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    <id>56803</id>
    <completedYear/>
    <publishedYear>2023</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
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    <pageNumber/>
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    <type>researchdata</type>
    <publisherName>Zenodo</publisherName>
    <publisherPlace>Geneva</publisherPlace>
    <creatingCorporation>Bundesanstalt für Materialforschung und -prüfung (BAM)</creatingCorporation>
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    <title language="eng">Small-angle scattering data analysis round robin - Anonymized results, figures and Jupyter notebook</title>
    <abstract language="eng">The intent of this round robin was to find out how comparable results from different researchers are, who analyse exactly the same processed, corrected dataset.&#13;
&#13;
This zip file contains the anonymized results and the jupyter notebook used to do the data processing, analysis and visualisation. Additionally, TEM images of the samples are included.</abstract>
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    <licence>Creative Commons - CC BY - Namensnennung 4.0 International</licence>
    <author>Brian Richard Pauw</author>
    <author>Glen Jacob Smales</author>
    <author>Julian Rosalie</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Round robin</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Small-angle scattering</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Data analysis</value>
    </subject>
    <collection role="ddc" number="543">Analytische Chemie</collection>
    <collection role="institutes" number="">5 Werkstofftechnik</collection>
    <collection role="institutes" number="">5.1 Mikrostruktur Design und Degradation</collection>
    <collection role="institutes" number="">6 Materialchemie</collection>
    <collection role="institutes" number="">6.5 Synthese und Streuverfahren nanostrukturierter Materialien</collection>
    <collection role="themenfelder" number="">Chemie und Prozesstechnik</collection>
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    <collection role="literaturgattung" number="">Graue Literatur</collection>
    <collection role="unnumberedseries" number="">Forschungsdatensätze der BAM</collection>
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  <doc>
    <id>56459</id>
    <completedYear/>
    <publishedYear>2022</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst>1</pageFirst>
    <pageLast>8</pageLast>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume/>
    <type>article</type>
    <publisherName>Wiley-VCH</publisherName>
    <publisherPlace>Weinheim</publisherPlace>
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    <completedDate>--</completedDate>
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    <title language="eng">Entering a new dimension in powder processing for advanced ceramics shaping</title>
    <abstract language="eng">Filigree structures can be manufactured via two-photon-polymerization (2PP) operating in the regime of non-linear light absorption. For the first time it is possible to apply this technique to the powder processing of ceramic structures with a feature size in the range of the critical defect size responsible for brittle fracture and, thus, affecting fracture toughness of high-performance ceramics. In this way, tailoring of advanced properties can be achieved already in the shaping process. Traditionally, 2PP relies on transparent polymerizable resins, which is diametrically opposed to the usually completely opaque ceramic resins and slurries. Here we present a transparent and photocurable suspension of nanoparticles (resin) with very high mass fractions of yttria-stabilized zirconia particles (YSZ). Due to the extremely well dispersed nanoparticles, scattering of light can be effectively suppressed at the process-relevant wavelength of 800 nm. Sintered ceramic structures with a resolution of down to 500 nm were obtained. Even at reduced densities of 1 to 4 g/cm³, the resulting compressive strength with 4,5 GPa is equivalent or even exceeding bulk monolithic yttria stabilized zirconia. A ceramic metamaterial is born, where the mechanical properties of yttria stabilized zirconia are altered by changing geometrical parameters and gives access to a new class of ceramic materials.</abstract>
    <parentTitle language="eng">Advanced materials</parentTitle>
    <identifier type="doi">10.1002/adma.202208653</identifier>
    <identifier type="issn">1521-4095</identifier>
    <identifier type="urn">urn:nbn:de:kobv:b43-564598</identifier>
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    <enrichment key="date_peer_review">05.12.2022</enrichment>
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    <licence>Creative Commons - CC BY - Namensnennung 4.0 International</licence>
    <author>Johanna Christiane Sänger</author>
    <author>Brian Richard Pauw</author>
    <author>Birte Riechers</author>
    <author>Andrea Zocca</author>
