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  <doc>
    <id>56075</id>
    <completedYear/>
    <publishedYear>2022</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst>1</pageFirst>
    <pageLast>11</pageLast>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume/>
    <type>conferenceobject</type>
    <publisherName/>
    <publisherPlace>Ghent, Belgium</publisherPlace>
    <creatingCorporation>OCAS</creatingCorporation>
    <contributingCorporation/>
    <belongsToBibliography>0</belongsToBibliography>
    <completedDate>--</completedDate>
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    <title language="eng">Experimental and numerical characterization of hydrogen diffusion in thick-walled submerged arc welded joint of S420G2+M offshore steel grade</title>
    <abstract language="eng">Offshore wind turbines are an important goal in national energy strategies worldwide. Foundation structures are manufactured from submerged arc welded (SAW) plates with thicknesses up to 200 mm. In that connection, high-strength steels like the S420G2+M are more and more applied offering the possibility for increased stability and load-bearing capacity of the foundations. These offshore steel grades can show a susceptibility for delayed hydrogen assisted cold cracking of the weld joints. For that purpose, a minimum waiting time (MWT) of up to 48 h (dependent on applied standards) is recommended before non-destructive testing is allowed and conducted. But this concept is based on older steel grades that have been used for three or more decades. Nowadays, the metallurgical improvements (clean steels, proper rolling, and heat treatment) of base materials and well as welding consumables must be anticipated. Hence, the MWT concept should be critically discussed as it is assumed to be very conservative. For that reason, the focus of this study was to investigate the diffusion behavior in S420G2+M steel and its multi-layer SAW joint. Electrochemical permeation experiments were carried at room temperature. Boundary conditions were anticipated in terms of using different sample thicknesses. From the experimental data, hydrogen diffusion coefficients and absorbed diffusible hydrogen concentrations had been calculated. It was shown that hydrogen diffusion in the base material is increased compared to the weld metal. In addition, the sample thickness had a significant on the calculated diffusion coefficients. The minimum and maximum diffusion coefficients had been used for numerical modelling of the hydrogen diffusion in the welding joint. It became clear that a MWT must be always regarded together with a critical initial diffusible hydrogen concentration for the evaluation of a possible delayed cracking as diffusion times were mostly &gt; 48 h due to the thick plates.</abstract>
    <parentTitle language="eng">Proceedings of the Fourth International Conference on Metals &amp; Hydrogen</parentTitle>
    <enrichment key="eventName">4th International Conference on Metals and Hydrogen - Steely &amp; Hydrogen 2022</enrichment>
    <enrichment key="eventPlace">Ghent, Belgium</enrichment>
    <enrichment key="eventStart">11.10.2022</enrichment>
    <enrichment key="eventEnd">13.10.2022</enrichment>
    <enrichment key="opus.source">publish</enrichment>
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    <author>Jonathan Nietzke</author>
    <author>Michael Rhode</author>
    <author>Tobias Mente</author>
    <author>Thomas Kannengießer</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Hydrogen</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Submerged arc welding</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Diffusion</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Minimum waiting time</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Electrochemical permeation</value>
    </subject>
    <collection role="ddc" number="620">Ingenieurwissenschaften und zugeordnete Tätigkeiten</collection>
    <collection role="institutes" number="">9 Komponentensicherheit</collection>
    <collection role="institutes" number="">9.4 Integrität von Schweißverbindungen</collection>
    <collection role="themenfelder" number="">Energie</collection>
    <collection role="themenfelder" number="">Material</collection>
    <collection role="themenfelder" number="">Degradationsmechanismen</collection>
    <collection role="fulltextaccess" number="">Datei im Netzwerk der BAM verfügbar ("Closed Access")</collection>
    <collection role="literaturgattung" number="">Graue Literatur</collection>
    <collection role="institutes" number="">9.0 Abteilungsleitung und andere</collection>
    <collection role="themenfelder" number="">Wasserstoff</collection>
  </doc>
  <doc>
    <id>55946</id>
    <completedYear/>
    <publishedYear>2022</publishedYear>
    <thesisYearAccepted/>
    <language>deu</language>
    <pageFirst>69</pageFirst>
    <pageLast>75</pageLast>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume>382</volume>
    <type>conferenceobject</type>
    <publisherName>DVS Media GmbH</publisherName>
    <publisherPlace>Düsseldorf</publisherPlace>
    <creatingCorporation>DVS Deutscher Verband für Schweißen und verwandte Verfahren e.V.</creatingCorporation>
    <contributingCorporation/>
    <belongsToBibliography>0</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
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    <title language="deu">Untersuchung von Spannungsrelaxationsrissmechanismen mittels Simulation einachsiger Spannungszustände in der Grobkornzone von UP-geschweißtem CrMoV-Stahl</title>
