<?xml version="1.0" encoding="utf-8"?>
<export-example>
  <doc>
    <id>46455</id>
    <completedYear/>
    <publishedYear>2018</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst>630</pageFirst>
    <pageLast>639</pageLast>
    <pageNumber/>
    <edition/>
    <issue>6</issue>
    <volume>74</volume>
    <type>article</type>
    <publisherName>International Union of Crystallography</publisherName>
    <publisherPlace/>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>1</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Blind lattice-parameter determination of cubic and tetragonal phases with high accuracy using a single EBSD pattern</title>
    <abstract language="eng">The Bravais lattices and their lattice parameters are blindly determined using electron backscatter diffraction (EBSD) patterns of materials with cubic or tetragonal crystal structures. Since the geometric relationships in a single EBSD pattern are overdetermined, the relative errors of determining the lattice parameters as well as the axial ratios are confined to about 0.7 ± 0.4% and 0.07 ± 0.03%, respectively, for ideal simulated EBSD patterns. The accuracy of the crystal orientation determination reaches about 0.06 ± 0.03°. With careful manual band detection, the accuracy of determining lattice parameters from experimental patterns can be as good as from simulated patterns, although the results from simulated patterns are often better than expermental patterns, which are lower quality and contain uncertain systematic errors. The reasonably high accuracy is obtained primarily because the detection of the diffracting-plane traces and zone axes is relatively accurate. The results here demonstrate that the developed procedure based on the EBSD technique presents a reliable tool for crystallographic characterization of the Bravais lattices of unknown phases.</abstract>
    <parentTitle language="eng">Acta Crystallographia</parentTitle>
    <identifier type="doi">10.1107/S2053273318010963</identifier>
    <identifier type="issn">2053-2733</identifier>
    <enrichment key="date_peer_review">05.11.2018</enrichment>
    <author>Gert Nolze</author>
    <author>M. Han</author>
    <author>C. Chen</author>
    <author>G. Zhao</author>
    <author>L. Li</author>
    <author>B. Yo</author>
    <author>X. Huang</author>
    <author>Y. Zhu</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>EBSD</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Bravais lattice</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Lattice parameters</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Kikuchi pattern</value>
    </subject>
    <collection role="ddc" number="543">Analytische Chemie</collection>
    <collection role="literaturgattung" number="">Verlagsliteratur</collection>
    <collection role="fulltextaccess" number="">Datei im Netzwerk der BAM verfügbar ("Closed Access")</collection>
  </doc>
  <doc>
    <id>1661</id>
    <completedYear/>
    <publishedYear>2002</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst>163</pageFirst>
    <pageLast>170</pageLast>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume>114</volume>
    <type>article</type>
    <publisherName>Elsevier</publisherName>
    <publisherPlace>Amsterdam</publisherPlace>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>1</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Enhanced Lewis acidity by aliovalent cation doping in metal fluorides</title>
    <abstract language="eng">A model regarding the generation of acidity in binary metal fluorides has been proposed and its validity has been examined for several binary fluoride systems with the general compositions MF3/M'F3 and MF2/M'F3. In accordance with this hypothesis, the binary systems (CrF3/AlF3, CrF3/FeF3 and AlF3/VF3) do not show acidities larger than the sum of the acidities of the component fluorides. The hypothesis predicts the generation of Lewis acidity when MF2 is the major component (host) and generation of Brønsted acidity when MF3 acts as the host for the MF2/M'F3. The experimental results (surface acidity and catalytic activity) confirmed the predictions made from this hypothesis for binary combinations MgF2/ M'F3 (M'=Cr, Al, Fe, V). The application of this model is discussed in terms of other parameters: ionic radii and the fluoride affinity of the metal fluorides involved.</abstract>
    <parentTitle language="eng">Journal of fluorine chemistry</parentTitle>
    <identifier type="old">1497</identifier>
    <identifier type="doi">10.1016/S0022-1139(02)00022-2</identifier>