    <author>Julian Rosalie</author>
    <author>Robert Maaß</author>
    <author>Heinz Sturm</author>
    <author>Jens Günster</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Two-photon-polymerization</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Ceramics</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Powder processing</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Transparency</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Meta material</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Yttria stabilized zirconia</value>
    </subject>
    <collection role="ddc" number="620">Ingenieurwissenschaften und zugeordnete Tätigkeiten</collection>
    <collection role="institutes" number="">5 Werkstofftechnik</collection>
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    <collection role="literaturgattung" number="">Verlagsliteratur</collection>
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    <collection role="unnumberedseries" number="">Wissenschaftliche Artikel der BAM</collection>
    <collection role="themenfelder" number="">Advanced Materials</collection>
    <thesisPublisher>Bundesanstalt für Materialforschung und -prüfung (BAM)</thesisPublisher>
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  <doc>
    <id>58709</id>
    <completedYear/>
    <publishedYear>2023</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst>1618</pageFirst>
    <pageLast>1629</pageLast>
    <pageNumber/>
    <edition/>
    <issue>6</issue>
    <volume>56</volume>
    <type>article</type>
    <publisherName>Wiley-Blackwell</publisherName>
    <publisherPlace>Oxford</publisherPlace>
    <creatingCorporation>International Union of Crystallography (IUCr)</creatingCorporation>
    <contributingCorporation/>
    <belongsToBibliography>1</belongsToBibliography>
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    <title language="eng">The human factor - Results of a small-angle scattering data analysis round robin</title>
    <abstract language="eng">A round-robin study has been carried out to estimate the impact of the human element in small-angle scattering data analysis. Four corrected datasets were provided to participants ready for analysis. All datasets were measured on samples containing spherical scatterers, with two datasets in dilute dispersions and two from powders. Most of the 46 participants correctly identified the number of populations in the dilute dispersions, with half of the population mean entries within 1.5% and half of the population width entries within 40%. Due to the added complexity of the structure factor, far fewer people submitted answers on the powder datasets. For those that did, half of the entries for the means and widths were within 44 and 86%, respectively. This round-robin experiment highlights several causes for the discrepancies, for which solutions are proposed.</abstract>
    <parentTitle language="eng">Journal of applied crystallography</parentTitle>
    <identifier type="doi">10.1107/S1600576723008324</identifier>
    <identifier type="urn">urn:nbn:de:kobv:b43-587091</identifier>
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Pauw et al.","order":0,"name":"copyright","label":"Copyright","explanation":{"URL":"https:\/\/journals.iucr.org\/services\/copyrightpolicy.html"},"group":{"name":"copyright_and_licencing","label":"Copyright and licencing"}},{"value":"Creative Commons Attribution (CC-BY)","order":1,"name":"license","label":"Licence","explanation":{"URL":"https:\/\/creativecommons.org\/licenses\/by\/4.0\/legalcode"},"group":{"name":"copyright_and_licencing","label":"Copyright and licencing"}}]}}</enrichment>
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    <licence>Creative Commons - CC BY - Namensnennung 4.0 International</licence>
    <author>Brian Richard Pauw</author>
    <author>Glen Jacob Smales</author>
    <author>A. S. Anker</author>
    <author>V. Annadurai</author>
    <author>D. M. Balazs</author>
    <author>Ralf Bienert</author>
    <author>W. G. Bouwman</author>
    <author>Ingo Breßler</author>
    <author>J. Breternitz</author>
    <author>E. S. Brok</author>
    <author>G. Bryant</author>
    <author>A. J. Clulow</author>
    <author>E. R. Crater</author>
    <author>F. De Geuser</author>
    <author>A. Del Giudice</author>
    <author>J. Deumer</author>
    <author>S. Disch</author>
    <author>S. Dutt</author>
    <author>K. Frank</author>
    <author>E. Fratini</author>
    <author>P. R. A. F. Garcia</author>
    <author>E. P. Gilbert</author>
    <author>Marc Benjamin Hahn</author>
    <author>J. Hallett</author>
    <author>M. Hohenschutz</author>
    <author>M. Hollamby</author>
    <author>S. Huband</author>
    <author>J. Ilavsky</author>
    <author>J. K. Jochum</author>
    <author>M. Juelsholt</author>
    <author>B. W. Mansel</author>
    <author>P. Penttilä</author>
    <author>R. K. Pittkowski</author>
    <author>G. Portale</author>
    <author>L. D. Pozzo</author>
    <author>L. Rochels</author>
    <author>Julian Rosalie</author>
    <author>Patrick E. J. Saloga</author>