    <abstract language="deu">Druckbehälter mit großen Wandstärken (250+ mm) aus hochwarmfesten, niedriglegierten Stählen werden hauptsächlich Mehrdraht-Unterpulver-(UP) geschweißt. Der damit verbundene hohe Energieeintrag führt unter anderem zu hohen lokalen Schweißeigenspannungen, welche bei unsachgemäßer Prozessführung der notwendigen Wärmenachbehandlung (PWHT) zu Spannungsrelaxationsrissen (SRR) führen. In den Bewertungskriterien zur Spannungsrelaxationsrissanfälligkeit finden weder die, mit klassischen, freischrumpfenden Schweißversuchen nicht abbildbaren, erhöhten Eigenspannungen aus der Schrumpfbehinderung der Bauteilsteifigkeit Beachtung, noch die damit einhergehenden metallurgischen Effekte wie bspw. das Ausscheidungswachstum während der PWHT und damit einhergehende Härteunterschiede an den Korngrenzen bzw. die vorzeitige Alterung durch Bildung differenter Sonderkarbide. Die Aufheizrate des PWHT als Einflussfaktor für die SRR-Bildung bleibt derzeit ebenfalls unbeachtet.&#13;
Daher wurde eine Versuchsmethodik entwickelt, die eine mögliche SRR-Anfälligkeit durch die Kopplung von thermischer und mechanischer Beanspruchung untersucht. Dazu wurden Proben mit unterschiedlichen Gefügen thermisch simuliert und während des PHWT repräsentativ mit sehr hohen Lasten/Eigenspannungen mechanisch beansprucht.&#13;
Dazu wurde an Kleinzugproben für das as-welded UP-Schweißgut und die thermisch simulierte GKZ eines 13CrMoV9-10 die Dehnung des Prüfbereichs bei variablen Querspannungen und Aufheizraten gemessen. Diese aufheizraten- und gefügeabhängige Längenänderung der Probe wurde durch mathematische Prozeduren analysiert. Damit war es möglich, singuläre werkstoffliche Effekte auf μm-Ebene (Ausscheidungswachstum) als summarische Längen- bzw. Volumenänderung per klassischer Kurvendiskussion zu beschreiben. Die erste und zweite Ableitung zeigten eine ausscheidungsabhängige Härtezunahme, welche von der Spannung und Aufheizrate im geringen Maß linear abhängig war. Gleichzeitig sind Volumenänderungen bei Bildung und Wachstum differenter Sonderkarbide bekannt, welche zusammen mit gefügespezifischen Untersuchungen und der neuen Versuchsmethodik zu einer verbesserten Beurteilung der SRR-Anfälligkeit von geschweißten CrMoV-Stählen beitragen sollen. Prinzipiell ist die vorgestellte Methodik jedoch werkstoff- und zustandsoffen, d.h. sowohl für Grundwerkstoff e als auch definierte Wärmebehandlungsbedingungen geeignet. Dies ermöglicht erstmals die Schaffung einer Transfergröße zwischen Labor und realen Schweißungen, unter Beibehaltung der Bauteilsteifigkeit, d.h. vereinfachte, aber realistische Eigenspannungsabbildung als Grundlage für weitergehende gefügespezifische metallurgische Effekte während des PWHT.</abstract>
    <parentTitle language="deu">DVS Berichte 382: DVS CONGRESS 2022 Große Schweißtechnische Tagung DVS CAMPUS</parentTitle>
    <identifier type="isbn">978-3-96144-190-7</identifier>
    <enrichment key="eventName">DVS Congress 2022</enrichment>
    <enrichment key="eventPlace">Koblenz, Germany</enrichment>
    <enrichment key="eventStart">19.09.2022</enrichment>
    <enrichment key="eventEnd">21.09.2022</enrichment>
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    <author>Michael Rhode</author>
    <author>Jonathan Nietzke</author>
    <author>Denis Czeskleba</author>
    <author>Thomas Kannengießer</author>
    <subject>
      <language>deu</language>
      <type>uncontrolled</type>
      <value>UP-Schweißen</value>
    </subject>
    <subject>
      <language>deu</language>
      <type>uncontrolled</type>
      <value>Spannungsrelaxationsriss</value>
    </subject>
    <subject>
      <language>deu</language>
      <type>uncontrolled</type>
      <value>Wärmenachbehandlung</value>
    </subject>
    <subject>
      <language>deu</language>
      <type>uncontrolled</type>
      <value>Ersatzgeometrie</value>
    </subject>
    <subject>
      <language>deu</language>
      <type>uncontrolled</type>
      <value>Prüfverfahren</value>
    </subject>
    <collection role="ddc" number="620">Ingenieurwissenschaften und zugeordnete Tätigkeiten</collection>
    <collection role="institutes" number="">9 Komponentensicherheit</collection>
    <collection role="institutes" number="">9.4 Integrität von Schweißverbindungen</collection>
    <collection role="themenfelder" number="">Material</collection>
    <collection role="themenfelder" number="">Degradationsmechanismen</collection>
    <collection role="literaturgattung" number="">Verlagsliteratur</collection>
    <collection role="fulltextaccess" number="">Datei im Netzwerk der BAM verfügbar ("Closed Access")</collection>
    <collection role="institutes" number="">9.0 Abteilungsleitung und andere</collection>
  </doc>
  <doc>
    <id>56008</id>
    <completedYear/>
    <publishedYear>2022</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst/>
    <pageLast/>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume/>
    <type>poster</type>
    <publisherName/>
    <publisherPlace/>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>0</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Experimental and numerical characterization of hydrogen diffusion in thick-walled submerged arc welded joint of S420G2+M offshore steel grade</title>