    <identifier type="issn">0022-1139</identifier>
    <identifier type="issn">1873-3328</identifier>
    <enrichment key="bibliotheksstandort">Sonderstandort: Publica-Schrank</enrichment>
    <enrichment key="date_peer_review">07.11.2002</enrichment>
    <author>E. Kemnitz</author>
    <author>Y. Zhu</author>
    <author>Burkart Adamczyk</author>
    <collection role="literaturgattung" number="">Verlagsliteratur</collection>
    <collection role="fulltextaccess" number="">Physisches Exemplar in der Bibliothek der BAM vorhanden ("Hardcopy Access")</collection>
  </doc>
  <doc>
    <id>39394</id>
    <completedYear/>
    <publishedYear>2017</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst>Tech. Suppl. 2017, 08008, 1</pageFirst>
    <pageLast>47</pageLast>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume>54</volume>
    <type>article</type>
    <publisherName>IOP Publishing</publisherName>
    <publisherPlace>Bristol, UK</publisherPlace>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>1</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Report of the CCQM-K123: trace elements in biodiesel fuel</title>
    <abstract language="eng">The CCQM-K123 key comparison was organized by the Inorganic Analysis Working Group (IAWG) of CCQM to assess and document the capabilities of the national metrology institutes (NMIs) or the designated institutes (DIs) to measure the mass fractions of sodium, calcium, potassium, magnesium phosphorous and sulfur in biodiesel fuel (BDF). The National Metrology Institute of Japan (NMIJ) and National Institute of Standards and Technology (NIST) acted as the coordinating laboratories.&#13;
Results were submitted by 11 NMIs and DIs. The participants used different measurement methods, though most of them used inductively coupled plasma-mass spectrometry (ICP-MS), isotope dilution technique with ICP-MS and inductively coupled plasma-optical emission spectrometry (ICP-OES) with microwave acid digestion.&#13;
The material was quite challenging and a number of questions were raised at the IAWG meeting. Concerning S, the variation in S results between participants, particularly those using IDMS methods was discussed at the IAWG meeting. BAM, NIST and NMIJ reviewed their experimental conditions, results and/or uncertainty calculations for IDMS. According to the additional evaluation and investigation, the variances between the revised results became smaller than the original one, the revised results were overlapping between IDMS measurements of S content at the k=2 level. It is not possible to calculate a KCRV with values being modified after submission. It was concluded that this KC does not support S measurements.&#13;
Accounting for relative expanded uncertainty, comparability of measurement results for each of Na, Ca, K, Mg and P was successfully demonstrated by the participating NMIs or DIs. It is expected that sodium, calcium, potassium, magnesium and phosphorus at mass fractions greater than approximately 0.1 mg/kg, 0.1 mg/kg, 0.05 mg/kg, 0.05 mg/kg and 0.1 mg/kg respectively in biodiesel fuel and similar matrices (fuels and oils etc.) can be determined by each participant using the same technique(s) employed for this key comparison to achieve similar uncertainties mentioned in the present report. Furthermore, the results of this key comparison can be utilized along with the IAWG core capability approach.</abstract>
    <parentTitle language="eng">Metrologia</parentTitle>
    <identifier type="doi">10.1088/0026-1394/54/1A/08008</identifier>
    <identifier type="url">http://iopscience.iop.org/article/10.1088/0026-1394/54/1A/08008/meta</identifier>
    <identifier type="issn">0026-1394</identifier>
    <identifier type="issn">1681-7575</identifier>
    <identifier type="urn">urn:nbn:de:kobv:b43-393941</identifier>
    <enrichment key="date_peer_review">15.03.2018</enrichment>
    <licence>Creative Commons - Namensnennung 3.0</licence>
    <author>T. Kuroiwa</author>
    <author>Y. Zhu</author>
    <author>K. Inagaki</author>
    <author>S. Long</author>
    <author>S. Christopher</author>
    <author>M. Puelles</author>
    <author>M. Porinsky</author>
    <author>N. Hatamleh</author>
    <author>J. Murby</author>
    <author>J. Merrick</author>
    <author>I. White</author>
    <author>D. Saxby</author>
    <author>R. Caciano de Sena</author>
    <author>M. Dominguez de Almeida</author>
    <author>Jochen Vogl</author>
    <author>Pranee Phukphatthanachai</author>
    <author>W.-H. Fung</author>
