject>
    <collection role="ddc" number="621">Angewandte Physik</collection>
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    <collection role="institutes" number="">3.6 Elektrochemische Energiematerialien</collection>
  </doc>
  <doc>
    <id>65644</id>
    <completedYear/>
    <publishedYear>2026</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
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    <title language="eng">MOF-derived Synthetic Carbon Anode Materials for Sodium-Ion Batteries</title>
    <abstract language="eng">Metal-organic frameworks (MOFs), particularly the zeolitic imidazolate framework (ZIF) family, are attractive precursors for advanced energy-storage materials. Upon pyrolysis, ZIFs can be transformed into electrically conductive carbon materials while preserving their original particle morphology, which is crucial for achieving high-performance sodium-ion battery anodes. Despite these advantages, large-scale implementation remains challenging due to the need for synthesis routes that balance performance, cost, and sustainability. The present study addresses these challenges by developing environmentally benign and economically feasible strategies for the scalable production of ZIF-8-derived carbon anodes suitable for industrial applications.</abstract>
    <enrichment key="eventName">Batterieforum Deutschland 2026</enrichment>
    <enrichment key="eventPlace">Berlin, Germany</enrichment>
    <enrichment key="eventStart">20.01.2026</enrichment>
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    <author>Shu-Han Wu</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Sodium-ion battery</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Negative electrode</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Metalorganic frameworks</value>
    </subject>
    <collection role="ddc" number="621">Angewandte Physik</collection>
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    <language>eng</language>
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    <volume>42</volume>
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    <publisherName>Elsevier Ltd.</publisherName>
    <publisherPlace>Amsterdam</publisherPlace>
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    <title language="eng">Chemically complex materials enable sustainable high-performance materials</title>
    <abstract language="eng">Chemically complex materials (CCMats) 􀀀 including high-entropy alloys, oxides, and related multi-principal element systems 􀀀 offer a paradigm shift in materials design by leveraging chemical diversity to simultaneously optimize functional, structural, and sustainability criteria. The vastness of the compositional and structural space in CCMats propels the field into an expanding exploratory state. To reconcile functional and structural performance across this immense parameter space remains an open challenge. This Perspective evaluates the opportunities and challenges associated with harnessing chemical complexity across a broad spectrum of applications, such as hydrogen storage, ionic conductors, catalysis, magnetics, dielectrics, semiconductors, optical materials, and multifunctional structural systems. It is delineated how three central design strategies: targeted substitution (SUB), defect engineering (DEF), and diversity management (DIV) enable the reconciliation of high functional performance with long-term structural stability and environmental responsibility.&#13;
Advances in computational thermodynamics, microstructure simulations, machine learning, and multimodal characterization are accelerating the exploration and optimization of CCMats, while robust data infrastructures and automated synthesis workflows are emerging as essential tools for navigating their complex compositional space. By fostering cross-disciplinary knowledge transfer and embracing data-driven design, CCMats are poised to deliver next-generation materials solutions that address urgent technological, energy, and&#13;
environmental demands.</abstract>
    <parentTitle language="eng">Current Opinion in Solid State and Materials Science</parentTitle>
    <identifier type="url">https://www.sciencedirect.com/science/article/pii/S1359028626000033?via%3Dihub</identifier>
    <identifier type="issn">1359-0286</identifier>
    <identifier type="doi">10.1016/j.cossms.2026.101256</identifier>
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    <author>Tilmann Hickel</author>
    <author>Anja Waske</author>
    <author>Ali Tehranchi</author>
    <author>Biswajit Bhattacharya</author>
    <author>Tomasz M. Stawski</author>
    <author>Tim-Patrick Fellinger</author>
    <author>Asad Mehmood</author>
    <author>Julia Witt</author>
    <author>Ozlem Ozcan</author>
    <author>Ana Guilherme Buzanich</author>
    <author>Sourabh Kumar</author>
    <author>Rajesh Kumar Mishra</author>
    <author>Marco Holzer</author>
    <author>Andrea Simone Stucchi de Camargo</author>
    <author>Leonardo Agudo Jácome</author>
    <author>Anna Manzoni</author>
    <author>Andrea Fantin</author>
    <author>Elisabeth John</author>
    <author>Vasile-Dan Hodoroaba</author>
    <author>Sophia Bührig</author>
    <author>Jegatheesan Murugan</author>
    <author>Niklas Marschall</author>
    <author>Janine George</author>
    <author>Reza Darvishi Kamachali</author>
    <author>Robert Maaß</author>
    <author>Franziska Emmerling</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Chemically complex materials</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Structural stability</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Functional performance</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Design strategies</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Sustainability</value>
    </subject>
    <collection role="ddc" number="620">Ingenieurwissenschaften und zugeordnete Tätigkeiten</collection>
    <collection role="institutes" number="">3 Gefahrgutumschließungen; Energiespeicher</collection>
    <collection role="institutes" number="">5 Werkstofftechnik</collection>
    <collection role="institutes" number="">5.1 Mikrostruktur Design und Degradation</collection>
    <collection role="institutes" number="">5.5 Materialmodellierung</collection>
    <collection role="institutes" number="">5.6 Glas</collection>
    <collection role="institutes" number="">6 Materialchemie</collection>
    <collection role="institutes" number="">6.1 Oberflächen- und Dünnschichtanalyse</collection>
    <collection role="institutes" number="">6.2 Material- und Oberflächentechnologien</collection>
    <collection role="institutes" number="">6.3 Strukturanalytik</collection>
    <collection role="institutes" number="">6.4 Materialinformatik</collection>
    <collection role="institutes" number="">6.6 Digitale Materialchemie</collection>
    <collection role="themenfelder" number="">Material</collection>
    <collection role="literaturgattung" number="">Verlagsliteratur</collection>
    <collection role="fulltextaccess" number="">Datei für die Öffentlichkeit verfügbar ("Open Access")</collection>
    <collection role="unnumberedseries" number="">Wissenschaftliche Artikel der BAM</collection>
    <collection role="institutes" number="">5.0 Abteilungsleitung und andere</collection>
    <collection role="institutes" number="">6.0 Abteilungsleitung und andere</collection>
    <collection role="themenfelder" number="">Materialdesign</collection>
    <collection role="institutes" number="">3.6 Elektrochemische Energiematerialien</collection>
    <thesisPublisher>Bundesanstalt für Materialforschung und -prüfung (BAM)</thesisPublisher>
    <file>https://opus4.kobv.de/opus4-bam/files/65559/CCmat_perspective_2026.pdf</file>
  </doc>
</export-example>