    <abstract language="eng">Offshore wind turbines are an important goal in national energy strategies worldwide. Foundation structures are manufactured from submerged arc welded (SAW) plates with thicknesses up to 200 mm. In that connection, high-strength steels like the S420G2+M are more and more applied offering the possibility for increased stability and load-bearing capacity of the foundations. These offshore steel grades can show a susceptibility for delayed hydrogen assisted cold cracking of the weld joints. For that purpose, a minimum waiting time (MWT) of up to 48 h (dependent on applied standards) is recommended before non-destructive testing is allowed and conducted. But this concept is based on older steel grades that have been used for three or more decades. Nowadays, the metallurgical improvements (clean steels, proper rolling, and heat treatment) of base materials and well as welding consumables must be anticipated. Hence, the MWT concept should be critically discussed as it is assumed to be very conservative. For that reason, the focus of this study was to investigate the diffusion behavior in S420G2+M steel and its multi-layer SAW joint. Electrochemical permeation experiments were carried at room temperature. Boundary conditions were anticipated in terms of using different sample thicknesses. From the experimental data, hydrogen diffusion coefficients and absorbed diffusible hydrogen concentrations had been calculated. It was shown that hydrogen diffusion in the base material is increased compared to the weld metal. In addition, the sample thickness had a significant on the calculated diffusion coefficients. The minimum and maximum diffusion coefficients had been used for numerical modelling of the hydrogen diffusion in the welding joint. It became clear that a MWT must be always regarded together with a critical initial diffusible hydrogen concentration for the evaluation of a possible delayed cracking as diffusion times were mostly &gt; 48 h due to the thick plates.</abstract>
    <enrichment key="eventName">4th International Conference on Metals and Hydrogen - Steely &amp; Hydrogen 2022</enrichment>
    <enrichment key="eventPlace">Ghent, Belgium</enrichment>
    <enrichment key="eventStart">11.10.2022</enrichment>
    <enrichment key="eventEnd">13.10.2022</enrichment>
    <enrichment key="opus.source">publish</enrichment>
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    <enrichment key="opus.urn.autoCreate">true</enrichment>
    <author>Jonathan Nietzke</author>
    <author>Florian Konert</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Hydrogen</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Submerged arc welding</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Minimum Waiting Time</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Cold Cracking</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Offshore steel grade</value>
    </subject>
    <collection role="ddc" number="621">Angewandte Physik</collection>
    <collection role="institutes" number="">9 Komponentensicherheit</collection>
    <collection role="institutes" number="">9.4 Integrität von Schweißverbindungen</collection>
    <collection role="themenfelder" number="">Energie</collection>
    <collection role="themenfelder" number="">Material</collection>
    <collection role="themenfelder" number="">Degradationsmechanismen</collection>
    <collection role="fulltextaccess" number="">Datei im Netzwerk der BAM verfügbar ("Closed Access")</collection>
    <collection role="literaturgattung" number="">Präsentation</collection>
    <collection role="institutes" number="">9.0 Abteilungsleitung und andere</collection>
    <collection role="themenfelder" number="">Wasserstoff</collection>
  </doc>
  <doc>
    <id>57600</id>
    <completedYear/>
    <publishedYear>2023</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst>1</pageFirst>
    <pageLast>9</pageLast>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume/>
    <type>article</type>
    <publisherName>Springer Nature</publisherName>
    <publisherPlace>Basel (CH)</publisherPlace>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>1</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Investigation of stress relief crack susceptibility of CrMoV steels coarse grain HAZ via simulation of uniaxial stress conditions during PWHT</title>
    <abstract language="eng">Creep-resistant steels such as the 13CrMoV9-10, used in the construction of thick-walled pressure vessels, are most commonly submerged arc welded (SAW). These steels can develop stress relief cracks (SRC) if the mandatory post weld heat treatment (PWHT) is performed improperly. Current PWHT parameters, such as heating rate and holding time at a specific holding temperature, are based on both empirical experience and conventional free shrinking welding experiments to characterize the SRC-susceptibility of the weld. These cannot adequately depict the higher residual stresses caused by the structurally induced stiffness of the surrounding construction. This study discusses the development of a repeatable, precise, and time-efficient methodology to study the effects of different stress levels and heating rates on the SRC susceptibility of the coarse grain heat-affected zone (CGHAZ). For that purpose, samples were thermically treated to simulate a coarse grain heat-affected zone (CGHAZ) and subsequently exposed to representative levels of stress during the heating phase of a PWHT. The recorded stress and heating rate–dependent strains were mathematically analyzed via curve tracing/calculus to identify interdependent effects. This procedure facilitates the measurement of material characteristics such as carbide growth on grain boundaries at the µm-scale via an integrated value over the entire sample volume. The first and second derivatives show a slight, precipitate-dependent, increase in hardness of the sample, depending on the heating rate and applied stress. This new methodology generates an improved assessment of the SRC susceptibility of SAW microstructures of creep-resistant CrMoV steels.</abstract>
    <parentTitle language="eng">Welding in the World</parentTitle>
    <identifier type="doi">10.1007/s40194-023-01539-x</identifier>
    <identifier type="urn">urn:nbn:de:kobv:b43-576007</identifier>
    <identifier type="issn">0043-2288</identifier>
    <enrichment key="opus.source">publish</enrichment>
    <enrichment key="date_peer_review">19.06.2023</enrichment>
    <enrichment key="PaperofMonth">1</enrichment>
    <licence>Creative Commons - CC BY - Namensnennung 4.0 International</licence>