    <author>H.-P. Yau</author>
    <author>T. O. Okumu</author>
    <author>J. N. Kang'iri</author>
    <author>J. A. S. Tellez</author>
    <author>E. Z. Campos</author>
    <author>E. C. Galvan</author>
    <author>N. Kaewkhomdee</author>
    <author>S. Taebunpakul</author>
    <author>U. Thiengmanee</author>
    <author>C. Yafa</author>
    <author>N. Tokman</author>
    <author>M. Tunc</author>
    <author>S. Z. Can</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Biodiesel</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Fuel</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Sulphur</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Reference measurement</value>
    </subject>
    <collection role="ddc" number="543">Analytische Chemie</collection>
    <collection role="ddc" number="621">Angewandte Physik</collection>
    <collection role="literaturgattung" number="">Verlagsliteratur</collection>
    <collection role="fulltextaccess" number="">Datei für die Öffentlichkeit verfügbar ("Open Access")</collection>
    <collection role="unnumberedseries" number="">Wissenschaftliche Artikel der BAM</collection>
    <thesisPublisher>Bundesanstalt für Materialforschung und -prüfung (BAM)</thesisPublisher>
    <file>https://opus4.kobv.de/opus4-bam/files/39394/CCQM-K123.pdf</file>
  </doc>
  <doc>
    <id>57264</id>
    <completedYear/>
    <publishedYear>2023</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst>1</pageFirst>
    <pageLast>24</pageLast>
    <pageNumber/>
    <edition/>
    <issue>3</issue>
    <volume>15</volume>
    <type>article</type>
    <publisherName>MDPI</publisherName>
    <publisherPlace>Basel, Schweiz</publisherPlace>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>1</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Efficient Purification of Cowpea Chlorotic Mottle Virus by a Novel Peptide Aptamer</title>
    <abstract language="eng">The cowpea chlorotic mottle virus (CCMV) is a plant virus explored as a nanotechnological platform. The robust self-assembly mechanism of its capsid protein allows for drug encapsulation and targeted delivery. Additionally, the capsid nanoparticle can be used as a programmable platform to display different molecular moieties. In view of future applications, efficient production and purification of plant viruses are key steps. In established protocols, the need for ultracentrifugation is a significant limitation due to cost, difficult scalability, and safety issues. In addition, the purity of the final virus isolate often remains unclear. Here, an advanced protocol for the purification of the CCMV from infected plant tissue was developed, focusing on efficiency, economy, and final purity. The protocol involves precipitation with PEG 8000, followed by affinity extraction using a novel peptide aptamer. The efficiency of the protocol was validated using size exclusion chromatography, MALDI-TOF mass spectrometry, reversed-phase HPLC, and sandwich immunoassay. Furthermore, it was demonstrated that the final eluate of the affinity column is of exceptional purity (98.4%) determined by HPLC and detection at 220 nm. The scale-up of our proposed method seems to be straightforward, which opens the way to the large-scale production of such nanomaterials. This highly improved protocol may facilitate the use and implementation of plant viruses as nanotechnological platforms for in vitro and in vivo applications.</abstract>
    <abstract language="deu">Das Cowpea Chlorotic Mottle Virus (CCMV) ist ein Pflanzenvirus, das als nanotechnologische Plattform erforscht wird. Der robuste Selbstorganisationsmechanismus seines Kapsidproteins ermöglicht die Verkapselung und gezielte Abgabe von Medikamenten. Darüber hinaus kann das Kapsid-Nanopartikel als programmierbare Plattform für die Präsentation verschiedener molekularer Komponenten verwendet werden. Im Hinblick auf künftige Anwendungen ist eine effiziente Produktion und Reinigung von Pflanzenviren von entscheidender Bedeutung. In etablierten Protokollen stellt die notwendige Ultrazentrifugation aufgrund von Kosten, schwieriger Skalierbarkeit und Sicherheitsaspekten eine erhebliche Einschränkung dar. Darüber hinaus bleibt die Reinheit des endgültigen Virusisolats oft unklar. Hier wurde ein fortschrittliches Protokoll für die Reinigung von CCMV aus infiziertem Pflanzengewebe entwickelt, wobei der Schwerpunkt auf Effizienz, Wirtschaftlichkeit und Reinheit lag. Das Protokoll beinhaltet eine Fällung mit Polyethylenglycol (PEG 8000), gefolgt von einer Affinitätsextraktion