    <author>S. Seibt</author>
    <author>A. J. Smith</author>
    <author>G. N. Smith</author>
    <author>G. A. Spiering</author>
    <author>Tomasz M. Stawski</author>
    <author>O. Taché</author>
    <author>Andreas Thünemann</author>
    <author>K. Toth</author>
    <author>A. E. Whitten</author>
    <author>J. Wuttke</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Round Robin</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Data analysis</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Small-angle scattering</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Nanomaterials</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Interlaboratory comparability</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Nanostructure quantification</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Methodology</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>MOUSE</value>
    </subject>
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    <publishedYear>2023</publishedYear>
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    <pageLast>23</pageLast>
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    <publisherName>Cornell University</publisherName>
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    <title language="eng">The human factor - Results of a small-angle scattering data analysis round robin</title>
    <abstract language="eng">A Round Robin study has been carried out to estimate the impact of the human element in small-angle scattering data analysis. Four corrected datasets were provided to participants ready for analysis. All datasets were measured on samples containing spherical scatterers, with two datasets in dilute dispersions, and two from powders.&#13;
&#13;
Most of the 46 participants correctly identified the number of populations in the dilute dispersions, with half of the population mean entries within 1.5 % and half of the population width entries within 40 %, respectively. Due to the added complexity of the structure factor, much fewer people submitted answers on the powder datasets.&#13;
&#13;
For those that did, half of the entries for the means and widths were within 44 % and 86 % respectively. This Round Robin experiment highlights several causes for the discrepancies, for which solutions are proposed.</abstract>
    <parentTitle language="eng">arXiv.org</parentTitle>
    <identifier type="doi">10.48550/arXiv.2303.03772</identifier>
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    <author>Brian Richard Pauw</author>
    <author>Glen Jacob Smales</author>
    <author>A. S. Anker</author>
    <author>D. M. Balazs</author>
    <author>F. L. Beyer</author>
    <author>Ralf Bienert</author>
    <author>W. G. Bouwman</author>
    <author>Ingo Breßler</author>
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    <author>G. Bryant</author>
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    <author>E. R. Crater</author>
    <author>F. De Geuser</author>
    <author>A. D. Giudice</author>
    <author>J. Deumer</author>
    <author>S. Disch</author>
    <author>S. Dutt</author>
    <author>K. Frank</author>
    <author>E. Fratini</author>
    <author>E. P. Gilbert</author>
    <author>Marc Benjamin Hahn</author>
    <author>J. Hallett</author>
    <author>Max Hohenschutz</author>
    <author>M. J. Hollamby</author>
    <author>S. Huband</author>
    <author>J. Ilavsky</author>
    <author>J. K. Jochum</author>
    <author>M. Juelsholt</author>
    <author>B. W. Mansel</author>
    <author>P. Penttilä</author>
    <author>R. K. Pittkowski</author>
    <author>G. Portale</author>
    <author>L. D. Pozzo</author>
    <author>P. Ricardo de Abreu Furtado Garcia</author>
    <author>L. Rochels</author>
    <author>Julian Rosalie</author>
    <author>P. E. J. Saloga</author>
    <author>S. Seibt</author>
    <author>A. J. Smith</author>
    <author>G. N. Smith</author>
    <author>V. Annadurai</author>
    <author>G. A. Spiering</author>
    <author>Tomasz Stawski</author>
    <author>O. Taché</author>
    <author>Andreas Thünemann</author>
    <author>K. Toth</author>
    <author>A. E. Whitten</author>
    <author>J. Wuttke</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Round robin</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Sall-angle scattering</value>
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    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Nanostructure quantification</value>
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    <subject>
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      <value>Nanostructure</value>
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      <value>SAXS</value>
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      <type>uncontrolled</type>
      <value>MOUSE</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>X-ray scattering</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Size distribution</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Nanoparticles</value>
    </subject>
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