    <author>Denis Czeskleba</author>
    <author>Jonathan Nietzke</author>
    <author>Michael Rhode</author>
    <author>Thomas Kannengießer</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Submerged arc welding</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Creep-resistant steel</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Stress relief cracking</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Component-like test</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Post weld heat treatment</value>
    </subject>
    <collection role="ddc" number="543">Analytische Chemie</collection>
    <collection role="ddc" number="620">Ingenieurwissenschaften und zugeordnete Tätigkeiten</collection>
    <collection role="institutes" number="">9 Komponentensicherheit</collection>
    <collection role="institutes" number="">9.4 Integrität von Schweißverbindungen</collection>
    <collection role="themenfelder" number="">Material</collection>
    <collection role="themenfelder" number="">Degradationsmechanismen</collection>
    <collection role="themenfelder" number="">Chemie und Prozesstechnik</collection>
    <collection role="literaturgattung" number="">Verlagsliteratur</collection>
    <collection role="fulltextaccess" number="">Datei für die Öffentlichkeit verfügbar ("Open Access")</collection>
    <collection role="unnumberedseries" number="">Wissenschaftliche Artikel der BAM</collection>
    <collection role="institutes" number="">9.0 Abteilungsleitung und andere</collection>
    <thesisPublisher>Bundesanstalt für Materialforschung und -prüfung (BAM)</thesisPublisher>
    <file>https://opus4.kobv.de/opus4-bam/files/57600/Czeskleba_CrMoV_SRC_PWHT_Simulated_HAZ_050623.pdf</file>
  </doc>
  <doc>
    <id>59366</id>
    <completedYear/>
    <publishedYear>2024</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst>1</pageFirst>
    <pageLast>9</pageLast>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume/>
    <type>article</type>
    <publisherName>Springer</publisherName>
    <publisherPlace/>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>1</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">In situ measurement of hydrogen concentration in steel using laser‑induced breakdown spectroscopy (LIBS)</title>
    <abstract language="deu">The ISO 3690 standard “Determination of hydrogen content in arc weld metal” requires a thermal activation of the diffusible hydrogen in a piece of weld metal for the subsequent ex situ concentration measurement by carrier gas hot extraction CGHE or thermal desorption spectroscopy (TCD). Laser-induced breakdown spectroscopy (LIBS) offers a time and spatially resolved, almost non-destructive, in situ measurement of hydrogen at surfaces without sample preparation. We measured hydrogen in steels, which were charged either electrochemically or by high-pressure hydrogen gas, and compared the results. Further, the feasibility of quantitative hydrogen line scan measurements with LIBS was demonstrated by measuring hydrogen at water jet cut surfaces. The hydrogen concentrations measured with the help of LIBS were compared with CGHE measurements. It was observed that hydrogen can be reliably measured with LIBS for concentrations larger than 2 wt.-ppm. The maximum hydrogen concentration achieved using electrochemical charging was 85.1 ppm. The results show that LIBS is a promising technique for time- and spatially resolved measurements of hydrogen in steels.</abstract>
    <parentTitle language="eng">Welding in the World</parentTitle>
    <identifier type="doi">10.1007/s40194-023-01677-2</identifier>
    <identifier type="urn">urn:nbn:de:kobv:b43-593664</identifier>
    <enrichment key="eventName">IIW Annual Assembly 2023</enrichment>
    <enrichment key="eventPlace">Singapore</enrichment>
    <enrichment key="opus.source">publish</enrichment>
    <enrichment key="date_peer_review">05.02.2024</enrichment>
    <licence>Creative Commons - CC BY - Namensnennung 4.0 International</licence>
    <author>Lukas Quackatz</author>
    <author>Axel Griesche</author>
    <author>Jonathan Nietzke</author>
    <author>Thomas Kannengießer</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>LIBS</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Hydrogen measurement</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Welding</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Stainless steel</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Diffusible hydrogen</value>
    </subject>
    <collection role="ddc" number="621">Angewandte Physik</collection>
    <collection role="institutes" number="">9 Komponentensicherheit</collection>
    <collection role="institutes" number="">9.4 Integrität von Schweißverbindungen</collection>
    <collection role="themenfelder" number="">Energie</collection>
    <collection role="literaturgattung" number="">Verlagsliteratur</collection>
    <collection role="fulltextaccess" number="">Datei für die Öffentlichkeit verfügbar ("Open Access")</collection>
    <collection role="unnumberedseries" number="">Wissenschaftliche Artikel der BAM</collection>
    <collection role="themenfelder" number="">Wasserstoff</collection>
    <thesisPublisher>Bundesanstalt für Materialforschung und -prüfung (BAM)</thesisPublisher>
    <file>https://opus4.kobv.de/opus4-bam/files/59366/s40194-023-01677-2.pdf</file>
  </doc>
  <doc>
    <id>54412</id>
    <completedYear/>
    <publishedYear>2022</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst>1</pageFirst>
    <pageLast>13</pageLast>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume/>
    <type>article</type>
    <publisherName>Springer Nature</publisherName>
    <publisherPlace/>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>1</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Characterization of Hydrogen Diffusion in Offshore Steel S420G2+M Multi-layer Submerged Arc Welded Joint</title>