mit einem neuartigen Peptid-Aptamer. Die Effizienz des Protokolls wurde mithilfe von Größenausschluss-Chromatographie (SEC), MALDI-TOF-Massenspektrometrie, Umkehrphasen-HPLC und Sandwich-Immunoassay validiert. Darüber hinaus wurde nachgewiesen, dass das endgültige Eluat der Affinitätssäule eine außergewöhnliche Reinheit (98,4 %) aufweist, die durch HPLC und Detektion bei 220 nm bestimmt wurde. Die Skalierung der von uns vorgeschlagenen Methode scheint einfach zu sein, was den Weg für eine größer angelegte Produktion solcher Nanomaterialien ebnet. Dieses stark verbesserte Protokoll könnte die Verwendung und Umsetzung von Pflanzenviren als nanotechnologische Plattformen für In-vitro- und In-vivo-Anwendungen erleichtern.</abstract>
    <parentTitle language="eng">Viruses</parentTitle>
    <identifier type="doi">10.3390/v15030697</identifier>
    <identifier type="urn">urn:nbn:de:kobv:b43-572645</identifier>
    <enrichment key="opus.source">publish</enrichment>
    <enrichment key="opus.doi.autoCreate">false</enrichment>
    <enrichment key="opus.urn.autoCreate">true</enrichment>
    <enrichment key="date_peer_review">03.04.2023</enrichment>
    <licence>Creative Commons - CC BY - Namensnennung 4.0 International</licence>
    <author>Georg Tscheuschner</author>
    <author>Marco Ponader</author>
    <author>Christopher Raab</author>
    <author>Prisca S. Weider</author>
    <author>Reni Hartfiel</author>
    <author>Jan Ole Kaufmann</author>
    <author>Jule L. Völzke</author>
    <author>Gaby Bosc-Bierne</author>
    <author>Carsten Prinz</author>
    <author>T. Schwaar</author>
    <author>Paul Andrle</author>
    <author>Henriette Bäßler</author>
    <author>Khoa Nguyen</author>
    <author>Y. Zhu</author>
    <author>A. S. J. S. Mey</author>
    <author>A. Mostafa</author>
    <author>I. Bald</author>
    <author>Michael G. Weller</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Affinity chromatography</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Nanoparticles</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Nanoscience</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Carrier protein</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Encapsulation</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Combinatorial peptide library</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Peptide binder</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Vigna unguiculata</value>
    </subject>
    <subject>
      <language>deu</language>
      <type>uncontrolled</type>
      <value>Augenbohne</value>
    </subject>
    <subject>
      <language>deu</language>
      <type>uncontrolled</type>
      <value>Schlangenbohne</value>
    </subject>
    <subject>
      <language>deu</language>
      <type>uncontrolled</type>
      <value>Pflanzenvirus</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Plant virus</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Upscaling</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Commercialization</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Reference material</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Nanocarrier</value>
    </subject>
    <collection role="ddc" number="620">Ingenieurwissenschaften und zugeordnete Tätigkeiten</collection>
    <collection role="institutes" number="">1 Analytische Chemie; Referenzmaterialien</collection>
    <collection role="institutes" number="">1.5 Proteinanalytik</collection>
    <collection role="institutes" number="">1.8 Umweltanalytik</collection>
    <collection role="institutes" number="">6 Materialchemie</collection>
    <collection role="institutes" number="">6.3 Strukturanalytik</collection>
    <collection role="themenfelder" number="">Material</collection>
    <collection role="literaturgattung" number="">Verlagsliteratur</collection>
    <collection role="fulltextaccess" number="">Datei für die Öffentlichkeit verfügbar ("Open Access")</collection>
    <collection role="unnumberedseries" number="">Wissenschaftliche Artikel der BAM</collection>
    <collection role="themenfelder" number="">Advanced Materials</collection>
    <thesisPublisher>Bundesanstalt für Materialforschung und -prüfung (BAM)</thesisPublisher>
    <file>https://opus4.kobv.de/opus4-bam/files/57264/Tscheuschner-2023-Viruses.pdf</file>
    <file>https://opus4.kobv.de/opus4-bam/files/57264/Tscheuschner-2023-Viruses Supplement Text.pdf</file>
    <file>https://opus4.kobv.de/opus4-bam/files/57264/Tscheuschner-2023-Viruses Supplement.zip</file>
  </doc>
</export-example>