    <abstract language="eng">As onshore installation capacity is limited, the increase in the number of offshore wind turbines (OWT) is a major goal. In that connection, the OWTs continuously increase in size and weight and demand adequate foundations concepts like monopiles or tripods. These components are typically manufactured from welded mild steel plates with thickness up to 200 mm. The predominant welding technique is submerged arc welding (SAW). In accordance with the standards, the occurrence of hydrogen-assisted cracking is anticipated by either a minimum waiting time (MWT, before non-destructive testing of the welded joint is allowed) at ambient or a hydrogen removal heat treatment (HRHT) at elevated temperatures. The effectiveness of both can be estimated by calculation of the diffusion time, i.e., diffusion coefficients. In this study, these coefficients are obtained for the first time for a thick-walled S420G2+M offshore steel grade and its multi-layer SAW joint. The electrochemical permeation technique at ambient temperature is used for the determination of diffusion coefficients for both the base material and the weld metal. The coefficients are within a range of 1025 to 1024 mm2/s (whereas the weld metal had the lowest) and are used for an analytical and numerical calculation of the hydrogen diffusion and the related MWT. The results showed that long MWT can occur, which would be necessary to significantly decrease the hydrogen concentration. Weld metal diffusion coefficients at elevated temperatures were calculated from hydrogen desorption experiments by carrier gas hot extraction. They are within a range of 1023 mm2/s and used for the characterization of a HRHT dwell-time. The analytical calculation shows the same tendency of long necessary times also at elevated temperatures. That means the necessary time is strongly influenced by the considered plate thickness and the estimation of any MWT/HRHT via diffusion coefficients should be critically discussed.</abstract>
    <parentTitle language="eng">Journal of Materials Engineering and Performance</parentTitle>
    <identifier type="issn">1059-9495</identifier>
    <identifier type="doi">10.1007/s11665-022-06679-7</identifier>
    <identifier type="urn">urn:nbn:de:kobv:b43-544127</identifier>
    <enrichment key="eventName">European Congress and Exhibition on Advanced Materials and Process - Euromat 2021</enrichment>
    <enrichment key="eventPlace">Online meeting</enrichment>
    <enrichment key="eventStart">13.09.2021</enrichment>
    <enrichment key="eventEnd">17.09.2021</enrichment>
    <enrichment key="opus.source">publish</enrichment>
    <enrichment key="date_peer_review">04.04.2022</enrichment>
    <licence>Creative Commons - CC BY - Namensnennung 4.0 International</licence>
    <author>Michael Rhode</author>
    <author>Jonathan Nietzke</author>
    <author>Tobias Mente</author>
    <author>Tim Richter</author>
    <author>Thomas Kannengießer</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Thick-walled</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Hydrogen diffusion</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Offshore</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Steel</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Submerged arc welding</value>
    </subject>
    <collection role="ddc" number="620">Ingenieurwissenschaften und zugeordnete Tätigkeiten</collection>
    <collection role="ddc" number="621">Angewandte Physik</collection>
    <collection role="institutes" number="">9 Komponentensicherheit</collection>
    <collection role="institutes" number="">9.2 Versuchsanlagen und Prüftechnik</collection>
    <collection role="institutes" number="">9.4 Integrität von Schweißverbindungen</collection>
    <collection role="themenfelder" number="">Energie</collection>
    <collection role="themenfelder" number="">Material</collection>
    <collection role="literaturgattung" number="">Verlagsliteratur</collection>
    <collection role="fulltextaccess" number="">Datei für die Öffentlichkeit verfügbar ("Open Access")</collection>
    <collection role="unnumberedseries" number="">Wissenschaftliche Artikel der BAM</collection>
    <collection role="institutes" number="">9.0 Abteilungsleitung und andere</collection>
    <thesisPublisher>Bundesanstalt für Materialforschung und -prüfung (BAM)</thesisPublisher>
    <file>https://opus4.kobv.de/opus4-bam/files/54412/Rhode_et_al-2022-Journal_of_Materials_Engineering_and_Performance.pdf</file>
  </doc>
  <doc>
    <id>63143</id>
    <completedYear/>
    <publishedYear>2025</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst>1</pageFirst>
    <pageLast>17</pageLast>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume/>
    <type>article</type>
    <publisherName>Springer Nature</publisherName>
    <publisherPlace/>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>1</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Combined heating rate and restraint condition effect on stress relief cracking during PWHT of thick-walled Cr–Mo-V steel SAW joints</title>
    <abstract language="eng">Creep-resistant steels such as 13CrMoV9-10 are utilized in the manufacture of thick-walled pressure vessels and are typically joined by submerged arc welding (SAW). However, these materials are susceptible to stress relief cracking (SRC) if the required post weld heat treatment (PWHT) is not applied correctly. Existing PWHT guidelines, encompassing heating rate and dwell (or holding) time at a given temperature, are derived from a synthesis of empirical knowledge and typically free-shrinkage weld experiments to assess the susceptibility to SRC. Therefore, this study discusses the combined effect of the PWHT heating rate under free-shrinkage compared to restrained shrinkage. Welding experiments were conducted (using plates with a thickness of 25 mm) for both shrinkage conditions for a variety of heating rates and maximum temperatures. In-situ acoustic emission analysis was used to locate propagating SRCs during PWHT. Hardness measurements, mechanical property characterization (Charpy impact strength), and microstructure correlation were used to evaluate the SRC susceptibility. The results suggested that the influence of heating rate could not be directly related to SRC formation and that the initial weld microstructure prior to PWHT was more relevant in terms of very high hardness in the coarse grain heat affected zone, especially that of the last beads in the top layer of the welding sequence. This was seen in the form of random, unexpected SRC occurrence in only one specimen at a heating rate commonly used in welding practice (approximately 100 K/h). In this context, the additional effect of an external shrinkage restraint on SRC must be considered in the form of increasing mechanical loads during welding, which are typically not within the scope of welding practice. To mitigate the probability of SRC during PWHT, it is imperative to reduce the welding heat input and to restrict the structural shrinkage restraint of the weld joint.</abstract>
    <parentTitle language="eng">Welding in the World</parentTitle>
    <identifier type="doi">10.1007/s40194-025-02062-x</identifier>
    <identifier type="issn">1878-6669</identifier>
    <identifier type="urn">urn:nbn:de:kobv:b43-631439</identifier>
    <enrichment key="opus.source">publish</enrichment>
    <enrichment key="date_peer_review">21.05.2025</enrichment>
    <enrichment key="opus.doi.autoCreate">false</enrichment>
    <enrichment key="opus.urn.autoCreate">true</enrichment>
    <licence>Creative Commons - CC BY - Namensnennung 4.0 International</licence>
    <author>Michael Rhode</author>
    <author>Denis Czeskleba</author>
    <author>H. Fleißner-Rieger</author>
    <author>Jonathan Nietzke</author>
    <author>Thomas Kannengießer</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Component test</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Stress relief cracking</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>PWHT</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Creep-resistant steel</value>
    </subject>
    <collection role="ddc" number="620">Ingenieurwissenschaften und zugeordnete Tätigkeiten</collection>
    <collection role="institutes" number="">9 Komponentensicherheit</collection>
    <collection role="institutes" number="">9.1 Komponenten für Energieträger</collection>
    <collection role="institutes" number="">9.4 Integrität von Schweißverbindungen</collection>
    <collection role="themenfelder" number="">Material</collection>
    <collection role="themenfelder" number="">Degradationsmechanismen</collection>
    <collection role="literaturgattung" number="">Verlagsliteratur</collection>
    <collection role="fulltextaccess" number="">Datei für die Öffentlichkeit verfügbar ("Open Access")</collection>
    <collection role="unnumberedseries" number="">Wissenschaftliche Artikel der BAM</collection>
    <thesisPublisher>Bundesanstalt für Materialforschung und -prüfung (BAM)</thesisPublisher>
    <file>https://opus4.kobv.de/opus4-bam/files/63143/s40194-025-02062-x_online_first.pdf</file>
  </doc>
  <doc>
    <id>61190</id>
    <completedYear/>
    <publishedYear>2024</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst>772</pageFirst>
    <pageLast>782</pageLast>
    <pageNumber/>
    <edition/>
    <issue>89</issue>
    <volume>89</volume>
    <type>article</type>
    <publisherName>Elsevier B.V.</publisherName>
    <publisherPlace>Amsterdam, Netherlands</publisherPlace>
    <creatingCorporation>Hydrogen Energy Publications LLC</creatingCorporation>
    <contributingCorporation/>
    <belongsToBibliography>1</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Trapping and diffusion in high-pressure hydrogen charged CoCrFeMnNi  high entropy alloy compared to austenitic steel 316L</title>
    <abstract language="eng">High entropy alloys (HEAs) have attracted considerable research attention as potential substitute materials for austenitic steels in high-pressure hydrogen environments. The corresponding hydrogen absorption, diffusion and trapping has received less scientific attention. Therefore, the CoCrFeMnNi-HEA was investigated and compared to an austenitic steel AISI 316L. Both were subjected to high-pressure hydrogen charging at 200 bar and 1000 bar. Thermal Desorption Analysis (TDA) was used to clarify the specific desorption behavior and hydrogen trapping. For this purpose, the underlying TDA spectra were analyzed in terms of a reasonable peak deconvolution into a defined number of peaks and the activation energies for the respective and predominant hydrogen trapping sites were then calculated. Both materials show comparable hydrogen diffusivity. However, there were significant differences in the absorbed hydrogen concentrations at both charging pressures. The calculated activation energies suggest strong hydrogen trapping in the CoCrFeMnNi-HEA.</abstract>
    <parentTitle language="eng">International Journal of Hydrogen Energy</parentTitle>
    <identifier type="issn">0360-3199</identifier>
    <identifier type="doi">10.1016/j.ijhydene.2024.09.393</identifier>
    <identifier type="urn">urn:nbn:de:kobv:b43-611901</identifier>
    <enrichment key="opus.source">publish</enrichment>
    <enrichment key="date_peer_review">06.01.2025</enrichment>
    <licence>Creative Commons - CC BY - Namensnennung 4.0 International</licence>
    <author>Michael Rhode</author>
    <author>Jonathan Nietzke</author>
    <author>Tobias Mente</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>High-entropy alloy</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Hydrogen diffusion</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Trapping</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>High-pressure charging</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Thermal desorption analysis</value>
    </subject>
    <collection role="ddc" number="620">Ingenieurwissenschaften und zugeordnete Tätigkeiten</collection>
    <collection role="institutes" number="">9 Komponentensicherheit</collection>
    <collection role="institutes" number="">9.4 Integrität von Schweißverbindungen</collection>
    <collection role="themenfelder" number="">Energie</collection>
    <collection role="themenfelder" number="">Material</collection>
    <collection role="themenfelder" number="">Degradationsmechanismen</collection>
    <collection role="literaturgattung" number="">Verlagsliteratur</collection>
    <collection role="fulltextaccess" number="">Datei für die Öffentlichkeit verfügbar ("Open Access")</collection>
    <collection role="unnumberedseries" number="">Wissenschaftliche Artikel der BAM</collection>
    <collection role="institutes" number="">9.0 Abteilungsleitung und andere</collection>
    <collection role="themenfelder" number="">Wasserstoff</collection>
    <collection role="themenfelder" number="">Materialdesign</collection>
    <thesisPublisher>Bundesanstalt für Materialforschung und -prüfung (BAM)</thesisPublisher>
    <file>https://opus4.kobv.de/opus4-bam/files/61190/IJHE_HPH2_TDA_HEA_316L_Rhode_011024.pdf</file>
  </doc>
  <doc>
    <id>53322</id>
    <completedYear/>
    <publishedYear>2021</publishedYear>
    <thesisYearAccepted/>
    <language>deu</language>
    <pageFirst/>
    <pageLast/>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume/>
    <type>lecture</type>
    <publisherName/>
    <publisherPlace/>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>0</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="deu">Diffusionsmessungen in UP-Mehrlagenschweißgut als effektives Tool gegen verzögerte Kaltrissbildung in Dickblechschweißungen</title>
    <abstract language="deu">Offshore-Windenergieanlagen bilden einen zentralen Bestandteil der zukünftigen Energieerzeugung. Hierzu notwendige Gründungs- und Turmstrukturen werden vorrangig aus UP-geschweißten Blechen aus hochfesten niedriglegierten Stählen mit Dicken bis zu 200 mm hergestellt. Die großen Blechdicken begünstigen hohe Schweißeigenspannungen und lange Diffusionswege für z.B. über den Schweißprozess eingebrachten Wasserstoff. Damit steigt das Risiko für eine wasserstoffunterstützte Kaltrissbildung (WKB) an. Zum sichereren Ausschluss von WKB in den geschweißten Komponenten wird in Abhängigkeit der Nahtgröße, Wärmeeinbringung und Stahlsorte eine Mindestwartezeit (MWZ) von bis zu 48 h empfohlen, bevor die zerstörungsfreie Prüfung durchgeführt wird. Es ist allerdings offen, ob die empfohlene MWZ zu konservativ ist. Einflüsse sind hier bspw. die schwierige Bewertung des Wasserstoffdiffusionsverhaltens im heterogenen UP-Mehrlagen-Schweißgut (SG) im Vergleich zum Grundwerkstoff (GW). Zudem sind nur sehr begrenzt H-Diffusions-koeffizienten für UP-Mehrlagen-SG als Grundlage zur Abschätzung des Zeitintervalls einer möglichen verzögerten Kaltrissbildung (somit MWZ) oder auch für Nachwärmprozeduren zur Wasserstoffreduktion (keine MWZ) verfügbar. Verlässliche H-Diffusionskoeffizienten sind daher ein adäquates Tool zur Bewertung des Risikos einer verzögerten WKB. Dieser Beitrag beschreibt Untersuchungen zur Charakterisierung der Wasserstoffdiffusionsverhalten in UP-Mehrlagen-SG eines 60 mm dicken Bleches einer Offshore-Stahlgüte. Dazu wurden Proben unterschiedlicher Dicke aus dem reinen Schweißgut extrahiert und über elektrochemische Permeation und Trägergasheißextraktion im Temperaturbereich bis 400 °C sehr interessante Ergebnisse zu den korrespon-dierenden Diffusionskoeffizienten erarbeitet. Es zeigte sich, dass:&#13;
&#13;
1. Diffusionskoeffizienten bei Umgebungstemperatur als Tool zur Bewertung einer MWZ geeignet sind. Jedoch veränderte sich der Diffusionskoeffizient mit der untersuchten Probendicke um bis zu einer Größenordnung, d. h. daraus abgeleitete Wartezeiten differieren dementsprechend.&#13;
&#13;
2. Dies deutet darauf hin, dass MWZs von bis zu 48 h einerseits möglicherweise zu konservativ gewählt sind, da der Wasserstoff schneller aus der Naht diffundiert. Andererseits muss aber auch die schnellere Diffusion in weitere potenziell risskritische Nahtbereiche, wie die WEZ, berücksichtigt werden. Daher ist noch keine direkte Aussage auf eine verallgemeinerte WKB-Anfälligkeit (ja/nein) innerhalb der MWZ möglich.&#13;
&#13;
3. Im Fall einer konservativen Prävention der WKB durch Wasserstoffarmglühen (Vermeidung der MWZ) sind die Diffusionskoeffizienten bei erhöhten Temperaturen bis 400 °C zur Abschätzung der notwendigen Haltezeiten geeignet, z. B. über die numerische Simulation der Wasserstoffdiffusion.</abstract>
    <enrichment key="eventName">DVS Congress 2021</enrichment>
    <enrichment key="eventPlace">Essen, Germany</enrichment>
    <enrichment key="eventStart">14.09.2021</enrichment>
    <enrichment key="eventEnd">17.09.2021</enrichment>
    <enrichment key="opus.source">publish</enrichment>
    <enrichment key="opus.doi.autoCreate">false</enrichment>
    <enrichment key="opus.urn.autoCreate">true</enrichment>
    <enrichment key="InvitedTalks">0</enrichment>
    <author>Jonathan Nietzke</author>
    <subject>
      <language>deu</language>
      <type>uncontrolled</type>
      <value>UP-Schweißen</value>
    </subject>
    <subject>
      <language>deu</language>
      <type>uncontrolled</type>
      <value>Offshore</value>
    </subject>
    <subject>
      <language>deu</language>
      <type>uncontrolled</type>
      <value>Windturbine</value>
    </subject>
    <subject>
      <language>deu</language>
      <type>uncontrolled</type>
      <value>Wasserstoff</value>
    </subject>
    <subject>
      <language>deu</language>
      <type>uncontrolled</type>
      <value>Diffusion</value>
    </subject>
    <collection role="ddc" number="621">Angewandte Physik</collection>
    <collection role="ddc" number="624">Ingenieurbau</collection>
    <collection role="institutes" number="">9 Komponentensicherheit</collection>
    <collection role="institutes" number="">9.4 Integrität von Schweißverbindungen</collection>
    <collection role="themenfelder" number="">Energie</collection>
    <collection role="themenfelder" number="">Infrastruktur</collection>
    <collection role="fulltextaccess" number="">Datei im Netzwerk der BAM verfügbar ("Closed Access")</collection>
    <collection role="literaturgattung" number="">Präsentation</collection>
    <collection role="institutes" number="">9.0 Abteilungsleitung und andere</collection>
  </doc>
  <doc>
    <id>53369</id>
    <completedYear/>
    <publishedYear>2021</publishedYear>
    <thesisYearAccepted/>
    <language>deu</language>
    <pageFirst>448</pageFirst>
    <pageLast>459</pageLast>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume>371</volume>
    <type>conferenceobject</type>
    <publisherName>DVS Media GmbH</publisherName>
    <publisherPlace>Düsseldorf</publisherPlace>
    <creatingCorporation>DVS Deutscher Verband für Schweißen und verwandte Verfahren e.V.</creatingCorporation>
    <contributingCorporation/>
    <belongsToBibliography>0</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="deu">Diffusionsmessungen in UP-Mehrlagenschweißgut als effektives Tool gegen verzögerte Kaltrissbildung in Dickblechschweißungen</title>
    <abstract language="deu">Offshore-Windenergieanlagen bilden einen zentralen Bestandteil der zukünftigen Energieerzeugung. Hierzu notwendige Gründungs- und Turmstrukturen werden vorrangig aus UP-geschweißten Blechen aus hochfesten niedriglegierten Stählen mit Dicken bis zu 200 mm hergestellt. Die großen Blechdicken begünstigen hohe Schweißeigenspannungen und lange Diffusionswege für z. B. über den Schweißprozess eingebrachten Wasserstoff. Damit steigt das Risiko für eine wasserstoffunterstützte Kaltrissbildung (WKB) an. Zum sichereren Ausschluss von WKB in den geschweißten Komponenten wird in Abhängigkeit der Nahtgröße, Wärmeeinbringung und Stahlsorte eine Mindestwartezeit (MWZ) von bis zu 48 h empfohlen, bevor die zerstörungsfreie Prüfung durchgeführt wird. Es ist allerdings offen, ob die empfohlene MWZ zu konservativ ist. Einflüsse sind hier bspw. die schwierige Bewertung des Wasserstoffdiffusionsverhaltens im heterogenen UP-Mehrlagen-Schweißgut (SG) im Vergleich zum Grundwerkstoff (GW).&#13;
Zudem sind nur sehr begrenzt H-Diffusionskoeffizienten für UP-Mehrlagen-SG als Grundlage zur Abschätzung des Zeitintervalls einer möglichen verzögerten Kaltrissbildung (somit MWZ) oder auch für Nachwärmprozeduren zur Wasserstoffreduktion (keine MWZ) verfügbar. Verlässliche H-Diffusionskoeffizienten sind daher ein adäquates Tool zur Bewertung des Risikos einer verzögerten WKB. Dieser Beitrag beschreibt Untersuchungen zur Charakterisierung der Wasserstoffdiffusionsverhalten in UP-Mehrlagen-SG eines 60 mm dicken Bleches einer Offshore-Stahlgüte.&#13;
Dazu wurden Proben unterschiedlicher Dicke aus dem reinen Schweißgut extrahiert und über elektrochemische Permeation und Trägergasheißextraktion im Temperaturbereich bis 400 °C sehr interessante Ergebnisse zu den korrespondierenden Diffusionskoeffizienten erarbeitet.</abstract>
    <parentTitle language="deu">DVS Berichte 371: DVS CONGRESS 2021 Große Schweißtechnische Tagung DVS CAMPUS</parentTitle>
    <identifier type="isbn">978-3-96144-146-4</identifier>
    <enrichment key="eventName">DVS Congress 2021</enrichment>
    <enrichment key="eventPlace">Online meeting</enrichment>
    <enrichment key="eventStart">14.09.2021</enrichment>
    <enrichment key="eventEnd">17.09.2021</enrichment>
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    <author>Michael Rhode</author>
    <author>Jonathan Nietzke</author>
    <author>Tobias Mente</author>
    <author>Thomas Kannengießer</author>
    <subject>
      <language>deu</language>
      <type>uncontrolled</type>
      <value>UP-Schweißen</value>
    </subject>
    <subject>
      <language>deu</language>
      <type>uncontrolled</type>
      <value>Wasserstoff</value>
    </subject>
    <subject>
      <language>deu</language>
      <type>uncontrolled</type>
      <value>Kaltriss</value>
    </subject>
    <subject>
      <language>deu</language>
      <type>uncontrolled</type>
      <value>Permeation</value>
    </subject>
    <subject>
      <language>deu</language>
      <type>uncontrolled</type>
      <value>Diffusion</value>
    </subject>
    <collection role="ddc" number="620">Ingenieurwissenschaften und zugeordnete Tätigkeiten</collection>
    <collection role="ddc" number="621">Angewandte Physik</collection>
    <collection role="institutes" number="">9 Komponentensicherheit</collection>
    <collection role="institutes" number="">9.4 Integrität von Schweißverbindungen</collection>
    <collection role="themenfelder" number="">Energie</collection>
    <collection role="themenfelder" number="">Material</collection>
    <collection role="themenfelder" number="">Degradationsmechanismen</collection>
    <collection role="literaturgattung" number="">Verlagsliteratur</collection>
    <collection role="fulltextaccess" number="">Datei im Netzwerk der BAM verfügbar ("Closed Access")</collection>
    <collection role="institutes" number="">9.0 Abteilungsleitung und andere</collection>
  </doc>
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